CN115553460A - 一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法 - Google Patents
一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法 Download PDFInfo
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- CN115553460A CN115553460A CN202211169552.6A CN202211169552A CN115553460A CN 115553460 A CN115553460 A CN 115553460A CN 202211169552 A CN202211169552 A CN 202211169552A CN 115553460 A CN115553460 A CN 115553460A
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Abstract
本发明公开了食品制备领域的一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法其以蔗糖为原料经过果糖基转移酶、多聚果糖蔗糖酶、轻度催化蔗糖得到5‑10%单糖、60‑70%双糖、10‑15%低聚果糖、10‑15%多聚果糖然后过滤得到清净液,复配营养素多种矿物质和多种维生素,杀菌、灌装得到液态特殊膳食用运动营养食品,或者经过浓缩、真空干燥得到固体粉末特殊膳食用运动营养食品。通过酶催化蔗糖转化得到比例合适的单糖、二糖、低聚果糖、多聚果糖的产品符合特殊膳食用运动营养食品补充能量类,并快速且逐级提供能量给人体。
Description
技术领域
本发明属于食品制备领域,具体是一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法。
背景技术
特殊膳食用食品按国家标准《GB13432特殊膳食用食品预包装食品标签》定义:为满足特殊的身体或生理状况和(或)满足疾病、紊乱等状态下的特殊膳食需求,专门加工或配方的食品。这类食品的营养素和(或)其他营养成分的含量与可类比的普通食品有显著不同。特殊膳食用食品主要分为婴幼儿谷类辅助食品、婴幼儿罐装辅助食品、其他特殊膳食食品等三大类,其他特殊膳食食品又包括辅助营养补充品、运动营养补充品、孕妇及乳母营养补充食品、其他。
特殊膳食用运动营养食品是随着我国经济水平和国民素质提高而健身意识也随之增长,运动营养食品逐渐的推广普及,从而得到越来越多人们的青睐。特殊膳食用运动营养食品能够满足运动人群特殊营养需求,调理代谢状态,有助于提高体能和体质,供应给运动补充能量、提高速度力量和耐力,运动后恢复等功能。在运动中会人会感觉到疲劳,若营养没得到及时补充,运动效果就会明显降低。而运动营养食品的作用就是及时补充和满足人在运动过程中所消耗的能量、营养素,最大效能地实现运动目标。
为了实现上述目的,现有技术公告号为CN1225184C的技术方案公开了一种棒状运动食品作为能量补充食品,这种技术方案以糖浆、干果、填充物、风味物质和食用油脂为载体作为能量提供物,但是这种能量补充物是以高热量食品作为能量供给,在糖浆和干果中含有大量多糖,需要转化后才能给人体进行供能,给能量补充过程带来一定滞后性。
发明内容
为了解决上述问题,本发明的目的是提供一种降低糖原转化时间,得到一种高倍速的特殊膳食用运动营养食品。
为了实现上述目的,本发明的技术方案如下:一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法包括将若干固定化酶进行一体化重组,随后将重组的固定化酶酶解于糖质组合物溶液中形成混合物,随后将混合物回收后添加营养素制备。
进一步,还包括以下步骤:
S1,固定化酶的配比,配比单糖酶和二糖酶,所述单糖酶和二糖酶的比例为13:1;
S2,固定化酶的一体化重组,将单糖酶和二糖酶在酸性环境中进行混合搅拌,随后在搅拌混合过程中加入卡拉胶和固化剂从而生成复合固化酶;
S3,酶解过程,将糖质组合物配成溶液,随后将复合固化酶放入溶液中;
S4,回收酶,将酶解后的复合固化酶进行过滤回收;
S5,营养素复配,将至少一种营养素加入复合固化酶中。
进一步,所述S1中的单糖酶包括固定化果糖基转移酶和固定化葡萄糖异构酶,所述二糖酶包括多聚果糖蔗糖酶和固定化蔗糖酶。
进一步,所述单糖酶的酶活力为固定化果糖基转移酶8000-10000U/g和固定化葡萄糖异构酶1200U-1500U/g,所述二糖酶的酶活力为多聚果糖蔗糖酶120-150U/g和固定化蔗糖酶500-800U/g。
进一步,所述步骤S2中固定化酶的比例为固定化果糖基转移酶55-65份、固定化多聚果糖蔗糖酶5-10份、固定化蔗糖酶10-15份和固定化验葡萄糖异构酶20-25份。
进一步,所述复合固化酶的配置方法包括将固定化酶混合,随后在固定化酶中添加到质量浓度0.05-0.07%壳聚糖和0.08-0.1%卡拉胶的稀乙酸溶液充分搅拌,然后用脉冲射流方式将固定化酶溶液喷到4-6倍0.5mol/L Cacl2溶液中,再过10-14目振动筛网落入搅拌速度200-350r/min的0.4mol/L氧化钾的水溶液中,用18-20目滤袋过滤后用4-5倍水清洗干净滤物,5-15℃冷风干燥后得到重组复合固定化酶。
进一步,所述步骤S3酶解过程中蔗糖溶解于水制成质量浓度为45-55%,加入重组复合固定化酶质量比为0.8-1.2%,在PH5.5-6.5,温度在45-60℃在生物反应器中催化10-12h,得5-10%单糖、60-70%双糖、10-15%低聚果糖和10-15%多聚果糖。
进一步,所述步骤S4回收酶过程利用40-60目滤布过滤回收固定化酶,滤液再过0.45-0.50μ滤袋,得到清净糖液。
进一步,所述步骤S5营养素复配中,营养素包括镁150-250mg/L、钙450-650mg/L、铁6-9mg/L、锌5-9mg/L、钾800-1350mg/L、硒20-45μg/L、铜0.8-1.35mg/L、碘24-54μg/L、锰1.5-2.0mg/L、磷300-900mg/L、维生素A320-350μg/L、维生素D4-9μg/L、维生素E8-18mg/L、维生素B11.2-2.7mg/L、维生素B20.8-1.8mg/L、维生素B6 0.8-1.8mg/L、维生素B12 1.6-3.6μg/L、维生素C40-90mg/L,烟酸8-18mg/L、叶酸200-225μg/L、生物素20-45μg/L、泛酸2.5-5mg/L和牛磺酸0.4-0.6g/L中一种或一种以上。
进一步,还包括以下步骤:
S6杀菌包装:配好的物料通过常规瞬时灭菌,最后自动灌装得200-300ml/瓶液态特殊膳食用运动营养食品,每天食用量400-900ml;
S7浓缩干燥:固态产品灭菌工序后浓缩成固形物含量78-80%,然后真空干燥得到水分含量小于10%,粉碎后得到固体粉料;
S8包装:自动包装机包装得到50g/袋的固体运动营养食品。
采用上述方案后实现了以下有益效果:1、通过酶催化蔗糖转化得到比例合适的单糖、二糖、低聚果糖、多聚果糖的产品符合特殊膳食用运动营养食品补充能量类,并快速且逐级提供能量给人体;
2、产品复合营养素矿物质、维生素、营养强化剂,补充能量同时获得均衡的营养补充。
3、本技术方案蔗糖及其蔗糖基在不同领域应用不断被开发,如通过果糖基转移酶转化蔗糖获得益生元低聚果糖,含量95%以低聚果糖产品属于营养强化剂,蔗糖与β-糊精通过熔融结晶的方法,制得医药辅料可压缩糖,蔗糖基团中羟基上取代氯,得到高倍速甜味剂蔗糖素等。
附图说明
图1为本发明实施例的检测情况图;
图2为本发明中微量元素检测数据图。
具体实施方式
下面通过具体实施方式进一步详细说明:
实施例1
请参考图1和图2,本实施例为本发明所述的酶催化蔗糖制备特殊膳食用运动营养食品的制备方法的一个实例,包括以下步骤:
酶催化蔗糖制备特殊膳食用运动营养食品方法包括以下步骤:
(1)固定化酶活力:固定化果糖基转移酶8000U/g,多聚果糖蔗糖酶120U/g,固定化蔗糖酶500U/g,固定化葡萄糖异构酶1200U/g;
(2)固定化酶一体化重组:固定化果糖基转移酶65份,固定化多聚果糖蔗糖酶5份,固定化蔗糖酶10份,固定化葡萄糖异构酶20份,混合均匀,添加到质量浓度0.05%壳聚糖和0.08%质量比卡拉胶的稀乙酸溶液充分搅拌。脉冲射流方式喷到4倍0.5mol/L Cacl2溶液中,再过10目振动筛网落入搅拌速度200r/min的0.4mol/L氧化钾的水溶液中。用18目滤袋过滤后用4倍水清洗干净滤物,5℃冷风干燥后得到重组复合固定化酶。
(3)酶解:蔗糖溶解于水制成糖液浓度质量比为45%,加入复合固定化酶质量比为0.8%,在PH5.5,温度在45℃在生物反应器中催化10h,得到5%单糖、70%双糖、10%低聚果糖、15%多聚果糖;
(4)回收酶:40目滤布过滤,回收固定化酶,滤液再过0.45μ滤袋,得到清净糖液;
(5)营养素复配:镁150mg/L,钙450mg/L,铁6mg/L,锌5mg/L,钾800mg/L,硒20μg/L,铜0.8mg/L,碘24μg/L,锰1.5mg/L,磷300mg/L,维生素A320μg/L,维生素D 4μg/L,维生素E8mg/L,维生素B1 1.2mg/L,维生素B2 0.8mg/L,维生素B6 0.8mg/L,维生素B12 1.6μg/L,维生素C 40mg/L,烟酸8mg/L,叶酸200μg/L,生物素20μg/L,泛酸2.5mg/L,牛磺酸0.4g/L;
(6)杀菌包装:混合均匀通过常规瞬时灭菌,自动灌装得200ml/瓶液态特殊膳食用运动营养食品;
实施例2
本实施例为本发明所述的酶催化蔗糖制备特殊膳食用运动营养食品的制备方法的另一个实例,包括以下步骤:
酶催化蔗糖制备特殊膳食用运动营养食品方法包括以下步骤:
(1)固定化酶活力:固定化果糖基转移酶9000U/g,多聚果糖蔗糖酶140U/g,固定化蔗糖酶600U/g,固定化葡萄糖异构酶1500U/g;
(2)固定化酶一体化重组:固定化果糖基转移酶55份,固定化多聚果糖蔗糖酶10份,固定化蔗糖酶10份,固定化葡萄糖异构酶25份,混合均匀,添加到质量浓度0.07%壳聚糖和0.1%卡拉胶的稀乙酸溶液充分搅拌。然后用脉冲射流方式喷到6倍0.5mol/L Cacl2溶液中,再过14目振动筛网落入搅拌速度350r/min的0.4mol/L氧化钾的水溶液中。用20目滤袋过滤后用5倍水清洗干净滤物,15℃冷风干燥后得到重组复合固定化酶。
(3)酶解:蔗糖溶解于水制成质量浓度为55%,加入复合固定化酶质量比为1.2%,在pH6.5,温度在60℃在生物反应器中催化12h,得到10%单糖、60%双糖、15%低聚果糖、15%多聚果糖;
(4)回收酶:60目滤布过滤,回收固定化酶,滤液再过0.50μ滤袋,得到清净糖液;
(5)营养素复配:镁250mg/L,钙650mg/L,铁9mg/L,锌9mg/L,钾1350mg/L,硒45μg/L,铜1.35mg/L,碘54μg/L,锰2.0mg/L,磷900mg/L,维生素A 350μg/L,维生素D 9μg/L,维生素E18mg/L,维生素B1 2.7mg/L,维生素B21.8mg/L,维生素B6 1.8mg/L,维生素B12 3.6μg/L,维生素C90mg/L,烟酸18mg/L,叶酸225μg/L,生物素45μg/L,泛酸5mg/L,牛磺酸0.6g/L;
(6)杀菌包装:瞬时灭菌,一半量用灌装液态特殊膳食用运动营养食品,300ml/瓶;
(7)浓缩干燥:另一半浓缩成固形物含量80%,真空干燥水分含量5%、粉碎后得到固体粉料;
(8)包装:自动包装机包装得到50g/袋的固体特殊膳食用运动营养食品。
实施例3
本实施例为本发明所述的酶催化蔗糖制备特殊膳食用运动营养食品的制备方法的再一个实例,包括以下步骤:
3.酶催化蔗糖制备特殊膳食用运动营养食品方法包括以下步骤:
(1)固定化酶活力:固定化果糖基转移酶10000U/g,多聚果糖蔗糖酶150U/g,固定化蔗糖酶800U/g,固定化葡萄糖异构酶1300U/g;
(2)固定化酶一体化重组:固定化果糖基转移酶55份,固定化多聚果糖蔗糖酶10份,固定化蔗糖酶15份,固定化葡萄糖异构酶20份,混合均匀,添加到质量浓度0.0g7%壳聚糖和0.08%卡拉胶的稀乙酸溶液充分搅拌。然后用脉冲射流方式喷到6倍0.5mol/L Cacl2溶液中,再过10目振动筛网落入搅拌速度350r/min的0.4mol/L氧化钾的水溶液中。用20目滤袋过滤后用4倍水清洗干净滤物,10℃冷风干燥后得到重组复合固定化酶。
(3)酶解:蔗糖溶解于水制成质量浓度为52%,加入复合固定化酶质量比为1.0%,在pH6.0,温度在50℃在生物反应器中催化11h;得到8%单糖、65%双糖、14%低聚果糖、13%多聚果糖;;
(4)回收酶:50目滤布过滤,回收固定化酶,滤液再过0.45μ滤袋,得到清净糖液;
(5)营养素复配:镁200mg/L,钙500mg/L,铁8mg/L,锌8mg/L,维生素A330μg/L,维生素D 6μg/L,维生素E12mg/L,维生素B1 2.0mg/L,维生素B2 1.5mg/L,维生素B6 1,5mg/L,维生素B12 2.5μg/L,维生素C 65mg/L,烟酸13mg/L,叶酸210μg/L,泛酸3mg/L,牛磺酸0.5g/L;
(6)杀菌包装:混合均匀通过瞬时灭菌
(7)浓缩干燥:浓缩成固形物含量78%,真空干燥水分含量4.3%、粉碎后得到固体粉料;
(8)包装:自动包装机包装得到50g/袋的固体特殊膳食用运动营养食品。
实施例4
本实施例为本发明所述的酶催化蔗糖制备特殊膳食用运动营养食品的又一个实例,包括以下步骤:
3.酶催化蔗糖制备特殊膳食用运动营养食品方法包括以下步骤:
(1)固定化酶活力:固定化果糖基转移酶9000U/g,多聚果糖蔗糖酶130U/g,固定化蔗糖酶600U/g,固定化葡萄糖异构酶14000U/g;
(2)固定化酶一体化重组:固定化果糖基转移酶60份,固定化多聚果糖蔗糖酶10份,固定化蔗糖酶10份,固定化验葡萄糖异构酶20份,混合均匀,添加到质量浓度0.06g%壳聚糖和0.1%卡拉胶的稀乙酸溶液充分搅拌。然后用脉冲射流方式喷到5倍0.5mol/L Cacl2溶液中,再过12目振动筛网落入搅拌速度300r/min的0.4mol/L氧化钾的水溶液中。用20目滤袋过滤后用5倍水清洗干净滤物,8℃冷风干燥后得到重组复合固定化酶。
(3)酶解:蔗糖溶解于水制成质量浓度为50%,加入复合固定化酶质量比为1.2%,在pH 5.5,温度在55℃在生物反应器中催化10h得到6%单糖、68%双糖、11%低聚果糖、15%多聚果糖;
(4)回收酶:50目滤布过滤,回收固定化酶,滤液再过0.50μ滤袋,得到清净糖液;
(5)营养素复配:钙600mg/L,铁8mg/L,锌6mg/L,磷500mg/L,维生素A350μg/L,维生素D 5μg/L,维生素E10mg/L,维生素B1 1.5mg/L,维生素B2 0.8mg/L,维生素B6 1.8mg/L,维生素B12 2.9μg/L,维生素C90 mg/L,牛磺酸0.4g/L;
(6)杀菌包装:配好的物料通过常规瞬时灭菌,自动灌装得250ml/瓶液态特殊膳食用运动营养食品。
需要说明的是,在本文中,诸如第一和第二等之类的关系术语仅仅用来将一个实体或者操作与另一个实体或操作区分开来,而不一定要求或者暗示这些实体或操作之间存在任何这种实际的关系或者顺序。而且,术语“包括”、“包含”或者其任何其他变体意在涵盖非排他性的包含,从而使得包括一系列要素的过程、方法、物品或者设备不仅包括那些要素,而且还包括没有明确列出的其他要素,或者是还包括为这种过程、方法、物品或者设备所固有的要素。
以上所述的仅是本发明的实施例,方案中公知的具体结构及特性等常识在此未作过多描述,所属领域普通技术人员知晓申请日或者优先权日之前发明所属技术领域所有的普通技术知识,能够获知该领域中所有的现有技术,并且具有应用该日期之前常规实验手段的能力,所属领域普通技术人员可以在本申请给出的启示下,结合自身能力完善并实施本方案,一些典型的公知结构或者公知方法不应当成为所属领域普通技术人员实施本申请的障碍。应当指出,对于本领域的技术人员来说,在不脱离本发明结构的前提下,还可以作出若干变形和改进,这些也应该视为本发明的保护范围,这些都不会影响本发明实施的效果和专利的实用性。本申请要求的保护范围应当以其权利要求的内容为准,说明书中的具体实施方式等记载可以用于解释权利要求的内容。
Claims (10)
1.一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法,其特征在于:包括将若干固定化酶进行一体化重组,随后将重组的固定化酶酶解于糖质组合物溶液中形成混合物,随后将混合物回收后添加营养素制备。
2.根据权利要求1所述的一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法,其特征在于:还包括以下步骤:
S1,固定化酶的配比,配比单糖酶和二糖酶,所述单糖酶和二糖酶的比例为13:1;
S2,固定化酶的一体化重组,将单糖酶和二糖酶在酸性环境中进行混合搅拌,随后在搅拌混合过程中加入卡拉胶和固化剂从而生成复合固化酶;
S3,酶解过程,将糖质组合物配成溶液,随后将复合固化酶放入溶液中;
S4,回收酶,将酶解后的复合固化酶进行过滤回收;
S5,营养素复配,将至少一种营养素加入复合固化酶中。
3.根据权利要求2所述的一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法,其特征在于:所述S1中的单糖酶包括固定化果糖基转移酶和固定化葡萄糖异构酶,所述二糖酶包括多聚果糖蔗糖酶和固定化蔗糖酶。
4.根据权利要求3所述的一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法,其特征在于:所述单糖酶的酶活力为固定化果糖基转移酶8000-10000U/g和固定化葡萄糖异构酶1200U-1500U/g,所述二糖酶的酶活力为多聚果糖蔗糖酶120-150U/g和固定化蔗糖酶500-800U/g。
5.根据权利要求2所述的一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法,其特征在于:所述步骤S2中固定化酶的比例为固定化果糖基转移酶55-65份、固定化多聚果糖蔗糖酶5-10份、固定化蔗糖酶10-15份和固定化验葡萄糖异构酶20-25份。
6.根据权利要求5所述的一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法,其特征在于:所述复合固化酶的配置方法包括将固定化酶混合,随后在固定化酶中添加到质量浓度0.05-0.07%壳聚糖和0.08-0.1%卡拉胶的稀乙酸溶液充分搅拌,然后用脉冲射流方式将固定化酶溶液喷到4-6倍0.5mol/L Cacl2溶液中,再过10-14目振动筛网落入搅拌速度200-350r/min的0.4mol/L氧化钾的水溶液中,用18-20目滤袋过滤后用4-5倍水清洗干净滤物,5-15℃冷风干燥后得到重组复合固定化酶。
7.根据权利要求2所述的一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法,其特征在于:所述步骤S3酶解过程中蔗糖溶解于水制成质量浓度为45-55%,加入重组复合固定化酶质量比为0.8-1.2%,在PH5.5-6.5,温度在45-60℃在生物反应器中催化10-12h,得5-10%单糖、60-70%双糖、10-15%低聚果糖和10-15%多聚果糖。
8.根据权利要求2所述的一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法,其特征在于:所述步骤S4回收酶过程利用40-60目滤布过滤回收固定化酶,滤液再过0.45-0.50μ滤袋,得到清净糖液。
9.根据权利要求2所述的一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法,其特征在于:所述步骤S5营养素复配中,营养素包括镁150-250mg/L、钙450-650mg/L、铁6-9mg/L、锌5-9mg/L、钾800-1350mg/L、硒20-45μg/L、铜0.8-1.35mg/L、碘24-54μg/L、锰1.5-2.0mg/L、磷300-900mg/L、维生素A320-350μg/L、维生素D4-9μg/L、维生素E 8-18mg/L、维生素B11.2-2.7mg/L、维生素B20.8-1.8mg/L、维生素B6 0.8-1.8mg/L、维生素B12 1.6-3.6μg/L、维生素C40-90mg/L,烟酸8-18mg/L、叶酸200-225μg/L、生物素20-45μg/L、泛酸2.5-5mg/L和牛磺酸0.4-0.6g/L中一种或一种以上。
10.根据权利要求2所述的一种利用酶催化蔗糖制备特殊膳食用运动营养食品的方法,其特征在于:还包括以下步骤:
S6杀菌包装:配好的物料通过常规瞬时灭菌,最后自动灌装得200-300ml/瓶液态特殊膳食用运动营养食品,每天食用量400-900ml;
S7浓缩干燥:固态产品灭菌工序后浓缩成固形物含量78-80%,然后真空干燥得到水分含量小于10%,粉碎后得到固体粉料;
S8包装:自动包装机包装得到50g/袋的固体运动营养食品。
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