CN114869837A - Apple extract moisturizing and anti-wrinkle WOW facial cream and preparation method thereof - Google Patents

Apple extract moisturizing and anti-wrinkle WOW facial cream and preparation method thereof Download PDF

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Publication number
CN114869837A
CN114869837A CN202210568280.0A CN202210568280A CN114869837A CN 114869837 A CN114869837 A CN 114869837A CN 202210568280 A CN202210568280 A CN 202210568280A CN 114869837 A CN114869837 A CN 114869837A
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China
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water
wow
oil
wrinkle
emulsifier
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CN202210568280.0A
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李永闯
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Individual
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/99Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/04Dispersions; Emulsions
    • A61K8/06Emulsions
    • A61K8/066Multiple emulsions, e.g. water-in-oil-in-water
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/342Alcohols having more than seven atoms in an unbroken chain
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/602Glycosides, e.g. rutin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • A61K8/604Alkylpolyglycosides; Derivatives thereof, e.g. esters
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

Abstract

The invention discloses an apple extract moisturizing and anti-wrinkle WOW facial cream and a preparation method thereof. The WOW type facial cream comprises the following raw materials in percentage by weight: 1-5% of a water-in-oil type emulsifier, 0.2-3% of an oil-in-water type emulsifier, 10-30% of an emollient, 0.1-2% of a thickener, 0.1-5% of an apple fruit cell culture extract, 0.1-0.5% of a preservative, and the balance of water. The W/O/W type face cream is successfully prepared by reasonably matching the water-in-oil type emulsifier and the oil-in-water type emulsifier and optimizing the process, has good stability, has good effects of moisturizing, replenishing water and removing wrinkles, can effectively prevent skin dryness and aging caused by ultraviolet rays, and avoids skin injury and hyperplastic wrinkles.

Description

Apple extract moisturizing and anti-wrinkle WOW facial cream and preparation method thereof
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to an apple extract moisturizing and anti-wrinkle WOW facial cream and a preparation method thereof.
Background
The cream is a common skin care product, has different skin care effects according to different types, is mainly used for replenishing water, moisturizing, whitening, fading spots and resisting aging, and at present, the cream on the market has various using functions, but has common effects and single efficacy, partial cream cannot achieve the moisturizing effect after being used for 1-2 hours, and the skin has no obvious improvement effect after being used for a long time, so that the cream is not beneficial to market popularization. Most of the existing face creams are oil-in-water type or water-in-oil type, and active ingredients (such as plant extract lamp) are dissolved in water phase. In the oil-in-water type face cream, the active ingredients are dissolved in an external water phase and are easy to change color along with the change of acid-base environment, so that the efficacy and the appearance stability of a face test product are influenced. In the water-in-oil type face cream, the plant extract is dissolved in the internal water phase, and although the face cream is favorable for locking water and keeping moisture, the face cream is not favorable for skin to absorb effective components, and the sticky feeling is obvious after the face cream is applied.
Disclosure of Invention
The invention aims to provide an apple extract moisturizing and anti-wrinkle WOW facial cream and a preparation method thereof, and aims to solve the technical problems.
In order to achieve the purpose, the technical scheme of the invention is as follows:
in a first aspect, the invention provides an apple extract moisturizing and anti-wrinkle WOW type facial cream, which comprises the following raw materials in percentage by weight: 1-5% of a water-in-oil type emulsifier, 0.2-3% of an oil-in-water type emulsifier, 10-30% of an emollient, 0.1-2% of a thickener, 0.1-5% of an apple fruit cell culture extract, 0.1-0.5% of a preservative, and the balance of water.
Preferably, the water-in-oil emulsifier comprises the following components in percentage by weight: 54% of arachidyl alcohol, 28% of behenyl alcohol and 18% of arachidyl glucoside.
Preferably, the oil-in-water type emulsifier consists of the following components in percentage by weight: 60% of octyl dodecanol, 20% of octyl dodecanol xyloside and 20% of PEG-30 dipolyhydroxystearate.
Preferably, the emollient comprises isononyl isononanoate.
Preferably, the thickener consists of the following components in percentage by weight: polyacrylate-1365%, polyisobutylene 30%, and polysorbate-205%.
Preferably, the preservative comprises at least one of phenoxyethanol and ethylhexyl glycerin.
Preferably, the weight percentage of the apple fruit cell culture extract in the raw material is 1-3%.
Preferably, the apple extract moisturizing and anti-wrinkle WOW type facial cream comprises the following raw materials in percentage by weight: 1.5-2.5% of water-in-oil type emulsifier, 0.8-1.3% of oil-in-water type emulsifier, 18-25% of emollient, 0.1-2% of thickener, 1-4% of apple fruit cell culture extract, 0.2-0.4% of preservative and the balance of water.
Preferably, the apple extract moisturizing and anti-wrinkle WOW type facial cream comprises the following raw materials in percentage by weight: 2% of water-in-oil emulsifier, 1% of oil-in-water emulsifier, 20% of emollient, 0.5% of thickening agent, 2% of apple fruit cell culture extract, 0.3% of preservative and the balance of water.
In a second aspect, the invention provides a method for preparing the apple extract moisturizing and anti-wrinkle WOW type facial cream, which comprises the following steps:
(1) mixing oil-in-water emulsifier and emollient to obtain phase A;
(2) mixing and stirring the thickening agent and water uniformly to obtain a phase B;
(3) mixing the apple fruit cell culture extract and the preservative, and uniformly stirring to obtain a phase C;
(4) and adding the phase A into the phase B, stirring uniformly, adding the phase C, and homogenizing to obtain the WOW type face cream.
Preferably, the rotating speed of stirring in the step (1) is 200-400 r/min, the temperature is 80-85 ℃, and the time is 20-40 min.
Preferably, the rotating speed of stirring in the step (2) is 200-400 r/min, the temperature is 80-85 ℃, and the time is 10-15 min.
Preferably, the rotating speed of stirring in the step (3) is 200-400 r/min, and the time is 5-10 min.
Preferably, the rotation speed of homogenizing in the step (4) is 8000-12000 r/min, and the time is 5-10 min.
Preferably, in the step (4), the phase A is uniformly added into the phase B within 10-30 min under the stirring of 200-400 r/min, and the stirring is continued for 10-30 min.
Compared with the prior art, the invention has the beneficial effects that:
the W/O/W type face cream is successfully prepared by reasonably matching the water-in-oil type emulsifier and the oil-in-water type emulsifier and optimizing the process, has good stability, has good effects of moisturizing, replenishing water and removing wrinkles, can effectively prevent skin dryness and aging caused by ultraviolet rays, and avoids skin injury and hyperplastic wrinkles.
Detailed Description
The following further describes the embodiments of the present invention. It should be noted that the description of the embodiments is provided to help understanding of the present invention, but the present invention is not limited thereto. In addition, the technical features involved in the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
Preparing raw materials: according to the weight percentage, 54 percent of arachidyl alcohol, 28 percent of behenyl alcohol and 18 percent of arachidyl alcohol glucoside are uniformly mixed to obtain a water-in-oil type emulsifier, 60 percent of octyl dodecanol, 20 percent of octyl dodecanol xyloside and 20 percent of PEG-30 dipolyhydroxystearate are uniformly mixed to obtain an oil-in-water type emulsifier, 1365 percent of polyacrylate, 30 percent of polyisobutylene and 205 percent of polysorbate are uniformly mixed to obtain an oil-in-water type emulsifier, and 80 percent of phenoxyethanol and 20 percent of ethylhexylglycerin are uniformly mixed to obtain the preservative.
Example 1
The embodiment provides an apple extract moisturizing and anti-wrinkle WOW type facial cream which comprises the following components in percentage by weight: 2% of water-in-oil emulsifier, 1% of oil-in-water emulsifier, 20% of isononyl isononanoate, 0.5% of thickening agent, 2% of apple fruit cell culture extract, 0.3% of preservative and the balance of water. The preparation method comprises the following steps:
(1) mixing an oil-in-water emulsifier and isononyl isononanoate, heating to 80 ℃, and stirring for 30min at the temperature of 400r/min to obtain a phase A;
(2) mixing and stirring the thickening agent and water, heating to 80 ℃, and stirring for 15min at the temperature of 400r/min to obtain a phase B;
(3) mixing the apple fruit cell culture extract and antiseptic, stirring at 200r/min for 10min to obtain phase C;
(4) adding phase A into phase B at constant speed within 25min under stirring at 300r/min, stirring for 20min, adding phase C, and homogenizing at 10000r/min for 8min to obtain WOW facial cream.
Example 2
The embodiment provides an apple extract moisturizing and anti-wrinkle WOW type facial cream which comprises the following components in percentage by weight: 1.5% of water-in-oil emulsifier, 0.8% of oil-in-water emulsifier, 18% of isononyl isononanoate, 2% of thickener, 1% of apple fruit cell culture extract, 0.2% of preservative and the balance of water. Then, the WOW type cream was prepared according to the preparation method of example 1.
Example 3
The embodiment provides an apple extract moisturizing and anti-wrinkle WOW type facial cream which comprises the following components in percentage by weight: 2.5% of a water-in-oil type emulsifier, 1.2% of an oil-in-water type emulsifier, 22% of an emollient agent, 1.5% of a thickener, 3.2% of an apple fruit cell culture extract, 0.4% of a preservative, and the balance water, and then a WOW type cream was prepared according to the preparation method of example 1.
Example 4
The embodiment provides an apple extract moisturizing and anti-wrinkle WOW type facial cream which comprises the following components in percentage by weight: 2% of a water-in-oil type emulsifier, 1.3% of an oil-in-water type emulsifier, 25% of an emollient, 1% of a thickener, 3% of an apple fruit cell culture extract, 0.4% of a preservative, and the balance of water, and then a WOW type cream was prepared according to the preparation method of example 1.
Example 5
The embodiment provides an apple extract moisturizing and anti-wrinkle WOW type facial cream which comprises the following components in percentage by weight: 2% of a water-in-oil type emulsifier, 1% of an oil-in-water type emulsifier, 20% of isononyl isononanoate, 0.5% of a thickener, 2% of an apple fruit cell culture extract, 0.3% of a preservative, and the balance water, and then a WOW type cream was prepared according to the preparation method of example 1.
Example 6
The embodiment provides an apple extract moisturizing and anti-wrinkle WOW type facial cream which comprises the following components in percentage by weight: 5% of water-in-oil type emulsifier, 0.2% of oil-in-water type emulsifier, 10% of isononyl isononanoate, 2% of thickening agent, 0.1% of apple fruit cell culture extract, 0.5% of preservative and the balance of water, and the preparation method comprises the following steps: (1) mixing an oil-in-water emulsifier and isononyl isononanoate, heating to 80 ℃, and stirring at 300r/min for 20min to obtain a phase A;
(2) mixing thickener and water, stirring, heating to 80 deg.C, stirring at 300r/min for 10min to obtain phase B;
(3) mixing the apple fruit cell culture extract and antiseptic, stirring at 400r/min for 15min to obtain phase C;
(4) adding phase A into phase B at constant speed within 10min under stirring at 200r/min, stirring for 10min, adding phase C, and homogenizing at 12000r/min for 5min to obtain WOW type facial cream.
Example 7
The embodiment provides an apple extract moisturizing and anti-wrinkle WOW type facial cream which comprises the following components in percentage by weight: water-in-oil type emulsifier 1%, oil-in-water type emulsifier 3%, isononyl isononanoate 30%, thickener 0.1%, apple fruit cell culture extract 5%, preservative 0.1%, and water in balance, and then WOW type cream was prepared according to the preparation method of example 1. The preparation method comprises the following steps:
(1) mixing an oil-in-water type emulsifier and isononyl isononanoate, heating to 85 ℃, and stirring at 200r/min for 40min to obtain a phase A;
(2) mixing and stirring the thickening agent and water, heating to 85 ℃, and stirring for 15min at the temperature of 200r/min to obtain a phase B;
(3) mixing the apple fruit cell culture extract and antiseptic, stirring at 200r/min for 10min to obtain phase C;
(4) adding phase A into phase B at constant speed within 20min under stirring at 400r/min, stirring for 30min, adding phase C, and homogenizing at 8000r/min for 15min to obtain WOW type facial cream.
Example 8
The embodiment provides a facial cream which comprises the following components in percentage by weight: 1% of a water-in-oil type emulsifier, 2% of an oil-in-water type emulsifier, 20% of isononyl isononanoate, 0.5% of a thickener, 2% of an apple fruit cell culture extract, 0.3% of a preservative, and the balance water, and then a cream was prepared according to the preparation method of example 1.
Comparative example 1
This comparative example provides a cream which was prepared by a method different from that of example 1 in that phase B was added to phase a at a constant speed over 25min under stirring at 300 r/min.
Effect example 1
The invention proceeds the following efficacy tests on the creams prepared in the above examples and comparative examples:
kunming mice with the weight of 18-22 g are selected as test animals, the number of the Kunming mice is 100, the Kunming mice are randomly divided into ten groups, 10 mice in each group are respectively male and female. The skin of the back of the mouse was selected as a test area (2 cm. times.2 cm), and the hair of the test area was removed. Mice were placed in thin cages approximately 30cm from the UVB lamp and the back was irradiated with slow rotation (3 times a week for 30min each). The UVB irradiation intensity is gradually increased from the beginning of irradiation to the 1 st, 2 th, 3 th and 4 th weeks and is respectively 60, 70, 80 and 90mJ/cm 2 90mJ/cm in 4-10 weeks 2 1g of cream product was applied to the skin of the test area one hour before each exposure, and the control group was left untreated. After the irradiation, the skin wrinkles of the mouse test area were observed, and the statistical results are shown in table 1.
TABLE 8
Serial number Source of cream Condition of the skin
1 Control group Dry skin, deep wrinkles and high number of wrinkles
2 Example 1 The skin still has good elasticity and almost no wrinkles
3 Example 2 The skin still has good elasticity and has few wrinkles
4 Example 3 The skin still has good elasticity and almost no wrinkles
5 Example 4 The skin has certain elasticity and almost has no wrinkles
6 Example 5 The skin has certain elasticity and small amount of fine wrinkles
7 Example 6 Poor skin elasticity with small amount of fine wrinkles
8 Example 7 Poor skin elasticity with small amount of fine wrinkles
9 Example 8 Poor skin elasticity with small amount of fine wrinkles
10 Comparative example 1 The skin has poor elasticity and long and thin obvious wrinkles
The embodiments of the present invention have been described in detail, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, and the scope of protection is still within the scope of the invention.

Claims (10)

1. The apple extract moisturizing and anti-wrinkle WOW type facial cream is characterized by comprising the following raw materials in percentage by weight: 1-5% of a water-in-oil type emulsifier, 0.2-3% of an oil-in-water type emulsifier, 10-30% of an emollient, 0.1-2% of a thickener, 0.1-5% of an apple fruit cell culture extract, 0.1-0.5% of a preservative, and the balance of water.
2. The apple extract moisturizing and anti-wrinkle WOW-type facial cream as claimed in claim 1, wherein the water-in-oil emulsifier is composed of the following components in percentage by weight: 54% of arachidyl alcohol, 28% of behenyl alcohol and 18% of arachidyl glucoside.
3. The apple extract moisturizing and anti-wrinkle WOW-type facial cream according to claim 1, wherein the oil-in-water emulsifier is composed of the following components in percentage by weight: 60% of octyl dodecanol, 20% of octyl dodecanol xyloside and 20% of PEG-30 dipolyhydroxystearate.
4. The apple extract moisturizing anti-wrinkle WOW cream of claim 1, wherein the emollient comprises isononyl isononanoate.
5. The apple extract moisturizing and anti-wrinkle WOW-type facial cream of claim 1, wherein the thickener is composed of the following components in percentage by weight: polyacrylate-1365%, polyisobutylene 30%, and polysorbate-205%.
6. The apple extract moisturizing and anti-wrinkle WOW-type facial cream as claimed in claim 1, wherein the weight percentage of the apple fruit cell culture extract in the raw material is 1-3%.
7. The apple extract moisturizing and anti-wrinkle WOW-type facial cream as claimed in claim 1, comprising the following raw materials by weight: 1.5-2.5% of water-in-oil type emulsifier, 0.8-1.3% of oil-in-water type emulsifier, 18-25% of emollient, 0.1-2% of thickener, 1-4% of apple fruit cell culture extract, 0.2-0.4% of preservative and the balance of water.
8. The apple extract moisturizing and anti-wrinkle WOW-type facial cream as claimed in claim 1, comprising the following raw materials by weight: 2% of water-in-oil emulsifier, 1% of oil-in-water emulsifier, 20% of emollient, 0.5% of thickening agent, 2% of apple fruit cell culture extract, 0.3% of preservative and the balance of water.
9. A method for preparing the apple extract moisturizing and anti-wrinkle WOW type facial cream as claimed in any one of claims 1 to 6, comprising the following steps:
(1) mixing oil-in-water emulsifier and emollient to obtain phase A;
(2) mixing and stirring the thickening agent and water uniformly to obtain a phase B;
(3) mixing the apple fruit cell culture extract and the preservative, and uniformly stirring to obtain a phase C;
(4) and adding the phase A into the phase B, stirring uniformly, adding the phase C, and homogenizing to obtain the WOW type face cream.
10. A preparation method of the apple extract moisturizing and anti-wrinkle WOW-type facial cream as claimed in claim 9, wherein the phase A is added into the phase B at a constant speed within 10-30 min under stirring at 200-400 r/min, and stirring is continued for 10-30 min.
CN202210568280.0A 2022-05-24 2022-05-24 Apple extract moisturizing and anti-wrinkle WOW facial cream and preparation method thereof Pending CN114869837A (en)

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CN202210568280.0A CN114869837A (en) 2022-05-24 2022-05-24 Apple extract moisturizing and anti-wrinkle WOW facial cream and preparation method thereof

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Application Number Priority Date Filing Date Title
CN202210568280.0A CN114869837A (en) 2022-05-24 2022-05-24 Apple extract moisturizing and anti-wrinkle WOW facial cream and preparation method thereof

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Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113081942A (en) * 2021-04-09 2021-07-09 广州市韵丽生物科技有限公司 Multi-dimensional hydration cream containing apple stem cells
CN113925791A (en) * 2021-09-29 2022-01-14 广州卓芬化妆品有限公司 Waterproof sunscreen composition and preparation method thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113081942A (en) * 2021-04-09 2021-07-09 广州市韵丽生物科技有限公司 Multi-dimensional hydration cream containing apple stem cells
CN113925791A (en) * 2021-09-29 2022-01-14 广州卓芬化妆品有限公司 Waterproof sunscreen composition and preparation method thereof

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