CN114831916A - Daily eye repair composition, preparation method and application thereof - Google Patents
Daily eye repair composition, preparation method and application thereof Download PDFInfo
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- CN114831916A CN114831916A CN202210507515.5A CN202210507515A CN114831916A CN 114831916 A CN114831916 A CN 114831916A CN 202210507515 A CN202210507515 A CN 202210507515A CN 114831916 A CN114831916 A CN 114831916A
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Abstract
The invention discloses a daily eye repair composition, a preparation method and application thereof, and belongs to the technical field of eye cosmetics. The preparation is prepared from acrylic acid (acrylate)/C10-30 alkanol acrylate cross-linked polymer, allantoin, triethanolamine, butanediol, menthyl lactate, ethanol, menthol, p-hydroxyacetophenone, caprylyl hydroximic acid, ascorbyl palmitate, hydroxyphenyl propionamide benzoic acid, modified corn starch, plant extract, isopropyl palmitate, hydroxypropyl cellulose, maltodextrin, anthocyanin, lutein, 1, 2-hexanediol, phenoxyethanol, ethylhexyl glycerol and the like. The preparation is suitable for use around eyes, can quickly nourish eye muscle tissues and brighten skin around the eyes, and can penetrate into cells around the eyes to promote self-repair of cells of part of the eyes, so that the effect of eye skin care is achieved. The product is mild, has no irritation, and has high safety.
Description
Technical Field
The invention belongs to the technical field of eye cosmetics, and particularly relates to a daily eye repair composition, a preparation method and application thereof.
Background
The skin around the eyes is the weakest skin of a human body, sweat glands and sebaceous glands of the skin around the eyes are rarely distributed, elastic fibers and collagen structures are lacked in a dermis layer, nerve fibers and capillary vessels of the skin around the eyes are high in distribution density, and the eyes are heavily loaded in work; and lymph circulation and blood circulation become slower with age, blood backflow is insufficient, skin around the eyes is darker, and various problems such as accumulation of hemoglobin in connective tissues and formation of dark circles are frequent.
The related technology discloses an anti-aging eye cream containing astaxanthin nanoemulsion and a preparation method and application thereof, and the anti-aging eye cream comprises the following components: honey, self-made astaxanthin extract, modified nano pearl powder, lily essential oil, tea saponin, natural oil, milk, water, aloe powder, glutathione and glycerol. The prepared eye cream has high astaxanthin content, good skin absorption rate, excellent oxidation resistance and wrinkle resistance and high safety.
The related technology discloses a mild firming and repairing eye cream and a preparation method and application thereof, wherein the eye cream comprises the following components: retinol palmitate, palmitoyl oligopeptide, further preferred eye creams include: retinol palmitate, palmitoyl oligopeptide, radix astragali extract, rhizoma Atractylodis Macrocephalae extract, and radix Altaicae extract. The composition has good effects of removing skin wrinkles and the like, is added into a matrix to prepare eye cream, and has mild, compact and repairing effects on the skin of eyes; it also has good stability.
The eye care products disclosed in the prior art mainly have the following defects: firstly, in order to specially improve certain specific effects, a plurality of products are produced, the effects of the products are relatively single, only moisture is preserved, eye bags are reduced, only black eye circles are faded, wrinkles are improved, and the eye conditions which actually occur are complex and compared, the effects of the products cannot be considered at the same time, and the eye problems cannot be comprehensively improved; ② although the eye mask can take effect quickly, after a period of time, side effects are easy to generate, such as new problems of fat particles and the like, and the fat particles are removed by means of operations and the like, thereby further increasing the eye burden.
Disclosure of Invention
In order to solve the problems in the prior art, the invention aims to provide a daily eye repair composition, a preparation method and application thereof.
The technical scheme adopted by the invention is as follows: the daily eye repair composition is mainly prepared from the following raw materials in parts by mass:
0.5-20 parts of acrylic acid (ester)/C10-30 parts of alkyl acrylate cross-linked polymer, 0.5-4 parts of allantoin, 10-90 parts of propylene glycol, 0.05-9 parts of dipropylene glycol, 1-7 parts of triethanolamine, 10-90 parts of butanediol, 0.08-30 parts of menthyl lactate, 20-130 parts of ethanol, 0.8-60 parts of menthol, 0.8-60 parts of borneol, 0.05-5 parts of camphor, 1-7 parts of p-hydroxyacetophenone, 0.8-40 parts of 1, 3-propanediol, 0.05-4 parts of caprylyl hydroximic acid, 0.005-2.5 parts of ascorbyl palmitate, 0.08-8 parts of hydroxyphenylpropionamide benzoic acid, 0.0001-5.5 parts of glucose, 0.0001-1.5 parts of modified corn starch, 0.19-280 parts of plant extract, 0.8-12 parts of isopropyl palmitate, 0.05-1.5 parts of hydroxypropyl cellulose, 0.05-1.5 parts of maltodextrin, 0.001-12 parts of anthocyanin, 0.01-11 parts of lutein, 1-7 parts of 1, 2-pentanediol, 1-7 parts of 1, 2-hexanediol, 0.05-8 parts of methyl diisopropyl propionamide, 0.05-8 parts of glycerol, 0.8-12 parts of menthane formyl ethylamine, 1-10 parts of phenoxyethanol, 0.05-8 parts of ethyl hexyl glycerol and 5-35 parts of water.
Preferably, the composition is mainly prepared from the following raw materials in parts by mass:
acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer 1-10 parts, allantoin 1-2 parts, propylene glycol 20-80 parts, dipropylene glycol 0.1-7 parts, triethanolamine 2-5 parts, butanediol 20-80 parts, menthyl lactate 1-20 parts, ethanol 30-100 parts, menthol 1-50 parts, borneol 1-50 parts, camphor 0.1-3 parts, p-hydroxyacetophenone 2-5 parts, 1, 3-propanediol 1-30 parts, caprylyl hydroximic acid 0.1-2 parts, ascorbyl palmitate 0.01-2 parts, hydroxyphenylpropionamide benzoic acid 0.1-6 parts, glucose 0.001-5 parts, modified corn starch 0.001-1 part, plant extract 0.28-200 parts, isopropyl palmitate 1-10 parts, hydroxypropyl cellulose 0.1-1 part, 0.1-1 part of maltodextrin, 0.01-10 parts of anthocyanin, 0.1-10 parts of lutein, 2-5 parts of 1, 2-pentanediol, 2-5 parts of 1, 2-hexanediol, 0.1-5 parts of methyl diisopropyl propionamide, 0.1-5 parts of glycerol, 1-10 parts of menthane formyl ethylamine, 2-8 parts of phenoxyethanol, 0.1-5 parts of ethylhexyl glycerol and 10-30 parts of water.
Preferably, the plant extract includes a combination of salvia miltiorrhiza extract, pomegranate fruit extract, rosa canina fruit extract, castanea sativa seed extract, cassia tora seed extract, mulberry fruit extract, astragalus mongholicus extract, safflower carthamus extract, coptis chinensis extract, ligusticum wallichii extract, ginseng extract, polygonatum sibiricum extract, saposhnikovia divaricata extract, cranberry fruit extract, schizonepeta cataria extract, lycium barbarum extract and chamomile flower extract.
Extract of Salvia MILTIORRHIZA (Salvia Miltiorrhiza): promoting endothelial repair, relieving inflammation, increasing capillary network opening amount, and increasing blood flow rate and flow rate, thereby improving microcirculation disturbance.
Pomegranate (PUNICA GRANATUM) fruit extract: the skin care product has the effects of resisting oxidation, diminishing inflammation, resisting bacteria and the like, and the effective components are anthocyanin, pomegranate polyphenol and ellagic acid which are extremely strong antioxidant substances and can effectively delay skin aging, preserve moisture and resist wrinkles.
Rosa CANINA (ROSA CANINA) fruit extract: the compound has proliferative activity on vascular endothelial cells, can enhance the strength of blood vessels and prevent red blood filaments of skin, and has the effect of increasing the content of ceramide in sebum and softening skin; inhibiting elastase, resisting wrinkle, and resisting aging by combining DOD-like activity.
Castanea sativa (CASTANEA SATIVA) seed extract: has good oxidation resistance, strong scavenging effect on various free radicals, and can be used as antioxidant for cosmetics; has effects in inhibiting elastase activity, slowing down elastin degradation, maintaining skin elasticity, and resisting aging.
Semen Cassiae (Cassia TORA) seed extract: has effects in regulating skin, tranquilizing mind, and relieving fatigue.
Mulberry (MORUS ALBA) fruit extract: contains reducing sugar, pentosan, galactoside, tannin, flavone, etc. Can inhibit elastase, and has antiaging effect; promoting the synthesis of fiber bud cell brain amide and softening and moistening skin; can well prevent and treat acne caused by high androgen; has contraction effect on collagen fiber, and can be used for reducing weight; promoting the activation of luciferase, and showing that the luciferase has anti-inflammatory efficacy; can inhibit tyrosinase activity, and has skin whitening effect.
Extract of Astragalus MONGHOLICUS (Astragalus MEMBRANACEUS MONGHOLICUS): has good skin compatibility and high polysaccharide content, and is a good film forming component. Can be used as emulsion stabilizer, skin film forming agent, and viscosity control agent.
Safflower (CARTHAMUS TINCTORIUS) extract: the natural pigments such as safflower yellow and safflower red extracted from safflower are safe and edible and can be used as coloring agent of high-grade cosmetics; the Carthami flos extract has effects of promoting blood circulation, resisting inflammation, resisting oxidation, whitening skin, preventing sunburn and resisting aging by improving skin blood circulation, promoting skin metabolism, scavenging free radicals, inhibiting melanin deposition, accelerating speckle and decolorizing, and absorbing ultraviolet, and can be used for treating contact dermatitis, seborrheic dermatitis, pruritus, and neurodermatitis; the safflower oil can be used as oily raw material of cosmetics to deeply supplement various nutritional ingredients of skin.
Extract of COPTIS CHINENSIS (COPTIS CHINENSIS): contains berberine, coptisine, methyl coptisine, tetrandrine, etc., and can be used for treating acute conjunctivitis, acute bacillary dysentery, acute gastroenteritis, hematemesis, carbuncle, furuncle, sore, and ulcer. Antibacterial, antifungal, antiviral, anti-amoebic, antiinflammatory, anti-diarrhea, cardiovascular, antipyretic, hypoglycemic, antioxidant, and blood system affecting effects. The product is mainly used for skin conditioning, antioxidation and sterilization in cosmetics.
Rhizoma Chuanxiong (Ligusticum CHUANXIONG) extract: can inhibit the generation of free radicals and effectively eliminate oxygen free radicals; at lower concentration, the activity of melanocyte can be effectively inhibited, and the generation of melanin is reduced, but the cytotoxicity effect is shown when the concentration is too high; it also has moisture absorption and moisture keeping effects.
GINSENG (PANAX GINSENG) extract: it can delay skin aging, prevent skin from drying and dehydrating, and increase skin elasticity, thereby protecting skin luster and tenderness, and preventing and reducing skin wrinkle, and the Ginseng radix active substance also has melanin reduction inhibiting effect, and can whiten and smooth skin. The hair conditioner can expand the capillary vessels of the head, increase the nutrition of the hair, improve the toughness of the hair, reduce the hair loss and the hair breakage and has the protection effect on the damaged hair.
Rhizoma Polygonati (Polygonatum SIBIRICUM) extract: in the culture of fiber bud cells and the like, the collagen proliferation is well promoted, so that the metabolism of the dermal layer of the skin can be enhanced, and the collagen anti-aging cosmetic has oxidation resistance and can be used in cosmetics for activating the skin and resisting wrinkles; has effects in promoting proliferation of vascular endothelial cells, strengthening and solidifying capillary vessels, and can be used for preventing and treating red blood streak.
Saposhnikovia DIVARICATA (Saposhnikovia DIVARICATA) extract: contains many coumarin compounds and chromone compounds. A small amount of the divaricate saposhnikovia root volatile oil is used for preparing essence; in the test of fat cell hydrolysis in a test tube, the radix Saposhnikoviae extract has effect in promoting fat hydrolysis, and can be used for weight reducing product; has effects in scavenging free radicals, and can be used as antioxidant; has certain inhibiting effect on melanin, and can be used as whitening product; can shrink pores, and can be used as astringent; it also has antibacterial and anti-inflammatory effects.
Bilberry (Vaccinium VITIS-IDAEA) fruit extract: can effectively prevent the formation of melanin in European clothes, and has whitening effect.
Herba Schizonepetae (SCHIZONEPETA TENUIFOLIA) extract: can be used for improving skin water metabolism and relieving skin aging.
Extract of Lycium barbarum (Lycium CHINENSE): has strong oxidation resistance. It has an oxidative radical absorption capacity of 25,000 (relative to blueberry 2,500), and is rich in calcium, potassium, iron, zinc, selenium, vitamin B and vitamin C. A study in China in 1991 showed that phytochemicals (phytochemicals) in Lycium barbarum can help prevent oxidation of DNA and restore damaged DNA.
Camomile (CHAMOMILLA RECUTITA) flower extract: can well relieve skin, resist skin sensitivity, and has antiinflammatory, antibacterial and antioxidant effects. The effects of soothing and deeply moisturizing can play a role in quickly relieving the skin problems.
A daily eye repair preparation made from the daily eye repair composition.
A method of preparing a daily eye repair formulation, the method of preparation comprising:
s1, selecting butanediol and menthyl lactate according to corresponding mass parts, mixing, heating and stirring until the menthyl lactate is completely dissolved, and obtaining a preparative phase A;
s2, selecting ethanol, menthol, borneol and camphor according to corresponding parts by weight, and mixing uniformly until the menthol, the borneol and the camphor are completely dissolved to obtain a prepared phase B;
s3, selecting p-hydroxyacetophenone, 1, 3-propylene glycol and caprylyl hydroximic acid according to corresponding parts by weight, mixing, heating and stirring until the p-hydroxyacetophenone and the caprylyl hydroximic acid are completely dissolved to obtain a prepared phase C;
s4, selecting glucose, modified corn starch, plant extract, isopropyl palmitate, hydroxypropyl cellulose, maltodextrin, anthocyanin and lutein according to corresponding parts by weight, mixing, adding deionized water, stirring until the mixture is completely dissolved, and filtering to obtain a preliminary phase D;
s5, selecting water and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer according to corresponding mass parts, mixing the mixture to a uniform water solution, adding allantoin, propylene glycol and dipropylene glycol, stirring, heating, homogenizing, cooling to 55-60 ℃, adding triethanolamine, mixing, and defoaming; cooling to 50-55 deg.C, adding the preparative phase A and the preparative phase C, and mixing for 10-13 min; cooling to 40-45 deg.C again, adding preparative phase B, preparative phase D, ascorbyl palmitate, hydroxyphenyl propionamide benzoic acid, 1, 2-pentanediol, 1, 2-hexanediol, methyl diisopropyl propionamide, glycerol, menthane formyl ethylamine, phenoxyethanol and ethylhexyl glycerol, mixing for 20-28min, and filtering.
In the preparation process, the raw materials play the following roles:
solvent and humectant efficacy: water, allantoin (skin protectants and anti-irritants), dipropylene glycol, butylene glycol, ethanol, glucose, and glycerol;
wetting agent: propylene glycol, 1, 3-propanediol;
film-forming agent: acrylic acid (ester)/C10-30 alkanol acrylate crosspolymer, modified corn starch;
complexing agent and stabilizer: triethanolamine, caprylyl hydroxamic acid;
a cooling agent: menthyl lactate, menthane formylethylamine;
antioxidant, anti-aging agent: borneol, p-hydroxyacetophenone, ascorbyl palmitate, plant extracts (salvia miltiorrhiza extract, pomegranate fruit extract, rosa canina fruit extract, castanea sativa seed extract, cassia tora seed extract, mulberry fruit extract, astragalus mongholicus extract, safflower carthamus extract, coptis chinensis extract, ligusticum wallichii extract, ginseng extract, polygonatum sibiricum extract, saposhnikovia divaricata extract, bilberry fruit extract, schizonepeta herb extract, lycium barbarum extract and chamomile flower extract), anthocyanin and lutein;
a allergy-relieving agent: menthol, hydroxyphenylpropionamide benzoic acid;
preservative: camphor, phenoxyethanol;
solubilizer: 1, 2-pentanediol, 1, 2-hexanediol;
emulsifier: methyl diisopropyl propionamide;
softening agent: ethyl hexyl glycerol;
nonionic surfactant: isopropyl palmitate;
thickening agent: hydroxypropyl cellulose (emulsifier, surfactant), maltodextrin.
Preferably, in the S1, the heating temperature is 40-45 ℃, and the stirring is carried out for 8-10 min;
in the step S2, the mixing time is 20-25 min.
Preferably, in the S3, the heating temperature is 60-70 ℃, and the heating and stirring time is 10-15 min;
in the step S4, the stirring time is 30-35 min.
Preferably, in the S5, the mixing time of the water and the acrylic/C10-30 alkanol acrylate crosslinked polymer is 10-15 min;
stirring the allantoin, the propylene glycol and the dipropylene glycol for 5-8min when heating; heating to 75-85 deg.C for 20-25 min;
the homogenizing treatment time is 3-5min, and the rotating speed is 2000-4000 r/min.
Preferably, in the S5, the filter cloth passes through 200-250 meshes.
An application of a daily eye repairing preparation in preparing eye cosmetics.
The invention has the beneficial effects that:
the invention provides a daily eye repair preparation which is prepared from acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, allantoin, propylene glycol, dipropylene glycol, triethanolamine, butanediol, menthyl lactate, ethanol, menthol, borneol, camphor, p-hydroxyacetophenone, 1, 3-propanediol, caprylyl hydroximic acid, ascorbyl palmitate, hydroxyphenylpropionamide benzoic acid, glucose, modified corn starch, plant extracts (salvia miltiorrhiza extract, pomegranate fruit extract, rosa canina fruit extract, europaea seed extract, cassia seed extract, mulberry fruit extract, astragalus mongholicus extract, safflower carthamus extract, coptis chinensis extract, ligusticum wallichii extract, ginseng extract, polygonatum sibiricum extract, saposhnikovia divaricata extract, bilberry extract, schizonepeta tenuifolia extract, medlar extract and chamomile flower extract), Isopropyl palmitate, hydroxypropyl cellulose, maltodextrin, anthocyanin, lutein, 1, 2-pentanediol, 1, 2-hexanediol, methyl diisopropyl propionamide, glycerol, menthane formyl ethylamine, phenoxyethanol, ethylhexyl glycerol and water.
The preparation is prepared by processing raw materials in multiple steps, and ensures that all the raw materials are fully dissolved by heating, stirring and other modes in each processing process, thereby further ensuring the quality of the product and the sufficiency of the content of effective components.
The preparation is suitable for use around eyes, can quickly nourish eye muscle tissues and brighten skin around the eyes, and can penetrate into cells around the eyes to promote self-repair of cells of part of the eyes, so that the effect of eye skin care is achieved. The product is mild, has no irritation, and has high safety.
Detailed Description
The present invention is further illustrated below with reference to specific examples. It will be appreciated by those skilled in the art that the following examples, which are set forth to illustrate the present invention, are intended to be part of the present invention, but not to be construed as limiting the scope of the present invention. The reagents used are all conventional products which are commercially available.
Example 1:
a method of preparing a daily eye repair formulation, the method of preparation comprising:
s1, selecting 10 parts of butanediol and 0.08 part of menthyl lactate according to corresponding mass parts, mixing, heating to 40 ℃, stirring for 8min until the menthyl lactate is completely dissolved, and obtaining a prepared phase A;
s2, selecting 20 parts of ethanol, 0.8 part of menthol, 0.8 part of borneol and 0.05 part of camphor according to corresponding mass parts, and mixing uniformly for 20min until the menthol, the borneol and the camphor are completely dissolved to obtain a prepared phase B;
s3, selecting 1 part of p-hydroxyacetophenone, 0.8 part of 1, 3-propylene glycol and 0.05 part of caprylyl hydroximic acid according to corresponding parts by weight, mixing, heating to 60 ℃, stirring for 10min until the p-hydroxyacetophenone and the caprylyl hydroximic acid are completely dissolved, and obtaining a preparation phase C;
s4, selecting 0.0001 part of glucose, 0.0001 part of modified corn starch, 0.19 part of plant extract (red sage root extract, pomegranate fruit extract, rosa canina fruit extract, castanea sativa seed extract, cassia tora seed extract, mulberry fruit extract, astragalus mongholicus extract, safflower carthamus extract, coptis chinensis extract, ligusticum wallichii extract, ginseng extract, polygonatum sibiricum extract, divaricate saposhnikovia root extract, bilberry fruit extract, schizonepeta cata extract, medlar extract and chamomile flower extract), 0.8 part of isopropyl palmitate, 0.05 part of hydroxypropyl cellulose, 0.05 part of maltodextrin, 0.001 part of anthocyanin and 0.01 part of lutein according to corresponding parts by mass, mixing, adding deionized water, stirring for 30min until the anthocyanins are completely dissolved, and filtering to obtain a prepared phase D;
s5, selecting 5 parts of water and 0.5 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer according to corresponding mass parts, mixing for 10min to obtain a uniform aqueous solution, adding 0.5 part of allantoin, 10 parts of propylene glycol and 0.05 part of dipropylene glycol, stirring for 5min, heating to 75 ℃, treating for 20min, homogenizing for 3min (the rotation speed is 2000-4000r/min), cooling to 55-60 ℃, adding 1 part of triethanolamine, mixing, and defoaming; cooling to 50-55 deg.C, adding the preparative phase A and the preparative phase C, and mixing for 10-13 min; cooling to 40-45 deg.C again, adding preparative phase B, preparative phase D, 0.005 part of ascorbyl palmitate, 0.08 part of hydroxyphenyl propionamide benzoic acid, 1 part of 1, 2-pentanediol, 1, 2-hexanediol, 0.05 part of methyl diisopropyl propionamide, 0.05 part of glycerol, 0.8 part of menthane formyl ethylamine, 1 part of phenoxyethanol and 0.05 part of ethyl hexyl glycerol, mixing for 20-28min, and filtering with 200 mesh filter cloth.
Example 2:
a method of making a daily eye repair formulation comprising:
s1, selecting 90 parts of butanediol and 30 parts of menthyl lactate according to corresponding mass parts, mixing, heating to 45 ℃, and stirring for 10min until the menthyl lactate is completely dissolved to obtain a prepared phase A;
s2, selecting 130 parts of ethanol, 60 parts of menthol, 60 parts of borneol and 5 parts of camphor according to corresponding mass parts, mixing uniformly for 25min until the menthol, the borneol and the camphor are completely dissolved to obtain a prepared phase B;
s3, selecting 7 parts of p-hydroxyacetophenone, 40 parts of 1, 3-propylene glycol and 4 parts of caprylyl hydroximic acid according to corresponding parts by weight, mixing, heating to 70 ℃, stirring for 15min until the p-hydroxyacetophenone and the caprylyl hydroximic acid are completely dissolved, and obtaining a preparation phase C;
s4, selecting 5.5 parts of glucose, 1.5 parts of modified corn starch, 280 parts of plant extracts (a red sage root extract, a pomegranate fruit extract, a rosa canina fruit extract, a castanea sativa seed extract, a cassia tora seed extract, a mulberry fruit extract, a mongolian milkvetch root extract, a safflower extract, a coptis chinensis extract, a ligusticum wallichii extract, a ginseng extract, a polygonatum sibiricum extract, a divaricate saposhnikovia root extract, a bilberry fruit extract, a schizonepeta herb extract, a medlar extract and a chamomile flower extract), 12 parts of isopropyl palmitate, 1.5 parts of hydroxypropyl fiber, 1.5 parts of maltodextrin, 12 parts of anthocyanin and 11 parts of lutein according to corresponding parts by mass, mixing, adding deionized water, stirring for 35min, completely dissolving, and filtering to obtain a preparation phase D;
s5, selecting 35 parts of water and 20 parts of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer according to corresponding mass parts, mixing for 15min to obtain a uniform water solution, adding 4 parts of allantoin, 90 parts of propylene glycol and 9 parts of dipropylene glycol, stirring for 8min, heating to 85 ℃, treating for 25min, homogenizing for 5min (the rotating speed is 2000-4000r/min), cooling to 55-60 ℃, adding 7 parts of triethanolamine, mixing, and defoaming; cooling to 50-55 deg.C, adding the preparative phase A and the preparative phase C, and mixing for 10-13 min; cooling to 40-45 deg.C again, adding preparative phase B, preparative phase D, 2.5 parts of ascorbyl palmitate, 8 parts of hydroxyphenyl propionamide benzoic acid, 7 parts of 1, 2-pentanediol, 7 parts of 1, 2-hexanediol, 8 parts of methyl diisopropyl propionamide, 8 parts of glycerol, 12 parts of menthane formyl ethylamine, 10 parts of phenoxyethanol and 8 parts of ethylhexyl glycerol, mixing for 20-28min, and filtering with 250 mesh filter cloth.
Example 3:
a method of preparing a daily eye repair formulation, the method of preparation comprising:
s1, selecting 20 parts of butanediol and 1 part of menthyl lactate according to corresponding mass parts, mixing, heating to 40 ℃, stirring for 8min until the menthyl lactate is completely dissolved, and obtaining a prepared phase A;
s2, selecting 30 parts of ethanol, 1 part of menthol, 1 part of borneol and 0.1 part of camphor according to corresponding mass parts, and mixing uniformly for 20min until the menthol, the borneol and the camphor are completely dissolved to obtain a prepared phase B;
s3, selecting 2 parts of p-hydroxyacetophenone, 1 part of 1, 3-propylene glycol and 0.1 part of caprylyl hydroximic acid according to corresponding parts by weight, mixing, heating to 60 ℃, stirring for 15min until the p-hydroxyacetophenone and the caprylyl hydroximic acid are completely dissolved, and obtaining a prepared phase C;
s4, selecting 0.001 part of glucose, 0.001 part of modified corn starch, 0.28 part of plant extract (red sage root extract, pomegranate fruit extract, rosa canina fruit extract, castanea sativa seed extract, cassia tora seed extract, mulberry fruit extract, astragalus mongholicus extract, safflower carthamus extract, coptis chinensis extract, ligusticum wallichii extract, ginseng extract, polygonatum sibiricum extract, divaricate saposhnikovia root extract, bilberry fruit extract, schizonepeta tenuifolia extract, medlar extract and chamomile extract), 1 part of isopropyl palmitate, 0.1 part of hydroxypropyl cellulose, 0.1 part of maltodextrin, 0.01 part of anthocyanin and 0.1 part of lutein according to corresponding mass parts, mixing, adding deionized water, stirring for 30min until complete dissolution, and filtering to obtain a preliminary phase D;
s5, selecting 10 parts of water and 1 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer according to corresponding mass parts, mixing for 10min to obtain a uniform water solution, adding 1 part of allantoin, 20 parts of propylene glycol and 0.1 part of dipropylene glycol, stirring for 5min, heating to 75 ℃, treating for 20min, homogenizing for 3min (the rotating speed is 2000-4000r/min), cooling to 55-60 ℃, adding 2 parts of triethanolamine, mixing, and defoaming; cooling to 50-55 deg.C, adding the preparative phase A and the preparative phase C, and mixing for 10-13 min; cooling to 40-45 deg.C again, adding preparative phase B, preparative phase D, 0.01 part of ascorbyl palmitate, 0.1 part of hydroxyphenyl propionamide benzoic acid, 2 parts of 1, 2-pentanediol, 2 parts of 1, 2-hexanediol, 0.1 part of methyl diisopropyl propionamide, 0.1 part of glycerol, 1 part of menthane formyl ethylamine, 2 parts of phenoxyethanol and 0.1 part of ethylhexyl glycerol, mixing for 20-28min, and filtering with 200 mesh filter cloth.
Example 4:
a method of preparing a daily eye repair formulation, the method of preparation comprising:
s1, selecting 80 parts of butanediol and 20 parts of menthyl lactate according to corresponding mass parts, mixing, heating to 45 ℃, and stirring for 10min until the menthyl lactate is completely dissolved to obtain a prepared phase A;
s2, selecting 100 parts of ethanol, 50 parts of menthol, 50 parts of borneol and 3 parts of camphor according to corresponding mass parts, mixing uniformly for 25min until the menthol, the borneol and the camphor are completely dissolved to obtain a prepared phase B;
s3, selecting 5 parts of p-hydroxyacetophenone, 30 parts of 1, 3-propylene glycol and 2 parts of caprylyl hydroximic acid according to corresponding parts by weight, mixing, heating to 70 ℃, stirring for 10min until the p-hydroxyacetophenone and the caprylyl hydroximic acid are completely dissolved, and obtaining a preparation phase C;
s4, selecting 5 parts of glucose, 1 part of modified corn starch, 200 parts of plant extracts (a red sage root extract, a pomegranate fruit extract, a rosa canina fruit extract, a castanea sativa seed extract, a cassia tora seed extract, a mulberry fruit extract, a mongolian milkvetch root extract, a safflower extract, a coptis chinensis extract, a ligusticum wallichii extract, a ginseng extract, a polygonatum sibiricum extract, a divaricate saposhnikovia root extract, a bilberry fruit extract, a schizonepeta herb extract, a medlar extract and a chamomile flower extract), 10 parts of isopropyl palmitate, 1 part of hydroxypropyl cellulose, 1 part of maltodextrin, 10 parts of anthocyanin and 10 parts of lutein according to corresponding parts by mass, mixing, adding deionized water, stirring for 35min until complete dissolution, and filtering to obtain a preliminary phase D;
s5, selecting 30 parts of water and 10 parts of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer according to corresponding mass parts, mixing for 15min to obtain a uniform water solution, adding 2 parts of allantoin, 80 parts of propylene glycol and 7 parts of dipropylene glycol, stirring for 8min, heating to 85 ℃, treating for 25min, homogenizing for 5min (the rotating speed is 2000-4000r/min), cooling to 55-60 ℃, adding 5 parts of triethanolamine, mixing, and defoaming; cooling to 50-55 deg.C, adding the preparative phase A and the preparative phase C, and mixing for 10-13 min; cooling to 40-45 deg.C again, adding preparative phase B, preparative phase D, 2 parts of ascorbyl palmitate, 6 parts of hydroxyphenyl propionamide benzoic acid, 5 parts of 1, 2-pentanediol, 5 parts of 1, 2-hexanediol, 5 parts of methyl diisopropyl propionamide, 5 parts of glycerol, 10 parts of menthane formyl ethylamine, 8 parts of phenoxyethanol and 5 parts of ethyl hexyl glycerol, mixing for 20-28min, and filtering with 250 mesh filter cloth.
And (4) testing results:
and (4) checking and numbering: GF 01152021429217.
Inspecting the product: yellow emulsion, 35 ml/count.
And (4) checking items: evaluating the safety of the cosmetics; the basis of the inspection is as follows: technical Specifications for cosmetic safety (2015 edition).
And (4) testing results:
and (3) microbial test results:
the data results show that: the detection results of all items in the microbial detection meet the requirements.
And (3) physical and chemical inspection results:
the data results show that: the detection results of all items in the physical and chemical inspection all meet the requirements.
Product inspection: and (4) checking and numbering: 01042100010028
The above results show that: the product meets the requirement of inspection basis (GB/T29665-2013 skin care emulsion).
And (4) checking and numbering: 01042100010030
The above results show that: all detection indexes meet the requirements.
The present invention is not limited to the above alternative embodiments, and any other products in various forms can be obtained by the present invention, and the present invention is within the protection scope of the present invention. The above embodiments should not be construed as limiting the scope of the present invention, and it will be understood by those skilled in the art that modifications may be made to the technical solutions described in the above embodiments, or equivalent substitutions may be made to some or all of the technical features thereof, without departing from the scope of the present invention, and at the same time, such modifications or substitutions may not make the essence of the corresponding technical solutions depart from the scope of the embodiments of the present invention.
Claims (10)
1. The daily eye repair composition is characterized by being mainly prepared from the following raw materials in parts by mass:
0.5-20 parts of acrylic acid (ester)/C10-30 parts of alkyl acrylate cross-linked polymer, 0.5-4 parts of allantoin, 10-90 parts of propylene glycol, 0.05-9 parts of dipropylene glycol, 1-7 parts of triethanolamine, 10-90 parts of butanediol, 0.08-30 parts of menthyl lactate, 20-130 parts of ethanol, 0.8-60 parts of menthol, 0.8-60 parts of borneol, 0.05-5 parts of camphor, 1-7 parts of p-hydroxyacetophenone, 0.8-40 parts of 1, 3-propanediol, 0.05-4 parts of caprylyl hydroximic acid, 0.005-2.5 parts of ascorbyl palmitate, 0.08-8 parts of hydroxyphenylpropionamide benzoic acid, 0.0001-5.5 parts of glucose, 0.0001-1.5 parts of modified corn starch, 0.19-280 parts of plant extract, 0.8-12 parts of isopropyl palmitate, 0.05-1.5 parts of hydroxypropyl cellulose, 0.05-1.5 parts of maltodextrin, 0.001-12 parts of anthocyanin, 0.01-11 parts of lutein, 1-7 parts of 1, 2-pentanediol, 1-7 parts of 1, 2-hexanediol, 0.05-8 parts of methyl diisopropyl propionamide, 0.05-8 parts of glycerol, 0.8-12 parts of menthane formyl ethylamine, 1-10 parts of phenoxyethanol, 0.05-8 parts of ethyl hexyl glycerol and 5-35 parts of water.
2. The daily eye repair composition according to claim 1, wherein the composition is prepared from the following raw materials in parts by mass:
acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer 1-10 parts, allantoin 1-2 parts, propylene glycol 20-80 parts, dipropylene glycol 0.1-7 parts, triethanolamine 2-5 parts, butanediol 20-80 parts, menthyl lactate 1-20 parts, ethanol 30-100 parts, menthol 1-50 parts, borneol 1-50 parts, camphor 0.1-3 parts, p-hydroxyacetophenone 2-5 parts, 1, 3-propanediol 1-30 parts, caprylyl hydroximic acid 0.1-2 parts, ascorbyl palmitate 0.01-2 parts, hydroxyphenylpropionamide benzoic acid 0.1-6 parts, glucose 0.001-5 parts, modified corn starch 0.001-1 part, plant extract 0.28-200 parts, isopropyl palmitate 1-10 parts, hydroxypropyl cellulose 0.1-1 part, 0.1-1 part of maltodextrin, 0.01-10 parts of anthocyanin, 0.1-10 parts of lutein, 2-5 parts of 1, 2-pentanediol, 2-5 parts of 1, 2-hexanediol, 0.1-5 parts of methyl diisopropyl propionamide, 0.1-5 parts of glycerol, 1-10 parts of menthane formyl ethylamine, 2-8 parts of phenoxyethanol, 0.1-5 parts of ethylhexyl glycerol and 10-30 parts of water.
3. The daily eye care composition according to any one of claims 1 to 2 wherein the plant extract comprises a combination of red sage extract, pomegranate fruit extract, rose hip extract, castanea sativa seed extract, cassia tora seed extract, mulberry fruit extract, astragalus mongholicus extract, safflower extract, coptis chinensis extract, ligusticum wallichii extract, ginseng extract, polygonatum rhizome extract, ledebouriella root extract, bilberry fruit extract, schizonepeta herb extract, lycium barbarum extract and chamomile flower extract.
4. A daily eye repair formulation made from the daily eye repair composition of any one of claims 1-2.
5. A method of making the daily eye repair formulation of claim 4 comprising:
s1, selecting butanediol and menthyl lactate according to corresponding mass parts, mixing, heating and stirring until the menthyl lactate is completely dissolved, and obtaining a preparative phase A;
s2, selecting ethanol, menthol, borneol and camphor according to corresponding parts by weight, and mixing uniformly until the menthol, the borneol and the camphor are completely dissolved to obtain a prepared phase B;
s3, selecting p-hydroxyacetophenone, 1, 3-propylene glycol and caprylyl hydroximic acid according to corresponding parts by weight, mixing, heating and stirring until the p-hydroxyacetophenone and the caprylyl hydroximic acid are completely dissolved, and obtaining a preparation phase C;
s4, selecting glucose, modified corn starch, plant extract, isopropyl palmitate, hydroxypropyl cellulose, maltodextrin, anthocyanin and lutein according to corresponding parts by weight, mixing, adding deionized water, stirring until the mixture is completely dissolved, and filtering to obtain a preliminary phase D;
s5, selecting water and acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer according to corresponding mass parts, mixing the mixture to a uniform water solution, adding allantoin, propylene glycol and dipropylene glycol, stirring, heating, homogenizing, cooling to 55-60 ℃, adding triethanolamine, mixing, and defoaming; cooling to 50-55 deg.C, adding the preparative phase A and the preparative phase C, and mixing for 10-13 min; cooling to 40-45 deg.C again, adding preparative phase B, preparative phase D, ascorbyl palmitate, hydroxyphenyl propionamide benzoic acid, 1, 2-pentanediol, 1, 2-hexanediol, methyl diisopropyl propionamide, glycerol, menthane formyl ethylamine, phenoxyethanol and ethylhexyl glycerol, mixing for 20-28min, and filtering.
6. The method for preparing a daily ophthalmic repair preparation according to claim 5 wherein in the step S1, the temperature is heated to 40-45 ℃ and the stirring is carried out for 8-10 min;
in the step S2, the mixing time is 20-25 min.
7. The method for preparing a daily ophthalmic repair preparation according to claim 5 wherein in the step S3, the heating temperature is 60-70 ℃, and the heating and stirring time is 10-15 min;
in the step S4, the stirring time is 30-35 min.
8. The method for preparing a daily eye-rejuvenating formulation as claimed in claim 5 wherein in said S5, the mixing time of water and acrylic/C10-30 alkanol acrylate crosspolymer is 10-15 min;
stirring the allantoin, the propylene glycol and the dipropylene glycol for 5-8min when heating; heating to 75-85 deg.C for 20-25 min;
the homogenizing treatment time is 3-5min, and the rotating speed is 2000-4000 r/min.
9. The method for preparing the daily eye-repair preparation according to claim 5, wherein in S5, 200-mesh and 250-mesh filter cloth is used.
10. Use of the daily eye repair formulation of claim 4 in the preparation of an eye cosmetic.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN116850235A (en) * | 2023-01-06 | 2023-10-10 | 唐建 | Pharmaceutical preparation for removing eye wrinkles and preparation method thereof |
GB2626306A (en) * | 2023-01-10 | 2024-07-24 | Delsys Tech Limited | Agrochemical compositions |
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CN110787082A (en) * | 2019-09-29 | 2020-02-14 | 广州达达眼健康管理有限公司 | Eye cell repair composition and eye care product containing same |
CN111419784A (en) * | 2020-05-07 | 2020-07-17 | 深圳市玉莱漫科技发展有限公司 | NMN-containing anti-wrinkle eye cream and preparation method and application thereof |
CN112618460A (en) * | 2021-01-05 | 2021-04-09 | 叶敏康 | Plant energy eye mask and preparation method thereof |
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2022
- 2022-05-10 CN CN202210507515.5A patent/CN114831916A/en active Pending
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110787082A (en) * | 2019-09-29 | 2020-02-14 | 广州达达眼健康管理有限公司 | Eye cell repair composition and eye care product containing same |
CN111419784A (en) * | 2020-05-07 | 2020-07-17 | 深圳市玉莱漫科技发展有限公司 | NMN-containing anti-wrinkle eye cream and preparation method and application thereof |
CN112618460A (en) * | 2021-01-05 | 2021-04-09 | 叶敏康 | Plant energy eye mask and preparation method thereof |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN116850235A (en) * | 2023-01-06 | 2023-10-10 | 唐建 | Pharmaceutical preparation for removing eye wrinkles and preparation method thereof |
GB2626306A (en) * | 2023-01-10 | 2024-07-24 | Delsys Tech Limited | Agrochemical compositions |
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