CN114703025A - Cleaning powder for dish washer - Google Patents

Cleaning powder for dish washer Download PDF

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Publication number
CN114703025A
CN114703025A CN202210335211.5A CN202210335211A CN114703025A CN 114703025 A CN114703025 A CN 114703025A CN 202210335211 A CN202210335211 A CN 202210335211A CN 114703025 A CN114703025 A CN 114703025A
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China
Prior art keywords
powder
industrial
industrial hemp
hemp
cleaning
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Pending
Application number
CN202210335211.5A
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Chinese (zh)
Inventor
刘亮亮
肖爱平
张晓伟
段盛文
冷鹃
廖丽萍
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Institute of Bast Fiber Crops of CAAS
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Institute of Bast Fiber Crops of CAAS
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Priority to CN202210335211.5A priority Critical patent/CN114703025A/en
Publication of CN114703025A publication Critical patent/CN114703025A/en
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22Organic compounds
    • C11D7/40Products in which the composition is not well defined
    • C11D7/44Vegetable products
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/48Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/02Inorganic compounds
    • C11D7/04Water-soluble compounds
    • C11D7/10Salts
    • C11D7/12Carbonates bicarbonates
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/02Inorganic compounds
    • C11D7/04Water-soluble compounds
    • C11D7/10Salts
    • C11D7/14Silicates
    • C11D2111/14

Abstract

The application discloses cleaning powder for a dish washing machine, which is characterized by comprising industrial hemp powder, an industrial hemp extract and a detergent. The application provides a cleaning powder for dish washer, including industry hemp powder, industry hemp extract to and the decontaminant, have characteristics natural, nontoxic, no external enzyme preparation that adds, when guaranteeing the washing effect, reduced chemical reagent's use amount, and the addition of industry hemp composition has also increased antibacterial effect.

Description

Cleaning powder for dish washer
Technical Field
The application relates to the technical field of cleaning agents, in particular to cleaning powder for dish-washing machines
Background
With the technological progress, more and more families choose to use dish washers to replace human hands to complete dish washing work. The washing dirt of the dish washer is mainly completed by the aid of the jetting action of strong water flow in a three-dimensional space, the heat energy action of the heated water and the oil and dirt removing action of detergent which are cooperated with each other. Because of different washing principles, the detergent for the dish washing machine does not need to be foamed, and part of insoluble particles can be added in the cleaning action of the detergent to increase the purposes of physical friction cleaning and the like, so that the detergent cannot be replaced by the conventional detergent.
However, most of the existing dishwasher powder is composed of chemicals, and because the existing dishwasher powder contains a large amount of alkali, the existing dishwasher powder can emit unpleasant odor at high temperature; along with the improvement of the quality of life, people are reluctant to use washing products consisting of excessive chemical raw materials, and the influence of the chemical raw materials on the environment is gradually paid attention to; however, natural substances are used to replace chemicals, and the cost is also required to be considered, so that the use cost of consumers is prevented from being increased due to high price.
Therefore, how to provide reliable and cheap detergent for dish-washing machine for consumer is a technical problem to be solved urgently by those skilled in the art.
Disclosure of Invention
In order to solve the above technical problems, a first object of the present invention is to provide a cleaning powder for a dish washer; the application provides a cleaning powder for dish washer, including industry hemp powder, industry hemp extract to and the decontaminant, have characteristics natural, nontoxic, no external enzyme preparation that adds, when guaranteeing the washing effect, reduced chemical reagent's use amount, and the addition of industry hemp composition has also increased antibacterial effect.
The technical scheme provided by the invention is as follows:
a cleaning powder for dish washer comprises industrial hemp powder, industrial hemp extract, and detergent.
Preferably, it comprises 30-50 parts by weight of industrial hemp powder, 3-10 parts by weight of industrial hemp extract, and 40-70 parts by weight of detergent.
Preferably, 40 parts by weight of industrial hemp powder, 5 parts by weight of industrial hemp extract, and 55 parts by weight of detergent are included.
Preferably, the industrial hemp powder comprises any one or more of industrial hemp stalk powder, industrial hemp leaf powder, hemp seed hull powder.
Preferably, the industrial hemp powder comprises 60-80% of industrial hemp stalk powder, 10-20% of industrial hemp leaf powder and 10-20% of hemp seed hull powder in percentage by mass; or the like, or, alternatively,
comprises 60-75% of industrial hemp stalk powder and 25-40% of industrial hemp leaf powder; or the like, or, alternatively,
comprises 60-80% of industrial hemp stalk powder and 20-40% of hemp seed hull powder; or the like, or, alternatively,
65-85% of fructus Cannabis seed shell powder, and 15-35% of industrial folium Cannabis powder.
Preferably, the industrial hemp stalk powder, the industrial hemp leaf powder, and the hemp seed hull powder have a particle size capable of passing through a 40-60 mesh sieve.
Preferably, the industrial cannabis extract is prepared by the following method: pulverizing industrial cannabis sativa flowers and/or leaves, placing in an ethanol solution for a first standing time of 24-48h, then for a second standing time of 20-24h, press-filtering to collect an extracting solution, distilling under reduced pressure to remove ethanol, and freeze-drying to obtain the industrial cannabis sativa extract.
Preferably, after the industrial cannabis sativa flowers and/or leaves are placed in ethanol, randomly stirring for 2-3 times in the first standing process, each time for 5-10min, with the stirring speed of 100-200 rpm;
extracting industrial flos Cannabis and/or leaf with ethanol for 2-3 times, mixing the collected extractive solutions, and processing.
Preferably, the detergent is a mixture of baking soda, potassium carbonate, sodium silicate.
Preferably, the detergent comprises 15-20% of baking soda, 70-75% of potassium carbonate and 5-10% of sodium silicate by mass percentage.
The cleaning powder for the dish washing machine comprises industrial hemp powder, an industrial hemp extract and a detergent, has the characteristics of being natural, non-toxic and free of an externally added enzyme preparation, and is dish washing machine powder containing an industrial hemp raw material. Wherein, the industrial hemp powder can increase the friction force and the washing effect; the industrial hemp extract has the bacteriostatic action, and can meet the requirements of dish cleaning by matching with a detergent to remove oil stains. The application provides a cleaning powder for dish washer when guaranteeing washing effect, has reduced chemical reagent's use amount, and the addition of industry hemp composition has also increased antibacterial effect.
Preferably, the industrial hemp powder comprises any one or more of industrial hemp stalk powder, industrial hemp leaf powder, and hemp seed hull powder. The industrial hemp stalk powder can increase the physical friction capacity of the dishwasher powder, has excellent porous adsorption capacity and can adsorb dirt such as oil stain and the like. The industrial hemp leaf powder and the hemp seed hull powder contain various active ingredients, can effectively increase the washing effect and the antibacterial effect, and are environment-friendly. The industrial hemp extract is an extract obtained by taking flowers and/or leaves of industrial hemp as raw materials and extracting the raw materials by using alcohol, and the extract has an effective bacteriostatic action and is natural and safe.
Wherein, the industrial hemp stalk powder, the industrial hemp leaf powder and the hemp seed hull powder can be used together, or two of them can be selected for use. Specifically, the industrial hemp powder comprises 60-80% of industrial hemp stalk powder, 10-20% of industrial hemp leaf powder and 10-20% of hemp seed hull powder in percentage by mass; or, comprises 60-75% industrial hemp stalk powder, 25-40% industrial hemp leaf powder; or, comprises 60-80% industrial hemp stalk powder, 20-40% hemp seed hull powder; or 65-85% of fructus Cannabis seed shell powder and 15-35% of industrial folium Cannabis powder.
Preferably, the industrial hemp stalk powder, the industrial hemp leaf powder and the hemp seed hull powder have a particle size of 40-60 mesh. Specifically, the industrial hemp stalk powder is prepared by the following method: cleaning industrial hemp stems, removing dirt, drying in the shade, pulverizing, sieving with 40-60 mesh sieve, and storing in dry and dark place. The industrial hemp leaf powder and the hemp seed hull powder are respectively prepared by drying industrial hemp leaf and hemp seed hull in the shade, pulverizing, sieving with a 40-60 mesh sieve, and storing in dry and dark place.
Preferably, the industrial cannabis extract is prepared by the following method: pulverizing industrial cannabis sativa flowers and/or leaves, placing in an ethanol solution for a first standing time of 24-48h, then for a second standing time of 20-24h, press-filtering to collect an extracting solution, distilling under reduced pressure to remove ethanol, and freeze-drying to obtain the industrial cannabis sativa extract. More preferably, after the industrial cannabis sativa flowers and/or leaves are placed in ethanol, randomly stirring for 2-3 times in the standing process, each time for 5-10min, wherein the stirring speed is 100-200rpm (more preferably 120 rpm); and extracting with ethanol for 2-3 times, press filtering after each extraction to collect extractive solution, mixing multiple extractive solutions, distilling under reduced pressure to remove ethanol, and lyophilizing to obtain industrial hemp extract.
Wherein the ethanol is 70-95% by volume, preferably 95% ethanol. The second standing is carried out after the first standing is carried out for 24-48h, so that the substances can be precipitated (particularly after the first standing is stirred), and the second standing process is also a slow extraction process, so that the extraction effect can be improved, and the energy consumption can be saved.
Preferably, the detergent is a mixture of baking soda, potassium carbonate and sodium silicate, and all the components are edible components, are less harmful to the environment and have the function of removing oil stains. More preferably, the detergent comprises 15-20% of baking soda, 70-75% of potassium carbonate and 5-10% of sodium silicate by mass percent.
The application provides a cleaning powder for dish washer, with save or sell behind the above-mentioned raw materials mixing (preferably through the agitator misce bene), add the dish washer during the use and correspond the position, cooperate the washing procedure and can wash the bowl dish.
Detailed Description
In order to make those skilled in the art better understand the technical solutions in the present application, the technical solutions in the embodiments of the present application will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present application, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present application.
The performance research of the cleaning powder for the dish washer provided by the application is as follows:
the samples were prepared as follows:
cleaning industrial hemp stems, removing dirt, drying in the shade, pulverizing, sieving with 40 mesh sieve, and storing in dry and dark place.
Industrial hemp leaf powder: drying industrial hemp leaves in the shade, pulverizing, sieving with a 40-mesh sieve, and storing in dry and dark place.
Hemp seed hull powder: drying fructus Cannabis shell in the shade, pulverizing, sieving with 40 mesh sieve, and storing in dry and dark place.
Industrial hemp extract: pulverizing industrial flos Cannabis and folium Cannabis, placing the powder in 95% ethanol solution, standing for 24-48 hr while stirring for 5min at 120rpm for 3 times. And standing the tank body for 24 hours after extraction, and performing filter pressing by using a filter screen to pour out an extracting solution. Extracting for three times, and mixing the three extractive solutions. Removing alcohol from the extractive solution by vacuum distillation, transferring into freeze dryer, and lyophilizing to obtain powder. Mixing the lyophilized powder with industrial folium Cannabis powder, and stirring.
(1) Inhibition of three strains by samples
The bacteriostatic activity of the samples was studied by the filter paper method, and the sensitivity of each sample to the strain was different, and the results are shown in table 1. By comparison, the industrial hemp extract shows the optimal inhibition zone effect among the inhibition effects of the three bacteria, and the inhibition effect is obvious. And the second is industrial hemp leaf powder and industrial hemp stalk powder, and the hemp seed shell powder has relatively weak bacteriostasis and certain inhibition effect. From the results, we can determine that the raw materials used in the cleaning powder for the dishwasher provided by the application have certain inhibition effects on three bacteria, and can be used for preparing subsequent products.
TABLE 1 zone of inhibition diameter of product for three strains
Figure BDA0003576546860000051
Note: the data are all 3 parallel tests; the measurement data are expressed as mean ± standard deviation (X ± S) diameter of zone of inhibition: the sensitivity is low at 6-10.5 mm, moderate at 10.5-14.5 mm, high at 14.5-20 mm and extremely at least 20 m; "-" indicates no detection.
(2) Research on minimum inhibitory concentration of sample on staphylococcus aureus
The bacteriostatic effect of the sample on the three strains is obvious through the bacteriostatic circle results of the sample, and the staphylococcus aureus with the best inhibitory effect is selected as a research object for determining the minimum bacteriostatic concentration of the sample. The results of the inhibition zones of the samples in table 2 show that the inhibition zones of the samples are obviously reduced along with the reduction of the concentration. At 2.5mg/ml, only the industrial hemp extract and the industrial hemp leaf powder still show certain bacteriostatic effect, but other samples have no obvious bacteriostatic effect.
TABLE 2 bacteriostatic circle diameter of samples of different concentrations against Staphylococcus aureus
Figure BDA0003576546860000052
Note: the data are all 3 parallel tests; the measurement data are expressed as mean ± standard deviation (X ± S) diameter of zone of inhibition: the sensitivity is low at 6-10.5 mm, moderate at 10.5-14.5 mm, high at 14.5-20 mm and extremely at least 20 mm; "-" indicates no detection.
(3) Evaluation of washing Effect
The cleaning powder for dish-washing machines prepared by the scheme is compared with the cleaning powder for dish-washing machines without natural components of industrial hemp and two commercially purchased dish-washing machine powders for washing effects.
The cleaning powder for the dish washer comprises 40 parts by weight of industrial hemp powder, 5 parts by weight of industrial hemp extract and 55 parts by weight of detergent. Wherein, the detergent comprises 20 percent of baking soda, 70 percent of potassium carbonate and 10 percent of sodium silicate by mass percentage.
The cleaning powder for the dish-washing machine which does not contain the natural components of industrial hemp comprises, by mass, 20% of baking soda, 70% of potassium carbonate and 10% of sodium silicate.
Two commercial dishwasher powders were purchased: the special washing powder for the simple environment dishwasher and the special dishwashing powder for the vertical white balance point dishwasher.
15g of each dishwasher powder were taken.
Tableware smeared with oil stains, milk stains and rice residues and drinking cups are respectively selected for washing, and the washing effect is evaluated by naked eyes. The results are shown in table 3, both commercial dishwasher powders and the cleaning powder for the industrial hemp natural dishwasher of the present scheme have good washing effect, both can complete the washing work cleanly, and the comparative dishwasher powder (i.e., the dishwasher powder without the natural component of the industrial hemp) has slight residue on greasy tableware and rice residue tableware. This demonstrates the addition of the natural ingredients of industrial hemp, which improves the cleaning ability of the original ingredients.
TABLE 3 evaluation of the powder washing effectiveness of different dish-washing machines
Figure BDA0003576546860000061
Note: the dishwasher powder is the dishwasher powder which is formed by removing other components of industrial hemp components according to the formula. Clean, no dirt can be seen by naked eyes; good, weak washing residue can be seen with naked eyes; typically, a significant wash residue is visible to the naked eye.
(4) Optimized evaluation of washing component ratio
The influence of the proportion of the industrial hemp powder and the detergent in the cleaning powder for the dish washer configured by the scheme on the washing effect is debugged. Fixing 5 weight parts of industrial hemp extract in the formula, adjusting the proportion of the detergent to 30-80 weight parts, and correspondingly 65-15 weight parts of industrial hemp powder. Wherein, the detergent comprises 20 percent of baking soda, 70 percent of potassium carbonate and 10 percent of sodium silicate by mass percentage.
15g of each dishwasher powder were taken.
Tableware smeared with oil stains, milk stains and rice residues and cups for drinking are respectively selected for washing, and the washing effect is visually evaluated. As a result, as shown in Table 4, when the ratio of the detergent was 40 to 70 parts by weight, the washing effect was maintained at a good level as a whole. When the concentration is too high or too low, the washing ability begins to decrease.
TABLE 4 Effect of detergent ratio on powder washing efficiency of dishwasher
Figure BDA0003576546860000071
Note: the dishwasher powder is the dishwasher powder formed by removing other components of industrial hemp components according to the formula. Clean, no dirt can be seen by naked eyes; good, weak washing residue can be seen with naked eyes; typically, a significant wash residue is visible to the naked eye.
(5) Optimized evaluation of extract component proportion
The influence of the proportion of the industrial hemp extract in the cleaning powder for the dish washer prepared by the scheme on the washing effect is debugged. Fixing 55 weight parts of detergent in the formula, adjusting the proportion of industrial hemp extract to 3-15 weight parts, and corresponding industrial hemp powder to 42-30 weight parts. Wherein, the detergent comprises 20 percent of baking soda, 70 percent of potassium carbonate and 10 percent of sodium silicate by mass percentage.
15g of each dishwasher powder were taken.
Tableware smeared with oil stains, milk stains and rice residues and drinking cups are respectively selected for washing, and the washing effect is evaluated by naked eyes. As a result, as shown in table 5, when the ratio of the industrial hemp extract is more than 10 parts by weight, the green color of the extract is observed with the naked eye after washing, and thus the ratio is controlled within 10 parts by weight.
TABLE 5 Effect of the ratio of Industrial hemp extracts on the powder washing effectiveness of a dishwasher
Figure BDA0003576546860000081
Note: the dishwasher powder is the dishwasher powder which is formed by removing other components of industrial hemp components according to the formula. Clean, no dirt can be seen by naked eyes; good, weak washing residue can be seen with naked eyes; typically, a significant wash residue is visible to the naked eye.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims (10)

1. A cleaning powder for a dishwasher, characterized by comprising industrial hemp powder, industrial hemp extract, and a detergent.
2. The cleaning powder for a dishwasher according to claim 1, comprising 30 to 50 parts by weight of industrial hemp powder, 3 to 10 parts by weight of industrial hemp extract, and 40 to 70 parts by weight of detergent.
3. The cleaning powder for a dishwasher according to claim 2, comprising 40 parts by weight of industrial hemp powder, 5 parts by weight of industrial hemp extract, and 55 parts by weight of detergent.
4. The cleaning powder for dish washing machine according to any one of claims 1 to 3, wherein the industrial hemp powder comprises any one or more of industrial hemp stalk powder, industrial hemp leaf powder, hemp seed hull powder.
5. The cleaning powder for dish-washing machines as claimed in claim 4, wherein the industrial hemp powder comprises 60-80% by mass of industrial hemp stalk powder, 10-20% by mass of industrial hemp leaf powder, and 10-20% by mass of hemp seed hull powder; or the like, or, alternatively,
comprises 60-75% of industrial hemp stalk powder and 25-40% of industrial hemp leaf powder; or the like, or, alternatively,
comprises 60-80% of industrial hemp stalk powder and 20-40% of hemp seed hull powder; or the like, or, alternatively,
65-85% of fructus Cannabis seed shell powder, and 15-35% of industrial folium Cannabis powder.
6. The cleaning powder for dish washing machine as claimed in claim 4, wherein the particle size of the industrial hemp stalk powder, the industrial hemp leaf powder, the hemp seed hull powder is such that it can pass through a 40-60 mesh sieve.
7. A dishwasher cleaning powder according to any one of claims 1 to 3 wherein the industrial cannabis extract is prepared by: pulverizing industrial cannabis sativa flowers and/or leaves, placing in ethanol solution, standing for 24-48h for the first time, standing for 20-24h for the second time, filter-pressing, collecting extractive solution, distilling under reduced pressure to remove ethanol, and lyophilizing to obtain industrial cannabis sativa extract.
8. The cleaning powder for dish-washing machines as claimed in claim 7, wherein after the industrial cannabis flowers and/or leaves are placed in ethanol, the mixture is randomly stirred for 2-3 times in the first standing process, each time for 5-10min, and the stirring speed is 100-200 rpm;
extracting industrial flos Cannabis and/or folium Cannabis with ethanol for 2-3 times, mixing the extractive solutions, and processing.
9. The cleaning powder for dish-washing machines as claimed in claim 1, wherein the detergent is a mixture of baking soda, potassium carbonate and sodium silicate.
10. The cleaning powder for the dish washing machine as claimed in claim 9, wherein the detergent comprises 15-20% of baking soda, 70-75% of potassium carbonate and 5-10% of sodium silicate by mass.
CN202210335211.5A 2022-03-31 2022-03-31 Cleaning powder for dish washer Pending CN114703025A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20110088799A (en) * 2010-01-29 2011-08-04 한중대학교 산학협력단 A method for preparing a soap and body cleanser using by a powdered hemp stem
CN106929216A (en) * 2017-03-13 2017-07-07 青岛农业大学 A kind of cleaning agent for dinnerware and cleaning method
CN110205206A (en) * 2019-05-07 2019-09-06 栾云鹏 A kind of dish washing liquid and preparation method thereof with bactericidal
CN111218354A (en) * 2018-11-27 2020-06-02 蒋佳军 A detergent prepared from Luffa cylindrica Roem extract
CN112940880A (en) * 2021-02-04 2021-06-11 云南根之然生物科技有限公司 Multifunctional handmade soap containing industrial hemp root extract and preparation method thereof
CN113999737A (en) * 2021-11-29 2022-02-01 云南人本生物科技有限公司 Plant enzyme detergent and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20110088799A (en) * 2010-01-29 2011-08-04 한중대학교 산학협력단 A method for preparing a soap and body cleanser using by a powdered hemp stem
CN106929216A (en) * 2017-03-13 2017-07-07 青岛农业大学 A kind of cleaning agent for dinnerware and cleaning method
CN111218354A (en) * 2018-11-27 2020-06-02 蒋佳军 A detergent prepared from Luffa cylindrica Roem extract
CN110205206A (en) * 2019-05-07 2019-09-06 栾云鹏 A kind of dish washing liquid and preparation method thereof with bactericidal
CN112940880A (en) * 2021-02-04 2021-06-11 云南根之然生物科技有限公司 Multifunctional handmade soap containing industrial hemp root extract and preparation method thereof
CN113999737A (en) * 2021-11-29 2022-02-01 云南人本生物科技有限公司 Plant enzyme detergent and preparation method thereof

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