KR20110088799A - A method for preparing a soap and body cleanser using by a powdered hemp stem - Google Patents

A method for preparing a soap and body cleanser using by a powdered hemp stem Download PDF

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KR20110088799A
KR20110088799A KR1020100008479A KR20100008479A KR20110088799A KR 20110088799 A KR20110088799 A KR 20110088799A KR 1020100008479 A KR1020100008479 A KR 1020100008479A KR 20100008479 A KR20100008479 A KR 20100008479A KR 20110088799 A KR20110088799 A KR 20110088799A
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oil
mixed
hemp
sodium hydroxide
solution
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주동식
이장국
이명욱
허덕규
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한중대학교 산학협력단
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/10Mixing; Kneading
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/14Shaping
    • C11D13/16Shaping in moulds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74Biological properties of particular ingredients
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/805Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Dermatology (AREA)
  • Biotechnology (AREA)
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  • Microbiology (AREA)
  • Mycology (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

PURPOSE: A method for preparing a powdered hemp stem is provided to ensure the functionality of hemp seed oil and the functionality of stem powder, to antibacterial properties, and to control various sitotoxism bacteria and virus. CONSTITUTION: A method for preparing a powdered hemp stem comprises the steps of: collecting, washing, selecting and sorting hemp; harvesting the stem after removing the skin of the hemp; and pulverizing the harvested hemp stem and powdering the pulverized hemp to obtain micropowder. In the third step, the hemp stem is pulverized in the size of 5-20 mesh through the first pulverizing step, in the size of 100-360 mesh through the second pulverizing step, and finally in the size of 150-400 mesh.

Description

헴프 줄기 분말을 이용한 비누 및 바디클렌저의 제조방법 {A method for preparing a soap and body cleanser using by a powdered hemp stem}A method for preparing a soap and body cleanser using by a powdered hemp stem}

본 발명은 항균성을 증대시켜주며 다양한 식중독 세균 및 바이러스를 제어하는 천연 헴프 줄기 분말이 함유된 비누 및 바디클렌저 제조 방법에 관한 것이다.
The present invention relates to a method for preparing soaps and body cleansers containing natural hemp stem powder that enhances antibacterial properties and controls various food poisoning bacteria and viruses.

[문헌 1] 정보석, 항약대사전, 영림사, 1998.[Reference 1] Information stone, medicinal metabolic dictionary, Younglimsa , 1998.

[문헌 2] Callaway et al., Natural selection for resistance to the allelopathic effects of invasive plants. Journal of Ecology, 93, pp.576-583, 2005.Callaway et al., Natural selection for resistance to the allelopathic effects of invasive plants.Journal of Ecology,93, pp. 576-583, 2005.

헴프는 삼, 대마를 지칭하며, 대마의 종자에는 지방유가 약 30% 함유되어 있다. 새로 짠 유중의 포화지방산은 4.5~9.5%, 불포화지방산에는 올레인산(olein산)이 약 12%, 리놀산(linol산)이 53%, 리놀레산(linolei산)이 25% 함유되어 있고 또 유중에는 카나비놀(canabinol)이 약간 함유되어 있다. 또 피틴(phytin)이 함유되어 있는데 종인 중은 1%로 잎, 줄기, 싹보다 많다. 종자에는 또 트리고넬린(trigonelline), 엘-(디)-이소루신 베타인 (L-(d)-isolucine bataine)도 함유되어 있다. (정보석, 항약대사전, 영림사, 1998) Hemp refers to hemp and hemp, and the hemp seeds contain about 30% fatty oil. Saturated fatty acid in freshly squeezed oil contains 4.5 ~ 9.5%, unsaturated fatty acid contains about 12% oleic acid (olein acid), 53% linoleic acid (linol acid), 25% linoleic acid (linolei acid). It contains some canabinol. It also contains phytin, 1% of which is more than leaves, stems and shoots. Seeds also contain trigonelline and L- (di) -isoleucine betaine (L- (d) -isolucine bataine). (Information Stone, Pharmacological Dictionary, Younglimsa , 1998)

또한, 대마는 면 보다 10배 이상 내구성이 강하며, 수분흡수력과 배출력이 면의 40배에 달할 정도로 뛰어나다. 섬유 자체의 항균ㆍ항독성이 있는데다 원적외선을 방출하고 전자파 및 자외선 차단효과까지 갖고 있는 대표적인 친환경적인 작물이다.In addition, hemp is 10 times more durable than cotton, and has excellent water absorption and discharge power of 40 times that of cotton. It is an eco-friendly crop that has antibacterial and anti-toxic properties of the fiber itself, emits far infrared rays, and has electromagnetic and ultraviolet ray blocking effects.

최근 헴프의 종자에 포함된 단백질과 오일이 최고 양질의 필수아미노산과 필수지방산으로 구성되었다는 사실이 알려지고 있다. 특히 종자오일은 80% 이상이 양질의 불포화지방산으로 구성되고 있는데, 특히 일반 식물 오일(oil)에서 찾기 어려운 감마리놀렌산(gamma linolenic acid, GLA)을 포함하고 있어서 체내의 면역작용에 큰 영향을 미친다. 특히, 이들 불포화지방산은 체내의 콜레스테롤 수치를 개선하여 순환기관의 질병을 치료할 뿐만 아니라 피부의 각종 염증과 최근에 우리 사회에서 문제가 되고 있는 아토피 피부염의 치료에 획기적인 효과가 있음이 입증되고 있다 (Callaway et al., Natural selection for resistance to the allelopathic effects of invasive plants. Journal of Ecology, 93, pp.576-583, 2005).Recently, it is known that proteins and oils contained in hemp seeds are composed of the highest quality essential amino acids and essential fatty acids. In particular, more than 80% of the seed oil is composed of high-quality unsaturated fatty acids, especially because it contains gamma linolenic acid (GLA), which is difficult to find in common plant oil (oil) has a great effect on the body's immune action. In particular, these unsaturated fatty acids improve cholesterol levels in the body and not only treat diseases of the circulatory organs, but also prove to have a remarkable effect on the treatment of various inflammations of the skin and atopic dermatitis, which has recently become a problem in our society. et al., Natural selection for resistance to the allelopathic effects of invasive plants. Journal of Ecology , 93 , pp. 576-583, 2005).

이에 따라 본 발명자들은 헴프 껍질 수확 후 폐기되는 자원의 효과적인 활용 기술의 개발과 헴프 종실 오일의 기능성과 줄기 분말의 기능성을 상승적으로 활용하기 위한 목적으로 헴프 줄기 분말이 함유된 항균 기능성이 향상된 비누 및 바디클렌저 제조방법을 본 발명에서 완성하였다.
Accordingly, the present inventors have developed a technique for effectively utilizing resources that are discarded after harvesting hemp husks, and a soap and body having improved antibacterial function containing hemp stem powder for the purpose of synergistically utilizing the functionality of hemp seed oil and the functionality of stem powder. Cleanser preparation method was completed in the present invention.

상기 목적에 따라, 본 발명은 항균성을 증대시켜주며 다양한 식중독 세균 및 바이러스를 제어하는 항균 기능성이 향상된 비누 및 바디클렌저를 제조하기 위한 헴프 줄기 분말 제조 방법을 제공한다.In accordance with the above object, the present invention provides a method for producing hemp stem powder for producing a soap and body cleanser to increase the antibacterial and to improve the antibacterial function to control various food poisoning bacteria and viruses.

본 발명의 제 1구현예로서, 본 발명은 헴프를 채취하여 수세, 선별 및 정선하는 제 1단계; 상기 제 1단계의 헴프의 껍질을 제거한 후에 줄기를 수확하는 제 2단계; 상기 제 2단계에서 수확한 헴프 줄기를 파쇄 및 분말화 시킨 후에 초미세분쇄기로 미세 분말화하여 미세분말을 수득하는 제 3단계 과정을 포함하는, 본 발명의 헴프 줄기 분말 원료의 제조방법을 제공한다.As a first embodiment of the present invention, the present invention comprises a first step of collecting, washing, selecting and selecting the hemp; A second step of harvesting the stem after removing the hemp shell of the first step; It provides a method for producing a hemp stem powder raw material of the present invention comprising a third step of obtaining a fine powder by pulverizing and powdering the hemp stem harvested in the second step and then finely powdered with an ultra fine grinding machine. .

상기 제 3단계에서, 껍질(인피)을 제거한 속대는 약 2cm 내지 5cm 크기(가로 2.0×세로 5.0)로 자르는 것이 바람직하다.In the third step, it is preferable to cut the bark from which the bark is removed to a size of about 2cm to 5cm (width 2.0 × length 5.0).

상기 제 3단계에서, 절단된 헴프 줄기의 파쇄는 제 1차 파쇄공정으로서 약 5 mesh 내지 20 mesh, 바람직하게는 8 내지 12 mesh로 파쇄하고, 제 2차 파쇄공정으로서 약 100 mesh 내지 360 mesh, 바람직하게는 200 내지 300 mesh로 파쇄하고, 최종적으로 초미니 분쇄기로 약 150 mesh 내지 400 mesh, 바람직하게는 180 내지 250 mesh로 미쇄 분말화함을 특징으로 한다.In the third step, crushing the cut hemp stem is crushed into about 5 mesh to 20 mesh, preferably 8 to 12 mesh as the first crushing process, about 100 mesh to 360 mesh, as the second crushing process Preferably, it is crushed to 200 to 300 mesh, and finally, the ultra-mini grinder is characterized in that the fine powder pulverized to about 150 mesh to 400 mesh, preferably 180 to 250 mesh.

따라서 본 발명은 상기 제조방법으로 제조된 헴프 줄기 분말 원료를 제공한다.Therefore, the present invention provides a hemp stem powder raw material prepared by the above method.

추가적으로 본 발명은 상기에서 제조된 헴프 줄기 분말 원료를 이용하여 항균성을 증대시켜주며 다양한 식중독 세균 및 바이러스를 제어하는 비누 및 바디클렌저를 제조할 수 있다. In addition, the present invention increases the antimicrobial activity by using the hemp stem powder raw material prepared above, and can manufacture soaps and body cleansers that control various food poisoning bacteria and viruses.

예를 들어, 본 발명의 제 2구현예로서, 본 발명의 헴프 줄기 분말 첨가 비누 제조 방법에 있어서, 본 발명은 혼합 가온한 (a) 헴프 종실 오일, (b) 코코넛 오일, (c) 팜오일 및 (d) 올리브 오일을 상호 혼합하여 오일용액 혼합물 (A)을 제조하는 제 1단계; 수산화나트륨을 녹인 정제수를 혼합하여 수산화나트륨 용액을 제조하는 제 2단계; 상기 제 1단계의 오일 용액 혼합물 (A) 및 제 2단계에서 얻은 수산화나트륨 용액을 상호 혼합한 혼합액(B)에 본 발명의 헴프 줄기 분말 원료를 첨가하고 혼합하여 비누원료를 얻는 제 3단계; 제 3단계에서 얻은 비누원료를 성형틀에 부어 보온 후에 상기 보온 틀에서 빼낸 비누를 숙성시키는 제 4단계를 포함하는 단계를 포함하는 제조공정으로 제조됨을 특징으로 하는 본 발명의 비누를 제조하는 제조방법을 제공한다.For example, as a second embodiment of the present invention, in the method for preparing a hemp stem powder-added soap of the present invention, the present invention provides a mixed warmed (a) hemp seed oil, (b) coconut oil, (c) palm oil. And (d) mixing the olive oil with each other to produce an oil solution mixture (A). A second step of preparing a sodium hydroxide solution by mixing purified water dissolved in sodium hydroxide; A third step of obtaining a soap raw material by adding and mixing the hemp stem powder raw material of the present invention to the mixed solution (B) in which the oil solution mixture (A) of the first step and the sodium hydroxide solution obtained in the second step are mixed with each other; Method of producing a soap of the present invention, characterized in that it is prepared by a manufacturing process comprising the step of pouring the soap raw material obtained in the third step to the mold to warm and then aged the soap taken out of the insulating mold To provide.

상기 제 1단계에서, (a) 헴프 종실 오일, (b) 코코넛 오일, (c) 팜오일 및 (d) 올리브 오일은 1∼10: 1∼10:1∼10:0.1∼10, 바람직하게는, 1∼5: 1∼4:1∼4:0.1∼1, 보다 바람직하게는 2∼4: 1∼3:1∼3:0.1∼0.8의 혼합중량비(w/w%)로 혼합하여 약 10∼80℃, 바람직하게는, 40∼60℃, 보다 바람직하게는 50∼55℃의 온도에서 가온함이 바람직하다.In the first step, (a) hemp seed oil, (b) coconut oil, (c) palm oil and (d) olive oil are 1 to 10: 1 to 10: 1 to 10: 0.1 to 10, preferably , 1 to 5: 1 to 4: 1 to 4: 0.1 to 1, more preferably 2 to 4: 1: 1: 1 to 3: 0.1 to 0.8, mixed at a mixed weight ratio (w / w%) of about 10 It is preferable to warm at the temperature of -80 degreeC, Preferably it is 40-60 degreeC, More preferably, it is 50-55 degreeC.

상기 제 2단계에서, 수산화나트륨 용액을 제조시에는 수산화나트륨을 정제수와 1: 1∼5, 바람직하게는 1; 1.5∼3.5의 중량혼합비로 혼합하여 약 10∼80℃, 바람직하게는, 40∼60℃, 보다 바람직하게는 50∼55℃의 온도에서 가온함이 바람직하다.In the second step, when preparing the sodium hydroxide solution, sodium hydroxide with purified water 1: 1 to 5, preferably 1; It is preferable to mix at a weight mixing ratio of 1.5 to 3.5 and to warm at a temperature of about 10 to 80 ° C, preferably 40 to 60 ° C, more preferably 50 to 55 ° C.

상기 제 3단계에서, 상기 제 1단계의 오일용액 혼합물 (A) 및 제 2단계에서 얻은 수산화나트륨 용액은 1: 1∼5, 바람직하게는 1; 1.5∼3.5의 부피 혼합비로 혼합하는 것이 바람직하고, 상기 혼합액(B)에는 상기 헴프 줄기 분말 원료를 총 중량대비 약 1-20% (w/w%), 바람직하게는 5-10% 혼합비로 혼합하는 것이 바람직하다.In the third step, the oil solution mixture (A) of the first step and the sodium hydroxide solution obtained in the second step are 1: 1 to 5, preferably 1; It is preferable to mix at a volume mixing ratio of 1.5 to 3.5, and the mixed solution (B) is mixed with the hemp stem powder raw material at a mixing ratio of about 1-20% (w / w%), preferably 5-10% of the total weight. It is desirable to.

상기 제 4단계에서 상기 비누원료는 성형틀에 부어 약 12 시간 내지 3일간, 바람직하게는 약 24시간 보온을 한 후에, 틀에서 빼낸 비누를 약 2주 내지 6개월, 바람직하게는 약 1개월 내지 2개월간 숙성시킴이 바람직하다. In the fourth step, the soap raw material is poured into a mold and kept warm for about 12 hours to 3 days, preferably about 24 hours, and then the soap taken out of the mold is about 2 weeks to 6 months, preferably about 1 month to Aging for 2 months is preferred.

또한, 본 발명의 제 3구현예로서, 본 발명의 헴프 줄기 분말 첨가 바디클렌저 제조 방법에 있어서, 본 발명은 혼합 가온한 혼합 가온한 (a) 헴프 종실 오일, (b) 코코넛 오일, (c) 팜오일 및 (d) 올리브 오일을 상호 혼합하여 오일용액 혼합물(A)을 제조하는 제 1단계; 수산화나트륨을 녹인 정제수를 혼합하여 수산화나트륨 용액을 제조하는 제 2단계; 상기 제 1단계의 오일용액 혼합물(A) 및 제 2단계에서 얻은 수산화나트륨 용액을 상호 혼합한 혼합액(B)에 본 발명의 헴프 줄기 분말 원료를 첨가하고 이를 계속적으로 교반하여 걸쭉한 반 겔 형태의 혼합액으로 제조하는 제 3단계; 상기 반겔 형태의 혼합액을 실온에 식혀 수분을 제거한 후에 포장용기에 숙성시키는 제 4단계; 제 4단계에서 숙성된 페이스트를 정제수와 혼합시켜 희석시키는 제 5단계; 제 5 단계에서 얻은 희석 페이스트에 계면활성제 및 코코베타인을 가해 혼합하고 티트리 에센셜 오일을 추가로 첨가하여 혼합시킨 후에 용기에 담는 제 6단계를 포함하는 제조공정으로 제조됨을 특징으로 하는 본 발명의 바디클렌저를 제조하는 제조방법을 제공한다.Further, as a third embodiment of the present invention, in the method for manufacturing a hemp stem powder-added body cleanser of the present invention, the present invention is a mixed warmed mixed warmed (a) hemp seed oil, (b) coconut oil, (c) A first step of preparing an oil solution mixture (A) by mixing palm oil and (d) olive oil with each other; A second step of preparing a sodium hydroxide solution by mixing purified water dissolved in sodium hydroxide; The hemp stem powder raw material of the present invention is added to the mixed solution (B) in which the oil solution mixture (A) of the first step and the sodium hydroxide solution obtained in the second step are mixed with each other, and the mixture is continuously stirred to form a thick semi-gel mixed solution. To prepare a third step; A fourth step of cooling the vangel mixed solution at room temperature to remove moisture and then aging the packaging container; A fifth step of diluting the paste aged in the fourth step by mixing with purified water; The body of the present invention, which is prepared by adding a surfactant and cocobetaine to the dilution paste obtained in the fifth step, mixing the mixture, and further adding tea tree essential oil, followed by mixing into a container. Provided are methods for preparing the cleanser.

상기 제 1단계에서, (a) 헴프 종실 오일, (b) 코코넛 오일, (c) 팜오일 및 (d)올리브 오일은 1∼10: 1∼10:1∼10:0.1∼10, 바람직하게는, 1∼5: 1∼4:1∼4:0.1∼1, 보다 바람직하게는 2∼4: 1∼3:1∼3:0.1∼0.8의 혼합중량비(w/w%)로 혼합하여 약 20∼100℃, 바람직하게는, 50∼80℃, 보다 바람직하게는 60∼70℃의 온도에서 가온함이 바람직하다.In the first step, (a) hemp seed oil, (b) coconut oil, (c) palm oil and (d) olive oil are 1 to 10: 1 to 10: 1 to 10: 0.1 to 10, preferably , 1 to 5: 1 to 4: 1 to 4: 0.1 to 1, more preferably 2 to 4: 1 to 3: 1 to 3: 3: 0.1 to 0.8, and mixed at a mixed weight ratio (w / w%) of about 20 It is preferable to warm at a temperature of -100 degreeC, Preferably it is 50-80 degreeC, More preferably, it is 60-70 degreeC.

상기 제 2단계에서, 수산화나트륨 용액을 제조시에는 수산화나트륨을 정제수와 1: 1∼8, 바람직하게는 1; 1.5∼6.5의 중량혼합비로 혼합하여 약 10∼80℃, 바람직하게는, 40∼60℃, 보다 바람직하게는 50∼55℃의 온도에서 가온함이 바람직하다.In the second step, when preparing the sodium hydroxide solution, sodium hydroxide with purified water 1: 1 to 8, preferably 1; It is preferred to mix at a weight mixing ratio of 1.5 to 6.5 and warm at a temperature of about 10 to 80 캜, preferably 40 to 60 캜, more preferably 50 to 55 캜.

상기 제 3단계에서, 상기 제 1단계의 오일용액 혼합물 (A) 및 제 2단계에서 얻은 수산화나트륨 용액은 1: 1∼5, 바람직하게는 1; 1.5∼3.5의 부피 혼합비로 혼합하는 것이 바람직하고, 상기 혼합액(B)에는 상기 헴프 줄기 분말 원료를 총 중량대비 약 1-20% (w/w%), 바람직하게는 5-10% 혼합비로 혼합하는 것이 바람직하다.In the third step, the oil solution mixture (A) of the first step and the sodium hydroxide solution obtained in the second step are 1: 1 to 5, preferably 1; It is preferable to mix at a volume mixing ratio of 1.5 to 3.5, and the mixed solution (B) is mixed with the hemp stem powder raw material at a mixing ratio of about 1-20% (w / w%), preferably 5-10% of the total weight. It is desirable to.

상기 제 3단계에서, 상기 제 2단계에서 얻은 반겔 형태의 혼합액은 혼합하고 잘 교반하면, 혼합한 다음 잘 교반시키면 순두부처럼 뭉글뭉글해졌다가 계속 교반하는 과정을 반복하여 교반하면 겔화와 크림화 상태가 되는데 이 상태를 지나서까지 계속 교반하면 일정한 점성을 가지는 걸쭉한 반겔 상태가 된다.In the third step, the mixed solution of the half-gel form obtained in the second step is mixed and stirred well, and then mixed and stirred well, it becomes lumpy like soft tofu, and the stirring is repeated, and the stirring process is repeated. If you continue stirring until after this state, a thick viscous state with a constant viscosity is obtained.

상기 제 4단계에서, 상기 반겔 형태의 혼합액을 실온에 식혀 수분을 제거한 후에 포장용기에는 약 2주 내지 약 6개월, 바람직하게는 약 1개월 내지 2개월 동안 숙성시킴이 바람직하고,In the fourth step, after the water mixture is cooled to room temperature to remove the vangel form, the packaging container is preferably aged for about 2 weeks to about 6 months, preferably about 1 month to 2 months,

상기 제 5단계에서, 제 4단계에서 숙성된 페이스트 및 정제수는 1: 1∼5, 바람직하게는 1: 1.5∼2.5의 부피 혼합비로 혼합시켜 희석시킴이 바람직하며,In the fifth step, the paste and purified water aged in the fourth step is preferably diluted by mixing in a volume mixing ratio of 1: 1 to 5, preferably 1: 1.5 to 2.5,

상기 제 6단계에서, 상기 제 5 단계에서 얻은 희석 페이스트(a)에 계면활성제(b), 및 코코베타인(c)은 각각 1∼10: 1∼10: 0.5∼2.5, 바람직하게는, 2∼8: 2∼8: 0.5∼1.5의 중량 혼합비로 혼합함이 바람직하고, 상기 혼합액 부피대비 약 0.01∼5(w/w/%), 바람직하게는 0.1∼2(w/w/%) 티트리 에센셜 오일을 추가로 첨가함이 바람직하다.In the sixth step, the surfactant (b) and cocobetaine (c) in the dilution paste (a) obtained in the fifth step are 1 to 10: 1 to 10: 0.5 to 2.5, preferably, 2 It is preferable to mix at a weight mixing ratio of 8 to 2 to 8: 0.5 to 1.5, and about 0.01 to 5 (w / w /%), preferably 0.1 to 2 (w / w /%) It is preferred to add further tri essential oils.

상기에서 제조된 본 발명의 비누 및 바디클렌저는 헴프 종실 오일의 기능성과 줄기 분말의 기능성을 상승적으로 활용 하여 항균성을 증대시켜주며 다양한 식중독 세균 및 바이러스를 제어하는 효과로 인해 헴프 줄기 분말이 함유된 항균 기능성이 향상된 비누 및 바디클렌저를 제조할 수 있다.Soap and body cleanser of the present invention prepared in the above synergistically utilizing the functionality of the hemp seed oil and the functionality of the stem powder to increase the antibacterial and antibacterial containing hemp stem powder due to the effect of controlling various food poisoning bacteria and viruses Soaps and body cleansers with improved functionality can be prepared.

따라서 본 발명은 상기 제조방법으로 제조된 헴프 함유 비누 및 바디클렌저를 제공한다.
Therefore, the present invention provides a hemp-containing soap and body cleanser prepared by the above method.

본 발명은 헴프 종실 오일의 기능성과 줄기 분말의 기능성을 상승적으로 활용하여 항균성을 증대시켜주며 다양한 식중독 세균 및 바이러스를 제어하는 효과로 인해 헴프 줄기 분말이 함유된 항균 기능성이 향상된 비누 및 바디클렌저 제조방법이 제품의 품질과 신뢰성을 대폭 향상시킬 수 있다.
The present invention increases the antimicrobial activity by synergistically utilizing the functionality of the hemp seed oil and the functionality of the stem powder, and a method for producing soap and body cleanser with improved antibacterial function due to the effect of controlling various food poisoning bacteria and viruses The quality and reliability of this product can be greatly improved.

이하, 본 발명을 실시예 및 실험예에 의해 상세히 설명한다.Hereinafter, the present invention will be described in detail with reference to Examples and Experimental Examples.

단, 하기 실시예 및 실험예는 본 발명을 예시하는 것일 뿐, 본 발명의 내용이 하기 실시예 및 실험예에 의해 한정되는 것은 아니다.
However, the following examples and experimental examples are illustrative of the present invention, and the content of the present invention is not limited by the following examples and experimental examples.

실시예Example 1.  One. 헴프Hemp 줄기 분말 제조 Stem powder manufacturer

상기 헴프 (한중대 헴프사업단, 20kg)의 껍질을 제거한 다음, 헴프 줄기(속대)를 1-2cm 정도 자른다. 자른 헴프 줄기를 파쇄기를 이용하여 10 mesh 크기로 1차 파쇄 후, 260 mesh 크기로 2차 파쇄한 다음 초미세분쇄기를 이용하여 3차 분말화 과정을 거친 후 최종적으로 200 mesh로 분쇄하여 헴프 줄기 분말 원료를 제조하였다.
After removing the shell of the hemp (Chinese hemp business group, 20kg), cut the hemp stem (cob) about 1-2cm. The chopped hemp stems are first crushed to a size of 10 mesh using a crusher, and then crushed to a size of 260 mesh, and then subjected to a tertiary pulverization process using an ultra-fine crusher, and finally crushed into 200 mesh to be hemp stem powder. Raw material was prepared.

실시예Example 2.  2. 헴프Hemp 줄기 분말 첨가 비누 제조 Stem Powder Additive Soap Manufacturer

헴프 종실 오일 (당진군 농협, 30kg), 코코넛 오일 (그린라이프, 20kg), 팜오일 (그린라이프,20kg), 올리브오일 (그린라이프, 20kg)을 각각 3:2:2:0.5의 비율로 계량 후에 한번에 혼합기 (Shinil Co.)를 이용하여 50-55℃에서 혼합하여 가온한다. 수산화나트륨 (대정상사)과 정제수도 각각 1.07:2.47의 비율로 계량한 다음 정제수에 수산화나트륨을 녹이면서 온도를 50-55℃로 맞춘다. 온도가 조절되면 오일용액과 수산화나트륨 용액을 혼합하여 블랜더 (Shinil Co.)로 저어주어 혼합액이 잘 혼합되도록 한다. 실시예 1에서 얻은 헴프 줄기 분말을 혼합액의 5-10%의 비율로 첨가한 후 다시 20분 정도 잘 저어준 후, 성형틀 (아크릴 제작)에 혼합액을 부은 다음 24시간 동안 보온 후 틀에서 빼낸 비누를 1개월간 숙성시킨 후에 제품으로 출하한다.
Hemp seed oil (Dangjin-gun Nonghyup, 30 kg), coconut oil (green life, 20 kg), palm oil (green life, 20 kg) and olive oil (green life, 20 kg) were weighed at a ratio of 3: 2: 2: 0.5, respectively. Mix and warm at 50-55 ° C using a mixer (Shinil Co.) at a time. Sodium hydroxide (Dae Sang Sang) and purified water were also weighed at a ratio of 1.07: 2.47, respectively, and the temperature was adjusted to 50-55 ° C while sodium hydroxide was dissolved in purified water. When the temperature is controlled, mix the oil solution with the sodium hydroxide solution and stir with a blender (Shinil Co.) to allow the mixture to mix well. The hemp stem powder obtained in Example 1 was added at a ratio of 5-10% of the mixed solution, and then stirred well for about 20 minutes.Then, the mixed solution was poured into a molding mold (acrylic production), and the soap was removed from the mold after keeping warm for 24 hours. After aging for 1 month, it is shipped as a product.

실시예Example 3.  3. 헴프Hemp 줄기 분말 첨가  Stem Powder Addition 바디클렌저Body cleanser 제조 Produce

상기 실시예 2에서 준비된 헴프 종실 오일, 코코넛 오일, 팜오일, 올리브오일을 각각 3:1.5:1.5:1.0의 비율 (중량비)로 계량 후 혼합기 (Shinil Co.)를 이용하여 60-70℃에서 혼합하여 가온한다. 수산화나트륨과 정제수도 각각 1.6:4.48의 비율로 계량한 다음 정제수에 수산화나트륨을 완전히 녹인 후 가온된 오일에 혼합하였다. 상기 혼합액(B)에는 상기 헴프 줄기 분말 원료를 총 중량대비 약 1-20%, 바람직하게는 5-10% 혼합비로 혼합하는 것이 바람직하다.Hemp seed oil, coconut oil, palm oil and olive oil prepared in Example 2 were weighed at a ratio (weight ratio) of 3: 1.5: 1.5: 1.0, respectively, and then mixed at 60-70 ° C. using a mixer (Shinil Co.). To warm up. Sodium hydroxide and purified water were also weighed at a ratio of 1.6: 4.48, respectively, and sodium hydroxide was completely dissolved in purified water, and then mixed with warm oil. In the mixed solution (B), the hemp stem powder raw material is preferably mixed at a mixing ratio of about 1-20%, preferably 5-10%, based on the total weight.

상기 오일을 혼합한 다음 잘 교반시키면 순두부처럼 뭉글뭉글해졌다가 계속 교반하는 과정을 반복하여 교반하면 겔화와 크림화 상태가 되는데 이 상태를 지나서까지 계속 교반하면 일정한 점성을 가지는 걸쭉한 반겔 상태가 된다. 반겔 상태의 혼합물을 실온에서 식힌 다음 수분을 제거하고 포장용기(지퍼백)에 1-2개월간 숙성시킨다. 숙성시킨 페이스트를 정제수와 1:2의 비율(부피비)로 혼합한 후 희석한다. When the oil is mixed well and then stirred well, it becomes lumpy like a soft tofu, and the stirring is repeated repeatedly to form a gelled and creamed state. If the stirring continues until this state, the oil becomes thick and thick gelled with constant viscosity. The gelled mixture is cooled at room temperature, then dehydrated and aged in a packaging container (zipper bag) for 1-2 months. The aged paste is mixed with purified water in a ratio of 1: 2 (volume ratio) and diluted.

희석된 페이스트 500 g과 코코넛 추출 계면활성제 LES (주,케이씨이아) 500 g을 계량하고 여기에 코코베타인 (주,케이씨이아) 100 g을 계량하여 잘 섞어준 다음 티트리 에센셜 오일 (주,케이씨이아) 0.1-1%를 넣고 혼합한 후 용기에 담아 제품을 출하한다.
Weigh 500 g of the diluted paste and 500 g of coconut extract surfactant LES Co., Ltd. and weigh 100 g of cocobetaine Co., Ltd., mix well, and then mix with tea tree essential oil. H) Add 0.1-1%, mix, and put the product in a container to ship the product.

Claims (13)

헴프를 채취하여 수세, 선별 및 정선하는 제 1단계; 상기 제 1단계의 헴프의 껍질을 제거한 후에 줄기를 수확하는 제 2단계; 상기 제 2단계에서 수확한 헴프 줄기를 파쇄 및 분말화 시킨 후에 초미세분쇄기로 미세분말화하여 미세분말을 수득하는 제 3단계 과정을 포함하는, 본 발명의 헴프 줄기 분말 원료의 제조방법.A first step of collecting, washing, and selecting hemps; A second step of harvesting the stem after removing the hemp shell of the first step; And a third step of obtaining fine powder by pulverizing and powdering the hemp stem harvested in the second step and then micropowdering with an ultra fine grinding machine. 제 1항에 있어서,
상기 제 3단계에서, 절단된 헴프 줄기의 파쇄는 제 1차 파쇄공정으로서 약 5 mesh 내지 20 mesh로 파쇄하고, 제 2차 파쇄공정으로서 약 100 mesh 내지 360 mesh로 파쇄하고, 최종적으로 초미니 분쇄기로 약 150 mesh 내지 400 mesh로 미쇄 분말화 함을 특징으로 하는 제조방법.
The method of claim 1,
In the third step, the crushed chopped hemp stem is crushed to about 5 mesh to 20 mesh as the first crushing process, crushed to about 100 mesh to 360 mesh as the second crushing process, and finally to the ultra mini grinder A method for producing a powder, which comprises pulverizing the powder into about 150 mesh to 400 mesh.
제 1항의 제조방법으로 제조된 헴프 줄기 분말 원료.Hemp stem powder raw material prepared by the method of claim 1. 혼합 가온한 (a) 헴프 종실 오일, (b) 코코넛 오일, (c) 팜오일 및 (d) 올리브 오일을 상호 혼합하여 오일용액 혼합물 (A)을 제조하는 제 1단계; 수산화나트륨을 녹인 정제수를 혼합하여 수산화나트륨 용액을 제조하는 제 2단계; 상기 제 1단계의 오일용액 혼합물 (A) 및 제 2단계에서 얻은 수산화나트륨 용액을 상호 혼합한 혼합액(B)에 본 발명의 헴프 줄기 분말 원료를 첨가하고 혼합하여 비누원료를 얻는 제 3단계; 제 3단계에서 얻은 비누원료를 성형틀에 부어 보온 후에 상기 보온 틀에서 빼낸 비누를 숙성시키는 제 4단계를 포함하는 단계를 포함하는 제조공정으로 제조됨을 특징으로 하는 본 발명의 비누를 제조하는 제조방법.A first step of mixing the mixed warmed (a) hemp seed oil, (b) coconut oil, (c) palm oil and (d) olive oil to form an oil solution mixture (A); A second step of preparing a sodium hydroxide solution by mixing purified water dissolved in sodium hydroxide; A third step of obtaining a soap raw material by adding and mixing the hemp stem powder raw material of the present invention to the mixed solution (B) in which the oil solution mixture (A) of the first step and the sodium hydroxide solution obtained in the second step are mixed with each other; Method of producing a soap of the present invention, characterized in that it is prepared by a manufacturing process comprising the step of pouring the soap raw material obtained in the third step to the mold to warm and then aged the soap taken out of the insulating mold . 제 4항에 있어서,
상기 제 1단계에서, (a) 헴프 종실 오일, (b) 코코넛 오일, (c) 팜오일 및 (d) 올리브 오일은 1∼10: 1∼10:1∼10:0.1∼10의 혼합 중량비(w/w%)로 혼합하여 약 10∼80℃의 온도에서 가온함을 특징으로 하는 제조방법.
The method of claim 4, wherein
In the first step, (a) hemp seed oil, (b) coconut oil, (c) palm oil and (d) olive oil are 1 to 10: 1 to 10: 1 to 10: 0.1 to 10 mixed weight ratio ( w / w%) and warmed at a temperature of about 10 to 80 ℃.
제 4항에 있어서,
상기 제 2단계에서, 수산화나트륨 용액을 제조시에는 수산화나트륨을 정제수와 1: 1∼5의 중량혼합비로 혼합하여 약 10∼80℃의 온도에서 가온함을 특징으로 하는 제조방법.
The method of claim 4, wherein
In the second step, when preparing the sodium hydroxide solution, sodium hydroxide is mixed with purified water in a weight mixing ratio of 1: 1 to 5, the production method characterized in that the heating at a temperature of about 10 ~ 80 ℃.
제 4항에 있어서,
상기 제 3단계에서, 상기 제 1단계의 오일용액 혼합물 (A) 및 제 2단계에서 얻은 수산화나트륨 용액은 1: 1∼5의 부피 혼합비로 혼합하고, 상기 혼합액(B)에는 상기 헴프 줄기 분말 원료를 총 중량대비 약 1-20% (w/w%)로 혼합함을 특징으로 하는 제조방법.
The method of claim 4, wherein
In the third step, the oil solution mixture (A) of the first step and the sodium hydroxide solution obtained in the second step are mixed in a volume mixing ratio of 1: 1 to 5, the mixed solution (B) is the hemp stem powder raw material To about 1-20% (w / w%) based on the total weight of the manufacturing method.
혼합 가온한 혼합 가온한 (a) 헴프 종실 오일, (b) 코코넛 오일, (c)팜오일 및 (d)올리브 오일을 상호 혼합하여 오일용액 혼합물(A)을 제조하는 제 1단계; 수산화나트륨을 녹인 정제수를 혼합하여 수산화나트륨 용액을 제조하는 제 2단계; 상기 제 1단계의 오일용액 혼합물(A) 및 제 2단계에서 얻은 수산화나트륨 용액을 상호 혼합한 혼합액(B)에 본 발명의 헴프 줄기 분말 원료를 첨가하고 이를 계속적으로 교반하여 걸쭉한 반 겔 형태의 혼합액으로 제조하는 제 3단계; 상기 반겔 형태의 혼합액을 실온에 식혀 수분을 제거한 후에 포장용기에 숙성시키는 제 4단계; 제 4단계에서 숙성된 페이스트를 정제수와 혼합시켜 희석시키는 제 5단계; 제 5 단계에서 얻은 희석 페이스트에 계면활성제 및 코코베타인을 가해 혼합하고 티트리 에센셜 오일을 추가로 첨가하여 혼합시킨 후에 용기에 담는 제 6단계를 포함하는 제조공정으로 제조됨을 특징으로 하는 본 발명의 바디클렌저를 제조하는 제조방법.Mixed warming The first step of mixing the mixed warmed (a) hemp seed oil, (b) coconut oil, (c) palm oil and (d) olive oil to prepare an oil solution mixture (A); A second step of preparing a sodium hydroxide solution by mixing purified water dissolved in sodium hydroxide; The hemp stem powder raw material of the present invention is added to the mixed solution (B) in which the oil solution mixture (A) of the first step and the sodium hydroxide solution obtained in the second step are mixed with each other, and the mixture is continuously stirred to form a thick semi-gel mixed solution. To prepare a third step; A fourth step of cooling the vangel mixed solution at room temperature to remove moisture and then aging the packaging container; A fifth step of diluting the paste aged in the fourth step by mixing with purified water; The body of the present invention, which is prepared by adding a surfactant and cocobetaine to the dilution paste obtained in the fifth step, mixing the mixture, and further adding tea tree essential oil, followed by mixing into a container. A method of making a cleanser. 제 8항에 있어서,
상기 제 1단계에서, (a) 헴프 종실 오일, (b) 코코넛 오일, (c) 팜오일 및 (d) 올리브 오일은 1∼10: 1∼10:1∼10:0.1∼10의 혼합 중량비(w/w%)로 혼합하여 약 20∼100℃의 온도에서 가온함을 특징으로 하는 제조방법.
The method of claim 8,
In the first step, (a) hemp seed oil, (b) coconut oil, (c) palm oil and (d) olive oil are 1 to 10: 1 to 10: 1 to 10: 0.1 to 10 mixed weight ratio ( w / w%) to warm to a temperature of about 20 to 100 ℃.
제 8항에 있어서,
상기 제 2단계에서, 수산화나트륨 용액을 제조시에는 수산화나트륨을 정제수와 1: 1∼8의 중량혼합비로 혼합하여 약 10∼80℃의 온도에서 가온함을 특징으로 하는 제조방법.
The method of claim 8,
In the second step, when preparing the sodium hydroxide solution, sodium hydroxide is mixed with purified water in a weight mixing ratio of 1: 1 to 8, characterized in that the warming at a temperature of about 10 ~ 80 ℃.
제 8항에 있어서,
상기 제 3단계에서, 상기 제 1단계의 오일용액 혼합물 (A) 및 제 2단계에서 얻은 수산화나트륨 용액은 1: 1∼5의 부피 혼합비로 혼합하고, 상기 혼합액(B)에는 상기 헴프 줄기 분말 원료를 총 중량대비 약 1-20% (w/w%)로 혼합함을 특징으로 하는 제조방법.
The method of claim 8,
In the third step, the oil solution mixture (A) of the first step and the sodium hydroxide solution obtained in the second step are mixed in a volume mixing ratio of 1: 1 to 5, the mixed solution (B) is the hemp stem powder raw material To about 1-20% (w / w%) based on the total weight of the manufacturing method.
제 8항에 있어서,
상기 6단계에서, 상기 제 5 단계에서 얻은 희석 페이스트(a)에 계면활성제(b), 및 코코베타인(c)은 각각 1∼10: 1∼10: 0.5∼2.5의 중량 혼합비)로 혼합되고, 상기 혼합액 부피대비 약 0.01∼5(w/w/%) 티트리 에센셜 오일을 추가로 첨가함을 특징으로 하는 제조방법.
The method of claim 8,
In the sixth step, the surfactant (b) and cocobetaine (c) are mixed in a dilution paste (a) obtained in the fifth step in a weight mixing ratio of 1 to 10: 1 to 10: 0.5 to 2.5, respectively) And about 0.01 to 5 (w / w /%) tea tree essential oil relative to the volume of the mixed solution.
제 8항의 제조방법으로 제조된 헴프 함유 비누 및 바디클렌저.

Hemp-containing soap and body cleanser prepared by the method of claim 8.

KR1020100008479A 2010-01-29 2010-01-29 A method for preparing a soap and body cleanser using by a powdered hemp stem KR20110088799A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10485751B2 (en) 2017-11-09 2019-11-26 Rachel Rohlman Anti-soap formulation
KR20220026103A (en) 2020-08-25 2022-03-04 이은주 Composition for improving scalp and hair condition comprising Hempseed extract and method for preparing the same
CN114703025A (en) * 2022-03-31 2022-07-05 中国农业科学院麻类研究所 Cleaning powder for dish washer

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10485751B2 (en) 2017-11-09 2019-11-26 Rachel Rohlman Anti-soap formulation
KR20220026103A (en) 2020-08-25 2022-03-04 이은주 Composition for improving scalp and hair condition comprising Hempseed extract and method for preparing the same
CN114703025A (en) * 2022-03-31 2022-07-05 中国农业科学院麻类研究所 Cleaning powder for dish washer

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