CN109055046A - A kind of preparation method of detergent for washing dishware with hand - Google Patents
A kind of preparation method of detergent for washing dishware with hand Download PDFInfo
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- CN109055046A CN109055046A CN201811129454.3A CN201811129454A CN109055046A CN 109055046 A CN109055046 A CN 109055046A CN 201811129454 A CN201811129454 A CN 201811129454A CN 109055046 A CN109055046 A CN 109055046A
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- detergent
- hand
- washing dishware
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/44—Vegetable products
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/02—Inorganic compounds
- C11D7/04—Water-soluble compounds
- C11D7/10—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/265—Carboxylic acids or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
- C11D7/3218—Alkanolamines or alkanolimines
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
- C11D7/3245—Aminoacids
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to a kind of preparation methods of detergent for washing dishware with hand, belong to detergent technical field.Detergent for washing dishware with hand prepared by the present invention is using natural plants as raw material, chemical addition agent is few, avoid the problem difficult to degrade using rear chemical residue, it is safer more environmentally friendly, with good washing cleaning action, tableware bacterium can be killed, while having fruity fragrant, there are higher use value, wide market；Cactus has clear thermally-sterilized effect, extracts cactus liquid by thermophilic digestion, good to skin compatibility as antipathogenic composition, injury is small, antibacterial not hurt hands；Wormwood bacteriostatic agent has very strong bactericidal effect to Escherichia coli, compensates for current many detergent to the helpless defect of Escherichia coli；Fragrant citrus pericarp, orange peel, D- limonene rich in pomelo peel have good cleaning, bactericidal effect with coconut oil foaming agent is added after alcoholic extraction, while detergent also being made to possess natural fruity fragrance, improve the mood of people.
Description
Technical field
The present invention relates to a kind of preparation methods of detergent for washing dishware with hand, belong to detergent technical field.
Background technique
According to the difference of mode of washing, dish washing detergent can be divided into detergent for washing dishware with hand and Dishwashing detergent for machine washing.By
It is not popularized also in dish-washing machine, at present still based on detergent for washing dishware with hand.Dish washing detergent is as a kind of detergent for household use, in day
Often life in it is close compared with we contact because its have the characteristics that clean effect it is good, washing after tableware smell faint scent,
As one of dairy products most common in modern life.Either family, eating and drinking establishment or high-grade hotel are required using meal
Has detergent.The main component of dish washing detergent includes surfactant, emulsifier, essence and pigment etc., and main wash is attached
In protein, grease, carbohydrate and their decomposition product in the materials such as plastics, ceramics, metal and glass, remove
Except this, it is also used for washing vegetable and fruit.In washing process, emulsifier can be such that grease decomposes by emulsification, will not dissolve in
The substance of water becomes the emulsion for being dissolved in water, is allowed to separate with cleaned object by surfactant, some dish washing detergents are also
With bacterial growth is inhibited, the function of transmission is prevented.
For detergent for washing dishware with hand as other cleaning products, main component is also surfactant.Difference is to eat
Tool detergent is mainly used for the washing of tableware, cooker, water fruits and vegetables etc., can wash the animal and plant oil polution on tableware or cooker,
And pesticide, chemical fertilizer on gourd, fruit and vegetable etc..Dish washing detergent has good wetting, emulsification, solubilising power, is disappeared in family
The maximum cleaning products of the amount of expense.Common dish washing detergent often contains various ingredients, and what is played a major role is surfactant.
Surfactant be it is a kind of can be aligned in solution surface, a small amount of surface that can significantly reduce solution is added
The organic compound of power.Surfactant is a kind of amphipathic compound, mainly includes two parts, and one end has good hydrophilic
Property, referred to as hydrophilic group；The other end has hydrophobicity, referred to as lipophilic group.
There is much common spot in daily life, including common spot and special spot, their huge numbers, property
It is not identical, therefore, to reach ideal clean effect, different physico-chemical process need to be used.It can be divided by processing mode
Several classes below, respectively dissolution, emulsification, chemical action, decomposition and Action of Surfactant.
It is gradually increased with the improvement of people ' s living standards with environmental consciousness, people increasingly pay attention to the health peace of itself
Full problem, the requirement to detergent are also increasingly stringenter.Dish washing detergent will not only have good detergency and economy, also
There should be the characteristics such as environmental protection, mild.
Summary of the invention
The technical problems to be solved by the invention: poor for existing detergent bacteria-eliminating efficacy, the problem more than chemical residual mentions
A kind of preparation method of detergent for washing dishware with hand is supplied.
In order to solve the above technical problems, the technical solution adopted by the present invention is that:
(1) fresh cactus is taken, surface spine is removed, obtains pest pear, take pest pear, fresh argy wormwood and fresh spinach
Dish impregnates in deionized water after chopping, obtains mixture；
(2) condensing unit is opened, mixture is warming up to 100 DEG C of boiling 1h, condensation reflux liquid is received in boiling, uses petroleum ether
Condensation reflux liquid is extracted, extract liquor is obtained, extract liquor is placed in Rotary Evaporators, is taken out after 1h, obtains extracting solution；
(3) mixture is filtered, removes filter residue, continued boiling concentration, obtain antibacterial liquid；
(4) fragrant citrus pericarp, orange peel and pomelo peel are taken, is washed with deionized water after wooden dipper white on skin is scraped off, is shredded after draining, is impregnated
In dehydrated alcohol, seal one week；
(5) it unseals, takes soak, coconut oil foaming agent, triethanolamine, sodium benzoate, sodium chloride and ethylenediamine tetra-acetic acid stirring
Uniformly, cleaning agent is obtained；
(6) it takes extracting solution, antibacterial liquid, cleaning agent and deionized water to be mixed, obtains detergent for washing dishware with hand.
The mass ratio of step (1) pest pear, fresh argy wormwood and fresh spinach is 2: 2: 1.
The revolving speed of step (2) described Rotary Evaporators is 100r/min.
Step (3) time for continuing boiling concentration is 30~60min.
The mass ratio of step (4) fragrant citrus pericarp, orange peel and pomelo peel is 2: 2: 5.
Step (5) soak, coconut oil foaming agent, triethanolamine, sodium benzoate, sodium chloride and ethylenediamine tetra-acetic acid
Mass ratio be 200: 3: 8: 4: 3: 1.
Step (6) extracting solution, antibacterial liquid, cleaning agent and deionized water mass ratio be 1: 7: 5: 3.
The present invention is compared with other methods, and advantageous effects are:
(1) cactus has clear thermally-sterilized effect, cactus liquid is extracted by thermophilic digestion, as antipathogenic composition, to skin
Compatibility is good, and injury is small, antibacterial not hurt hands；Wormwood bacteriostatic agent has very strong bactericidal effect to Escherichia coli, compensates for and works as
Preceding many detergent are to the helpless defect of Escherichia coli；Fragrant citrus pericarp, orange peel, D- lemon rich in pomelo peel
Alkene has good cleaning, bactericidal effect, while also detergent is possessed with coconut oil foaming agent is added after alcoholic extraction
Natural fruity fragrance, improves the mood of people；
(2) detergent for washing dishware with hand prepared by the present invention is mainly using natural plants as raw material, and chemical addition agent is few, and avoiding makes
It is safer more environmentally friendly with rear chemical residue problem difficult to degrade, there is good washing cleaning action, tableware can be killed
Bacterium, while having fruity fragrant, there are higher use value, wide market.
Specific embodiment
The fresh cactus of 200~400g is taken, surface spine is removed, obtains pest pear, take the stingless celestial being of 100~200g
The palm, the fresh argy wormwood of 100~200g and the fresh spinach of 50~100g, are immersed in 500~1000g deionized water after chopping, obtain
Mixture；Condensing unit is opened, mixture is warming up to 100 DEG C of boiling 1h, receives condensation reflux liquid in boiling, with 30~
60g petroleum ether extracts condensation reflux liquid, obtains extract liquor, and extract liquor is placed in Rotary Evaporators, adjusts revolving speed and is
It is taken out after 100r/min, 1h, obtains extracting solution；Mixture is filtered, filter residue is removed, continues boiling and 30~60min is concentrated, obtain
Antibacterial liquid；20~40g fragrant citrus pericarp, 20~40g orange peel and 50~100g pomelo peel are taken, uses deionization after wooden dipper white on skin is scraped off
Water is cleaned, and is shredded, is immersed in 300~600g dehydrated alcohol after draining, and is sealed one week；Deblocking, takes 200~400g soak, 3
~6g coconut oil foaming agent, 8~16g triethanolamine, 4~8g sodium benzoate, 3~6g sodium chloride and 1~2g ethylenediamine tetra-acetic acid
It stirs evenly, obtains cleaning agent；10~20g extracting solution, 70~140g antibacterial liquid, 50~100g cleaning agent and 30~60g is taken to go
Ionized water is mixed, and obtains detergent for washing dishware with hand.
The fresh cactus of 200g is taken, surface spine is removed, obtains pest pear, take 100g pest pear, 100g new
Fresh argy wormwood and the fresh spinach of 50g, are immersed in 500g deionized water after chopping, obtain mixture；Condensing unit is opened, will be mixed
Object is warming up to 100 DEG C of boiling 1h, receives condensation reflux liquid in boiling, is extracted, is obtained to condensation reflux liquid with 30g petroleum ether
To extract liquor, extract liquor is placed in Rotary Evaporators, adjusting revolving speed is 100r/min, takes out after 1h, obtains extracting solution；It will mix
Object filtering is closed, filter residue is removed, continues boiling and 30min is concentrated, obtain antibacterial liquid；Take 20g fragrant citrus pericarp, 20g orange peel and 50g shaddock
Skin is washed with deionized water after scraping off wooden dipper white on skin, shreds after draining, is immersed in 300g dehydrated alcohol, seals one week；Solution
Envelope, takes 200g soak, 3g coconut oil foaming agent, 8g triethanolamine, 4g sodium benzoate, 3g sodium chloride and 1g ethylenediamine tetra-acetic acid
It stirs evenly, obtains cleaning agent；It takes 10g extracting solution, 70g antibacterial liquid, 50g cleaning agent and 30g deionized water to be mixed, obtains
Detergent for washing dishware with hand.
The fresh cactus of 300g is taken, surface spine is removed, obtains pest pear, take 150g pest pear, 150g new
Fresh argy wormwood and the fresh spinach of 75g, are immersed in 750g deionized water after chopping, obtain mixture；Condensing unit is opened, will be mixed
Object is warming up to 100 DEG C of boiling 1h, receives condensation reflux liquid in boiling, is extracted, is obtained to condensation reflux liquid with 45g petroleum ether
To extract liquor, extract liquor is placed in Rotary Evaporators, adjusting revolving speed is 100r/min, takes out after 1h, obtains extracting solution；It will mix
Object filtering is closed, filter residue is removed, continues boiling and 45min is concentrated, obtain antibacterial liquid；Take 30g fragrant citrus pericarp, 30g orange peel and 85g shaddock
Skin is washed with deionized water after scraping off wooden dipper white on skin, shreds after draining, is immersed in 450g dehydrated alcohol, seals one week；Solution
Envelope, takes 300g soak, 5g coconut oil foaming agent, 12g triethanolamine, 6g sodium benzoate, 5g sodium chloride and 1g ethylenediamine tetrem
Acid stirs evenly, and obtains cleaning agent；15g extracting solution, 100g antibacterial liquid, 75g cleaning agent and 45g deionized water is taken to be mixed,
Obtain detergent for washing dishware with hand.
The fresh cactus of 400g is taken, surface spine is removed, obtains pest pear, take 200g pest pear, 200g new
Fresh argy wormwood and the fresh spinach of 100g, are immersed in 1000g deionized water after chopping, obtain mixture；Condensing unit is opened, will be mixed
It closes object and is warming up to 100 DEG C of boiling 1h, receive condensation reflux liquid in boiling, condensation reflux liquid is extracted with 60g petroleum ether,
Extract liquor is obtained, extract liquor is placed in Rotary Evaporators, adjusting revolving speed is 100r/min, takes out after 1h, obtains extracting solution；It will
Mixture filtering, removes filter residue, continues boiling and 60min is concentrated, obtain antibacterial liquid；Take 40g fragrant citrus pericarp, 40g orange peel and 100g
Pomelo peel is washed with deionized water after scraping off wooden dipper white on skin, shreds after draining, is immersed in 600g dehydrated alcohol, sealing one
Week；Deblocking, takes 400g soak, 6g coconut oil foaming agent, 16g triethanolamine, 8g sodium benzoate, 6g sodium chloride and 2g ethylenediamine
Tetraacethyl stirs evenly, and obtains cleaning agent；Take 20g extracting solution, 140g antibacterial liquid, 100g cleaning agent and the mixing of 60g deionized water
Stirring, obtains detergent for washing dishware with hand.
Reference examples: the detergent for washing dishware with hand of Dongguan company production.
The detergent for washing dishware with hand that example and reference examples are prepared is detected, specific detection is as follows:
Gross activity object content: using the gross activity object content of chloroform extraction method measurement detergent.
Detergency: uniformly smearing a certain amount of artificial synthesized dirt on plate, after drying, plate is placed on certain dense
Surfactant solution under degree is washed.Because dirt can be in conjunction with surfactant, solution in washing process
Foam can be reduced, so, the terminal of washing can be measured with foam volume, and it is half that the surfactant foam layer for being selected as solution, which disappears,
Until, the size of detergency is indicated with the number to be washed dishes.
Foaming properties: the surfactant samples of preparation are diluted 10 times, then measures 5mL and is placed in 100mL graduated cylinder, are added
250mg/L hard water is added in 500mL tool plug graduated cylinder to 100mL, is uniformly shaken 20 times, divided up and down with identical dynamics and rhythm
Not Ce Liang 0min, 5min, 10min when sample solution foam height, be measured in parallel (two obtained under the conditions of repeatability three times
5%) difference between secondary independent experiment result is no more than, take its mean value as measurement result.
Specific test result such as table 1.
1 performance characterization contrast table of table
| Detection project | Example 1 | Example 2 | Example 3 | Reference examples |
| Gross activity object content/% | 20.3 | 22.0 | 23.6 | 15.0 |
| Detergency | 3.7 | 3.9 | 4.1 | 1.6 |
| Foam height/mm | 320 | 322 | 330 | 178 |
As shown in Table 1, there is detergent for washing dishware with hand prepared by the present invention good detergency, foaming properties and active matter to contain
Amount.
Claims (7)
1. a kind of preparation method of detergent for washing dishware with hand, which is characterized in that specific production step are as follows:
(1) fresh cactus is taken, surface spine is removed, obtains pest pear, take pest pear, fresh argy wormwood and fresh spinach
Dish impregnates in deionized water after chopping, obtains mixture；
(2) condensing unit is opened, mixture is warming up to 100 DEG C of boiling 1h, condensation reflux liquid is received in boiling, uses petroleum ether
Condensation reflux liquid is extracted, extract liquor is obtained, extract liquor is placed in Rotary Evaporators, is taken out after 1h, obtains extracting solution；
(3) mixture is filtered, removes filter residue, continued boiling concentration, obtain antibacterial liquid；
(4) fragrant citrus pericarp, orange peel and pomelo peel are taken, is washed with deionized water after wooden dipper white on skin is scraped off, is shredded after draining, is impregnated
In dehydrated alcohol, seal one week；
(5) it unseals, takes soak, coconut oil foaming agent, triethanolamine, sodium benzoate, sodium chloride and ethylenediamine tetra-acetic acid stirring
Uniformly, cleaning agent is obtained；
(6) it takes extracting solution, antibacterial liquid, cleaning agent and deionized water to be mixed, obtains detergent for washing dishware with hand.
2. a kind of preparation method of detergent for washing dishware with hand as described in claim 1, which is characterized in that step (1) described nothing
The mass ratio for piercing cactus, fresh argy wormwood and fresh spinach is 2: 2: 1.
3. a kind of preparation method of detergent for washing dishware with hand as described in claim 1, which is characterized in that step (2) described rotation
The revolving speed for turning evaporimeter is 100r/min.
4. a kind of preparation method of detergent for washing dishware with hand as described in claim 1, which is characterized in that step (3) it is described after
The time of continuous boiling concentration is 30~60min.
5. a kind of preparation method of detergent for washing dishware with hand as described in claim 1, which is characterized in that step (4) described orange
The mass ratio of sub- skin, orange peel and pomelo peel is 2: 2: 5.
6. a kind of preparation method of detergent for washing dishware with hand as described in claim 1, which is characterized in that step (5) described leaching
The mass ratio for steeping liquid, coconut oil foaming agent, triethanolamine, sodium benzoate, sodium chloride and ethylenediamine tetra-acetic acid is 200: 3: 8: 4: 3
∶1。
7. a kind of preparation method of detergent for washing dishware with hand as described in claim 1, which is characterized in that step (6) is described to be mentioned
The mass ratio for taking liquid, antibacterial liquid, cleaning agent and deionized water is 1: 7: 5: 3.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811129454.3A CN109055046A (en) | 2018-09-27 | 2018-09-27 | A kind of preparation method of detergent for washing dishware with hand |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811129454.3A CN109055046A (en) | 2018-09-27 | 2018-09-27 | A kind of preparation method of detergent for washing dishware with hand |
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| CN109055046A true CN109055046A (en) | 2018-12-21 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111961535A (en) * | 2020-08-27 | 2020-11-20 | 刘克武 | Antibacterial detergent containing wormwood extract |
| WO2022077953A1 (en) * | 2020-10-15 | 2022-04-21 | 崔万哲 | Detergent and preparation method therefor |
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|---|---|---|---|---|
| CN101838596A (en) * | 2009-03-22 | 2010-09-22 | 游晓宇 | Purely natural liquid detergent for fruits, vegetables and tableware |
| CN102010801A (en) * | 2010-12-11 | 2011-04-13 | 江晨 | Detergent formula |
| CN105969553A (en) * | 2016-06-27 | 2016-09-28 | 施安之 | Plant detergent and preparation method thereof |
| CN106867692A (en) * | 2017-02-10 | 2017-06-20 | 王鑫 | A kind of Multifunctional detergent and preparation method thereof |
| CN107216959A (en) * | 2017-07-04 | 2017-09-29 | 湖南云从科技有限公司 | A kind of cleaning formula of natural degreasing and preparation method thereof |
| CN107603777A (en) * | 2017-11-01 | 2018-01-19 | 许秦甫 | A kind of Chinese medicine environmental-protective detergent and preparation method thereof |
| CN107794140A (en) * | 2017-10-19 | 2018-03-13 | 谭志华 | A kind of fruits and vegetables cleaning agent and preparation method thereof |
-
2018
- 2018-09-27 CN CN201811129454.3A patent/CN109055046A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101838596A (en) * | 2009-03-22 | 2010-09-22 | 游晓宇 | Purely natural liquid detergent for fruits, vegetables and tableware |
| CN102010801A (en) * | 2010-12-11 | 2011-04-13 | 江晨 | Detergent formula |
| CN105969553A (en) * | 2016-06-27 | 2016-09-28 | 施安之 | Plant detergent and preparation method thereof |
| CN106867692A (en) * | 2017-02-10 | 2017-06-20 | 王鑫 | A kind of Multifunctional detergent and preparation method thereof |
| CN107216959A (en) * | 2017-07-04 | 2017-09-29 | 湖南云从科技有限公司 | A kind of cleaning formula of natural degreasing and preparation method thereof |
| CN107794140A (en) * | 2017-10-19 | 2018-03-13 | 谭志华 | A kind of fruits and vegetables cleaning agent and preparation method thereof |
| CN107603777A (en) * | 2017-11-01 | 2018-01-19 | 许秦甫 | A kind of Chinese medicine environmental-protective detergent and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111961535A (en) * | 2020-08-27 | 2020-11-20 | 刘克武 | Antibacterial detergent containing wormwood extract |
| WO2022077953A1 (en) * | 2020-10-15 | 2022-04-21 | 崔万哲 | Detergent and preparation method therefor |
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Application publication date: 20181221 |