CN106336959A - Natural active washing composition and preparation method thereof - Google Patents
Natural active washing composition and preparation method thereof Download PDFInfo
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- CN106336959A CN106336959A CN201610738084.8A CN201610738084A CN106336959A CN 106336959 A CN106336959 A CN 106336959A CN 201610738084 A CN201610738084 A CN 201610738084A CN 106336959 A CN106336959 A CN 106336959A
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- natural
- cleaning compositions
- natural activity
- enzyme
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/825—Mixtures of compounds all of which are non-ionic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2079—Monocarboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Detergent Compositions (AREA)
Abstract
The invention discloses a natural active washing composition and a preparation method thereof. The natural active washing composition is prepared from, by weight, 15-35 parts of a natural nonionic surfactant, 2-8 parts of a composite bio-enzyme, 10-25 parts of sodium citrate, 50-70 parts of deionized water and 1-5 part of a pH regulator. The pH value of the natural active washing composition is 6-9. As pure natural products are adopted as main ingredients of the natural active washing composition, the natural active washing composition has an excellent washing effect and is healthy, safe and free of pollution.
Description
Technical field
The invention belongs to cosmetics of everyday use technical field is and in particular to a kind of natural activity cleaning compositions and its preparation side
Method.
Background technology
It is surfactant that washing agent is the main component of (washing adjustment) again, and surfactant is to contain parent in molecular structure
The water base and two-part organic compound of lipophilic group.It is usually that can ion be decomposed in aqueous according to surfactant,
It is classified as two big class of ionic surfactant and nonionic surface active agent again.Ionic surfactant can divide again
For cationic surfactant, anion surfactant and three kinds of zwitterionic surfactant.Washing in the market
The species of agent includes the multiple products such as washing powder, soap, liquid detergent, soap powder, color bleaching liquor.
On market, the product of existing washing agent either washing powder, liquid detergent or other forms is chemical washing mostly
Agent, the wash removability of chemical detergent is essentially from surfactant.Because surfactant have can reduce capillary
Effect, can penetrate in the fiber gap that Lian Shui cannot ooze people, extrude ensconcing the dirt in fiber gap.And it is chemical
Washing agent then squeezes among these spaces, and shipwreck, to clean them, causes the residual of chemical reagent.People are in extensive useization
While learning washing agent wash my hair, chopsticks of washing the dishes, laundry clothes, have a bath, the chemical substance of residual is accumulated over a long period and is not only polluted environment, also
Can affect healthy.But the urbanization of human lives is inevasible, city life is also not to the dependence of cleaning agent
Evitable.So, improve washing agent, using not harmful to human, do not destroy living environment, non-toxic and non-pollution washing agent just becomes
For the task of top priority.There is presently no and appoint any washing agent to adopt pure natural product completely as primary raw material.
Content of the invention
In order to overcome the deficiencies in the prior art, it is an object of the invention to provide a kind of natural activity cleaning compositions, adopt
With pure natural product crop main component, not only there is good clean result, and healthy and safe, pollution-free.
For solving the above problems, the technical solution adopted in the present invention is as follows:
A kind of natural activity cleaning compositions, it includes following components in parts by weight:
Natural nonionic surfactant 15-35 part
Compound biological enzyme 2-8 part
Sodium citrate 10-25 part
Deionized water 50-70 part
Ph conditioning agent 1-5 part;
The ph value of this natural activity cleaning compositions is 6-9.
As further scheme, natural activity cleaning compositions of the present invention include in parts by weight with the following group
Point:
Natural nonionic surfactant 18-22 part
Compound biological enzyme 3-5 part
Sodium citrate 15-20 part
Deionized water 58-64 part
Ph conditioning agent 2-4 part.
As further scheme, natural activity cleaning compositions of the present invention also include 3-8 part soapberry and extract
Thing.
As further scheme, natural activity cleaning compositions of the present invention also include 1-5 part pollen essence.
As further scheme, pollen spices of the present invention is selected from Jasmine, white orchid, lavender, contains in perfume
A kind of flower, the natural essence obtaining after sequentially passing through air-dried, milled processed.
As further scheme, natural nonionic surfactant of the present invention is Tea Saponin or sucrose-fatty
One of ester or two kinds of mixing.
As further scheme, compound biological enzyme of the present invention is protein decomposition enzyme, lipolytic enzyme, starch
Two or more mixing in catabolic enzyme, cellulolytic enzyme, mannonase peroxidase, laccase, shellac enzyme.
A kind of preparation method of described natural activity cleaning compositions, this preparation method comprises the following steps:
1) the natural nonionic surfactant of formula ratio is dissolved in the deionized water of part formulation amount, stirring is all
Even, obtain mixed liquor;
2) in step 1) mixed liquor in sequentially add compound biological enzyme and the sodium citrate of formula ratio, stir;
3) add remaining deionized water, continue to stir.
As further scheme, in preparation method of the present invention, step 2) add sodium citrate after be additionally added 3-8
Part soapberry extract.
As further scheme, in preparation method of the present invention, step 3) add remaining deionized water follow-up
The continuous pollen essence adding 1-5 part prefabricated.
Compared to existing technology, the beneficial effects of the present invention is:
1. natural activity cleaning compositions of the present invention adopt pure natural components, have good dirt-removing power and life
Thing activity;
2. natural activity cleaning compositions of the present invention can be separately as washing agent using it is also possible to be processed into powder
Shape or soap, due to its Nantural non-toxic, can be not only used for cleaning tableware and can also use vegetables and fruit, safety and sanitation, to environment
Pollution-free.
With reference to specific embodiment, the present invention is described in further detail.
Specific embodiment
Natural activity cleaning compositions of the present invention, it includes following components in parts by weight:
Natural nonionic surfactant 15-35 part
Compound biological enzyme 2-8 part
Sodium citrate 10-25 part
Deionized water 50-70 part
Ph conditioning agent 1-5 part;
The ph value of this natural activity cleaning compositions is 6-9.
As further scheme, natural activity cleaning compositions of the present invention include in parts by weight with the following group
Point:
Natural nonionic surfactant 18-22 part
Compound biological enzyme 3-5 part
Sodium citrate 15-20 part
Deionized water 58-64 part
Ph conditioning agent 2-4 part.
As further scheme, natural activity cleaning compositions of the present invention also include 3-8 part soapberry and extract
Thing.Main component in soapberry extract of the present invention is sapindoside, and soapberry extract has antibacterial and makees
With the effect of suppression bacterium can be played in the formula of volume of the present invention, be a kind of natural antiseptic.In addition sapindoside tool
There is stronger dirt-removing power, degradable, and no hazard residue, rinse simple and convenient, free from extraneous odour, little to skin irritation.
As further scheme, natural activity cleaning compositions of the present invention also include 1-5 part pollen essence.Tool
The pollen spices of the present invention of body is selected from, but not limited to, Jasmine, white orchid, lavender, spends containing one of perfume (or spice), successively
Through the natural essence air-drying, obtain after milled processed.Instead of natural flavor with natural pollen essence in the present invention, add
It is added to the cleaning compositions that can obtain diverse fragrant flavour in cleaning compositions.
As further scheme, natural nonionic surfactant of the present invention is Tea Saponin or sucrose-fatty
One of ester or two kinds of mixing.Tea Saponin of the present invention derives from tea seed cake.Tea Saponin is that one kind is natural well
Nonionic surfactant, in Tea Saponin molecular structure, one end of sugared body is hydrophobic grouping, leads to the hydrophilic radical of the other end
Cross ehter bond to be connected, because hydrophobic grouping is made up of the glucoside unit that organic acid is connected with ester bond form, Tea Saponin has
Condition for the surface-active action that can rise.Tea Saponin can reduce the surface-active of water, also decontamination, foaming, wetting,
The kinds of surface activity such as dispersion, steady bubble emulsification.The particle of the emulsion particle of Tea Saponin is little, be evenly distributed and have good stability,
A kind of nonionic surfactant of natural superior performance, Tea Saponin have stronger foamability, be 4- in acidity
In 11 scope, Tea Saponin can normally foam, and keeps stability.Therefore in the present invention without interpolation chemical blowing agent.
Additionally, Tea Saponin also has good biologically active, in the research of the present invention, find that there is significantly impervious antiinflammation, main
Will be in the incipient stage of inflammation, Tea Saponin can allow the permeability normalization of interrupted capillary pair, and meanwhile, Tea Saponin is also
There is the effect of the secretion of hormone such as adrenal gland in stimulating animal body and matter hormone (corticosterone), corticosterone is to sugared generation
The effect of thanking is very strong, and it can be by promoting the new utilization suppressing blood sugar from birth of gluconeogenesis and glucose.Sucrose fatty ester
It is by sucrose and aliphatic acid synthesis, there is good steady bubble, viscosity is adjusted, disperse the surface-actives such as increase-volume, infiltration;And no
Malicious, non-stimulated, degradability is good.Preferably in scheme, the natural nonionic surfactant that the present invention adopts is Tea Saponin and sugarcane
The mixture of sugar fatty acid ester, using the excitant that not only can reduce surfactant after both are compounding, can also improve table
Face activity, sucrose fatty ester also helps stablizing of Tea Saponin foaming characteristic simultaneously.Both compounding ratios are with Tea Saponin and sugarcane
The mass ratio of sugar fatty acid ester is 1:(0.2-0.6).
Enzyme preparation is the auxiliary element of washing agent, and the effect using its catalyst can remove various dirts substantially, consequently facilitating
The cleaning ingredients such as surfactant can be easier, more effectively remove dirt.But there is limitation in effect of single enzyme
Property, also tend to meet being actually needed of washing agent.Therefore, the present invention uses compound biological enzyme, specifically, the present invention
Described compound biological enzyme is protein decomposition enzyme, lipolytic enzyme, amylolytic enzyme, cellulolytic enzyme, mannonase mistake
Two or more mixing in oxide enzyme, laccase, shellac enzyme.
A kind of preparation method of described natural activity cleaning compositions, this preparation method comprises the following steps:
1) the natural nonionic surfactant of formula ratio is dissolved in the deionized water of part formulation amount, stirring is all
Even, obtain mixed liquor;
2) in step 1) mixed liquor in sequentially add compound biological enzyme and the sodium citrate of formula ratio, stir;
3) add remaining deionized water, continue to stir.
As further scheme, in preparation method of the present invention, step 2) add sodium citrate after be additionally added 3-8
Part soapberry extract.
As further scheme, in preparation method of the present invention, step 3) add remaining deionized water follow-up
The continuous pollen essence adding 1-5 part prefabricated.
The following is part specific embodiment of the present invention, the raw material being adopted in the following embodiments, reagent remove special limit
All can be obtained by commercial channel outside fixed.
Embodiment 1
A kind of natural activity cleaning compositions, it includes following components in parts by weight:
15 parts of Tea Saponin
Cellulolytic enzyme and 2 parts of the compound biological enzyme of protein decomposition enzyme composition
10 parts of sodium citrate
50 parts of deionized water
1 part of ph conditioning agent;
The ph value of this natural activity cleaning compositions is 6;It is prepared by the following method and form:
1) Tea Saponin of formula ratio is dissolved in the deionized water of part formulation amount, stirs, obtain mixed liquor;
2) in step 1) mixed liquor in sequentially add answering of the cellulolytic enzyme of formula ratio and protein decomposition enzyme composition
Close biology enzyme and sodium citrate, stir;
3) add remaining deionized water, continue to stir.
Embodiment 2
A kind of natural activity cleaning compositions, it includes following components in parts by weight:
Tea Saponin and 35 parts of sucrose-fatty ester admixture
Cellulolytic enzyme and 8 parts of the compound biological enzyme of amylolytic enzyme composition
25 parts of sodium citrate
70 parts of deionized water
5 parts of ph conditioning agent;
The ph value of this natural activity cleaning compositions is 7, and Tea Saponin is 1:0.2 with the mass ratio of sucrose fatty ester;Should
Natural activity cleaning compositions are prepared by the following method and form:
1) it is dissolved in the deionization of part formulation amount with sucrose fatty ester after the Tea Saponin of formula ratio being mixed in proportion
In water, stir, obtain mixed liquor;
2) in step 1) mixed liquor in sequentially add the compound of the cellulolytic enzyme of formula ratio and amylolytic enzyme composition
Biology enzyme and sodium citrate, stir;
3) add remaining deionized water, continue to stir.
Embodiment 3
A kind of natural activity cleaning compositions include following components in parts by weight:
18 parts of Tea Saponin
Cellulolytic enzyme and 3 parts of the compound biological enzyme of amylolytic enzyme composition
15 parts of sodium citrate
3 parts of soapberry extract
1 part of lavender pollen
58 parts of deionized water
2 parts of ph conditioning agent;
The ph value of this natural activity cleaning compositions is 6;It is prepared by the following method and form:
1) Tea Saponin of formula ratio is dissolved in the deionized water of part formulation amount, stirs, obtain mixed liquor;
2) in step 1) mixed liquor in sequentially add answering of the cellulolytic enzyme of formula ratio and protein decomposition enzyme composition
Close biology enzyme, sodium citrate, soapberry extract, stir;
3) add remaining deionized water and lavender pollen, continue to stir.
Embodiment 4
A kind of natural activity cleaning compositions include following components in parts by weight:
Tea Saponin and 22 parts of sucrose-fatty ester admixture
Cellulolytic enzyme and 5 parts of the compound biological enzyme of protein decomposition enzyme composition
Sodium citrate 15-20 part
8 parts of soapberry extract
5 parts of lavender pollen
64 parts of deionized water
4 parts of ph conditioning agent;
The ph value of this natural activity cleaning compositions is 9;It is prepared by the following method and form:
1) it is dissolved in after the Tea Saponin of formula ratio being mixed with sucrose fatty ester in the deionized water of part formulation amount, stir
Mix uniformly, obtain mixed liquor;
2) in step 1) mixed liquor in sequentially add answering of the cellulolytic enzyme of formula ratio and protein decomposition enzyme composition
Close biology enzyme, sodium citrate, soapberry extract, lavender pollen, stir;
3) add remaining deionized water, continue to stir.
Effect detection
1. detergency test
According to the method for gb9985-2000 standard, people is purchased to the natural activity cleaning compositions obtained by embodiment 1-4
Work dirt, 250ppm hard water, dirt pottery sprayer and foam level method test the instrument needed for detergency.Weigh reality with electronic balance
Apply the natural activity cleaning compositions 5.0g described in a 1-4, the hard water that 1000ml concentration is 250ppm is poured in basin, separately by 1
000ml concentration is that the hard water of 250ppm is put in people's tubualted bottle, under room temperature (25 DEG C), opens the delivery port of tubualted bottle, hard water stream
In people's basin, punching spumes, and after hard water stops flowing out (process about 45s), plate scrubbed by 102mm pig palm fibre paintbrush, clockwise and inverse
Hour hands brush 5 times respectively, after being repeated 2 times, the dirt major part being applied on plate is washed off, finally will partly not wash off again it is known that
Foam is wholly absent, the number of record plate.Result is referring to table 1.
Table 1
--- | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
Plate number | 7 | 9 | 8 | 10 |
2. frothing capacity test
By Roche foam meter constant temperature at 25 DEG C, weigh the natural activity cleaning compositions 5.0g of embodiment 1-4 respectively, add
1l distilled water, stirring and dissolving, after thermostatic reaches 25 DEG C, draw test solution with 200ml quantitation funnel, rinse along foam meter tube wall
Once, then take test solution to put people's foam meter bottom alignment master scale to 50ml, then draw test solution with 200ml quantitation funnel, Gu
Determine hopper centre position, put down test solution, record foam height (mm), result retains integer.Result is referring to table 2.
Table 2
---- | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
Foam height (mm) | 166 | 175 | 160 | 170 |
3. foaming stability test
By Roche foam meter constant temperature at 25 DEG C, weigh the natural activity cleaning compositions 5.0g of embodiment 1-4 respectively, add
1l distilled water, stirring and dissolving, after making thermostatic reach 25 DEG C, draw test solution with 200ml quantitation funnel, along the punching of foam meter tube wall
Wash once, then take test solution to put people's foam meter bottom alignment master scale to 50ml, then draw test solution with 200ml quantitation funnel,
Fixed funnel center, records the foam height (mm) of 5,10,15,20,25,30 minutes respectively after putting down test solution, result is protected
Stay integer.Result is referring to table 3.
Table 3
(foam height) of different time | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
5 minutes foam heights mm | 187 | 189 | 191 | 180 |
10 minutes foam heights mm | 174 | 179 | 180 | 171 |
15 minutes foam heights mm | 169 | 172 | 175 | 166 |
20 minutes foam heights mm | 157 | 160 | 161 | 154 |
25 minutes foam heights mm | 137 | 141 | 143 | 136 |
30 minutes foam heights mm | 118 | 121 | 120 | 115 |
4. security toxicological experiment
Toxicological test is carried out to the natural activity cleaning compositions of embodiment 1-4, according to " foodsafety Toxicological Assessment journey
Sequence and method " gb 15193-2003, using maximum tolerance metering experiment method, dosage is set to 10000mg/kg bw, from 20
Kunming mice, male and female half and half.Animal fasting i6h before test, does not limit drinking-water.Give animal 500mg/ml concentration using administration by gavage
Sample solution, gavage amount is 0.4ml/20g body weight.Observe the poisoning manifestations of animal and death condition after gavage, weigh weekly 1
Secondary, observe 14d.
The oral result of the test of chmice acute shows: the natural activity cleaning compositions of embodiment 1-4 belong to washing of nontoxic level
Wash agent.
Above-mentioned embodiment is only the preferred embodiment of the present invention it is impossible to limit the scope of protection of the invention with this,
The change of any unsubstantiality that those skilled in the art is done on the basis of the present invention and replacement belong to institute of the present invention
Claimed scope.
Claims (10)
1. a kind of natural activity cleaning compositions are it is characterised in that it includes following components in parts by weight:
Natural nonionic surfactant 15-35 part
Compound biological enzyme 2-8 part
Sodium citrate 10-25 part
Deionized water 50-70 part
Ph conditioning agent 1-5 part;
The ph value of this natural activity cleaning compositions is 6-9.
2. natural activity cleaning compositions according to claim 1 it is characterised in that it include in parts by weight following
Component:
Natural nonionic surfactant 18-22 part
Compound biological enzyme 3-5 part
Sodium citrate 15-20 part
Deionized water 58-64 part;
Ph conditioning agent 2-4 part.
3. natural activity cleaning compositions according to claim 1 it is characterised in that this natural activity cleaning compositions also
Including 3-8 part soapberry extract.
4. the natural activity cleaning compositions according to any one of claim 1 are it is characterised in that this natural activity washing group
Compound also includes 1-5 part pollen essence.
5. natural activity cleaning compositions according to claim 4 are it is characterised in that described pollen spices is selected from jasmine
Flower, white orchid, lavender, containing one of perfume (or spice) flower, the natural essence that obtains after sequentially passing through air-dried, milled processed.
6. the natural activity cleaning compositions according to any one of claim 1-5 are it is characterised in that described natural nonionic
Surfactant is one of Tea Saponin or sucrose fatty ester or two kinds of mixing.
7. the natural activity cleaning compositions according to any one of claim 1-5 are it is characterised in that described compound biological enzyme
For protein decomposition enzyme, lipolytic enzyme, amylolytic enzyme, cellulolytic enzyme, mannonase peroxidase, laccase,
Two or more mixing in shellac enzyme.
8. a kind of preparation method of natural activity cleaning compositions as claimed in claim 1 is it is characterised in that this preparation method
Comprise the following steps:
1) the natural nonionic surfactant of formula ratio is dissolved in the deionized water of part formulation amount, stirs, obtain
To mixed liquor;
2) in step 1) mixed liquor in sequentially add compound biological enzyme and the sodium citrate of formula ratio, stir;
3) add remaining deionized water, continue to stir.
9. the preparation method of natural activity cleaning compositions according to claim 8 is it is characterised in that step 2) add lemon
It is additionally added 3-8 part soapberry extract after lemon acid sodium.
10. the preparation method of natural activity cleaning compositions according to claim 8 is it is characterised in that step 3) add
The prefabricated pollen essence of 1-5 part is continuously added after remaining deionized water.
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CN113637538A (en) * | 2021-07-05 | 2021-11-12 | 桂林理工大学 | Small white shoe cleaning agent and preparation method thereof |
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Application publication date: 20170118 |