CN114599663A - 含有瑞鲍迪苷d的晶析物的制造方法及含有瑞鲍迪苷d的晶析物 - Google Patents

含有瑞鲍迪苷d的晶析物的制造方法及含有瑞鲍迪苷d的晶析物 Download PDF

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Publication number
CN114599663A
CN114599663A CN202080074650.4A CN202080074650A CN114599663A CN 114599663 A CN114599663 A CN 114599663A CN 202080074650 A CN202080074650 A CN 202080074650A CN 114599663 A CN114599663 A CN 114599663A
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China
Prior art keywords
rebaudioside
crystallization
rebd
mass
solution
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CN202080074650.4A
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English (en)
Chinese (zh)
Inventor
浦井聡一郎
内海唯
高柳圭佑
西堀友之
三井亮辉
横尾芳明
长尾浩二
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Suntory Holdings Ltd
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Suntory Holdings Ltd
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Publication of CN114599663A publication Critical patent/CN114599663A/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H15/00—Compounds containing hydrocarbon or substituted hydrocarbon radicals directly attached to hetero atoms of saccharide radicals
    • C07H15/20—Carbocyclic rings
    • C07H15/24—Condensed ring systems having three or more rings
    • C07H15/256—Polyterpene radicals
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Preparation or treatment thereof
    • A23L2/52—Adding ingredients
    • A23L2/60—Sweeteners
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • A23L27/33—Artificial sweetening agents containing sugars or derivatives
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
    • A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • A23L27/30—Artificial sweetening agents
    • A23L27/33—Artificial sweetening agents containing sugars or derivatives
    • A23L27/36—Terpene glycosides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0004—Crystallisation cooling by heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/02—Crystallisation from solutions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H1/00—Processes for the preparation of sugar derivatives
    • C07H1/06—Separation; Purification
    • C07H1/08—Separation; Purification from natural products
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Polymers & Plastics (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Proteomics, Peptides & Aminoacids (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Saccharide Compounds (AREA)
  • Seasonings (AREA)
  • Non-Alcoholic Beverages (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
CN202080074650.4A 2019-11-01 2020-10-30 含有瑞鲍迪苷d的晶析物的制造方法及含有瑞鲍迪苷d的晶析物 Pending CN114599663A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
JP2019-200256 2019-11-01
JP2019200256 2019-11-01
PCT/JP2020/040974 WO2021085643A1 (ja) 2019-11-01 2020-10-30 レバウディオサイドｄ含有晶析物の製造方法およびレバウディオサイドｄ含有晶析物

Publications (1)

Publication Number Publication Date
CN114599663A true CN114599663A (zh) 2022-06-07

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CN202080074650.4A Pending CN114599663A (zh) 2019-11-01 2020-10-30 含有瑞鲍迪苷d的晶析物的制造方法及含有瑞鲍迪苷d的晶析物

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Country Link
US (1) US20230027601A1 (https=)
EP (1) EP4052771B1 (https=)
JP (2) JP7187710B2 (https=)
CN (1) CN114599663A (https=)
AU (1) AU2020374113A1 (https=)
BR (1) BR112022008220A2 (https=)
MY (1) MY208792A (https=)
WO (1) WO2021085643A1 (https=)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117264000A (zh) * 2023-09-19 2023-12-22 安徽金禾实业股份有限公司 一种从生物酶法催化甜菊糖反应液中提取莱鲍迪苷d的方法

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8444756B2 (en) 2003-08-07 2013-05-21 Ivoclar Vivadent Ag Lithium silicate materials
CN114437152B (zh) * 2021-12-31 2024-03-26 蚌埠市华东生物科技有限公司 一种甜菊糖苷水提液的脱色除杂方法
WO2025178136A1 (ja) * 2024-02-22 2025-08-28 守田化学工業株式会社 ステビオール配糖体の新規組み合わせ

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1030762A (zh) * 1987-07-21 1989-02-01 罗格H·吉奥弗尼托 从植物原料中提取卡哈苡苷的方法
US20060142555A1 (en) * 2004-12-23 2006-06-29 Council Of Scientific And Industrial Research Process for production of steviosides from stevia rebaudiana bertoni
WO2011046423A1 (en) * 2009-10-15 2011-04-21 Purecircle Sdn Bhd High-purity rebaudioside d and applications
US20130071339A1 (en) * 2010-03-12 2013-03-21 Avetik Markosyan High-purity steviol glycosides
CN103709215A (zh) * 2013-12-31 2014-04-09 天津北洋百川生物技术有限公司 一种从甜菊糖结晶母液糖中提取莱鲍迪甙d的方法
CN108289487A (zh) * 2015-10-02 2018-07-17 可口可乐公司 具有改进的风味特征曲线的甜菊醇糖苷甜味剂
CN109415736A (zh) * 2016-03-14 2019-03-01 谱赛科美国股份有限公司 高溶解性甜菊醇糖苷
CN109640693A (zh) * 2016-06-14 2019-04-16 谱赛科美国股份有限公司 甜菊醇糖苷组合物，生产方法和用途

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9994606B2 (en) * 2011-12-16 2018-06-12 Almendra Pte Ltd. Process for the purification of Rebaudioside A and compositions thereof
CN111163631A (zh) 2017-10-12 2020-05-15 三得利控股株式会社 富含瑞鲍迪苷m的甜菊植物
CN109645432A (zh) * 2019-02-20 2019-04-19 史迪威生物科技（苏州）有限公司 一种结晶法制备甜菊糖型餐桌糖方法

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1030762A (zh) * 1987-07-21 1989-02-01 罗格H·吉奥弗尼托 从植物原料中提取卡哈苡苷的方法
US20060142555A1 (en) * 2004-12-23 2006-06-29 Council Of Scientific And Industrial Research Process for production of steviosides from stevia rebaudiana bertoni
WO2011046423A1 (en) * 2009-10-15 2011-04-21 Purecircle Sdn Bhd High-purity rebaudioside d and applications
JP2013507914A (ja) * 2009-10-15 2013-03-07 ピュアサークル スドゥン バハド 高純度のレバウジオシドｄとその適用
EP2708548A2 (en) * 2009-10-15 2014-03-19 Purecircle SDN BHD High-Purity Rebaudioside D and Applications
US20130071339A1 (en) * 2010-03-12 2013-03-21 Avetik Markosyan High-purity steviol glycosides
CN103709215A (zh) * 2013-12-31 2014-04-09 天津北洋百川生物技术有限公司 一种从甜菊糖结晶母液糖中提取莱鲍迪甙d的方法
CN108289487A (zh) * 2015-10-02 2018-07-17 可口可乐公司 具有改进的风味特征曲线的甜菊醇糖苷甜味剂
CN109415736A (zh) * 2016-03-14 2019-03-01 谱赛科美国股份有限公司 高溶解性甜菊醇糖苷
CN109640693A (zh) * 2016-06-14 2019-04-16 谱赛科美国股份有限公司 甜菊醇糖苷组合物，生产方法和用途

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN117264000A (zh) * 2023-09-19 2023-12-22 安徽金禾实业股份有限公司 一种从生物酶法催化甜菊糖反应液中提取莱鲍迪苷d的方法

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Publication number Publication date
MY208792A (en) 2025-05-29
JP7627248B2 (ja) 2025-02-05
BR112022008220A2 (pt) 2022-07-12
JP2022166190A (ja) 2022-11-01
EP4052771B1 (en) 2025-10-22
WO2021085643A1 (ja) 2021-05-06
AU2020374113A1 (en) 2022-05-26
JP7187710B2 (ja) 2022-12-12
EP4052771A4 (en) 2023-10-25
EP4052771A1 (en) 2022-09-07
JPWO2021085643A1 (ja) 2021-12-23
US20230027601A1 (en) 2023-01-26

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Application publication date: 20220607