CN114468432A - 一种羽绒服用防水面料及其制备方法 - Google Patents

一种羽绒服用防水面料及其制备方法 Download PDF

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CN114468432A
CN114468432A CN202210222813.XA CN202210222813A CN114468432A CN 114468432 A CN114468432 A CN 114468432A CN 202210222813 A CN202210222813 A CN 202210222813A CN 114468432 A CN114468432 A CN 114468432A
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CN114468432B (zh
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陈岩
刘汉春
吴昆明
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Gaofan Zhejiang Information Technology Co Ltd
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Abstract

本发明公开了羽绒服防水面料领域的一种羽绒服用防水面料，所述防水面料从内至外依次为保暖层、透气防水层、吸水供热层以及基布层，所述保暖层、透气防水层、吸水供热层以及基布层之间通过热压复合制成。本发明防水面料中的基布层通过与含氟防水处理剂、醋酸、渗透剂以及柔软剂组成的混合液浸泡后，使得该基布层具备较高的防水、防泼水性能，降低防水结构损坏机率，同时当意外渗入液体时，因为吸水供热层由电气石粉、铝粉、碳酸钠以及石墨粉制成，使得吸水供热层会持续产生热量，并且石墨粉的设置使得吸水供热层还具有一定锁水作用，热量通过透气防水层反馈给保暖层，避免在意外渗水时影响到保暖层的保温性能。

Description

一种羽绒服用防水面料及其制备方法
技术领域
本发明公开羽绒服防水面料领域，具体为一种羽绒服用防水面料及其制备方法。
背景技术
随着物质生活水平的不断发展，羽绒服已经成为人们在冬天的常备保暖服装。
为了保证羽绒服的保暖效果，羽绒服一般采用防水面料制备，而传统的羽绒服只能起到单一的防水保护，当羽绒服外的防水结构损坏导致意外进水时现有的防水面料不能起到阻挡液体继续渗透的同时会干涉到羽绒服的保暖性能，导致羽绒服无法提供保暖。为此，我们提出一种羽绒服用防水面料及其制备方法。
发明内容
本发明的目的在于提供一种羽绒服用防水面料及其制备方法，以解决上述背景技术中提出的问题。
为实现上述目的，本发明提供如下技术方案：一种羽绒服用防水面料，所述防水面料从内至外依次为保暖层、透气防水层、吸水供热层以及基布层，所述保暖层、透气防水层、吸水供热层以及基布层之间通过热压复合制成；
其中，所述吸水供热层为将吸水自热物质和抗菌涂层物同时涂布至面料基体后对所述面料基体采用整理液整理后获得。
进一步改进在于，所述整理液按重量份数包括：3-8份铵盐溶液、1-5份十二烷醇、1-3份氯化氢、1-3份氯代甲苯和1-3份二甲胺。
进一步改进在于，所述吸水自热物质的制备方法为：取电气石粉、铝粉、碳酸钠以及石墨粉末混合均匀，从而得到吸水自热物质。
进一步改进在于，所述吸水自热物质的制备原料按重量份数包括：2-8份电气石粉、1-4份铝粉、2-6份碳酸钠以及5-10份石墨烯粉末。
进一步改进在于，所述面料基体由为涤纶或尼龙纱线编织而成；
所述抗菌涂层物的制备方法为：将聚氨酯树脂、甲壳素、抑菌粉体和交联剂进行混合搅拌均匀，搅拌后添加稀释剂调整粘度在17000～20000mPa·s，得抗菌涂层物。
进一步改进在于，所述抗菌涂层中的稀释剂为丁酮、二甲基甲酰胺、甲苯其中至少一种。
进一步改进在于，所述基布层的制备方法为：通过尼龙纱线或涤纶编织得到基体，将基体放入含氟防水处理剂、醋酸、渗透剂以及柔软剂组成的混合液内浸泡20-30min，然后经60-70℃焙烘1-2h得到。
进一步改进在于，所述透气防水层为防水透气膜、聚氨酯薄膜或高分子防水透气材料加复合面料复合而成。
一种羽绒服用防水面料的制备方法：
(1)将聚氨酯树脂、甲壳素、抑菌粉体和交联剂进行混合搅拌均匀，搅拌后添加稀释剂得到抗菌涂层物，将由电气石粉、铝粉、碳酸钠以及石墨粉末混合均匀得到吸水自热物质，同时将抗菌涂层物和吸水自热物质涂布面料基体两面，然后在90℃下烘干至完全干燥，得到吸水供热层；
(2)将铵盐溶液、十二烷醇、氯化氢、氯代甲苯和二甲胺混合得到整理液后，再通过整理液对所述吸水供热层进行清洗，清洗后将吸水供热层干燥；
(3)在所述吸水供热层的一面依次热压复合透气防水层和保暖层，在吸水供热层的另一面热压复合基布层，即得到所述的羽绒服用防水面料。
与现有技术相比，本发明的有益效果是：本发明防水面料中的基布层通过与含氟防水处理剂、醋酸、渗透剂以及柔软剂组成的混合液浸泡后，使得该基布层具备较高的防水、防泼水性能，降低防水结构损坏机率，同时当意外渗入液体时，因为吸水供热层由电气石粉、铝粉、碳酸钠以及石墨粉制成，使得吸水供热层会持续产生热量，并且石墨粉的设置使得吸水供热层还具有一定锁水作用，从而使得吸水供热层能持续提供热量，热量通过透气防水层反馈给保暖层，避免在意外渗水时影响到保暖层的保温性能，同时吸水供热层同抗菌涂层均匀涂布在面料基体表面，以避免意外进入的液体在面料内部滋生细菌，使得吸水供热层吸水供热更加稳定且安全。
具体实施方式
下面将结合本发明实施例，对本发明实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部的实施例。基于本发明中的实施例，本领域普通技术人员在没有做出创造性劳动前提下所获得的所有其他实施例，都属于本发明保护的范围。
实施例1
本发明提供一种羽绒服用防水面料，防水面料从内至外依次为保暖层、透气防水层、吸水供热层以及基布层，其中，透气防水层为防水透气膜。所述保暖层、透气防水层、吸水供热层以及基布层之间通过热压复合制成；
吸水供热层为将吸水自热物质和抗菌涂层物同时涂布至面料基体后对面料基体采用整理液整理后获得。
整理液按重量份数包括：3份铵盐溶液、1份十二烷醇、1份氯化氢、1份氯代甲苯和1份二甲胺；
吸水自热物质的制备方法为：取电气石粉、铝粉、碳酸钠以及石墨粉末混合均匀，从而得到吸水自热物质；
吸水自热物质的制备原料按重量份数包括：2份电气石粉、1份铝粉、2-6份碳酸钠以及5份石墨烯粉末；
面料基体由为涤纶或尼龙纱线编织而成；
抗菌涂层物的制备方法为：将聚氨酯树脂、甲壳素、抑菌粉体和交联剂进行混合搅拌均匀，搅拌后添加稀释剂调整粘度在18000mPa·s，得抗菌涂层物；
抗菌涂层中的稀释剂为丁酮；
基布层的制备方法为：通过尼龙纱线编织得到基体，将基体放入含氟防水处理剂、醋酸、渗透剂以及柔软剂组成的混合液内浸泡20min，然后经60℃焙烘1h得到。
实施例2
本发明提供一种羽绒服用防水面料，防水面料从内至外依次为保暖层、透气防水层、吸水供热层以及基布层，其中，透气防水层为防水透气膜。所述保暖层、透气防水层、吸水供热层以及基布层之间通过热压复合制成；
吸水供热层为将吸水自热物质和抗菌涂层物同时涂布至面料基体后对面料基体采用整理液整理后获得。
整理液按重量份数包括：3份铵盐溶液、1份十二烷醇、1份氯化氢、1份氯代甲苯和1份二甲胺；
吸水自热物质的制备方法为：取电气石粉、铝粉、碳酸钠以及石墨粉末混合均匀，从而得到吸水自热物质；
吸水自热物质的制备原料按重量份数包括：6份电气石粉、3份铝粉、4份碳酸钠以及8份石墨烯粉末；
面料基体由为涤纶或尼龙纱线编织而成；
抗菌涂层物的制备方法为：将聚氨酯树脂、甲壳素、抑菌粉体和交联剂进行混合搅拌均匀，搅拌后添加稀释剂调整粘度在18000mPa·s，得抗菌涂层物；
抗菌涂层中的稀释剂为丁酮；
基布层的制备方法为：通过尼龙纱线编织得到基体，将基体放入含氟防水处理剂、醋酸、渗透剂以及柔软剂组成的混合液内浸泡20min，然后经60℃焙烘1h得到。
实施例3
本发明提供一种羽绒服用防水面料，防水面料从内至外依次为保暖层、透气防水层、吸水供热层以及基布层，其中，透气防水层为防水透气膜。所述保暖层、透气防水层、吸水供热层以及基布层之间通过热压复合制成；
吸水供热层为将吸水自热物质和抗菌涂层物同时涂布至面料基体后对面料基体采用整理液整理后获得。
整理液按重量份数包括：3份铵盐溶液、1份十二烷醇、1份氯化氢、1份氯代甲苯和1份二甲胺；
吸水自热物质的制备方法为：取电气石粉、铝粉、碳酸钠以及石墨粉末混合均匀，从而得到吸水自热物质；
吸水自热物质的制备原料按重量份数包括：1份电气石粉、2份铝粉、1份碳酸钠以及3份石墨烯粉末；
面料基体由为涤纶或尼龙纱线编织而成；
抗菌涂层物的制备方法为：将聚氨酯树脂、甲壳素、抑菌粉体和交联剂进行混合搅拌均匀，搅拌后添加稀释剂调整粘度在18000mPa·s，得抗菌涂层物；
抗菌涂层中的稀释剂为丁酮；
基布层的制备方法为：通过尼龙纱线编织得到基体，将基体放入含氟防水处理剂、醋酸、渗透剂以及柔软剂组成的混合液内浸泡20min，然后经60℃焙烘1h得到。
对比例1
一种羽绒服用防水面料，其与实施例2的步骤基本相同，唯一区别在于在制备吸水自热物质时不添加电气石粉。
对比例2
一种羽绒服用防水面料，其与实施例2的步骤基本相同，唯一区别在于在制备抗菌涂层物时不添加甲壳素和抑菌粉体。
对比例3
一种羽绒服用防水面料，其与实施例2的步骤基本相同，唯一区别在于将基体放入醋酸、渗透剂以及柔软剂组成的混合液内浸泡20min，然后经60℃焙烘1h得到。
对比例4
一种羽绒服用防水面料，其与实施例2的步骤基本相同，唯一区别在于将将基体放入含氟防水处理剂以及柔软剂组成的混合液内浸泡20min，然后经60℃焙烘1h得到。
上述各实施例和对比例在具体制备过程中，将聚氨酯树脂、甲壳素、抑菌粉体和交联剂进行混合搅拌均匀，搅拌后添加稀释剂得到抗菌涂层物，将由电气石粉、铝粉、碳酸钠以及石墨粉末混合均匀得到吸水自热物质，同时将抗菌涂层物和吸水自热物质涂布面料基体两面，然后在90℃下烘干至完全干燥，得到吸水供热层，将铵盐溶液、十二烷醇、氯化氢、氯代甲苯和二甲胺混合得到整理液后，再通过整理液对所述吸水供热层进行清洗，清洗后将吸水供热层干燥，在所述吸水供热层的一面依次热压复合透气防水层和保暖层，在吸水供热层的另一面热压复合基布层，即得到所述的羽绒服用防水面料。
取上述实施例2以及对比例1-4制得的一种羽绒服用防水面料，分别进行如下测试：
(1)防泼水性能:参照拒水性WATER REPELLENCY。是指测定织物表面抗拒被水沾湿的性能，如泼水测试。1-5级，1级完全沾湿。
(2)抗菌性能：参照《GB/T 20944-2007纺织品抗菌性能的评价》，(Ⅰ-Ⅴ级，Ⅰ级抗菌度最优)。
(3)保暖性能：参照《GB/T 11048-1989纺织品保温性能试验方法》，(Ⅰ-Ⅴ级，Ⅰ级保暖性能最优)。
(4)防水性能：参照标准号为AATCC 35-2000，标准名称为防水测试：雨水实验。1-5级，1级完全沾湿。
各项测试结果参见下表：
Figure BDA0003534347240000071
从上表可看出，本发明制备的羽绒服用防水面料中的吸水自热物质对面料的保温性产生显著的影响，从实施例2与对比例1-4中可看出，吸水自热物质能在使用时有效的加强该面料的保温性能，同时从实施例2与对比例1中可看出，吸水自热物质中的电气石粉对使得吸水自热物质能有效的提供保温性，同时从实施例2以及对比例2中可看出，该防水面料中的甲壳素和抑菌粉体进一步提高该面料的抗菌性能，从实施例2与对比例3和对比例4中可看出，基体放入含氟防水处理剂、醋酸、渗透剂以及柔软剂组成的混合液内浸泡后，面料的防泼水及防水性能具有明显的提升。
尽管已经示出和描述了本发明的实施例，对于本领域的普通技术人员而言，可以理解在不脱离本发明的原理和精神的情况下可以对这些实施例进行多种变化、修改、替换和变型，本发明的范围由所附权利要求及其等同物限定。

Claims (9)

1.一种羽绒服用防水面料，其特征在于：所述防水面料从内至外依次为保暖层、透气防水层、吸水供热层以及基布层，所述保暖层、透气防水层、吸水供热层以及基布层之间通过热压复合制成；
其中，所述吸水供热层为将吸水自热物质和抗菌涂层物同时涂布至面料基体后对所述面料基体采用整理液整理后获得。
2.根据权利要求1所述的一种羽绒服用防水面料，其特征在于：所述整理液按重量份数包括：3-8份铵盐溶液、1-5份十二烷醇、1-3份氯化氢、1-3份氯代甲苯和1-3份二甲胺。
3.根据权利要求1所述的一种羽绒服用防水面料，其特征在于：所述吸水自热物质的制备方法为：取电气石粉、铝粉、碳酸钠以及石墨粉末混合均匀，从而得到吸水自热物质。
4.根据权利要求3所述的一种羽绒服用防水面料，其特征在于：所述吸水自热物质的制备原料按重量份数包括：2-8份电气石粉、1-4份铝粉、2-6份碳酸钠以及5-10份石墨烯粉末。
5.根据权利要求1所述的一种羽绒服用防水面料，其特征在于：所述面料基体由为涤纶或尼龙纱线编织而成；
所述抗菌涂层物的制备方法为：将聚氨酯树脂、甲壳素、抑菌粉体和交联剂进行混合搅拌均匀，搅拌后添加稀释剂调整粘度在17000～20000mPa·s，得抗菌涂层物。
6.根据权利要求5所述的一种羽绒服用防水面料，其特征在于：所述抗菌涂层中的稀释剂为丁酮、二甲基甲酰胺、甲苯其中至少一种。
7.根据权利要求1所述的一种羽绒服用防水面料，其特征在于：所述基布层的制备方法为：通过尼龙纱线或涤纶编织得到基体，将基体放入含氟防水处理剂、醋酸、渗透剂以及柔软剂组成的混合液内浸泡20-30min，然后经60-70℃焙烘1-2h得到。
8.根据权利要求1所述的一种羽绒服用防水面料，其特征在于：所述透气防水层为防水透气膜、聚氨酯薄膜或高分子防水透气材料加复合面料复合而成。
9.根据权利要求1-8任一项所述的一种羽绒服用防水面料的制备方法，其特征在于：
(1)将聚氨酯树脂、甲壳素、抑菌粉体和交联剂进行混合搅拌均匀，搅拌后添加稀释剂得到抗菌涂层物，将由电气石粉、铝粉、碳酸钠以及石墨粉末混合均匀得到吸水自热物质，同时将抗菌涂层物和吸水自热物质涂布面料基体两面，然后在90℃下烘干至完全干燥，得到吸水供热层；
(2)将铵盐溶液、十二烷醇、氯化氢、氯代甲苯和二甲胺混合得到整理液后，再通过整理液对所述吸水供热层进行清洗，清洗后将吸水供热层干燥；
(3)在所述吸水供热层的一面依次热压复合透气防水层和保暖层，在吸水供热层的另一面热压复合基布层，即得到所述的羽绒服用防水面料。
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