CN114425654A - A system and method for fabricating interdigital transducers for acoustic wave devices based on femtosecond laser processing masks - Google Patents

A system and method for fabricating interdigital transducers for acoustic wave devices based on femtosecond laser processing masks Download PDF

Info

Publication number
CN114425654A
CN114425654A CN202111633866.2A CN202111633866A CN114425654A CN 114425654 A CN114425654 A CN 114425654A CN 202111633866 A CN202111633866 A CN 202111633866A CN 114425654 A CN114425654 A CN 114425654A
Authority
CN
China
Prior art keywords
femtosecond laser
interdigital transducer
mask
acoustic wave
laser
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN202111633866.2A
Other languages
Chinese (zh)
Other versions
CN114425654B (en
Inventor
王勇
张磊
刘峰江
耿娇
孙潇雨
石理平
仇旻
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Westlake University
Original Assignee
Westlake University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Westlake University filed Critical Westlake University
Priority to CN202111633866.2A priority Critical patent/CN114425654B/en
Publication of CN114425654A publication Critical patent/CN114425654A/en
Application granted granted Critical
Publication of CN114425654B publication Critical patent/CN114425654B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K26/00Working by laser beam, e.g. welding, cutting or boring
    • B23K26/36Removing material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K26/00Working by laser beam, e.g. welding, cutting or boring
    • B23K26/02Positioning or observing the workpiece, e.g. with respect to the point of impact; Aligning, aiming or focusing the laser beam
    • B23K26/06Shaping the laser beam, e.g. by masks or multi-focusing
    • B23K26/064Shaping the laser beam, e.g. by masks or multi-focusing by means of optical elements, e.g. lenses, mirrors or prisms
    • B23K26/0643Shaping the laser beam, e.g. by masks or multi-focusing by means of optical elements, e.g. lenses, mirrors or prisms comprising mirrors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K26/00Working by laser beam, e.g. welding, cutting or boring
    • B23K26/02Positioning or observing the workpiece, e.g. with respect to the point of impact; Aligning, aiming or focusing the laser beam
    • B23K26/06Shaping the laser beam, e.g. by masks or multi-focusing
    • B23K26/064Shaping the laser beam, e.g. by masks or multi-focusing by means of optical elements, e.g. lenses, mirrors or prisms
    • B23K26/0648Shaping the laser beam, e.g. by masks or multi-focusing by means of optical elements, e.g. lenses, mirrors or prisms comprising lenses
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K26/00Working by laser beam, e.g. welding, cutting or boring
    • B23K26/08Devices involving relative movement between laser beam and workpiece
    • B23K26/082Scanning systems, i.e. devices involving movement of the laser beam relative to the laser head
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23KSOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K26/00Working by laser beam, e.g. welding, cutting or boring
    • B23K26/70Auxiliary operations or equipment
    • B23K26/702Auxiliary equipment
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50Manufacturing or production processes characterised by the final manufactured product

Landscapes

  • Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Engineering & Computer Science (AREA)
  • Plasma & Fusion (AREA)
  • Mechanical Engineering (AREA)
  • Laser Beam Processing (AREA)

Abstract

本发明公开了一种基于飞秒激光加工掩膜制备声波器件叉指换能器的系统及方法,该方法利用聚焦飞秒激光在金属薄膜上直写出叉指换能器掩膜,然后将掩膜置于压电衬底上蒸镀金属,最后移除掩膜获得叉指换能器结构。本发明相比于传统微电子光刻工艺,省去了匀胶、烘干、光刻、显影、剥离等过程,大大简化了叉指换能器的制备工艺,具有低成本、工艺简便、绿色环保、可重复使用、易于大规模生产等优点,在大波长、低频声波微流体器件制备方面具有广阔的应用前景。The invention discloses a system and method for preparing an interdigital transducer for acoustic wave devices based on a femtosecond laser processing mask. The method utilizes a focused femtosecond laser to directly write the interdigital transducer mask on a metal film, and then The mask is placed on the piezoelectric substrate to evaporate metal, and finally the mask is removed to obtain the interdigital transducer structure. Compared with the traditional microelectronic photolithography process, the invention saves the processes of glue uniformization, drying, photolithography, development, peeling, etc., greatly simplifies the preparation process of the interdigital transducer, and has the advantages of low cost, simple process and green Due to the advantages of environmental protection, reusability, and easy mass production, it has broad application prospects in the preparation of large-wavelength and low-frequency acoustic wave microfluidic devices.

Description

一种基于飞秒激光加工掩膜制备声波器件叉指换能器的系统 及方法A system and method for fabricating interdigital transducers for acoustic wave devices based on femtosecond laser processing masks

技术领域technical field

本发明涉及一种基于飞秒激光加工掩膜制备声波器件叉指换能器的系统及方法,属于声波器件制备技术领域。The invention relates to a system and method for preparing an interdigital transducer of an acoustic wave device based on a femtosecond laser processing mask, and belongs to the technical field of preparation of an acoustic wave device.

背景技术Background technique

声表面波是一种沿着固体表面传播的弹性波,最早由英国科学家瑞利在研究地震波过程中发现,所以这种波又被称为瑞利波。但由于受到当时科学水平的限制,最初的声表面波研究主要集中在地震波领域,并未得到实际应用。直到1965年美国科学家怀特和沃特尔默利用叉指换能器在压电衬底上通过施加射频信号直接激励出了声表面波,叉指换能器的发明奠定了声表面波应用的基础。随着技术的进步,更多的声表面波相继被发现,包括:水平剪切波、乐甫波、西沙瓦波等,这些波一般都需要叉指换能器激励产生。目前,声表面波技术已广泛应用在通信、电子、量子声学、传感和微流体等领域。SAW is an elastic wave that propagates along a solid surface. It was first discovered by British scientist Rayleigh in the process of studying seismic waves, so this kind of wave is also called Rayleigh wave. However, due to the limitation of the scientific level at that time, the initial surface acoustic wave research was mainly concentrated in the field of seismic waves, and it was not practically applied. Until 1965, American scientists White and Walthermer used the interdigital transducer to directly excite the surface acoustic wave by applying a radio frequency signal on the piezoelectric substrate. The invention of the interdigital transducer laid the foundation for the application of the surface acoustic wave. . With the advancement of technology, more surface acoustic waves have been discovered successively, including: horizontal shear wave, Love wave, Sishawar wave, etc. These waves generally need to be excited by interdigital transducers. At present, surface acoustic wave technology has been widely used in the fields of communication, electronics, quantum acoustics, sensing and microfluidics.

在声表面波技术的诸多应用中,近年来声表面波在传感和微流体方面的应用尤为瞩目,且一般基于声波模态中的瑞利模态,即瑞利波,而瑞利波的激励一般只需在压电衬底上做上一层金属化的叉指换能器(叉指电极对)即可。一般来说,对于声波传感,往往需要声波器件工作在高频状态,而高频往往对应更小的波长,即更小的叉指电极宽度,所以在器件制备上常采用高精度、高分辨率的微电子光刻工艺。而对于声波器件用作微流体用途,如实现微流体驱动、微粒/细胞分离、富集等功能,往往需要声波器件工作在低频状态,所以叉指电极尺寸较大(百微米级),无需高精度的微电子光刻工艺。Among the many applications of surface acoustic wave technology, the application of surface acoustic wave in sensing and microfluidics is particularly noticeable in recent years, and is generally based on the Rayleigh mode in the acoustic wave mode, that is, Rayleigh wave, and the Rayleigh wave The excitation generally only needs to make a layer of metallized interdigital transducer (interdigital electrode pair) on the piezoelectric substrate. Generally speaking, for acoustic wave sensing, acoustic wave devices are often required to work at high frequencies, and high frequencies often correspond to smaller wavelengths, that is, smaller interdigital electrode widths, so high-precision, high-resolution device preparation is often used. rate of microelectronic lithography. For the use of acoustic wave devices as microfluidics, such as the realization of microfluidic drive, particle/cell separation, enrichment and other functions, the acoustic wave device is often required to work in a low frequency state, so the size of the interdigital electrode is large (hundred microns), no need for high Precision microelectronic lithography process.

目前声波器件叉指换能器(叉指电极)的制备仍采用标准的微电子光刻工艺,这种工艺在制备过程中一般需要经过匀胶、烘干、光刻、显影、蒸镀、剥离等步骤,且需要在超净间内完成。对于匀胶过程,一般需要将压电衬底吸附于匀胶机上高速旋转,这对于一些柔性压电衬底(如压电薄膜生长于柔性衬底上),不仅难以吸附于匀胶机上,且高速旋转会破坏衬底的平整性,从而影响光刻加工的精度。同时,由于需要匀胶机进行匀胶,所以该工艺一般仅应用于平面加工。对于烘干过程,往往需要将压电衬底上的光刻胶加热到100℃以上,这对于一些温度稳定性差的压电衬底,如PVDF,会破坏压电衬底的压电特性。此外,微电子光刻工艺中的显影与剥离过程,会产生化学废液污染环境。因此亟需一种低成本、高效率、工艺简单、绿色环保的叉指换能器制备方法。At present, the preparation of the interdigital transducer (interdigital electrode) of the acoustic wave device still adopts the standard microelectronic lithography process. This process generally needs to go through the steps of uniform glue, drying, photolithography, development, evaporation, and peeling during the preparation process. and other steps, and need to be completed in a clean room. For the glue leveling process, it is generally necessary to adsorb the piezoelectric substrate on the glue machine and rotate at a high speed. For some flexible piezoelectric substrates (such as piezoelectric films grown on flexible substrates), it is not only difficult to adsorb on the glue machine, but also High-speed rotation will destroy the flatness of the substrate, thereby affecting the accuracy of lithography. At the same time, this process is generally only applied to plane processing due to the need for a glue gluer to do glue evenly. For the drying process, it is often necessary to heat the photoresist on the piezoelectric substrate to above 100°C, which will destroy the piezoelectric properties of the piezoelectric substrate for some piezoelectric substrates with poor temperature stability, such as PVDF. In addition, the development and stripping process in the microelectronic lithography process will produce chemical waste liquid to pollute the environment. Therefore, there is an urgent need for a low-cost, high-efficiency, simple process, and green and environmentally friendly preparation method for an interdigital transducer.

发明内容SUMMARY OF THE INVENTION

本发明提供了一种基于飞秒激光加工掩膜制备声波器件叉指换能器的系统及方法。飞秒激光加工技术具有加工精度高、热影响区小、加工速度快、操作简单、低成本的优点,尤其适用于大尺寸叉指换能器掩膜的快速制备。利用飞秒激光直写出叉指换能器掩膜,然后将掩膜图案转移到压电衬底上获得金属化的叉指电极结构为声波器件叉指换能器的快速制备提供了较好的解决途径。另外,由于掩膜的柔性,上述方法可实现曲面上金属图案化的制备,且在制备过程中省去了匀胶、烘干、光刻、显影、剥离等工艺,不会在制备过程中产生任何化学废液污染环境,解决了现有微电子光刻工艺在制备大尺寸叉指换能器过程中成本高、过程繁琐、操作工艺复杂的问题。The invention provides a system and method for preparing an interdigital transducer of an acoustic wave device based on a femtosecond laser processing mask. Femtosecond laser processing technology has the advantages of high processing precision, small heat-affected zone, fast processing speed, simple operation and low cost, and is especially suitable for the rapid preparation of large-sized IDT masks. The mask of the interdigital transducer is directly written by the femtosecond laser, and then the mask pattern is transferred to the piezoelectric substrate to obtain the metallized interdigital electrode structure, which provides a better method for the rapid preparation of the interdigital transducer for acoustic wave devices. solution. In addition, due to the flexibility of the mask, the above method can realize the preparation of metal patterning on the curved surface, and in the preparation process, processes such as gluing, drying, photolithography, development, peeling, etc. are omitted, and no production will occur during the preparation process. Any chemical waste liquid pollutes the environment, and solves the problems of high cost, cumbersome process and complicated operation process in the process of preparing large-size interdigital transducers in the existing microelectronic lithography process.

一种基于飞秒激光加工掩膜制备声波器件叉指换能器的方法,包括:以薄膜为加工对象,利用飞秒激光加工出叉指换能器掩膜;然后将叉指换能器掩膜置于压电衬底上,进行镀膜加工;镀膜完成后,移去叉指换能器掩膜,获得叉指换能器的叉指电极结构。A method for preparing an interdigital transducer for an acoustic wave device based on a femtosecond laser processing mask, comprising: taking a thin film as a processing object, using a femtosecond laser to process an interdigital transducer mask; The film is placed on the piezoelectric substrate, and the coating process is performed; after the coating is completed, the mask of the interdigital transducer is removed to obtain the interdigital electrode structure of the interdigital transducer.

作为优选,所述基于飞秒激光加工掩膜制备声波器件叉指换能器的方法,包括如下步骤:Preferably, the method for preparing an interdigital transducer for an acoustic wave device based on a femtosecond laser processing mask includes the following steps:

S1:搭建飞秒激光直写系统,利用该系统在薄膜(比如可以为金属薄膜)上直写出叉指换能器图案,获得叉指换能器掩膜;S1: Build a femtosecond laser direct writing system, and use this system to directly write the interdigital transducer pattern on the thin film (such as a metal thin film) to obtain the interdigital transducer mask;

S2:将叉指换能器掩膜固定于压电衬底上并置于金属镀膜系统中蒸镀金属;S2: fix the interdigital transducer mask on the piezoelectric substrate and place it in a metal coating system to evaporate metal;

S3:待金属蒸镀完成后,从压电衬底上移去叉指换能器掩膜,获得叉指换能器结构。S3: After the metal evaporation is completed, the interdigital transducer mask is removed from the piezoelectric substrate to obtain an interdigital transducer structure.

作为优选,所述薄膜为金属薄膜。Preferably, the thin film is a metal thin film.

作为进一步优选,所述金属薄膜为铝箔或钢箔,厚度为5~15μm。作为更进一步优选,所述金属薄膜为钢箔,厚度为10μm。As a further preference, the metal thin film is aluminum foil or steel foil, and the thickness is 5-15 μm. As a further preference, the metal thin film is a steel foil with a thickness of 10 μm.

加工时,利用定位件(比如胶带、夹具等)将薄膜固定于三维定位机构上,所述三维定位机构由一个实现水平方向(XY)移动的二维电动位移台和一个实现纵向(Z)方向移动的一维手动位移台组成,两者结合实现激光光束聚焦及叉指换能器图案化路径扫描。具体讲,通过调节一维手动位移台上金属薄膜到聚焦元件的距离使激光焦点处于(金属)薄膜顶面,利用位移台控制器(或者电脑)控制二维电动位移台依次完成图案化路径扫描,使飞秒激光在(金属)薄膜上直写出叉指换能器图案,获得掩膜;其中叉指换能器的叉指电极对应区域,薄膜材料在飞秒激光作用下去除。During processing, the film is fixed on the three-dimensional positioning mechanism by using positioning parts (such as tapes, clamps, etc.) It is composed of a moving one-dimensional manual stage. The combination of the two realizes the laser beam focusing and the patterned path scanning of the interdigital transducer. Specifically, by adjusting the distance from the metal film on the one-dimensional manual stage to the focusing element, the laser focus is placed on the top surface of the (metal) film, and the stage controller (or computer) is used to control the two-dimensional electric stage to scan the patterned path in turn. , the femtosecond laser directly writes the interdigital transducer pattern on the (metal) thin film to obtain a mask; in the area corresponding to the interdigital electrode of the interdigital transducer, the thin film material is removed under the action of the femtosecond laser.

作为优选,还包括用于控制二维电动位移台的位移台控制器。Preferably, a stage controller for controlling the two-dimensional electric stage is also included.

作为优选,飞秒激光直写工艺中,所用飞秒激光器的中心波长为900~1100μm,脉冲宽度为120~140fs,加工过程中,激光脉冲重复频率为1~3kHz,加工功率为60~100mW,与掩模相对移动速度为0.15~0.25mm/s(或者二维电动位移台的移动速度为0.15~0.25mm/s)。作为进一步优选,加工过程中所述飞秒激光器的中心波长为1030nm,脉冲重复频率为2kHz,脉冲宽度为130fs,加工功率为80mW,样品移动速度为0.2mm/s。Preferably, in the femtosecond laser direct writing process, the center wavelength of the femtosecond laser used is 900-1100 μm, the pulse width is 120-140 fs, the laser pulse repetition frequency is 1-3 kHz, and the processing power is 60-100 mW during the processing. The moving speed relative to the mask is 0.15 to 0.25 mm/s (or the moving speed of the two-dimensional electric stage is 0.15 to 0.25 mm/s). As a further preference, the center wavelength of the femtosecond laser is 1030 nm, the pulse repetition frequency is 2 kHz, the pulse width is 130 fs, the processing power is 80 mW, and the sample moving speed is 0.2 mm/s during the processing.

作为优选,采用蒸镀工艺进行镀膜,镀膜厚度为50~150nm。作为进一步优选,金属薄膜蒸镀厚度为100nm。Preferably, an evaporation process is used for coating, and the thickness of the coating is 50-150 nm. As a further preference, the thickness of the metal thin film vapor deposition is 100 nm.

作为优选,所述压电衬底可以选择现有的各种压电衬底材料,包括但不限于LiNbO3、LiTaO3、PZT、PVDF、AlN、ZnO等。Preferably, the piezoelectric substrate can be selected from various existing piezoelectric substrate materials, including but not limited to LiNbO 3 , LiTaO 3 , PZT, PVDF, AlN, ZnO, and the like.

作为优选,所述镀膜用材料选自金、银、铜、铝、钼等。Preferably, the coating material is selected from gold, silver, copper, aluminum, molybdenum and the like.

实际加工时,利用胶带将叉指换能器掩膜固定于压电衬底上,比如所述的叉指换能器掩膜可通过聚酰亚胺胶带固定于压电衬底上。将上述固定有掩膜的压电衬底置于高真空蒸发镀膜系统中蒸镀金属,金属蒸镀厚度由镀膜时间控制,蒸镀速度为

Figure BDA0003441896920000031
(进一步优选为
Figure BDA0003441896920000032
),镀膜厚度为50~100nm。待金属蒸镀完成后,撕去压电衬底和掩膜上的聚酰亚胺胶带,移除掩膜,获得叉指换能器的叉指电极结构。In actual processing, the interdigital transducer mask is fixed on the piezoelectric substrate with adhesive tape. For example, the interdigital transducer mask can be fixed on the piezoelectric substrate by polyimide adhesive tape. The above-mentioned piezoelectric substrate fixed with a mask is placed in a high-vacuum evaporation coating system to evaporate metal, and the thickness of metal evaporation is controlled by the coating time, and the evaporation speed is
Figure BDA0003441896920000031
(more preferably
Figure BDA0003441896920000032
), and the coating thickness is 50 to 100 nm. After the metal evaporation is completed, the polyimide tape on the piezoelectric substrate and the mask is torn off, and the mask is removed to obtain the interdigital electrode structure of the interdigital transducer.

作为优选,所述叉指换能器掩膜的最小波长为120μm,即叉指电极的宽度为30μm以上。Preferably, the minimum wavelength of the interdigital transducer mask is 120 μm, that is, the width of the interdigital electrode is more than 30 μm.

作为优选,所述叉指电极宽度为30~300微米,作为进一步优选,所述叉指电极宽度为30~150微米。Preferably, the width of the interdigital electrodes is 30-300 microns, and as a further preference, the width of the interdigital electrodes is 30-150 microns.

一种基于飞秒激光加工掩膜制备声波器件叉指换能器的系统,包括:A system for preparing an interdigital transducer of an acoustic wave device based on a femtosecond laser processing mask, comprising:

用于加工叉指换能器掩膜的飞秒激光直写装置;Femtosecond laser direct writing device for processing interdigital transducer masks;

对固定有叉指换能器掩膜的压电衬底进行镀膜加工的镀膜装置。A coating device for coating a piezoelectric substrate with an interdigital transducer mask fixed.

作为优选,所述飞秒激光直写装置包括:Preferably, the femtosecond laser direct writing device comprises:

提供飞秒激光的飞秒激光器;Femtosecond lasers that provide femtosecond lasers;

控制激光光束通断的快门元件;A shutter element that controls the on-off of the laser beam;

功率调节元件,对飞秒激光器出射激光进行功率调整;Power adjustment element, to adjust the power of the femtosecond laser output laser;

光路准直元件,对飞秒激光光束进行准直调整;The optical path collimation element is used to collimate and adjust the femtosecond laser beam;

扩束元件,对准直后的飞秒激光进行扩束;Beam expanding element to expand the beam of the collimated femtosecond laser;

光路导向调节装置,对扩束后的飞秒激光进行爬升及落下导向;Optical path guide adjustment device, which guides the expanded femtosecond laser to climb and fall;

聚焦元件,对导向后的光束进行聚焦,经聚焦元件聚焦后的激光垂直照射至待加工薄膜表面进行述飞秒激光直写加工。The focusing element focuses the guided beam, and the laser focused by the focusing element is irradiated vertically to the surface of the film to be processed to perform the femtosecond laser direct writing process.

作为优选,所述快门元件选自电动快门或机械快门,用于控制激光光束通断;Preferably, the shutter element is selected from an electric shutter or a mechanical shutter for controlling the on-off of the laser beam;

作为优选,所述功率调节元件选自中性密度衰减片或半波片与偏振片的组合,用于调节激光功率;Preferably, the power adjustment element is selected from a neutral density attenuation plate or a combination of a half-wave plate and a polarizer, for adjusting the laser power;

作为优选,所述光路准直元件为两个平行放置的全反射镜,调节光路高低及左右使其平行于光学平台;Preferably, the optical path collimating element is two parallel total reflection mirrors, and the height and the left and right of the optical path are adjusted to make it parallel to the optical platform;

作为优选,所述扩束元件由两个共焦放置的凸透镜组成,两个凸透镜的焦距分别为40~80mm和100~200mm;作为进一步优选,所述两个凸透镜的焦距分别为50mm和150mm。Preferably, the beam expanding element is composed of two confocally placed convex lenses, and the focal lengths of the two convex lenses are 40-80 mm and 100-200 mm respectively; as a further preference, the focal lengths of the two convex lenses are 50 mm and 150 mm, respectively.

作为优选,所述光路导向调节装置由三个45度放置的全反射镜组成,利用两个45度放置的全反射镜实现光路高度的纵向爬升及水平导向;利用另一个45度放置的全反射镜使光路方向改变90度,垂直入射到金属薄膜顶面。Preferably, the optical path guide adjustment device is composed of three total reflection mirrors placed at 45 degrees, and two total reflection mirrors placed at 45 degrees are used to achieve vertical climbing and horizontal guidance of the optical path height; another total reflection mirror placed at 45 degrees is used to achieve vertical climbing and horizontal guidance; The mirror changes the direction of the light path by 90 degrees, and is vertically incident on the top surface of the metal film.

作为优选,所述聚焦元件为聚焦透镜(凸透镜),焦距为10~30mm。作为进一步优选,聚焦透镜的焦距为20mm。Preferably, the focusing element is a focusing lens (convex lens) with a focal length of 10-30 mm. As a further preference, the focal length of the focusing lens is 20mm.

作为可以选择的方案,所述飞秒激光直写装置还包括如下元件中的一种或者多种组合:As an optional solution, the femtosecond laser direct writing device further includes one or more combinations of the following elements:

一个或多个光路导向元件;one or more light path guiding elements;

用于给样品打光的照明光源;Illumination source for illuminating the sample;

用于辅助调整样品位置、光学聚焦的CCD相机;CCD camera used to assist in adjusting sample position and optical focusing;

用于定位所述薄膜的三维定位机构;a three-dimensional positioning mechanism for positioning the film;

用于控制飞秒激光器出射激光参数或三维定位机构移动路径的计算机或控制器。A computer or controller for controlling the parameters of the femtosecond laser output laser or the movement path of the three-dimensional positioning mechanism.

作为具体的选择,所述照明光源为鹅颈灯,用于对金属薄膜打光,使CCD相机清晰观察激光聚焦及加工过程。As a specific choice, the illumination light source is a gooseneck lamp, which is used to illuminate the metal film, so that the CCD camera can clearly observe the laser focusing and processing process.

作为一种优选的方案,本发明用于制备叉指换能器掩膜的飞秒激光直写装置,包括:一台飞秒激光器,沿飞秒激光器出射激光方向依次设置有电动快门、半波片、偏振片、两个平行全反射镜(第一全反射镜、第二全反射镜)、扩束元件(即两个共焦放置的凸透镜)、光路导向调节装置、聚焦透镜及固定有金属薄膜的三维定位机构。利用三维定位机构中的一维手动位移台调节激光在金属薄膜上的聚焦,位移台控制器控制二维电动位移台依次沿指定路径移动,完成激光烧蚀切割,获得叉指换能器掩膜。激光聚焦及直写过程由CCD相机实时记录,CCD相机通过信号线与计算机相连;二维电动位移台通过信号线与位移台控制器相连;飞秒激光器通过信号线与计算机相连,由计算机控制。As a preferred solution, the femtosecond laser direct writing device used for preparing the interdigital transducer mask of the present invention includes: a femtosecond laser, and an electric shutter, a half-wave film, polarizer, two parallel total reflection mirrors (first total reflection mirror, second total reflection mirror), beam expander (ie, two confocally placed convex lenses), optical path guide adjustment device, focusing lens and fixed metal The three-dimensional positioning mechanism of the film. The one-dimensional manual stage in the three-dimensional positioning mechanism is used to adjust the focus of the laser on the metal film, and the stage controller controls the two-dimensional electric stage to move along the specified path in turn to complete the laser ablation and cutting, and obtain the interdigital transducer mask. . The laser focusing and direct writing process are recorded in real time by a CCD camera, which is connected to the computer through a signal line; the two-dimensional motorized stage is connected to the stage controller through a signal line; the femtosecond laser is connected to the computer through a signal line and controlled by the computer.

实际工作时,飞秒激光经快门元件、功率调节、光束准直、扩束、爬升、落下、聚焦,形成的聚焦光斑垂直照射至金属薄膜上,金属薄膜固定在安装于二维电动位移台上的一维手动位移台上,位移台控制器控制三维定位机构中的二维电动位移台依次沿指定路径移动,直写出叉指换能器掩膜。In actual work, the femtosecond laser passes through the shutter element, power adjustment, beam collimation, beam expansion, climbing, falling, and focusing, and the formed focused spot is irradiated vertically to the metal film, which is fixed on the two-dimensional electric displacement stage. On the one-dimensional manual displacement stage, the displacement stage controller controls the two-dimensional electric displacement stage in the three-dimensional positioning mechanism to move along the specified path in turn, and directly write the interdigital transducer mask.

初次加工时,所述飞秒激光器的出射激光能量通过调节激光器的脉冲重复频率实现初次调整,使其高于金属薄膜的烧蚀阈值。利用功率调节元件(半波片与偏振片组合)进一步调节激光功率。当然,当实验条件稳定后,可以省去调节步骤和调节元件,直接采用最后的工作参数进行自动化加工。也就是说,作为一种优化方案,功率调节元件可以被省略。During initial processing, the emitted laser energy of the femtosecond laser is initially adjusted by adjusting the pulse repetition frequency of the laser so that it is higher than the ablation threshold of the metal thin film. The laser power is further adjusted using a power adjustment element (a combination of a half-wave plate and a polarizer). Of course, when the experimental conditions are stable, the adjustment steps and adjustment elements can be omitted, and the final working parameters can be directly used for automatic processing. That is, as an optimized solution, the power adjustment element can be omitted.

本发明提出的一种基于飞秒激光加工掩膜制备声波器件叉指换能器的系统及方法,其优点是:A system and method for preparing an interdigital transducer of an acoustic wave device based on a femtosecond laser processing mask proposed by the present invention has the following advantages:

(1)本发明利用聚焦飞秒激光在金属薄膜上直写出叉指换能器图案,可实现叉指换能器掩膜的低成本、快速、批量、高精度制备。(1) The present invention utilizes the focused femtosecond laser to directly write the interdigital transducer pattern on the metal film, which can realize the low-cost, rapid, batch, and high-precision preparation of the interdigital transducer mask.

(2)本发明相比于传统微电子光刻工艺省去了匀胶、烘干、光刻、显影、剥离等工艺,工艺简单、灵活性高,最小加工波长达到了120μm,尤其适用于低频声波微流体器件的低成本、快速制备。同时避免了使用高温烘干过程,适用于热敏性压电衬底上金属化图案的制备,且避免产生化学废液污染环境。(2) Compared with the traditional microelectronic lithography process, the present invention omits processes such as glue uniformization, drying, photolithography, development, and stripping, the process is simple, the flexibility is high, and the minimum processing wavelength reaches 120 μm, which is especially suitable for low frequency. Low-cost and rapid fabrication of sonic microfluidic devices. At the same time, the high-temperature drying process is avoided, which is suitable for the preparation of metallized patterns on the heat-sensitive piezoelectric substrate, and avoids the generation of chemical waste liquid to pollute the environment.

(3)本发明所述掩膜具有较高的柔性,可实现柔性或曲面上金属化图案的制备。(3) The mask of the present invention has high flexibility and can realize the preparation of metallized patterns on flexible or curved surfaces.

附图说明Description of drawings

图1为本发明提出的飞秒激光加工叉指换能器掩膜装置的结构示意图,其中:1是飞秒激光器,2是电动快门,3是半波片,4是偏振片,5是全反射镜,6是全反射镜,7是凸透镜,8是凸透镜,9是全反射镜,10是全反射镜,11是全反射镜,12聚焦透镜,13是金属薄膜,14是一维手动位移台,15是二维电动位移台,16是位移台控制器,17是鹅颈灯,18是CCD相机,19是计算机。1 is a schematic structural diagram of a femtosecond laser processing interdigital transducer mask device proposed by the present invention, wherein: 1 is a femtosecond laser, 2 is an electric shutter, 3 is a half-wave plate, 4 is a polarizer, and 5 is a full Mirror, 6 is total reflection mirror, 7 is convex lens, 8 is convex lens, 9 is total reflection mirror, 10 is total reflection mirror, 11 is total reflection mirror, 12 is focusing lens, 13 is metal film, 14 is one-dimensional manual displacement stage, 15 is a two-dimensional motorized stage, 16 is a stage controller, 17 is a gooseneck lamp, 18 is a CCD camera, and 19 is a computer.

图2为本发明加工出的不同波长叉指换能器掩膜实物图,其中(a)波长为400μm;(b)波长为300μm;(c)波长为200μm。FIG. 2 is a physical diagram of the interdigital transducer masks with different wavelengths processed by the present invention, wherein (a) the wavelength is 400 μm; (b) the wavelength is 300 μm; (c) the wavelength is 200 μm.

图3为本发明制备声波器件叉指换能器流程图。Fig. 3 is the flow chart of preparing the interdigital transducer of the acoustic wave device according to the present invention.

图4为本发明在不同压电衬底上制备出的声波器件实物图,其中(a)LiNbO3衬底,器件波长400μm;(b)LiNbO3衬底,器件波长300μm;(c)PVDF衬底(500μm厚),器件波长300μm;(d)PVDF衬底(200μm厚),器件波长300μm。Figure 4 is a physical diagram of acoustic wave devices prepared on different piezoelectric substrates according to the present invention, wherein (a) LiNbO 3 substrate, the device wavelength is 400 μm; (b) LiNbO 3 substrate, the device wavelength is 300 μm; (c) PVDF substrate Bottom (500 μm thick), device wavelength 300 μm; (d) PVDF substrate (200 μm thick), device wavelength 300 μm.

图5为本发明在不同压电衬底上制备出的声波器件(波长为400μm)的信号传输与反射光谱,其中(a)LiNbO3衬底;(b)PVDF衬底。Figure 5 shows the signal transmission and reflection spectra of acoustic wave devices (wavelength 400 μm) prepared on different piezoelectric substrates of the present invention, wherein (a) LiNbO 3 substrate; (b) PVDF substrate.

具体实施方式Detailed ways

为了使本发明的目的、技术方案及优点更加清楚明白,下面通过具体实施方式结合附图对本发明作进一步详细说明。应当理解,此处所描述的具体实施例仅仅用以解释本发明,并不用于限定本发明。In order to make the objectives, technical solutions and advantages of the present invention clearer, the present invention will be further described in detail below through specific embodiments in conjunction with the accompanying drawings. It should be understood that the specific embodiments described herein are only used to explain the present invention, but not to limit the present invention.

本发明提出了一种基于飞秒激光加工掩膜制备声波器件叉指换能器的系统及方法。在加工方式上,利用聚焦飞秒激光在金属薄膜上直写出叉指换能器掩膜,然后将掩膜置于压电衬底上蒸镀金属,获得叉指电极结构;在制备工艺上,相比于传统微电子光刻工艺,本发明省去了匀胶、烘干、光刻、显影、剥离等工艺,大大简化了制备流程,且制备的掩膜成本低、精度高、可实现重复使用。The invention provides a system and method for preparing an interdigital transducer of an acoustic wave device based on a femtosecond laser processing mask. In the processing method, the interdigital transducer mask is directly written on the metal film by the focused femtosecond laser, and then the mask is placed on the piezoelectric substrate to evaporate metal to obtain the interdigital electrode structure; in the preparation process , Compared with the traditional microelectronic lithography process, the present invention omits the processes of uniform glue, drying, photolithography, development, stripping, etc., which greatly simplifies the preparation process, and the prepared mask has low cost, high precision, and can be realized reuse.

本发明提出的一种基于飞秒激光加工掩膜制备声波器件叉指换能器的系统及方法,其飞秒激光直写装置光路结构如图1所示,包括:飞秒激光器1、电动快门2、半波片3、偏振片4、全反射镜5、全反射镜6、凸透镜7、凸透镜8、全反射镜9、全反射镜10、全反射镜11、聚焦透镜12、金属薄膜13、一维手动位移台14、二维电动位移台15、位移台控制器16、鹅颈灯17、CCD相机18和计算机19。A system and method for preparing an interdigital transducer of an acoustic wave device based on a femtosecond laser processing mask proposed by the present invention, the optical path structure of the femtosecond laser direct writing device is shown in Figure 1, including: a femtosecond laser 1, an electric shutter 2. Half-wave plate 3, polarizer 4, total reflection mirror 5, total reflection mirror 6, convex lens 7, convex lens 8, total reflection mirror 9, total reflection mirror 10, total reflection mirror 11, focusing lens 12, metal film 13, One-dimensional manual stage 14 , two-dimensional electric stage 15 , stage controller 16 , gooseneck lamp 17 , CCD camera 18 and computer 19 .

所述的电动快门2主要用于控制激光光束通断,设置的位置可根据实际需要进行调整。The electric shutter 2 is mainly used to control the on-off of the laser beam, and the setting position can be adjusted according to actual needs.

所述的光学半波片3和偏振片4组合使用,主要用于调整激光功率,也可以替换为其他功率调节元件,如中性密度衰减片。The optical half-wave plate 3 and the polarizer 4 are used in combination, mainly for adjusting the laser power, and can also be replaced with other power adjusting elements, such as a neutral density attenuation plate.

所述的全反射镜5和全反射镜6平行放置,主要调节激光光路俯仰及左右,起到光路准直作用,全反射镜5和全反射镜6可根据实际需要进行增减,设置的位置可在激光扩束前根据实际需要进行调整。The total reflection mirror 5 and the total reflection mirror 6 are placed in parallel, mainly adjust the pitch and left and right of the laser optical path, and play the role of optical path collimation. The total reflection mirror 5 and the total reflection mirror 6 can be increased or decreased according to actual needs. It can be adjusted according to actual needs before laser beam expansion.

所述的凸透镜7和凸透镜8共焦放置,主要起到光束扩束作用。The convex lens 7 and the convex lens 8 are placed confocally and mainly play the role of beam expansion.

所述的全反射镜9、全反射镜10、全反射镜11主要起到光路高度提升、落下等导向作用,全反射镜9将激光光路方向改变90度,由水平传播变为竖直爬升,全反射镜10将垂直爬升的激光光路方向改变90度变为水平传播,全反射镜11将水平传播的激光光路方向改变90度,竖直入射到聚焦透镜12中央。The total reflection mirror 9, the total reflection mirror 10, and the total reflection mirror 11 mainly play a guiding role in raising and falling of the optical path. The total reflection mirror 9 changes the direction of the laser light path by 90 degrees, from horizontal propagation to vertical climbing, The total reflection mirror 10 changes the direction of the vertically climbing laser light path by 90 degrees to horizontally propagate, and the total reflection mirror 11 changes the direction of the horizontally propagated laser light path by 90 degrees, and vertically enters the center of the focusing lens 12 .

所述的聚焦透镜12主要起到光束聚焦作用,聚焦后的激光垂直入射到待加工金属薄膜13表面。The focusing lens 12 mainly plays the role of focusing the light beam, and the focused laser is vertically incident on the surface of the metal film 13 to be processed.

所述的金属薄膜13通过胶带固定于三维定位机构上,所述的三维定位机构由一维手动位移台14和二维电动位移台15组成,一维手动位移台14安装于二维电动位移台15上,二维电动位移台15通过信号线与位移台控制器16相连,由位移台控制器16控制(当然在软件兼容和功能允许的情况下,也可以由计算机19统一控制)。一维手动位移台14主要用于调整聚焦透镜12到待加工金属薄膜13的距离,使激光焦点处于待加工金属薄膜13顶面,二维电动位移台15主要用于加工过程中实现待加工金属薄膜13的水平方向移动,形成图案化的切割路径。The metal film 13 is fixed on the three-dimensional positioning mechanism by tape, and the three-dimensional positioning mechanism is composed of a one-dimensional manual displacement stage 14 and a two-dimensional electric displacement stage 15, and the one-dimensional manual displacement stage 14 is installed on the two-dimensional electric displacement stage. 15, the two-dimensional electric stage 15 is connected to the stage controller 16 through a signal line, and is controlled by the stage controller 16 (of course, if the software is compatible and the function allows, it can also be controlled by the computer 19 uniformly). The one-dimensional manual displacement stage 14 is mainly used to adjust the distance between the focusing lens 12 and the metal film 13 to be processed, so that the laser focus is on the top surface of the metal film 13 to be processed, and the two-dimensional electric displacement stage 15 is mainly used to realize the metal film to be processed during the processing. The horizontal direction of the film 13 moves to form a patterned cutting path.

所述的鹅颈灯17用于给金属薄膜13照明,以便在CCD相机18下观察聚焦透镜12对金属薄膜13的聚焦及对整个加工过程进行实时监测。The gooseneck lamp 17 is used for illuminating the metal film 13 , so as to observe the focusing of the metal film 13 by the focusing lens 12 under the CCD camera 18 and monitor the whole process in real time.

所述的CCD相机18通过信号线与计算机19相连,由计算机19屏幕实时成像,所述的飞秒激光器1通过信号线与计算机19相连,由计算机19控制。The CCD camera 18 is connected to the computer 19 through a signal line, and is imaged in real time by the computer 19 screen. The femtosecond laser 1 is connected to the computer 19 through a signal line, and is controlled by the computer 19 .

加工前,首先将相关光学元件按照图1顺序依次置入光学平台,搭建飞秒激光直写光路。加工过程中,飞秒激光器1产生飞秒激光,飞秒激光先经电动快门2,再经半波片3和偏振片4调节至适当功率后,入射到全反射镜5上,经全反射镜5和全反射镜6对激光光路准直后,反射激光垂直入射到凸透镜7和凸透镜8组成的扩束系统,经扩束后,飞秒激光先经全反射镜9垂直爬升,再经全反射镜10水平传播,最后经全反射镜11垂直向下入射到聚焦透镜12上,调节一维手动位移台14上金属薄膜13到聚焦透镜12的距离,使激光焦点处于金属薄膜13顶面,位移台控制器16控制二维电动位移台15上的金属薄膜13依次沿指定路径移动完成扫描切割,获得叉指换能器掩膜。随后,经过镀膜、移除掩模即可得到叉指换能器的叉指电极结构。Before processing, first place the relevant optical components into the optical platform in the order shown in Figure 1 to build a femtosecond laser direct writing optical path. During the processing, the femtosecond laser 1 generates a femtosecond laser. The femtosecond laser first passes through the electric shutter 2, and then is adjusted to an appropriate power by the half-wave plate 3 and the polarizer 4, and then is incident on the total reflection mirror 5, and then passes through the total reflection mirror. 5 and the total reflection mirror 6 are aligned with the laser light path, and the reflected laser is vertically incident on the beam expansion system composed of the convex lens 7 and the convex lens 8. After the beam expansion, the femtosecond laser first climbs vertically through the total reflection mirror 9, and then passes through the total reflection. The mirror 10 propagates horizontally, and finally enters the focusing lens 12 vertically downward through the total reflection mirror 11, and adjusts the distance from the metal film 13 on the one-dimensional manual displacement stage 14 to the focusing lens 12, so that the laser focus is on the top surface of the metal film 13, and the displacement is The stage controller 16 controls the metal thin film 13 on the two-dimensional electric displacement stage 15 to move along the specified path in sequence to complete the scanning and cutting, and obtain the interdigital transducer mask. Then, after coating and removing the mask, the interdigital electrode structure of the interdigital transducer can be obtained.

实施例1:飞秒激光直写加工叉指换能器掩膜。Example 1: Femtosecond laser direct writing processing of an interdigital transducer mask.

本发明实施例中,所用飞秒激光器为Amplitude公司的掺镱飞秒光纤激光器(Tangerine HP),飞秒激光中心波长1030nm,脉冲宽度130fs,最高重复频率35MHz,单脉冲能量200μJ,光场分布为高斯分布;所用金属薄膜为钢箔,厚度为10μm,大小为5cm×5cm,作为一种替代的方案,钢箔亦可替换成铝箔或其他金属薄膜。In the embodiment of the present invention, the femtosecond laser used is a ytterbium-doped femtosecond fiber laser (Tangerine HP) of Amplitude Company, the center wavelength of the femtosecond laser is 1030 nm, the pulse width is 130 fs, the maximum repetition frequency is 35 MHz, the single pulse energy is 200 μJ, and the light field distribution is Gaussian distribution; the metal film used is a steel foil with a thickness of 10 μm and a size of 5cm×5cm. As an alternative, the steel foil can also be replaced with aluminum foil or other metal films.

本实施例的具体加工步骤如下:The concrete processing steps of this embodiment are as follows:

S1:计算机19上完成叉指换能器掩膜团案化移动路径编程,并通过SD内存卡将路径程序写入二维位移台控制器16;S1: The computer 19 completes the group-based movement path programming of the interdigital transducer mask, and writes the path program into the two-dimensional stage controller 16 through the SD memory card;

S2:将钢箔13通过胶带固定于一维手动位移台14和二维电动位移台15组成的三维定位机构上;S2: fix the steel foil 13 on the three-dimensional positioning mechanism composed of the one-dimensional manual displacement stage 14 and the two-dimensional electric displacement stage 15 by tape;

S3:计算机19控制飞秒激光器1发出脉冲激光,将各光学元件按照图1顺序依次置入光学平台,调试光路使飞秒激光经电动快门2、半波片3、偏振片4、全反射镜5、全反射镜6、凸透镜7、凸透镜8、全反射镜9、全反射镜10、全反射镜11和聚焦透镜12后垂直入射到钢箔13表面,设定飞秒激光的脉冲重复重复频率为2kHz,旋转偏振片使激光平均功率为80mW。S3: The computer 19 controls the femtosecond laser 1 to emit pulsed laser light, and the optical elements are placed in the optical platform in the order shown in Figure 1, and the optical path is adjusted so that the femtosecond laser passes through the electric shutter 2, the half-wave plate 3, the polarizer 4, and the total reflection mirror. 5. The total reflection mirror 6, the convex lens 7, the convex lens 8, the total reflection mirror 9, the total reflection mirror 10, the total reflection mirror 11 and the focusing lens 12 are vertically incident on the surface of the steel foil 13, and the pulse repetition frequency of the femtosecond laser is set is 2kHz, and the polarizer is rotated so that the average laser power is 80mW.

S4:打开鹅颈灯17给钢箔13照明,在CCD相机18下调节一维手动位移台14的纵向进给,使飞秒激光经聚焦透镜12聚焦后的焦点处于钢箔13顶面。S4 : Turn on the gooseneck lamp 17 to illuminate the steel foil 13 , adjust the longitudinal feed of the one-dimensional manual displacement stage 14 under the CCD camera 18 , so that the femtosecond laser is focused by the focusing lens 12 on the top surface of the steel foil 13 .

S5:设定二维电动位移台15的进给速度为0.2mm/s,位移台控制器16依次加载步骤S1所述程序,使二维电动位移台15带动其上的钢箔13依次沿指定路径移动完成扫描切割,获得叉指换能器掩膜。S5: Set the feeding speed of the two-dimensional electric stage 15 to 0.2 mm/s, and the stage controller 16 sequentially loads the program described in step S1, so that the two-dimensional electric stage 15 drives the steel foil 13 on it in turn along the specified The path movement completes the scan cut and obtains the interdigital transducer mask.

图2为本发明加工出的不同波长叉指换能器掩膜实物图,其中(a)波长为400μm,叉指电极对数为15对,声孔经为6000μm;(b)波长为300μm,指电极对数为15对,声孔径为5000μm;(c)波长为200μm,指电极对数为5对,声孔径为3000μm。Fig. 2 is the actual picture of the interdigital transducer masks with different wavelengths processed by the present invention, wherein (a) the wavelength is 400 μm, the number of pairs of interdigital electrodes is 15, and the acoustic aperture is 6000 μm; (b) the wavelength is 300 μm, The number of electrode pairs is 15, and the acoustic aperture is 5000 μm; (c) The wavelength is 200 μm, the number of electrode pairs is 5, and the acoustic aperture is 3000 μm.

实施例2:基于飞秒激光加工掩膜制备声波器件叉指换能器。Example 2: Fabrication of an interdigital transducer for acoustic wave devices based on a femtosecond laser processing mask.

本发明实施例中,所用金属镀膜设备为爱发科真空技术(苏州)有限公司的高真空蒸发镀膜系统,镀膜过程中,腔体真空度为5×10-4Pa,蒸镀速度为

Figure BDA0003441896920000091
金属蒸镀厚度为100nm。作为一种替代的方案,金属蒸镀亦可通过真空溅射镀膜设备实现。In the embodiment of the present invention, the metal coating equipment used is the high-vacuum evaporation coating system of Aifake Vacuum Technology (Suzhou) Co., Ltd. During the coating process, the vacuum degree of the cavity is 5×10 -4 Pa, and the evaporation rate is
Figure BDA0003441896920000091
The metal vapor deposition thickness was 100 nm. As an alternative solution, metal evaporation can also be achieved by vacuum sputtering coating equipment.

本实施例的具体加工步骤如下:The concrete processing steps of this embodiment are as follows:

S1:将叉指换能器掩膜通过聚酰亚胺胶带固定于压电衬底上;S1: fix the interdigital transducer mask on the piezoelectric substrate through polyimide tape;

S2:将固定有叉指换能器掩膜的压电衬底置于高真空蒸发镀膜系统中蒸镀金膜,设置金属蒸镀速度

Figure BDA0003441896920000101
蒸镀时间为33min,即镀膜厚度为100nm。S2: Place the piezoelectric substrate fixed with the interdigital transducer mask in a high-vacuum evaporation coating system to evaporate gold film, and set the metal evaporation speed
Figure BDA0003441896920000101
The evaporation time is 33min, that is, the coating thickness is 100nm.

S3:蒸镀完成后,移除掩膜获得声波器件叉指换能器的叉指电极结构。S3: After the evaporation is completed, the mask is removed to obtain the interdigital electrode structure of the interdigital transducer of the acoustic wave device.

图3为本发明制备声波器件叉指换能器流程图,首先利用聚焦飞秒激光直写出掩膜,然后将掩膜固定于压电衬底上,接着将压电衬底和掩膜置于高真空蒸发镀膜系统中蒸镀金属,最后移除掩膜获得叉指换能器结构。Fig. 3 is the flow chart of preparing the interdigital transducer of acoustic wave device according to the present invention. First, the mask is directly written by the focused femtosecond laser, then the mask is fixed on the piezoelectric substrate, and then the piezoelectric substrate and the mask are placed Metal is evaporated in a high vacuum evaporation coating system, and finally the mask is removed to obtain an interdigital transducer structure.

图4为本发明在不同压电衬底上制备出的声波器件实物图,其中(a)LiNbO3衬底,叉指电极对数为15对,波长400μm,声孔径为6000μm;(b)LiNbO3衬底,叉指电极对数为15对,波长300μm,声孔径为5000μm;(c)PVDF衬底(500μm厚),叉指电极对数为15对,波长300μm,声孔径为5000μm;(d)PVDF衬底(200μm厚),叉指电极对数为15对,波长300μm,声孔径为5000μm。Figure 4 is a physical diagram of acoustic wave devices prepared on different piezoelectric substrates according to the present invention, wherein (a) LiNbO 3 substrate, the number of pairs of interdigital electrodes is 15, the wavelength is 400 μm, and the acoustic aperture is 6000 μm; (b) LiNbO 3 Substrate, the number of pairs of interdigital electrodes is 15, the wavelength is 300 μm, and the acoustic aperture is 5000 μm; (c) PVDF substrate (500 μm thick), the number of pairs of interdigital electrodes is 15, the wavelength is 300 μm, and the acoustic aperture is 5000 μm; ( d) PVDF substrate (200 μm thick) with 15 pairs of interdigital electrodes, a wavelength of 300 μm, and an acoustic aperture of 5000 μm.

图5为本发明在不同压电衬底上制备出的声波器件(波长为400μm)的信号传输与反射光谱,其中(a)LiNbO3衬底,声波激励出的模态为瑞利(R0)模态;(b)PVDF衬底,声波激励出的模态为零阶反对称(A0)模态。Figure 5 is the signal transmission and reflection spectra of acoustic wave devices (wavelength is 400 μm) prepared on different piezoelectric substrates according to the present invention, wherein (a) LiNbO 3 substrate, the mode excited by the acoustic wave is Rayleigh (R0) mode; (b) PVDF substrate, the mode excited by the acoustic wave is the zero-order antisymmetric (A0) mode.

以上内容是结合具体的实施方式对本发明所作的进一步详细说明,不能认定本发明的具体实施只局限于这些说明。对于本发明所属技术领域的普通技术人员来说,在不脱离本发明构思的前提下,还可以做出若干简单推演或替换,都应当视为属于本发明的保护范围。The above content is a further detailed description of the present invention in conjunction with specific embodiments, and it cannot be considered that the specific implementation of the present invention is limited to these descriptions. For those of ordinary skill in the technical field of the present invention, without departing from the concept of the present invention, some simple deductions or substitutions can be made, which should be regarded as belonging to the protection scope of the present invention.

Claims (9)

1. A method for manufacturing an acoustic wave device interdigital transducer based on a femtosecond laser processing mask is characterized by comprising the following steps: processing an interdigital transducer mask by using femtosecond laser by taking the film as a processing object; then, placing the mask on a piezoelectric substrate, and performing film coating processing; and after the film coating is finished, removing the interdigital transducer mask to obtain the interdigital electrode structure of the interdigital transducer.
2. The method for fabricating an acoustic wave device interdigital transducer based on a femtosecond laser process mask according to claim 1, wherein the thin film is a metal thin film.
3. The method for manufacturing an acoustic wave device interdigital transducer based on a femtosecond laser processing mask according to claim 2, wherein the metal thin film is an aluminum foil or a steel foil and has a thickness of 5-15 μm.
4. The method for fabricating an acoustic wave device interdigital transducer based on a femtosecond laser process mask according to claim 1, wherein in the femtosecond laser direct writing process, the center wavelength of the femtosecond laser used is 900 to 1100 μm, the pulse width is 120 to 140fs, the laser pulse repetition frequency is 1 to 3kHz, the process power is 60 to 100mW, and the relative movement speed with the mask is 0.15 to 0.25 mm/s.
5. The method for fabricating an acoustic wave device interdigital transducer based on a femtosecond laser process mask according to claim 1, wherein the interdigital electrode width of the interdigital transducer is 30 μm or more.
6. The method for manufacturing an acoustic wave device interdigital transducer based on a femtosecond laser processing mask, according to claim 1, wherein the metal coating is performed by an evaporation process, and the coating thickness is 50-150 nm.
7. A system for fabricating acoustic wave device interdigital transducers based on a femtosecond laser processed mask, comprising:
the femtosecond laser direct writing device is used for processing the interdigital transducer mask;
and a coating device for coating the piezoelectric substrate fixed with the interdigital transducer mask.
8. The system for fabricating an acoustic wave device interdigital transducer based on a femtosecond laser process mask according to claim 7, wherein the femtosecond laser direct writing apparatus comprises:
a femtosecond laser providing femtosecond laser;
the shutter element is used for controlling the on-off of the laser emitted by the femtosecond laser;
the power adjusting element is used for adjusting the power of the laser emitted by the femtosecond laser;
the light path collimation element is used for collimating and adjusting the femtosecond laser;
the beam expanding element is used for expanding the collimated femtosecond laser;
the light path guiding and adjusting device is used for guiding the expanded femtosecond laser to climb and fall;
and the focusing element is used for focusing the guided light beam and vertically irradiating the light beam to the surface of the film to be processed to perform the femtosecond laser direct writing processing.
9. The system for fabricating an acoustic wave device interdigital transducer based on a femtosecond laser process mask according to claim 7, wherein the femtosecond laser direct writing apparatus further comprises one or more combinations of the following elements:
one or more optical path directing elements;
an illumination light source;
a CCD camera for assisting in adjusting the position of the sample and optically focusing;
a three-dimensional positioning mechanism for positioning the film;
and the computer or the controller is used for controlling the parameters of the emergent laser of the femtosecond laser and the moving path of the three-dimensional positioning mechanism.
CN202111633866.2A 2021-12-29 2021-12-29 System and method for preparing interdigital transducer of acoustic wave device based on femtosecond laser processing mask Active CN114425654B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111633866.2A CN114425654B (en) 2021-12-29 2021-12-29 System and method for preparing interdigital transducer of acoustic wave device based on femtosecond laser processing mask

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111633866.2A CN114425654B (en) 2021-12-29 2021-12-29 System and method for preparing interdigital transducer of acoustic wave device based on femtosecond laser processing mask

Publications (2)

Publication Number Publication Date
CN114425654A true CN114425654A (en) 2022-05-03
CN114425654B CN114425654B (en) 2024-07-05

Family

ID=81311019

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202111633866.2A Active CN114425654B (en) 2021-12-29 2021-12-29 System and method for preparing interdigital transducer of acoustic wave device based on femtosecond laser processing mask

Country Status (1)

Country Link
CN (1) CN114425654B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115246626A (en) * 2022-07-04 2022-10-28 南京理工大学 Method for preparing wave modulation flexible film based on femtosecond laser processing
CN115401314A (en) * 2022-09-22 2022-11-29 杭州奥创光子技术有限公司 A kind of processing equipment and processing method of metal mask plate

Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101299911A (en) * 2007-05-02 2008-11-05 安迪克连接科技公司 Method for making a multilayered circuitized substrate
CN107717216A (en) * 2017-11-06 2018-02-23 武汉光谷航天三江激光产业技术研究院有限公司 A kind of femtosecond laser parallel micromachining method and device
JP2018074430A (en) * 2016-10-31 2018-05-10 太陽誘電株式会社 Method for manufacturing acoustic wave device and method for manufacturing wafer
CN111085773A (en) * 2020-01-14 2020-05-01 华侨大学 Laser drilling device and method for metal film-assisted brittle material
CN212217441U (en) * 2020-01-14 2020-12-25 华侨大学 Laser drilling device for metal film-assisted brittle materials
CN112643206A (en) * 2020-12-29 2021-04-13 中国科学院长春光学精密机械与物理研究所 Method for inducing super-regular nano-grating by femtosecond laser based on assistance of chromium film
CN112872597A (en) * 2021-01-21 2021-06-01 北京理工大学 Method for preparing super-hydrophobic surface by combining femtosecond laser direct writing and electroplating method
CN112975142A (en) * 2021-03-02 2021-06-18 北京航空航天大学杭州创新研究院 Film material patterning processing method based on femtosecond laser controllable etching
CN113092439A (en) * 2021-03-31 2021-07-09 吉林大学重庆研究院 Flexible ultra-smooth SERS substrate prepared by femtosecond laser processing technology, processing method and application
CN113084363A (en) * 2021-03-24 2021-07-09 西湖大学 Device and method for femtosecond laser processing photoresponse liquid crystal elastomer comb teeth
CN113523596A (en) * 2021-07-08 2021-10-22 西湖大学 Device and method for femtosecond laser processing patterned photodeformable cross-linked liquid crystal polymer structure

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101299911A (en) * 2007-05-02 2008-11-05 安迪克连接科技公司 Method for making a multilayered circuitized substrate
JP2018074430A (en) * 2016-10-31 2018-05-10 太陽誘電株式会社 Method for manufacturing acoustic wave device and method for manufacturing wafer
CN107717216A (en) * 2017-11-06 2018-02-23 武汉光谷航天三江激光产业技术研究院有限公司 A kind of femtosecond laser parallel micromachining method and device
CN111085773A (en) * 2020-01-14 2020-05-01 华侨大学 Laser drilling device and method for metal film-assisted brittle material
CN212217441U (en) * 2020-01-14 2020-12-25 华侨大学 Laser drilling device for metal film-assisted brittle materials
CN112643206A (en) * 2020-12-29 2021-04-13 中国科学院长春光学精密机械与物理研究所 Method for inducing super-regular nano-grating by femtosecond laser based on assistance of chromium film
CN112872597A (en) * 2021-01-21 2021-06-01 北京理工大学 Method for preparing super-hydrophobic surface by combining femtosecond laser direct writing and electroplating method
CN112975142A (en) * 2021-03-02 2021-06-18 北京航空航天大学杭州创新研究院 Film material patterning processing method based on femtosecond laser controllable etching
CN113084363A (en) * 2021-03-24 2021-07-09 西湖大学 Device and method for femtosecond laser processing photoresponse liquid crystal elastomer comb teeth
CN113092439A (en) * 2021-03-31 2021-07-09 吉林大学重庆研究院 Flexible ultra-smooth SERS substrate prepared by femtosecond laser processing technology, processing method and application
CN113523596A (en) * 2021-07-08 2021-10-22 西湖大学 Device and method for femtosecond laser processing patterned photodeformable cross-linked liquid crystal polymer structure

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115246626A (en) * 2022-07-04 2022-10-28 南京理工大学 Method for preparing wave modulation flexible film based on femtosecond laser processing
CN115401314A (en) * 2022-09-22 2022-11-29 杭州奥创光子技术有限公司 A kind of processing equipment and processing method of metal mask plate

Also Published As

Publication number Publication date
CN114425654B (en) 2024-07-05

Similar Documents

Publication Publication Date Title
US10556293B2 (en) Laser machining device and laser machining method
JP4612733B2 (en) Pulse laser processing equipment
CN114425654A (en) A system and method for fabricating interdigital transducers for acoustic wave devices based on femtosecond laser processing masks
CN104741798B (en) A kind of complex foci space-time synchronous hole-drilling system and method
CN106624391A (en) Multilayer material layered milling machining system and method based on space combination laser focal point
CN109079318B (en) Femtosecond laser preparation system and method for silicon photonic crystal waveguide device
JP4835927B2 (en) Method of splitting hard and brittle plate
CN105458529A (en) Method for efficiently making large-depth-diameter-ratio micropore arrays
JP5132726B2 (en) Pulse laser processing apparatus and pulse laser processing method
TW200800456A (en) Laser processing method and laser processing apparatus
JP4866778B2 (en) Beam irradiation apparatus and beam irradiation method
CN106624389A (en) Optical fiber cutting device and method based on ultra-short pulse lasers
CN108422109A (en) A kind of laser processing device and laser processing of controllable ovality micropore
CN115805365B (en) Composite deflection laser filling scanning system, method, device and equipment
CN109202277A (en) Laser processing device
CN107301974A (en) The processing method of chip
JP5240267B2 (en) Laser processing apparatus, workpiece processing method, and workpiece dividing method
CN115319278A (en) Wafer laser de-bonding system and method based on two-dimensional acousto-optic deflector
TW201805099A (en) Laser processing apparatus and wafer producing method
CN208195946U (en) A kind of laser processing device of controllable ovality micropore
JP2003344792A (en) How to draw glass
CN107363422A (en) Laser processing device
JP3667705B2 (en) Laser processing apparatus and processing method
TW202231393A (en) Laser processing apparatus, methods of operating the same, and methods of processing workpieces using the same
TW202132035A (en) Laser processing apparatus, methods of operating the same, and methods of processing workpieces using the same

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
CB03 Change of inventor or designer information

Inventor after: Qiu Min

Inventor after: Wang Yong

Inventor after: Geng Jiao

Inventor after: Zhang Lei

Inventor after: Liu Fengjiang

Inventor after: Sun Xiaoyu

Inventor after: Shi Liping

Inventor before: Wang Yong

Inventor before: Zhang Lei

Inventor before: Liu Fengjiang

Inventor before: Geng Jiao

Inventor before: Sun Xiaoyu

Inventor before: Shi Liping

Inventor before: Qiu Min

CB03 Change of inventor or designer information
GR01 Patent grant
GR01 Patent grant