CN114293024B - 一种从粗铅中回收锡、碲、铜的精炼方法 - Google Patents
一种从粗铅中回收锡、碲、铜的精炼方法 Download PDFInfo
- Publication number
- CN114293024B CN114293024B CN202111639047.9A CN202111639047A CN114293024B CN 114293024 B CN114293024 B CN 114293024B CN 202111639047 A CN202111639047 A CN 202111639047A CN 114293024 B CN114293024 B CN 114293024B
- Authority
- CN
- China
- Prior art keywords
- alkali
- copper
- tellurium
- slag
- tin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000010949 copper Substances 0.000 title claims abstract description 41
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 title claims abstract description 38
- 229910052714 tellurium Inorganic materials 0.000 title claims abstract description 37
- PORWMNRCUJJQNO-UHFFFAOYSA-N tellurium atom Chemical compound [Te] PORWMNRCUJJQNO-UHFFFAOYSA-N 0.000 title claims abstract description 36
- 229910052718 tin Inorganic materials 0.000 title claims abstract description 36
- 229910052802 copper Inorganic materials 0.000 title claims abstract description 35
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 title claims abstract description 34
- 238000000034 method Methods 0.000 title claims abstract description 28
- 238000007670 refining Methods 0.000 title claims abstract description 21
- 239000003513 alkali Substances 0.000 claims abstract description 68
- 239000002893 slag Substances 0.000 claims abstract description 54
- 238000003756 stirring Methods 0.000 claims abstract description 28
- 150000003839 salts Chemical class 0.000 claims abstract description 21
- 238000007664 blowing Methods 0.000 claims abstract description 11
- 238000001816 cooling Methods 0.000 claims abstract description 8
- 238000002844 melting Methods 0.000 claims abstract description 7
- 230000008018 melting Effects 0.000 claims abstract description 7
- 239000012535 impurity Substances 0.000 claims abstract description 4
- 239000007788 liquid Substances 0.000 claims description 26
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 12
- 239000000155 melt Substances 0.000 claims description 10
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 8
- 229910052760 oxygen Inorganic materials 0.000 claims description 8
- 239000001301 oxygen Substances 0.000 claims description 8
- 238000005507 spraying Methods 0.000 claims description 8
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- 239000002023 wood Substances 0.000 claims description 7
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 6
- 239000011780 sodium chloride Substances 0.000 claims description 6
- 238000005868 electrolysis reaction Methods 0.000 claims description 5
- 239000000843 powder Substances 0.000 claims description 5
- OMZSGWSJDCOLKM-UHFFFAOYSA-N copper(II) sulfide Chemical compound [S-2].[Cu+2] OMZSGWSJDCOLKM-UHFFFAOYSA-N 0.000 claims description 4
- 239000000428 dust Substances 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 4
- NIFIFKQPDTWWGU-UHFFFAOYSA-N pyrite Chemical compound [Fe+2].[S-][S-] NIFIFKQPDTWWGU-UHFFFAOYSA-N 0.000 claims description 3
- 229910052683 pyrite Inorganic materials 0.000 claims description 3
- 239000011028 pyrite Substances 0.000 claims description 3
- 238000005987 sulfurization reaction Methods 0.000 claims description 2
- 238000005266 casting Methods 0.000 claims 1
- 230000001590 oxidative effect Effects 0.000 claims 1
- 238000011084 recovery Methods 0.000 abstract description 13
- 238000000926 separation method Methods 0.000 abstract description 9
- 230000000694 effects Effects 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 abstract description 3
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 239000002184 metal Substances 0.000 description 5
- 229910052751 metal Inorganic materials 0.000 description 5
- 206010039509 Scab Diseases 0.000 description 4
- 150000001447 alkali salts Chemical class 0.000 description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 230000001276 controlling effect Effects 0.000 description 2
- 230000002035 prolonged effect Effects 0.000 description 2
- 238000005086 pumping Methods 0.000 description 2
- 235000017550 sodium carbonate Nutrition 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical compound [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 229910000978 Pb alloy Inorganic materials 0.000 description 1
- 229910001294 Reinforcing steel Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000010000 carbonizing Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000012943 hotmelt Substances 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052745 lead Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 1
- 229910001887 tin oxide Inorganic materials 0.000 description 1
- 238000004073 vulcanization Methods 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Manufacture And Refinement Of Metals (AREA)
Abstract
Description
Claims (6)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202111639047.9A CN114293024B (zh) | 2021-12-30 | 2021-12-30 | 一种从粗铅中回收锡、碲、铜的精炼方法 |
Applications Claiming Priority (1)
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CN202111639047.9A CN114293024B (zh) | 2021-12-30 | 2021-12-30 | 一种从粗铅中回收锡、碲、铜的精炼方法 |
Publications (2)
Publication Number | Publication Date |
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CN114293024A CN114293024A (zh) | 2022-04-08 |
CN114293024B true CN114293024B (zh) | 2022-10-25 |
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CN202111639047.9A Active CN114293024B (zh) | 2021-12-30 | 2021-12-30 | 一种从粗铅中回收锡、碲、铜的精炼方法 |
Country Status (1)
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CN (1) | CN114293024B (zh) |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101705372B (zh) * | 2009-11-25 | 2011-09-21 | 郴州市金贵银业股份有限公司 | 高锡粗铅提锡工艺 |
CN103540762B (zh) * | 2012-07-11 | 2015-06-17 | 陕西锌业有限公司 | 一种工频无心感应电炉熔铅除铜精炼工艺 |
CN103849780A (zh) * | 2013-08-13 | 2014-06-11 | 湖南水口山有色金属集团有限公司 | 含锡粗铅的精炼方法和铅精炼生产方法 |
CN104212995B (zh) * | 2014-09-26 | 2016-09-07 | 铜陵有色金属集团铜冠新技术有限公司 | 铅铋合金高温碱性除锡方法 |
CN112695206B (zh) * | 2020-12-10 | 2022-10-18 | 北京高能时代环境技术股份有限公司 | 一种粗铅火法精炼除铜剂、制备方法及应用 |
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2021
- 2021-12-30 CN CN202111639047.9A patent/CN114293024B/zh active Active
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CN114293024A (zh) | 2022-04-08 |
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PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
CB03 | Change of inventor or designer information |
Inventor after: Wang Qin Inventor after: Shi Yu Inventor after: He Ying Inventor after: Gui Zhenfeng Inventor after: Shi Junyang Inventor after: Shi Hongjiao Inventor after: Tong Zhibo Inventor after: Liang Jinfeng Inventor after: Shi Rencai Inventor after: Xu Chen Inventor after: Wang Xiaoming Inventor before: Shi Junyang Inventor before: He Ying Inventor before: Shi Hongjiao Inventor before: Tong Zhibo Inventor before: Wang Qin Inventor before: Liang Jinfeng Inventor before: Shi Rencai Inventor before: Xu Chen Inventor before: Wang Xiaoming Inventor before: Shi Yu |
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CB03 | Change of inventor or designer information | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A Refining Method for Recovering Tin, Tellurium, and Copper from Crude Lead Effective date of registration: 20230811 Granted publication date: 20221025 Pledgee: Hunan Leiyang Rural Commercial Bank Co.,Ltd. Pledgor: LEIYANG YANXIN NON-FERROUS METALS Co.,Ltd. Registration number: Y2023980051856 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20221025 Pledgee: Hunan Leiyang Rural Commercial Bank Co.,Ltd. Pledgor: LEIYANG YANXIN NON-FERROUS METALS Co.,Ltd. Registration number: Y2023980051856 |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A refining method for recovering tin, tellurium, and copper from crude lead Granted publication date: 20221025 Pledgee: Hunan Leiyang Rural Commercial Bank Co.,Ltd. Pledgor: LEIYANG YANXIN NON-FERROUS METALS Co.,Ltd. Registration number: Y2024980009661 |