CN114191341A - 一种天然洗手液制备方法 - Google Patents
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- 235000018597 common camellia Nutrition 0.000 claims abstract description 12
- 238000001035 drying Methods 0.000 claims abstract description 5
- 241001122767 Theaceae Species 0.000 claims abstract 3
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- 241000628997 Flos Species 0.000 claims description 6
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- YZIYKJHYYHPJIB-UUPCJSQJSA-N chlorhexidine gluconate Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C(O)=O.C1=CC(Cl)=CC=C1NC(=N)NC(=N)NCCCCCCNC(=N)NC(=N)NC1=CC=C(Cl)C=C1 YZIYKJHYYHPJIB-UUPCJSQJSA-N 0.000 claims description 3
- -1 compound quaternary ammonium salt Chemical class 0.000 claims description 3
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- 229910021641 deionized water Inorganic materials 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
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- 238000002156 mixing Methods 0.000 claims description 3
- 238000010298 pulverizing process Methods 0.000 claims description 3
- 239000001397 quillaja saponaria molina bark Substances 0.000 claims description 3
- 229930182490 saponin Natural products 0.000 claims description 3
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 4
- 230000009286 beneficial effect Effects 0.000 abstract description 3
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- 238000004659 sterilization and disinfection Methods 0.000 abstract description 3
- 241000526900 Camellia oleifera Species 0.000 description 5
- 239000000344 soap Substances 0.000 description 5
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- 239000003899 bactericide agent Substances 0.000 description 2
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
本发明公开了一种天然洗手液制备方法，具体步骤如下：(1)原料处理；(2)酶解；(3)原料粉萃取；(4)浓缩；(5)山茶花萃取；(6)调配天然洗手液。本发明的有益条件在于：制备方便，成本低，可将油茶饼粕与油茶壳中有效成分有效提取，保证手部清洁效果，促进清洁杀菌，减压干燥。
Description
技术领域
本发明涉及一种天然洗手液制备方法。
背景技术
在日常生活中我们经常需要吸收，使用皂类产品能够快速清洁双手，然而皂类的清洁方式具有高碱性，使用后手部非常干涩，而且对手具有较大的刺激。现在的皂类产品与洗手液类产品中都会添加杀菌剂，但是杀菌剂的增加对皮肤具有损害。在榨油过程中会产生油茶壳和油茶饼粕，一般都会当废料作为肥料，非常浪费资源，而且油茶中含有多种天然成分，具有抗氧化左右，同时也可作为具有一定活性作用的活性剂，是一种制作洗手液的有益原料。
发明内容
为解决上述问题，本发明的目的是提供一种制备方便、成本低、可将油茶饼粕与油茶壳中有效成分有效提取、保证手部清洁效果、促进清洁杀菌、减压干燥的天然洗手液制备方法。
为实现上述目的，本发明的技术方案：
一种天然洗手液制备方法，具体步骤如下：
(1)原料处理：油茶饼粕和油茶壳混合粉碎，过60目筛，得原料粉，原料粉在2.1MPa、240s条件下蒸汽闪爆；
(2)酶解：原料粉在恒温55℃，调节pH值6，固液比9:1，加入复合酶 0.5％，搅拌均匀后酶解1.5h；
(3)原料粉萃取：通过微波灭酶萃取，微波功率6W/g物料，反应时间15 分钟，过滤得到滤液，用回收乙醇洗涤滤渣三次，固液分离后滤渣干燥，回收乙醇；
(4)浓缩：滤液加热到50℃，0.04MPa真空浓缩至原体积的15％，测定茶皂素含量，备用；
(5)山茶花萃取：山茶花去花萼4℃预冷2小时，破壁粉碎，加95％乙醇，微波萃取15分钟，过滤得滤液，滤液加热到40℃，0.02MPa真空浓缩至原体积的15％，备用；
(6)调配天然洗手液：加入葡萄糖酸氯已定0.25％、复合季铵盐0.25％、原料粉提取液15％、山茶花提取液15％、用去离子水补足到100％。
作为优选，所述的步骤(2)中的复合酶为质量比为1:1的蛋白酶和纤维素酶。
作为优选，所述的步骤(5)中山茶花破碎粉与乙醇的料液比为1:5。
本发明的有益条件在于：制备方便，成本低，可将油茶饼粕与油茶壳中有效成分有效提取，保证手部清洁效果，促进清洁杀菌，减压干燥。
具体实施方式
一种天然洗手液制备方法，具体步骤如下：(1)原料处理：油茶饼粕和油茶壳混合粉碎，过60目筛，得原料粉，原料粉在2.1MPa、240s条件下蒸汽闪爆；(2)酶解：原料粉在恒温55℃，调节pH值6，固液比9:1，加入复合酶0.5％，搅拌均匀后酶解1.5h；(3)原料粉萃取：通过微波灭酶萃取，微波功率6W/g物料，反应时间15分钟，过滤得到滤液，用回收乙醇洗涤滤渣三次，固液分离后滤渣干燥，回收乙醇；(4)浓缩：滤液加热到50℃，0.04MPa真空浓缩至原体积的15％，测定茶皂素含量，备用；(5)山茶花萃取：山茶花去花萼4℃预冷2 小时，破壁粉碎，加95％乙醇，微波萃取15分钟，过滤得滤液，滤液加热到40℃， 0.02MPa真空浓缩至原体积的15％，备用；(6)调配天然洗手液：加入葡萄糖酸氯已定0.25％、复合季铵盐0.25％、原料粉提取液15％、山茶花提取液15％、用去离子水补足到100％。所述的步骤(2)中的复合酶为质量比为1:1的蛋白酶和纤维素酶。所述的步骤(5)中山茶花破碎粉与乙醇的料液比为1:5。
本发明的步骤(1)中进行蒸汽闪爆，使得空间间隙更大，提高提取率，酶解破坏细胞壁，是的溶出量更多，原料粉萃取中微波使蛋白变性，更易分离有效成分，本产品洗手液减压干燥，保留更多天然有效成分，步骤(6)中的的葡萄糖酸氯已定与复合季铵盐两种物质本身就有消毒功效，加入原料粉提取液与山茶花提取液后更加增强，提高清洁效果。
本行业的技术人员应该了解，本发明不受上述实施例的限制，上述实施例和说明书中描述的只是说明本发明的原理，在不脱离本发明精神和范围的前提下，本发明还会有各种变化和改进，这些变化和改进都落入要求保护的本发明范围内。本发明要求保护范围由所附的权利要求书及其等效物界定。
Claims (3)
1.一种天然洗手液制备方法，其特征在于，具体步骤如下：
(1)原料处理：油茶饼粕和油茶壳混合粉碎，过60目筛，得原料粉，原料粉在2.1MPa、240s条件下蒸汽闪爆；
(2)酶解：原料粉在恒温55℃，调节pH值6，固液比9:1，加入复合酶0.5％，搅拌均匀后酶解1.5h；
(3)原料粉萃取：通过微波灭酶萃取，微波功率6W/g物料，反应时间15分钟，过滤得到滤液，用回收乙醇洗涤滤渣三次，固液分离后滤渣干燥，回收乙醇；
(4)浓缩：滤液加热到50℃，0.04MPa真空浓缩至原体积的15％，测定茶皂素含量，备用；
(5)山茶花萃取：山茶花去花萼4℃预冷2小时，破壁粉碎，加95％乙醇，微波萃取15分钟，过滤得滤液，滤液加热到40℃，0.02MPa真空浓缩至原体积的15％，备用；
(6)调配天然洗手液：加入葡萄糖酸氯已定0.25％、复合季铵盐0.25％、原料粉提取液15％、山茶花提取液15％、用去离子水补足到100％。
2.根据权利要求1所述的一种天然洗手液制备方法，其特征在于，所述的步骤(2)中的复合酶为质量比为1:1的蛋白酶和纤维素酶。
3.根据权利要求1所述的一种天然洗手液制备方法，其特征在于，所述的步骤(5)中山茶花破碎粉与乙醇的料液比为1:5。
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| CN102973469A (zh) * | 2012-12-25 | 2013-03-20 | 江南大学 | 一种含茶籽粕提取物的温和洗手液 |
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| CN109998955A (zh) * | 2019-04-15 | 2019-07-12 | 陕西师范大学 | 一种山茶花抑菌洗手液及其制备方法 |
| CN110407889A (zh) * | 2019-07-09 | 2019-11-05 | 合肥学院 | 一种提取油茶饼粕中茶皂素的方法 |
| CN112168770A (zh) * | 2020-10-08 | 2021-01-05 | 福建省梦娇兰日用化学品有限公司 | 一种含天然植物提取改良配方的婴童保湿抑菌洗手液 |
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Patent Citations (5)
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| CN102973469A (zh) * | 2012-12-25 | 2013-03-20 | 江南大学 | 一种含茶籽粕提取物的温和洗手液 |
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| CN109998955A (zh) * | 2019-04-15 | 2019-07-12 | 陕西师范大学 | 一种山茶花抑菌洗手液及其制备方法 |
| CN110407889A (zh) * | 2019-07-09 | 2019-11-05 | 合肥学院 | 一种提取油茶饼粕中茶皂素的方法 |
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