CN113995053A - Feed for sows in lactation period and preparation method thereof - Google Patents

Feed for sows in lactation period and preparation method thereof Download PDF

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CN113995053A
CN113995053A CN202111282390.2A CN202111282390A CN113995053A CN 113995053 A CN113995053 A CN 113995053A CN 202111282390 A CN202111282390 A CN 202111282390A CN 113995053 A CN113995053 A CN 113995053A
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feed
weight
sows
mixed
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郜丽欢
孙宇
刁小东
王雨涵
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Hefei Shengjia Biotechnology Co ltd
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Hefei Shengjia Biotechnology Co ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K50/00Feeding-stuffs specially adapted for particular animals
    • A23K50/30Feeding-stuffs specially adapted for particular animals for swines
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/10Animal feeding-stuffs obtained by microbiological or biochemical processes
    • A23K10/12Animal feeding-stuffs obtained by microbiological or biochemical processes by fermentation of natural products, e.g. of vegetable material, animal waste material or biomass
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/20Animal feeding-stuffs from material of animal origin
    • A23K10/22Animal feeding-stuffs from material of animal origin from fish
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/30Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K10/00Animal feeding-stuffs
    • A23K10/30Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
    • A23K10/37Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/10Organic substances
    • A23K20/142Amino acids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/10Organic substances
    • A23K20/174Vitamins
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/20Inorganic substances, e.g. oligoelements
    • A23K20/28Silicates, e.g. perlites, zeolites or bentonites
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/20Inorganic substances, e.g. oligoelements
    • A23K20/30Oligoelements
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K40/00Shaping or working-up of animal feeding-stuffs
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    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026After-treatment
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P60/00Technologies relating to agriculture, livestock or agroalimentary industries
    • Y02P60/80Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
    • Y02P60/87Re-use of by-products of food processing for fodder production

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Abstract

The invention discloses a feed for sows in a lactation period and a preparation method thereof. The modified zeolite powder and the coarse feed are fermented together, and then mixed forage powder, mixed protein powder, compound vitamin and water are added, and the mixture is evenly mixed and granulated to obtain the feed. The feed for the lactating sows, prepared by the method, is good in palatability, provides balanced nutrition for the lactating sows, can adsorb toxin and heavy metals, avoids intestinal absorption, is discharged out of bodies along with excrement, supplements microelements such as selenium and calcium for the lactating sows, prevents postpartum lactation heat of the sows, improves intestinal health, increases feed intake, and improves lactation yield and lactation capacity.

Description

Feed for sows in lactation period and preparation method thereof
Technical Field
The invention belongs to the technical field of animal feed preparation, and particularly relates to a feed for sows in a lactation period and a preparation method thereof.
Background
A lactating sow is generally a sow which is post-parturition of a pregnant sow and is in lactation. The levels of energy, protein, lysine and other nutrients required by a lactating sow are determined by the sow's own body weight, milk production and feeding environment.
The high and low lactation yield of the whole-period lactating sows determines the good and bad production performance of the lactating piglets, and the lactation yield of the lactating sows is obviously reduced in summer, so that a series of problems of increased death rate of the piglets in the lactation period, reduced weight of the weaned piglets, increased diarrhea rate of the weaned piglets, reduced activity of the weaned piglets and the like are caused. At present, additives such as sweetening agents, flavoring agents or gamma-aminobutyric acid are added into the feed of nursing sows to improve the feed intake of the sows, so that the lactation yield is improved. Compared with other seasons, the effect of improving the feed intake by simply adding the phagostimulants in summer is not ideal, and the heat stress problem of the sows cannot be effectively solved, so that the problem of insufficient lactation is difficult to thoroughly solve.
The invention Chinese patent CN 107319163B discloses a lactating sow compound feed and a preparation and use method thereof, aiming at the problems that the prior lactating sow has low lactation yield in summer and can not meet the normal demand of piglets, the invention provides the lactating sow compound feed which comprises the following raw materials: each ton of feed comprises 700kg of corn-. The feed disclosed by the invention is reasonable in formula and high in nutrition level, can effectively improve the summer feed intake of lactating sows, enhances the digestion and absorption capacity and the heat stress resistance of the sows, improves the lactation performance of the sows by more than 20% compared with the lactation performance of the sows fed with other feeds, and has important economic benefits. However, the nutrient components added in the invention have poor absorption effect on the sows, and the nutrition is seriously lost in the sows.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides a sow feed in a lactation period and a preparation method thereof.
The preparation method of the feed for sows in the lactation period comprises the following steps:
(1) uniformly mixing 40-60 parts of mixed fermentation product, 20-40 parts of mixed forage powder, 5-15 parts of mixed protein powder, 1-3 parts of composite vitamin and 15-25 parts of water in parts by weight to obtain mixed feed;
(2) and (2) placing the mixed feed obtained in the step (1) into a feed granulator for granulation to obtain the feed for the sows in the lactation period, wherein the particle size is 0.5-1.5 cm.
The preparation method of the mixed fermentation product comprises the following steps:
s1: uniformly mixing 30-50 parts of corn flour, 30-50 parts of sorghum flour, 15-25 parts of wheat bran, 10-20 parts of bean curd residue and 30-50 parts of water in parts by weight to obtain a coarse mixture;
s2: uniformly mixing 8-20 parts by weight of modified zeolite powder, 0.4-0.6 part by weight of bacillus subtilis and 80-120 parts by weight of the crude mixture obtained in the step S1 to obtain a fermentation substrate;
s3: and (4) placing the fermentation substrate obtained in the step (S2) into a fermentation tank, and sealing and fermenting for 30-40 hours at 23-27 ℃ to obtain a mixed fermentation product.
The preparation method of the modified zeolite powder comprises the following steps:
t1: putting the zeolite powder into a tubular furnace, heating to 400-420 ℃ at the initial temperature of 20-30 ℃ at the heating rate of 4-6 ℃/min, keeping for 1-3 hours, then cooling to 70-90 ℃ at the cooling rate of 8-12 ℃/min, transferring to 4-6 ℃ and keeping for 20-40 minutes to obtain physically modified zeolite powder;
t2: adding 15-25 parts by weight of the physically modified zeolite powder obtained in the step T1 into 40-60 parts by weight of the modification solution, uniformly mixing, soaking at 50-70 ℃ for 2-4 hours, and filtering to obtain a filter cake to obtain a mixture A;
t3: and (4) transferring the mixture A obtained in the step T2 to an oven at 50-70 ℃ for drying for 8-12 hours to obtain the modified zeolite powder.
The preparation method of the modified liquid comprises the following steps: adding 4-6 parts by weight of silane coupling agent, 15-25 parts by weight of sulfur-containing amino acid and 5-7 parts by weight of functional yeast liquid into 40-60 parts by weight of water, and uniformly mixing to obtain the modified liquid.
The silane coupling agent is at least one of vinyltriethoxysilane, vinyltrimethoxysilane and vinyltris (beta-methoxyethoxy) silane. Preferably, the silane coupling agent is vinyltriethoxysilane.
The sulfur-containing amino acid is at least one of methionine, cystine and cystine. Preferably, the sulfur-containing amino acid is methionine.
The zeolite powder has a pore structure, has adsorption and ion exchange effects on toxins, but has insufficient specific surface area and limited adsorption capacity. The zeolite powder is thermally modified, the temperature is raised, the moisture and organic matters in the zeolite powder are removed, so that the pore passages of the zeolite powder are unobstructed, the specific surface area is increased, the adsorption effect and the ion exchange performance of the zeolite powder are fully exerted, and then the zeolite powder is subjected to quenching treatment to form thermal shock, so that impurities are easily separated, the stability of the pore structure is facilitated, and the collapse of pores is prevented; the zeolite powder modified by selenium-calcium-rich yeast and sulfur-containing amino acid is used, the zeolite powder contacts with amino group in the sulfur-containing amino acid, the sulfur-containing amino acid is fixed on the surface of the zeolite powder by a coupling agent, the selenium in the selenium-calcium-rich yeast replaces the sulfur in the sulfur-containing amino acid to form seleno-amino acid, the calcium-chelated amino acid in the selenium-calcium-rich yeast forms amino acid chelated calcium, and after the amino acid is fixed on the surface of the zeolite powder, selenium and calcium elements are fixed on the amino acid, so that the surface modification of the zeolite powder is realized, the silicon content on the surface of the zeolite powder can be reduced, the porosity is improved, the average crystal and particle size of the silicon-containing zeolite powder material are reduced, and the porosity and ion exchange performance of the zeolite powder are improved. Sodium sulfite is formed by sodium and oxygen left by substituted sulfur and sodium selenite raw materials, the sodium sulfite is incompletely ionized under an acidic condition, the ion exchange performance of the zeolite powder is modified, a certain promotion effect on an ionization reaction can be achieved, sodium bisulfite is generated, the sodium bisulfite can be used for chemical detoxification of mycotoxin in pig feed, harm of joint protection mycotoxin to pig intestines can be effectively relieved, healthy intestines are kept, a proper amount of selenium element and calcium element are added, the foraging and digestion capacity of sows is improved, the body health of the sows is improved, and the number and the milk secretion quality of the sows are increased.
The modified zeolite powder has a honeycomb network crystal structure, enters a pig body through an oral cavity, is absorbed by intestinal mucosa and enters blood and lymph tissue, has higher specific surface area and adsorption capacity, can adsorb microorganisms such as low molecular compounds, toxic compounds, mycotoxin and the like in the body, dissolves some small molecular substances and discharges the small molecular substances out of the body; the modified zeolite powder can be used as an adsorbent of heavy metals to adsorb lead, chromium, copper and the like through cation exchange characteristics, and the antibacterial and anti-diarrhea functions of the feed for the lactating sows added with the modified zeolite powder are obviously enhanced; after the sow parturites, the requirement of the produced milk on calcium is suddenly increased, the secretion of parathyroid hormone and calcitonin can not adapt to the sudden change, postpartum paralysis is caused when the sow is lack of calcium, namely, the symptoms of milk fever are caused, the feed for the lactating sow added with the modified zeolite powder can improve the resistance of the sow and can also participate in adjusting the calcium stabilizing matrix of the postpartum sow, the ash content, the calcium content and the phosphorus content and the strength of the lacuna bone are increased, and the calcium content in serum is adjusted, so that the generation of the milk fever is avoided, the number of effective nipples is increased, and the milk secretion quality is improved.
The preparation method of the functionalized yeast liquid comprises the following steps: inoculating 1-2 parts of yeast to 90-110 parts of liquid culture medium by weight, and culturing at 28-30 ℃ for 1-2 days to obtain a functionalized yeast liquid;
the liquid culture medium comprises, by weight, 10-15 parts of honey, 10 parts of a functional agent, 0.5-1 part of glucose, 0.3-0.5 part of peptone and 80-100 parts of water.
The functional agent is FeSO4、CuSO4、ZnSO4、MnSO4、MgSO4、NaSeO3KI and CaCl2ToOne of them is less. Preferably, the functional agent is NaSeO3And CaCl2The mixture is composed according to the mass ratio of 1 (1.5-2.0).
Selenium and calcium elements are added into the selenium-calcium-enriched yeast in the process of culturing the yeast, and the selenium and calcium are absorbed and utilized during the growth of the yeast, so that the selenium and calcium are organically combined with protein and polysaccharide in the yeast body and converted into biological selenium and biological calcium, thereby eliminating chemical selenium and chemical calcium, and avoiding toxic and side effects on pig organisms and gastrointestinal stimulation. The yeast is rich in protein, sugar and 18 vitamins, and can be used as a selenium source and a calcium source and also provide other beneficial nutrients.
The preparation method of the mixed forage powder comprises the following steps: according to the weight portion, 10-30 portions of pasture, 3-7 portions of caulis spatholobi, 3-7 portions of acanthopanax sessiliflorus, 3-7 portions of cowherb seed, 8-12 portions of dandelion and 3-7 portions of rehmannia are crushed by a beater and pass through a 60-100 mesh sieve, and the mixed forage powder is obtained.
The mixed protein powder is a mixture of fish meal, pea protein powder and seaweed powder according to the mass ratio of (1-3) to 1.
The compound vitamin is a mixture consisting of vitamin C, vitamin E, vitamin B1 and vitamin B6 according to the mass ratio of (4-6): (2-3): (1-3): 1.2.
The mixed forage powder comprises pasture, caulis Spatholobi, acanthopanax sessiliflorus, cowherb seed, dandelion and rehmannia, wherein the caulis Spatholobi can promote blood circulation and nourish blood, dredge tendons and activate collaterals, and the acanthopanax sessiliflorus is rich in protocatechuic acid, has good antibacterial effect, and can cause diseases such as bacterial infection, diarrhea and the like due to weak resistance of textile sows after delivery and easy corrosion of intestines and stomach by bacteria; the cowherb seed and the dandelion can help the sow to diminish inflammation and induce diuresis, and avoid urinary system infection and the like.
A large amount of fish meal, pea protein powder, seaweed meal and compound vitamins are added into the feed, so that rich protein is provided for the sows in the lactation period, the nutrition is supplemented, and the milk yield and the average number of piglets are increased.
The invention has the beneficial effects that:
1. the feed for the lactating sows, prepared by the method, is good in palatability, provides balanced nutrition for the lactating sows, can adsorb toxin and heavy metals, avoids intestinal absorption, is discharged out of bodies along with excrement, supplements microelements such as selenium and calcium for the lactating sows, prevents postpartum lactation heat of the sows, improves intestinal health, increases feed intake, and improves lactation yield and lactation capacity.
2. The inventor introduces modified zeolite powder, and modifies the zeolite powder by a physical method to improve the pore structure of the zeolite; then, zeolite powder modified by selenium-calcium-rich yeast and sulfur-containing amino acid is used, after the amino acid is fixed on the surface of the zeolite powder, selenium and calcium elements are fixed on the amino acid, so that the surface modification of the zeolite powder is realized, and the modified zeolite powder has a honeycomb network crystal structure and can adsorb microorganisms such as low molecular compounds, toxic compounds, mycotoxin and the like in vivo; on the other hand, the antibacterial and anti-diarrhea functions of the feed for the sows in the lactation period of the modified zeolite powder are obviously enhanced.
Detailed Description
The raw materials used in the examples were as follows:
zeolite powder, purchased from Tianjin Zeolite mining Co., Ltd, North Tibet, CAS number: 1318-02-1, particle size: 2 mm.
Vinyltriethoxysilane: coupling agent a151, purchased from carumurus facilis chemicals, inc, CAS no: 78-08-0, content: 98 percent.
Methionine, purchased from serotonine biotechnology limited, hannan, CAS no: 63-6803, content: 99 percent.
Bacillus subtilis, latin name: bacillus subtilis, number: cic 10275, effective bacterial activity: 1000 hundred million CFU/g, purchased from China center for Industrial culture Collection of microorganisms.
In the examples, the yeast is saccharomyces cerevisiae, and the name of Latin: saccharomyces cerevisiae, accession number: cic 1001, effective bacterial activity: 1000 hundred million CFU/g, purchased from China center for Industrial culture Collection of microorganisms.
Corn flour, purchased from sierra, bioengineering, ltd, cat #: REL 0941.
Sorghum flour, purchased from mingwang food ltd.
Wheat bran, purchased from kyushu chemical limited, shandong, cat # o: 781-23578.
The bean curd refuse is purchased from information services Co., Ltd, Heishan City, and has a product number of 001.
NaSeO3Purchased from north Heibo five encyclopedia, Inc., CAS number: 10102-18-8, model: food grade, content: 99 percent.
CaCl2Purchased from porch nakoco new materials technology limited, CAS No.: 10043-52-4, model: food grade, content: 98 percent.
Pasture, purchased from bihai pasture limited, zhengyang county, model: 2020.
spatholobus stem, Latin scientific name: spatholus subelectus Dunn has the effects of dispelling wind, promoting blood circulation, relaxing tendons and activating collaterals, and is purchased from Yihongtang pharmaceutical industry Co., Ltd.
Acanthopanax sessiliflorus, Latin, famous: eleutherococcus sessiliflorus (Rupr. & Maxim.) s.y.hu, has the effects of dispelling wind and eliminating dampness, invigorating stomach and inducing diuresis, and is purchased from billion hong Tang pharmaceutical industry limited company in the city of hauo.
Cowherb seed, Latin's name: the vaccine for treating amenorrhea, dysmenorrhea, galactorrhea, acute mastitis, stranguria and painful urination has the effects of activating blood circulation to promote menstruation, promoting lactation, diminishing swelling, inducing diuresis and treating stranguria, and is purchased from Yi hong Tang pharmaceutical industry limited company in the city of Hao Zhou.
Dandelion, latin scientific name: taraxacum mongolicum hand-Mazz, belonging to Compositae, contains various health nutritional components such as taraxanol, taraxacin, choline, organic acid, inulin, etc. Sweet in nature and taste, slightly bitter and cold. It enters liver and stomach meridians. Has the effects of promoting urination, relieving diarrhea, eliminating jaundice, benefiting gallbladder, etc., and is purchased from Yi Hongtong pharmaceutical industry Co Ltd.
Rehmannia, Latin scientific name: rehmannia glutinosa (Gaetn.) libosh.ex fisch.et mey, has the efficacies of nourishing yin and tonifying kidney, nourishing blood and enriching blood and cooling blood, and is purchased from a billion Hongtong pharmaceutical industry limited company in the city of Hao Zhou.
Fish meal, purchased from Ministry of agricultural feeds in Yuzhou district, Yulin.
Pea protein powder, purchased from west apres bioengineering, ltd, cat #: 5623, content 80%.
Seaweed meal, purchased from the Fufeng Sinote Biotech limited.
Example 1
The preparation method of the feed for sows in the lactation period comprises the following steps:
(1) uniformly mixing 50 parts of mixed fermentation product, 30 parts of mixed forage powder, 10 parts of mixed protein powder, 2 parts of compound vitamin and 20 parts of water in parts by weight to obtain mixed feed;
(2) and (2) placing the mixed feed obtained in the step (1) into a feed granulator for granulation to obtain the feed for the sows in the lactation period, wherein the particle size is 1 cm.
The preparation method of the mixed fermentation product comprises the following steps:
s1: uniformly mixing 40 parts of corn flour, 40 parts of sorghum flour, 20 parts of wheat bran, 15 parts of bean curd residue and 40 parts of water in parts by weight to obtain a crude mixture;
s2: uniformly mixing 18 parts of modified zeolite powder, 0.5 part of bacillus subtilis and 100 parts of the crude mixture obtained in the step S1 according to parts by weight to obtain a fermentation substrate;
s3: and (4) placing the fermentation substrate obtained in the step (S2) into a fermentation tank, and sealing and fermenting for 36 hours at 25 ℃ to obtain a mixed fermentation product.
The preparation method of the modified zeolite powder comprises the following steps:
t1: putting the zeolite powder into a tubular furnace, heating to 420 ℃ at an initial temperature of 25 ℃ at a heating rate of 5 ℃/min, keeping for 2 hours, then cooling to 80 ℃ at a cooling rate of 10 ℃/min, transferring to a container filled with water at 5 ℃ and quenching for 30 minutes in a water-proof manner to obtain physically modified zeolite powder;
t2: adding 20 parts by weight of the physically modified zeolite powder obtained in the step T1 into 50 parts by weight of the modification solution, uniformly mixing, soaking at 60 ℃ for 3 hours, and filtering to obtain a filter cake to obtain a mixture A;
t3: and (3) transferring the mixture A obtained in the step T2 to an oven at 60 ℃ for drying for 10 hours to obtain the modified zeolite powder.
The preparation method of the modified liquid comprises the following steps: adding 5 parts by weight of silane coupling agent, 20 parts by weight of sulfur-containing amino acid and 6 parts by weight of yeast liquid into 50 parts by weight of water, and uniformly mixing to obtain modified liquid.
The silane coupling agent is vinyl triethoxysilane.
The sulfur-containing amino acid is methionine.
The preparation method of the yeast liquid comprises the following steps: inoculating 2 parts by weight of yeast to 100 parts by weight of liquid medium, and culturing at 29 ℃ for 1 day to obtain yeast liquid.
The liquid medium is composed of 12 parts by weight of honey, 0.8 part by weight of glucose, 0.4 part by weight of peptone and 90 parts by weight of water.
The preparation method of the mixed forage powder comprises the following steps: according to the weight parts, 20 parts of pasture, 5 parts of caulis spatholobi, 5 parts of acanthopanax sessiliflorus, 5 parts of cowherb seed, 10 parts of dandelion and 5 parts of rehmannia are crushed by a beater and pass through a 80-mesh sieve to obtain mixed forage powder.
The mixed protein powder is a mixture of fish meal, pea protein powder and seaweed powder in a mass ratio of 2:1: 1.
The compound vitamin is a mixture of vitamin C, vitamin E, vitamin B1 and vitamin B6 according to the mass ratio of 5:2.3:2: 1.2.
Example 2
The preparation method of the feed for sows in the lactation period comprises the following steps:
(1) uniformly mixing 50 parts of mixed fermentation product, 30 parts of mixed forage powder, 10 parts of mixed protein powder, 2 parts of compound vitamin and 20 parts of water in parts by weight to obtain mixed feed;
(2) and (2) placing the mixed feed obtained in the step (1) into a feed granulator for granulation to obtain the feed for the sows in the lactation period, wherein the particle size is 1 cm.
The preparation method of the mixed fermentation product comprises the following steps:
s1: uniformly mixing 40 parts of corn flour, 40 parts of sorghum flour, 20 parts of wheat bran, 15 parts of bean curd residue and 40 parts of water in parts by weight to obtain a crude mixture;
s2: uniformly mixing 18 parts of modified zeolite powder, 0.5 part of bacillus subtilis and 100 parts of the crude mixture obtained in the step S1 according to parts by weight to obtain a fermentation substrate;
s3: and (4) placing the fermentation substrate obtained in the step (S2) into a fermentation tank, and sealing and fermenting for 36 hours at 25 ℃ to obtain a mixed fermentation product.
The preparation method of the modified zeolite powder comprises the following steps:
t1: putting the zeolite powder into a tubular furnace, heating to 420 ℃ at an initial temperature of 25 ℃ at a heating rate of 5 ℃/min, keeping for 2 hours, then cooling to 80 ℃ at a cooling rate of 10 ℃/min, transferring to 5 ℃ and keeping for 30 minutes to obtain physically modified zeolite powder;
t2: adding 20 parts by weight of the physically modified zeolite powder obtained in the step T1 into 50 parts by weight of the modification solution, uniformly mixing, soaking at 60 ℃ for 3 hours, and filtering to obtain a filter cake to obtain a mixture A;
t3: and (3) transferring the mixture A obtained in the step T2 to an oven at 60 ℃ for drying for 10 hours to obtain the modified zeolite powder.
The preparation method of the modified liquid comprises the following steps: adding 5 parts by weight of silane coupling agent, 20 parts by weight of sulfur-containing amino acid and 6 parts by weight of functionalized yeast liquid into 50 parts by weight of water, and uniformly mixing to obtain modified liquid.
The silane coupling agent is vinyl triethoxysilane.
The sulfur-containing amino acid is methionine.
The preparation method of the functionalized yeast liquid comprises the following steps: inoculating 2 parts by weight of yeast to 100 parts by weight of liquid culture medium, and culturing at 29 ℃ for 1 day to obtain a functionalized yeast liquid;
the liquid medium comprises 12 parts of honey, 8 parts of functional agent, 0.8 part of glucose, 0.4 part of peptone and 90 parts of water in parts by weight.
The functional agent is NaSeO3
The preparation method of the mixed forage powder comprises the following steps: according to the weight parts, 20 parts of pasture, 5 parts of caulis spatholobi, 5 parts of acanthopanax sessiliflorus, 5 parts of cowherb seed, 10 parts of dandelion and 5 parts of rehmannia are crushed by a beater and pass through a 80-mesh sieve to obtain mixed forage powder.
The mixed protein powder is a mixture of fish meal, pea protein powder and seaweed powder in a mass ratio of 2:1: 1.
The compound vitamin is a mixture of vitamin C, vitamin E, vitamin B1 and vitamin B6 according to the mass ratio of 5:2.3:2: 1.2.
Example 3
The preparation method of the feed for sows in the lactation period comprises the following steps:
(1) uniformly mixing 50 parts of mixed fermentation product, 30 parts of mixed forage powder, 10 parts of mixed protein powder, 2 parts of compound vitamin and 20 parts of water in parts by weight to obtain mixed feed;
(2) and (2) placing the mixed feed obtained in the step (1) into a feed granulator for granulation to obtain the feed for the sows in the lactation period, wherein the particle size is 1 cm.
The preparation method of the mixed fermentation product comprises the following steps:
s1: uniformly mixing 40 parts of corn flour, 40 parts of sorghum flour, 20 parts of wheat bran, 15 parts of bean curd residue and 40 parts of water in parts by weight to obtain a crude mixture;
s2: uniformly mixing 18 parts of modified zeolite powder, 0.5 part of bacillus subtilis and 100 parts of the crude mixture obtained in the step S1 according to parts by weight to obtain a fermentation substrate;
s3: and (4) placing the fermentation substrate obtained in the step (S2) into a fermentation tank, and sealing and fermenting for 36 hours at 25 ℃ to obtain a mixed fermentation product.
The preparation method of the modified zeolite powder comprises the following steps:
t1: putting the zeolite powder into a tubular furnace, heating to 420 ℃ at an initial temperature of 25 ℃ at a heating rate of 5 ℃/min, keeping for 2 hours, then cooling to 80 ℃ at a cooling rate of 10 ℃/min, transferring to 5 ℃ and keeping for 30 minutes to obtain physically modified zeolite powder;
t2: adding 20 parts by weight of the physically modified zeolite powder obtained in the step T1 into 50 parts by weight of the modification solution, uniformly mixing, soaking at 60 ℃ for 3 hours, and filtering to obtain a filter cake to obtain a mixture A;
t3: and (3) transferring the mixture A obtained in the step T2 to an oven at 60 ℃ for drying for 10 hours to obtain the modified zeolite powder.
The preparation method of the modified liquid comprises the following steps: adding 5 parts by weight of silane coupling agent, 20 parts by weight of sulfur-containing amino acid and 6 parts by weight of functionalized yeast liquid into 50 parts by weight of water, and uniformly mixing to obtain modified liquid.
The silane coupling agent is vinyl triethoxysilane.
The sulfur-containing amino acid is methionine.
The preparation method of the functionalized yeast liquid comprises the following steps: inoculating 2 parts by weight of yeast to 100 parts by weight of liquid culture medium, and culturing at 29 ℃ for 1 day to obtain a functionalized yeast liquid;
the liquid medium comprises 12 parts of honey, 8 parts of functional agent, 0.8 part of glucose, 0.4 part of peptone and 90 parts of water in parts by weight.
The functional agent is CaCl2
The preparation method of the mixed forage powder comprises the following steps: according to the weight parts, 20 parts of pasture, 5 parts of caulis spatholobi, 5 parts of acanthopanax sessiliflorus, 5 parts of cowherb seed, 10 parts of dandelion and 5 parts of rehmannia are crushed by a beater and pass through a 80-mesh sieve to obtain mixed forage powder.
The mixed protein powder is a mixture of fish meal, pea protein powder and seaweed powder in a mass ratio of 2:1: 1.
The compound vitamin is a mixture of vitamin C, vitamin E, vitamin B1 and vitamin B6 according to the mass ratio of 5:2.3:2: 1.2.
Example 4
The preparation method of the feed for sows in the lactation period comprises the following steps:
(1) uniformly mixing 50 parts of mixed fermentation product, 30 parts of mixed forage powder, 10 parts of mixed protein powder, 2 parts of compound vitamin and 20 parts of water in parts by weight to obtain mixed feed;
(2) and (2) placing the mixed feed obtained in the step (1) into a feed granulator for granulation to obtain the feed for the sows in the lactation period, wherein the particle size is 1 cm.
The preparation method of the mixed fermentation product comprises the following steps:
s1: uniformly mixing 40 parts of corn flour, 40 parts of sorghum flour, 20 parts of wheat bran, 15 parts of bean curd residue and 40 parts of water in parts by weight to obtain a crude mixture;
s2: uniformly mixing 18 parts of modified zeolite powder, 0.5 part of bacillus subtilis and 100 parts of the crude mixture obtained in the step S1 according to parts by weight to obtain a fermentation substrate;
s3: and (4) placing the fermentation substrate obtained in the step (S2) into a fermentation tank, and sealing and fermenting for 36 hours at 25 ℃ to obtain a mixed fermentation product.
The preparation method of the modified zeolite powder comprises the following steps:
t1: putting the zeolite powder into a tubular furnace, heating to 420 ℃ at an initial temperature of 25 ℃ at a heating rate of 5 ℃/min, keeping for 2 hours, then cooling to 80 ℃ at a cooling rate of 10 ℃/min, transferring to 5 ℃ and keeping for 30 minutes to obtain physically modified zeolite powder;
t2: adding 20 parts by weight of the physically modified zeolite powder obtained in the step T1 into 50 parts by weight of the modification solution, uniformly mixing, soaking at 60 ℃ for 3 hours, and filtering to obtain a filter cake to obtain a mixture A;
t3: and (3) transferring the mixture A obtained in the step T2 to an oven at 60 ℃ for drying for 10 hours to obtain the modified zeolite powder.
The preparation method of the modified liquid comprises the following steps: adding 5 parts by weight of silane coupling agent, 20 parts by weight of sulfur-containing amino acid and 6 parts by weight of functionalized yeast liquid into 50 parts by weight of water, and uniformly mixing to obtain modified liquid.
The silane coupling agent is vinyl triethoxysilane.
The sulfur-containing amino acid is methionine.
The preparation method of the functionalized yeast liquid comprises the following steps: inoculating 2 parts by weight of yeast to 100 parts by weight of liquid culture medium, and culturing at 29 ℃ for 1 day to obtain a functionalized yeast liquid;
the liquid medium comprises 12 parts of honey, 8 parts of functional agent, 0.8 part of glucose, 0.4 part of peptone and 90 parts of water in parts by weight.
The functional agent is NaSeO3And CaCl2According to the mass ratio1: 1.8 of the composition.
The preparation method of the mixed forage powder comprises the following steps: according to the weight parts, 20 parts of pasture, 5 parts of caulis spatholobi, 5 parts of acanthopanax sessiliflorus, 5 parts of cowherb seed, 10 parts of dandelion and 5 parts of rehmannia are crushed by a beater and pass through a 80-mesh sieve to obtain mixed forage powder.
The mixed protein powder is a mixture of fish meal, pea protein powder and seaweed powder in a mass ratio of 2:1: 1.
The compound vitamin is a mixture of vitamin C, vitamin E, vitamin B1 and vitamin B6 according to the mass ratio of 5:2.3:2: 1.2.
Example 5
The preparation method of the feed for sows in the lactation period comprises the following steps:
(1) uniformly mixing 50 parts of mixed fermentation product, 30 parts of mixed forage powder, 10 parts of mixed protein powder, 2 parts of compound vitamin and 20 parts of water in parts by weight to obtain mixed feed;
(2) and (2) placing the mixed feed obtained in the step (1) into a feed granulator for granulation to obtain the feed for the sows in the lactation period, wherein the particle size is 1 cm.
The preparation method of the mixed fermentation product comprises the following steps:
s1: uniformly mixing 40 parts of corn flour, 40 parts of sorghum flour, 20 parts of wheat bran, 15 parts of bean curd residue and 40 parts of water in parts by weight to obtain a crude mixture;
s2: uniformly mixing 18 parts of modified zeolite powder, 0.5 part of bacillus subtilis and 100 parts of the crude mixture obtained in the step S1 according to parts by weight to obtain a fermentation substrate;
s3: and (4) placing the fermentation substrate obtained in the step (S2) into a fermentation tank, and sealing and fermenting for 36 hours at 25 ℃ to obtain a mixed fermentation product.
The preparation method of the modified zeolite powder comprises the following steps:
t1: putting the zeolite powder into a tubular furnace, heating to 420 ℃ at an initial temperature of 25 ℃ at a heating rate of 5 ℃/min, keeping for 2 hours, then cooling to 80 ℃ at a cooling rate of 10 ℃/min, transferring to 5 ℃ and keeping for 30 minutes to obtain physically modified zeolite powder;
t2: adding 20 parts by weight of the physically modified zeolite powder obtained in the step T1 into 50 parts by weight of the modification solution, uniformly mixing, soaking at 60 ℃ for 3 hours, and filtering to obtain a filter cake to obtain a mixture A;
t3: and (3) transferring the mixture A obtained in the step T2 to an oven at 60 ℃ for drying for 10 hours to obtain the modified zeolite powder.
The preparation method of the modified liquid comprises the following steps: adding 5 parts by weight of silane coupling agent and 20 parts by weight of sulfur-containing amino acid into 50 parts by weight of water, and uniformly mixing to obtain the modified liquid.
The silane coupling agent is vinyl triethoxysilane.
The sulfur-containing amino acid is methionine.
The preparation method of the mixed forage powder comprises the following steps: according to the weight parts, 20 parts of pasture, 5 parts of caulis spatholobi, 5 parts of acanthopanax sessiliflorus, 5 parts of cowherb seed, 10 parts of dandelion and 5 parts of rehmannia are crushed by a beater and pass through a 80-mesh sieve to obtain mixed forage powder.
The mixed protein powder is a mixture of fish meal, pea protein powder and seaweed powder in a mass ratio of 2:1: 1.
The compound vitamin is a mixture of vitamin C, vitamin E, vitamin B1 and vitamin B6 according to the mass ratio of 5:2.3:2: 1.2.
Example 6
The preparation method of the feed for sows in the lactation period comprises the following steps:
(1) uniformly mixing 50 parts of mixed fermentation product, 30 parts of mixed forage powder, 10 parts of mixed protein powder, 2 parts of compound vitamin and 20 parts of water in parts by weight to obtain mixed feed;
(2) and (2) placing the mixed feed obtained in the step (1) into a feed granulator for granulation to obtain the feed for the sows in the lactation period, wherein the particle size is 1 cm.
The preparation method of the mixed fermentation product comprises the following steps:
s1: uniformly mixing 40 parts of corn flour, 40 parts of sorghum flour, 20 parts of wheat bran, 15 parts of bean curd residue and 40 parts of water in parts by weight to obtain a crude mixture;
s2: uniformly mixing 18 parts of modified zeolite powder, 0.5 part of bacillus subtilis and 100 parts of the crude mixture obtained in the step S1 according to parts by weight to obtain a fermentation substrate;
s3: and (4) placing the fermentation substrate obtained in the step (S2) into a fermentation tank, and sealing and fermenting for 36 hours at 25 ℃ to obtain a mixed fermentation product.
The preparation method of the modified zeolite powder comprises the following steps:
putting zeolite powder into a tubular furnace, heating to 420 ℃ at an initial temperature of 25 ℃ at a heating rate of 5 ℃/min, keeping for 2 hours, then cooling to 80 ℃ at a cooling rate of 10 ℃/min, transferring to 5 ℃ and keeping for 30 minutes to obtain modified zeolite powder;
the preparation method of the mixed forage powder comprises the following steps: according to the weight parts, 20 parts of pasture, 5 parts of caulis spatholobi, 5 parts of acanthopanax sessiliflorus, 5 parts of cowherb seed, 10 parts of dandelion and 5 parts of rehmannia are crushed by a beater and pass through a 80-mesh sieve to obtain mixed forage powder.
The mixed protein powder is a mixture of fish meal, pea protein powder and seaweed powder in a mass ratio of 2:1: 1.
The compound vitamin is a mixture of vitamin C, vitamin E, vitamin B1 and vitamin B6 according to the mass ratio of 5:2.3:2: 1.2.
Comparative example 1
The preparation method of the feed for sows in the lactation period comprises the following steps:
(1) uniformly mixing 50 parts of mixed fermentation product, 30 parts of mixed forage powder, 10 parts of mixed protein powder, 2 parts of compound vitamin and 20 parts of water in parts by weight to obtain mixed feed;
(2) and (2) placing the mixed feed obtained in the step (1) into a feed granulator for granulation to obtain the feed for the sows in the lactation period, wherein the particle size is 1 cm.
The preparation method of the mixed fermentation product comprises the following steps:
s1: uniformly mixing 40 parts of corn flour, 40 parts of sorghum flour, 20 parts of wheat bran, 15 parts of bean curd residue and 40 parts of water in parts by weight to obtain a crude mixture;
s2: uniformly mixing 18 parts by weight of zeolite powder, 0.5 part by weight of bacillus subtilis and 100 parts by weight of the crude mixture obtained in the step S1 to obtain a fermentation substrate;
s3: and (4) placing the fermentation substrate obtained in the step (S2) into a fermentation tank, and sealing and fermenting for 36 hours at 25 ℃ to obtain a mixed fermentation product.
The preparation method of the mixed forage powder comprises the following steps:
according to the weight parts, 20 parts of pasture, 5 parts of caulis spatholobi, 5 parts of acanthopanax sessiliflorus, 5 parts of cowherb seed, 10 parts of dandelion and 5 parts of rehmannia are crushed by a beater and pass through a 80-mesh sieve to obtain mixed forage powder.
The mixed protein powder is prepared from fish meal, pea protein powder and seaweed powder according to a mass ratio of 2:1:1, in a mixture of the components.
The compound vitamin comprises vitamin C, vitamin E, vitamin B1 and vitamin B6 according to the mass ratio of 5:2.3:2:1.2 of the composition.
Test example 1
The sanitation indexes of the feeds for the lactating sows in the examples and the comparative examples are tested, the test standards adopt GB 13078-.
Table 1: hygiene index test
Figure BDA0003331657430000161
The zeolite powder is a molecular sieve with honeycomb-like crystals, can adsorb low molecular compounds, toxic compounds, mycotoxin and the like, adsorbs heavy metals through cation exchange characteristics, and is discharged out of a body, and has certain antibacterial performance and heavy metal adsorption performance, and toxins and heavy metals are discharged out of the body along with the metabolism of the body. After the zeolite powder is modified, the pore structure is more stable, the comparative area is larger, sulfur-containing amino acid is fixed on the surface of the zeolite powder, the silicon content on the surface of the zeolite powder is reduced, the porosity is improved, the average crystal and particle size of the silicon-containing zeolite powder material are reduced, and the antibacterial property, adsorbability and cation exchange property of the zeolite powder are further enhanced.
Test example 2
The lactation performance test of the sows in the lactation period is carried out on the feed for the sows in the lactation period in the examples and the comparative examples, 140 sows which are just produced are selected, randomly divided into 7 groups, and 20 sows in each group are fed by adopting the feed for the sows in the lactation period in the examples and the comparative examples respectively, and the feeding management is carried out according to the daily management rules of a pig farm.
Wherein: average daily lactation yield of sows (total milk yield of sows in 2-21 days after production) is 400; the average diarrhea rate of the sows is 400 per 2-21 days of postnatal diarrhea of each group of sows; the average incidence rate of milk fever of the sows is the total frequency/400 of the milk fever diseases of each group of sows occurring within the 2 nd to 21 th days after delivery, and the test results are shown in the table 2.
Table 2: sow lactation performance test
Figure BDA0003331657430000171
The modified zeolite powder has a honeycomb network crystal structure, enters a pig body through an oral cavity, is absorbed by intestinal mucosa and enters blood and lymph tissue, has higher specific surface area and adsorption capacity, can adsorb microorganisms such as low molecular compounds, toxic compounds, mycotoxin and the like in the body, dissolves some small molecular substances and discharges the small molecular substances out of the body; the modified zeolite powder can be used as an adsorbent of heavy metals to adsorb lead, chromium, copper and the like through cation exchange characteristics, and the antibacterial and anti-diarrhea functions of the feed for the lactating sows added with the modified zeolite powder are obviously enhanced;
the selenium-rich yeast and the calcium-rich yeast are introduced with sulfur-containing amino acid to modify the zeolite powder, selenium and calcium in the yeast are fixed on the amino acid on the surface of the zeolite powder, and the zeolite powder is further modified to improve the porosity, adsorption capacity and ion exchange performance of the zeolite powder. The modified zeolite powder and the generated sodium bisulfite can be used for chemical detoxification of mycotoxin in the pig feed, can effectively reduce the harm of joint protection mycotoxin to the intestinal tracts of pigs, keep healthy intestinal tracts and obviously enhance the diarrhea resistance function; after the delivery of the sow, the calcium requirement of the produced milk is suddenly increased, the secretion of the parathyroid hormone and the calcitonin cannot adapt to the sudden change, postpartum paralysis is caused when the sow is lack of calcium, namely, the symptoms of milk fever are caused, the feed for the lactating sow added with the calcium-rich yeast and the modified zeolite powder can improve the resistance of the sow and can also participate in adjusting the calcium stabilizing matrix of the postpartum sow, the ash content, the calcium content and the phosphorus content of the cavity bone are increased, the calcium content in the serum is adjusted, the occurrence of the milk fever is avoided, and the milk secretion quality is improved.

Claims (10)

1. The preparation method of the feed for sows in the lactation period is characterized by comprising the following steps:
(1) uniformly mixing the mixed fermentation product, the mixed forage powder, the mixed protein powder, the compound vitamin and the water to obtain a mixed feed;
(2) and (3) placing the mixed feed obtained in the step (1) into a feed granulator for granulation to obtain the feed for the sows in the lactation period.
2. The method for preparing the feed for sows in lactation according to claim 1, wherein the method for preparing the mixed fermentation product comprises the following steps:
s1: uniformly mixing 30-50 parts of corn flour, 30-50 parts of sorghum flour, 15-25 parts of wheat bran, 10-20 parts of bean curd residue and 30-50 parts of water in parts by weight to obtain a coarse mixture;
s2: uniformly mixing 8-20 parts by weight of modified zeolite powder, 0.4-0.6 part by weight of bacillus subtilis and 80-120 parts by weight of the crude mixture obtained in the step S1 to obtain a fermentation substrate;
s3: and (4) placing the fermentation substrate obtained in the step (S2) into a fermentation tank, and sealing and fermenting for 30-40 hours at 23-27 ℃ to obtain a mixed fermentation product.
3. The preparation method of the feed for sows in lactation as claimed in claim 2, wherein the preparation method of the modified zeolite powder comprises the following steps:
t1: putting the zeolite powder into a tubular furnace, heating to 400-420 ℃ at the initial temperature of 20-30 ℃ at the heating rate of 4-6 ℃/min, keeping for 1-3 hours, then cooling to 70-90 ℃ at the cooling rate of 8-12 ℃/min, transferring to 4-6 ℃ and keeping for 20-40 minutes to obtain physically modified zeolite powder;
t2: adding 15-25 parts by weight of the physically modified zeolite powder obtained in the step T1 into 40-60 parts by weight of the modification solution, uniformly mixing, soaking at 50-70 ℃ for 2-4 hours, and filtering to obtain a filter cake to obtain a mixture A;
t3: and (4) transferring the mixture A obtained in the step T2 to an oven at 50-70 ℃ for drying for 8-12 hours to obtain the modified zeolite powder.
4. The method for preparing the feed for sows in lactation as claimed in claim 3, wherein the method for preparing the modified liquid comprises the following steps: adding 4-6 parts by weight of silane coupling agent, 15-25 parts by weight of sulfur-containing amino acid and 5-7 parts by weight of functional yeast liquid into 40-60 parts by weight of water, and uniformly mixing to obtain the modified liquid.
5. The method for preparing the feed for sows in lactation according to claim 4, wherein the method for preparing the functionalized yeast liquid comprises the following steps: according to the weight portion, 1-2 portions of yeast are inoculated on 90-110 portions of liquid culture medium, and cultured for 1-2 days at 28-30 ℃ to obtain the functionalized yeast liquid.
6. The method of preparing a feed for lactating sows as claimed in claim 5, wherein the liquid medium consists of, in parts by weight, 10 to 15 parts of honey, 10 parts of a functional agent, 0.5 to 1 part of glucose, 0.3 to 0.5 part of peptone and 80 to 100 parts of water.
7. The method for preparing the feed for sows in lactation according to claim 1, wherein the method for preparing the mixed forage comprises the following steps: according to the weight portion, 10-30 portions of pasture, 3-7 portions of caulis spatholobi, 3-7 portions of acanthopanax sessiliflorus, 3-7 portions of cowherb seed, 8-12 portions of dandelion and 3-7 portions of rehmannia are crushed by a beater and pass through a 60-100 mesh sieve, and the mixed forage powder is obtained.
8. The method for preparing the feed for sows in lactation according to claim 1, wherein the mixed protein powder is a mixture of fish meal, pea protein powder and seaweed powder in a mass ratio of (1-3):1.
9. The method for preparing a feed for lactating sows as in claim 1, wherein the vitamin complex is a mixture of vitamin C, vitamin E, vitamin B1 and vitamin B6 in a mass ratio of (4-6): 2-3): 1-3): 1.2.
10. A feed for sows in lactation prepared by the process of any one of claims 1 to 9.
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