CN113981613A - 一种熔喷过滤材料及其制备方法 - Google Patents

一种熔喷过滤材料及其制备方法 Download PDF

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CN113981613A
CN113981613A CN202111226530.4A CN202111226530A CN113981613A CN 113981613 A CN113981613 A CN 113981613A CN 202111226530 A CN202111226530 A CN 202111226530A CN 113981613 A CN113981613 A CN 113981613A
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顾运顺
许坚
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Shanghai Doujing Environmental Protection Technology Co ltd
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    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/54Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by welding together the fibres, e.g. by partially melting or dissolving
    • D04H1/542Adhesive fibres
    • D04H1/544Olefin series
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D1/00Treatment of filament-forming or like material
    • D01D1/10Filtering or de-aerating the spinning solution or melt
    • D01D1/106Filtering
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/10Other agents for modifying properties
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/44Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds
    • D01F6/46Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds of polyolefins
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H1/00Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
    • D04H1/40Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
    • D04H1/54Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by welding together the fibres, e.g. by partially melting or dissolving
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/01Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with hydrogen, water or heavy water; with hydrides of metals or complexes thereof; with boranes, diboranes, silanes, disilanes, phosphines, diphosphines, stibines, distibines, arsines, or diarsines or complexes thereof
    • D06M11/05Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with hydrogen, water or heavy water; with hydrides of metals or complexes thereof; with boranes, diboranes, silanes, disilanes, phosphines, diphosphines, stibines, distibines, arsines, or diarsines or complexes thereof with water, e.g. steam; with heavy water
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    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16Synthetic fibres, other than mineral fibres
    • D06M2101/18Synthetic fibres consisting of macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/20Polyalkenes, polymers or copolymers of compounds with alkenyl groups bonded to aromatic groups
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    • D10B2401/06Load-responsive characteristics
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Abstract

本发明涉及过滤材料技术领域,尤其是一种熔喷过滤材料,包括聚丙烯、水柱极母粒、碳酸钙、增韧剂。还公开了一种熔喷过滤材料的制备方法,将聚丙烯、水柱极母粒、碳酸钙、增韧剂称量混合后加入挤出机料仓,混合料在料仓烘干后进入挤出机,挤出机的1‑7区温度均为165‑240℃,经过熔体箱过滤后通过计量泵输送至模头及喷丝板喷出,喷丝板喷出的丝经过超纯水在线水柱极水幕后吸附到成网上成型,最后经过80‑110℃的烘箱烘干后收卷,即得到熔喷过滤材料。本发明所得到的一种熔喷过滤材料及其制备方法,能有效增加材料的硬度,同时保证其韧性,不易断裂,使其具有玻璃纤维或者符合材料的性能。

Description

一种熔喷过滤材料及其制备方法
技术领域
本发明涉及过滤材料技术领域,尤其是一种熔喷过滤材料及其制备方法。
背景技术
现有技术中,对于聚丙烯熔喷后形成的过滤材料,其材料比较柔软,硬挺度不高,所以使用过程中具有很大的限制,尤其是打折后没有挺度,对材料折叠成型后,使用效果差。
发明内容
本发明为了解决上述技术不足而提供一种熔喷过滤材料及其制备方法,其能有效增加材料的硬度及韧性,提升性能。
本发明公开了一种熔喷过滤材料,包括聚丙烯、水柱极母粒、碳酸钙、增韧剂,其中各组分的质量分数为:聚丙烯100分、水柱极母粒1-4份、碳酸钙7-20份、增韧剂2-10份。其中增韧剂为梦色丽(上海)材料科技有限公司生产的F82型号增韧剂。
所述聚丙烯的容值为1500-1800g/10min。
所述碳酸钙的颗粒粗细为1000-3000目。
一种熔喷过滤材料的制备方法,将聚丙烯、水柱极母粒、碳酸钙、增韧剂称量混合后加入挤出机料仓,混合料在料仓烘干后进入挤出机,挤出机的1-7区温度均为165-240℃,经过熔体箱过滤后通过计量泵输送至模头及喷丝板喷出,喷丝板喷出的丝经过超纯水在线水柱极水幕后吸附到成网上成型,最后经过80-110℃的烘箱烘干后收卷,即得到熔喷过滤材料。
其中挤出机一区温度为165-175℃、二区温度为180-190℃、三区温度为195-215℃、四区温度为220-225℃、五区温度为225-230℃、六区温度为230-235℃、七区温度为235-240℃;经烘箱烘干后过一道热风去除水汽,最后收卷,如缺少除湿会造成收卷后的布料内有水汽。
熔体箱内过滤过程中的过滤网精度为300-500目。
本发明所得到的一种熔喷过滤材料及其制备方法,能有效增加材料的硬挺度,同时保证其韧性,不易断裂,使其具有玻纤或者复合材料的使用性能。
本发明所得到的熔喷过滤材料,其相对于玻纤相同过滤效率的条件下具有更低的过滤阻力,达到高效低阻的高标准过滤性能。
具体实施方式
为更进一步阐述本发明为实现预定发明目的所采取的技术手段及功效,以下结合较佳实施例,对依据本发明的具体实施方式、结构、特征及其功效,详细说明如后。
实施例1:
本发明公开了一种熔喷过滤材料,包括聚丙烯、水柱极母粒、碳酸钙、增韧剂,其中各组分的质量分数为:聚丙烯100分、水柱极母粒1份、碳酸钙7份、增韧剂2份。
所述聚丙烯的容值为1500g/10min。
所述碳酸钙的颗粒粗细为1000目。
一种熔喷过滤材料的制备方法,将聚丙烯、水柱极母粒、碳酸钙、增韧剂称量混合后加入挤出机料仓,混合料在料仓烘干后进入挤出机,挤出机一区温度为165℃、二区温度为180℃、三区温度为195℃、四区温度为220℃、五区温度为225℃、六区温度为230℃、七区温度为235℃;经过熔体箱过滤后通过计量泵输送至模头及喷丝板喷出,喷丝板喷出的丝经过超纯水在线水柱极水幕后吸附到成网上成型,最后经过80℃的烘箱烘干,利用热风吹干过滤材料上的水汽后收卷,即得到熔喷过滤材料。
熔体箱内过滤过程中的过滤网精度为300目。
实施例2:
本发明公开了一种熔喷过滤材料,包括聚丙烯、水柱极母粒、碳酸钙、增韧剂,其中各组分的质量分数为:聚丙烯100分、水柱极母粒4份、碳酸钙20份、增韧剂10份。
所述聚丙烯的容值为1800g/10min。
所述碳酸钙的颗粒粗细为3000目。
一种熔喷过滤材料的制备方法,将聚丙烯、水柱极母粒、碳酸钙、增韧剂称量混合后加入挤出机料仓,混合料在料仓烘干后进入挤出机,挤出机一区温度为175℃、二区温度为190℃、三区温度为215℃、四区温度为225℃、五区温度为230℃、六区温度为235℃、七区温度为240℃;经过熔体箱过滤后通过计量泵输送至模头及喷丝板喷出,喷丝板喷出的丝经过超纯水在线水柱极水幕后吸附到成网上成型,最后经过110℃的烘箱烘干,利用热风吹干过滤材料上的水汽后收卷,即得到熔喷过滤材料。
熔体箱内过滤过程中的过滤网精度为500目。
实施例3:
本发明公开了一种熔喷过滤材料,包括聚丙烯、水柱极母粒、碳酸钙、增韧剂,其中各组分的质量分数为:聚丙烯100分、水柱极母粒2份、碳酸钙16份、增韧剂7份。
所述聚丙烯的容值为1600g/10min。
所述碳酸钙的颗粒粗细为2000目。
一种熔喷过滤材料的制备方法,将聚丙烯、水柱极母粒、碳酸钙、增韧剂称量混合后加入挤出机料仓,混合料在料仓烘干后进入挤出机,挤出机一区温度为170℃、二区温度为185℃、三区温度为205℃、四区温度为223℃、五区温度为228℃、六区温度为232℃、七区温度为238℃;经过熔体箱过滤后通过计量泵输送至模头及喷丝板喷出,喷丝板喷出的丝经过超纯水在线水柱极水幕后吸附到成网上成型,最后经过100℃的烘箱烘干,利用热风吹干过滤材料上的水汽后收卷,即得到熔喷过滤材料。
熔体箱内过滤过程中的过滤网精度为400目。
实施例4:
本发明公开了一种熔喷过滤材料,包括聚丙烯、水柱极母粒、碳酸钙、增韧剂,其中各组分的质量分数为:聚丙烯100分、水柱极母粒3份、碳酸钙12份、增韧剂5份。
所述聚丙烯的容值为1700g/10min。
所述碳酸钙的颗粒粗细为2500目。
一种熔喷过滤材料的制备方法,将聚丙烯、水柱极母粒、碳酸钙、增韧剂称量混合后加入挤出机料仓,混合料在料仓烘干后进入挤出机,挤出机一区温度为175℃、二区温度为185℃、三区温度为210℃、四区温度为225℃、五区温度为230℃、六区温度为235℃、七区温度为240℃;经过熔体箱过滤后通过计量泵输送至模头及喷丝板喷出,喷丝板喷出的丝经过超纯水在线水柱极水幕后吸附到成网上成型,最后经过90℃的烘箱烘干,利用热风吹干过滤材料上的水汽后收卷,即得到熔喷过滤材料。
熔体箱内过滤过程中的过滤网精度为400目。
以上所述,仅是本发明的较佳实施例而已,并非对本发明作任何形式上的限制,虽然本发明已以较佳实施例揭示如上,然而并非用以限定本发明,任何本领域技术人员,在不脱离本发明技术方案范围内,当可利用上述揭示的技术内容做出些许更动或修饰为等同变化的等效实施例,但凡是未脱离本发明技术方案内容,依据本发明的技术实质对以上实施例所作的任何简化修改、等同变化与修饰,均仍属于本发明技术方案的范围内。

Claims (5)

1.一种熔喷过滤材料,其特征是:包括聚丙烯、水柱极母粒、碳酸钙、增韧剂,其中各组分的质量分数为:聚丙烯100分、水柱极母粒1-4份、碳酸钙7-20份、增韧剂2-10份。
2.根据权利要求1所述的一种熔喷过滤材料,其特征是:所述聚丙烯的容值为1500-1800g/10min。
3.根据权利要求1所述的一种熔喷过滤材料,其特征是:所述碳酸钙的颗粒粗细为1000-3000目。
4.一种熔喷过滤材料的制备方法,其特征是:将聚丙烯、水柱极母粒、碳酸钙、增韧剂称量混合后加入挤出机料仓,混合料在料仓烘干后进入挤出机,挤出机的1-7区温度均为165-240℃,经过熔体箱过滤后通过计量泵输送至模头及喷丝板喷出,喷丝板喷出的丝经过超纯水在线水柱极水幕后吸附到成网上成型,最后经过80-110℃的烘箱烘干后收卷,即得到熔喷过滤材料。
5.根据权利要求4所述的一种熔喷过滤材料的制备方法,其特征是:熔体箱内过滤过程中的过滤网精度为300-500目。
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