CN113502196A - 一种温和不刺激皂苷组合物的制备方法及其应用 - Google Patents
一种温和不刺激皂苷组合物的制备方法及其应用 Download PDFInfo
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- CN113502196A CN113502196A CN202110681540.0A CN202110681540A CN113502196A CN 113502196 A CN113502196 A CN 113502196A CN 202110681540 A CN202110681540 A CN 202110681540A CN 113502196 A CN113502196 A CN 113502196A
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- Prior art keywords
- saponin
- mild non
- irritating
- resin
- saponin composition
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229930182490 saponin Natural products 0.000 title claims abstract description 49
- 150000007949 saponins Chemical class 0.000 title claims abstract description 49
- 239000001397 quillaja saponaria molina bark Substances 0.000 title claims abstract description 46
- 239000000203 mixture Substances 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 239000002085 irritant Substances 0.000 title claims abstract description 7
- 231100000021 irritant Toxicity 0.000 title claims abstract description 7
- 239000011347 resin Substances 0.000 claims abstract description 33
- 229920005989 resin Polymers 0.000 claims abstract description 33
- 238000003756 stirring Methods 0.000 claims abstract description 29
- 239000007788 liquid Substances 0.000 claims abstract description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 238000001179 sorption measurement Methods 0.000 claims abstract description 22
- 238000000034 method Methods 0.000 claims abstract description 21
- 241000931143 Gleditsia sinensis Species 0.000 claims abstract description 20
- 239000006228 supernatant Substances 0.000 claims abstract description 18
- 239000002244 precipitate Substances 0.000 claims abstract description 17
- 239000012153 distilled water Substances 0.000 claims abstract description 14
- 239000000843 powder Substances 0.000 claims abstract description 14
- 239000000706 filtrate Substances 0.000 claims abstract description 12
- -1 inorganic acid salt Chemical class 0.000 claims abstract description 11
- 238000000605 extraction Methods 0.000 claims abstract description 10
- 239000012535 impurity Substances 0.000 claims abstract description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 9
- 238000001914 filtration Methods 0.000 claims abstract description 8
- 239000008394 flocculating agent Substances 0.000 claims abstract description 8
- 150000007522 mineralic acids Chemical class 0.000 claims abstract description 7
- 238000000909 electrodialysis Methods 0.000 claims abstract description 6
- 239000000284 extract Substances 0.000 claims abstract description 6
- 239000011552 falling film Substances 0.000 claims abstract description 6
- 238000007710 freezing Methods 0.000 claims abstract description 6
- 230000008014 freezing Effects 0.000 claims abstract description 6
- 238000005352 clarification Methods 0.000 claims abstract description 5
- 238000007670 refining Methods 0.000 claims abstract description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 47
- 239000004925 Acrylic resin Substances 0.000 claims description 23
- 229920002401 polyacrylamide Polymers 0.000 claims description 23
- 125000000129 anionic group Chemical group 0.000 claims description 20
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 19
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 claims description 19
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 18
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 18
- 150000003333 secondary alcohols Chemical class 0.000 claims description 18
- IQDGSYLLQPDQDV-UHFFFAOYSA-N dimethylazanium;chloride Chemical compound Cl.CNC IQDGSYLLQPDQDV-UHFFFAOYSA-N 0.000 claims description 17
- 239000000440 bentonite Substances 0.000 claims description 16
- 229910000278 bentonite Inorganic materials 0.000 claims description 16
- 231100000344 non-irritating Toxicity 0.000 claims description 15
- 229920000178 Acrylic resin Polymers 0.000 claims description 14
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims description 9
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 claims description 6
- 239000012752 auxiliary agent Substances 0.000 claims description 6
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 5
- 239000000920 calcium hydroxide Substances 0.000 claims description 5
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims description 5
- 230000008569 process Effects 0.000 claims description 4
- 229920000289 Polyquaternium Polymers 0.000 claims description 3
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 3
- SRSXLGNVWSONIS-UHFFFAOYSA-N benzenesulfonic acid Chemical compound OS(=O)(=O)C1=CC=CC=C1 SRSXLGNVWSONIS-UHFFFAOYSA-N 0.000 claims description 3
- 229940092714 benzenesulfonic acid Drugs 0.000 claims description 3
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims description 2
- 229920001568 phenolic resin Polymers 0.000 claims description 2
- 239000003822 epoxy resin Substances 0.000 claims 1
- 239000005007 epoxy-phenolic resin Substances 0.000 claims 1
- 229920000647 polyepoxide Polymers 0.000 claims 1
- 239000000047 product Substances 0.000 abstract description 13
- 230000000694 effects Effects 0.000 abstract description 12
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- 230000000052 comparative effect Effects 0.000 description 24
- 239000004005 microsphere Substances 0.000 description 23
- 239000004094 surface-active agent Substances 0.000 description 15
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 14
- 229910052739 hydrogen Inorganic materials 0.000 description 10
- 239000001257 hydrogen Substances 0.000 description 10
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 8
- 229910021645 metal ion Inorganic materials 0.000 description 8
- 239000005909 Kieselgur Substances 0.000 description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical group OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 6
- RPNUMPOLZDHAAY-UHFFFAOYSA-N Diethylenetriamine Chemical compound NCCNCCN RPNUMPOLZDHAAY-UHFFFAOYSA-N 0.000 description 5
- 241000196324 Embryophyta Species 0.000 description 5
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- 239000008367 deionised water Substances 0.000 description 5
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- 238000005406 washing Methods 0.000 description 5
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 239000004744 fabric Substances 0.000 description 4
- 150000002500 ions Chemical class 0.000 description 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 3
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- 239000002131 composite material Substances 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 3
- 238000005189 flocculation Methods 0.000 description 3
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- 238000006386 neutralization reaction Methods 0.000 description 3
- 229920000768 polyamine Polymers 0.000 description 3
- 244000044167 Acacia concinna Species 0.000 description 2
- 235000015841 Acacia concinna Nutrition 0.000 description 2
- 239000004593 Epoxy Substances 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 240000003377 Shepherdia canadensis Species 0.000 description 2
- 235000018324 Shepherdia canadensis Nutrition 0.000 description 2
- DWAQJAXMDSEUJJ-UHFFFAOYSA-M Sodium bisulfite Chemical group [Na+].OS([O-])=O DWAQJAXMDSEUJJ-UHFFFAOYSA-M 0.000 description 2
- 229920002125 Sokalan® Polymers 0.000 description 2
- 241001122767 Theaceae Species 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
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- 235000010267 sodium hydrogen sulphite Nutrition 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 150000008130 triterpenoid saponins Chemical class 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- INLFWQCRAJUDCR-IQVMEADQSA-N (1R,2S,4S,5'S,6R,7S,8R,9S,12S,13S)-5',7,9,13-tetramethylspiro[5-oxapentacyclo[10.8.0.02,9.04,8.013,18]icosane-6,2'-oxane] Chemical compound O([C@@H]1[C@@H]([C@]2(CC[C@@H]3[C@@]4(C)CCCCC4CC[C@H]3[C@@H]2C1)C)[C@@H]1C)[C@]11CC[C@H](C)CO1 INLFWQCRAJUDCR-IQVMEADQSA-N 0.000 description 1
- 240000001548 Camellia japonica Species 0.000 description 1
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 description 1
- 206010015946 Eye irritation Diseases 0.000 description 1
- 241000533849 Gleditsia Species 0.000 description 1
- 102000001554 Hemoglobins Human genes 0.000 description 1
- 108010054147 Hemoglobins Proteins 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 241001494479 Pecora Species 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 241000580938 Sapindus Species 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
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- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
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- 229930182495 oleanane-type triterpene Natural products 0.000 description 1
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- 239000005011 phenolic resin Substances 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
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- 229910052708 sodium Inorganic materials 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/825—Mixtures of compounds all of which are non-ionic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Abstract
Description
实施例 | 刺激性H/D | 表面张力(mN/m) |
实施例1 | 15.2 | 42.5 |
实施例2 | 14.9 | 42.1 |
实施例3 | 14.7 | 42.4 |
实施例4 | 15.1 | 41.9 |
对比例1 | 8.7 | 38.4 |
对比例2 | 9.2 | 39.1 |
对比例3 | 7.4 | 35.6 |
对比例4 | 7.9 | 37.7 |
对比例5 | 8.5 | 38.7 |
对比例6 | 8.2 | 38.9 |
Claims (10)
Priority Applications (1)
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CN202110681540.0A CN113502196B (zh) | 2021-06-19 | 2021-06-19 | 一种温和不刺激皂苷组合物的制备方法及其应用 |
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CN202110681540.0A CN113502196B (zh) | 2021-06-19 | 2021-06-19 | 一种温和不刺激皂苷组合物的制备方法及其应用 |
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Publication Number | Publication Date |
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CN113502196A true CN113502196A (zh) | 2021-10-15 |
CN113502196B CN113502196B (zh) | 2023-05-09 |
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Country Status (1)
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Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6156817A (en) * | 1998-11-12 | 2000-12-05 | Kabushiki Kaisha Erubu | Functional form and process for the production of the same |
US20070041924A1 (en) * | 2005-08-19 | 2007-02-22 | Bioderm Research | Sebum Control Compositions Based on Saponins and Sapogenins |
CN101401897A (zh) * | 2008-11-06 | 2009-04-08 | 云南白药集团股份有限公司 | 重楼皂苷提取液的除杂纯化方法 |
CN102241725A (zh) * | 2010-05-13 | 2011-11-16 | 福建源华林业生物科技有限公司 | 日化用无患子皂苷的水提制备方法 |
CN104921998A (zh) * | 2015-06-24 | 2015-09-23 | 陈琳仁 | 一种无患子色素、皂苷和多糖的同时提取工艺及无患子皂苷的制备与应用 |
CN112110979A (zh) * | 2020-10-26 | 2020-12-22 | 长沙中战茶油集团有限公司 | 一种提取茶皂素的方法 |
-
2021
- 2021-06-19 CN CN202110681540.0A patent/CN113502196B/zh active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6156817A (en) * | 1998-11-12 | 2000-12-05 | Kabushiki Kaisha Erubu | Functional form and process for the production of the same |
US20070041924A1 (en) * | 2005-08-19 | 2007-02-22 | Bioderm Research | Sebum Control Compositions Based on Saponins and Sapogenins |
CN101401897A (zh) * | 2008-11-06 | 2009-04-08 | 云南白药集团股份有限公司 | 重楼皂苷提取液的除杂纯化方法 |
CN102241725A (zh) * | 2010-05-13 | 2011-11-16 | 福建源华林业生物科技有限公司 | 日化用无患子皂苷的水提制备方法 |
CN104921998A (zh) * | 2015-06-24 | 2015-09-23 | 陈琳仁 | 一种无患子色素、皂苷和多糖的同时提取工艺及无患子皂苷的制备与应用 |
CN112110979A (zh) * | 2020-10-26 | 2020-12-22 | 长沙中战茶油集团有限公司 | 一种提取茶皂素的方法 |
Non-Patent Citations (2)
Title |
---|
刘锁兰 主编: "《中药学专业知识(一)第1版》", 30 April 2016, 中国医药科技出版社 * |
杜方麓 等主编: "《中药化学(第1版)》", 30 June 2006, 中国中医药出版社出版 * |
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Effective date of registration: 20240219 Address after: 528437 card 1402, floor 14, Beiji building, No. 6, Xiangxing Road, Torch Development Zone, Zhongshan City, Guangdong Province Patentee after: Guangdong jingcui Biotechnology Co.,Ltd. Country or region after: China Address before: 528437 card 1402, floor 14, Beiji building, No. 6, Xiangxing Road, Torch Development Zone, Zhongshan City, Guangdong Province Patentee before: Guangdong jingcui Biotechnology Co.,Ltd. Country or region before: China Patentee before: Institute of Biophysics, Chinese Academy of Sciences |