CN113150704B - 一种稳定性好的抗酸膜及其制备方法 - Google Patents
一种稳定性好的抗酸膜及其制备方法 Download PDFInfo
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- CN113150704B CN113150704B CN202110473363.7A CN202110473363A CN113150704B CN 113150704 B CN113150704 B CN 113150704B CN 202110473363 A CN202110473363 A CN 202110473363A CN 113150704 B CN113150704 B CN 113150704B
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- acid
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- adhesive
- resistant film
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- 239000002253 acid Substances 0.000 title claims abstract description 90
- 238000002360 preparation method Methods 0.000 title abstract description 37
- 239000010410 layer Substances 0.000 claims abstract description 76
- 239000000853 adhesive Substances 0.000 claims abstract description 68
- 230000001070 adhesive effect Effects 0.000 claims abstract description 68
- 229920001084 poly(chloroprene) Polymers 0.000 claims abstract description 68
- 239000002048 multi walled nanotube Substances 0.000 claims abstract description 54
- 239000003292 glue Substances 0.000 claims abstract description 38
- 239000012790 adhesive layer Substances 0.000 claims abstract description 32
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 66
- DMBHHRLKUKUOEG-UHFFFAOYSA-N diphenylamine Chemical compound C=1C=CC=CC=1NC1=CC=CC=C1 DMBHHRLKUKUOEG-UHFFFAOYSA-N 0.000 claims description 56
- 239000010954 inorganic particle Substances 0.000 claims description 48
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical group [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 46
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N 1,4-Benzenediol Natural products OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 claims description 45
- 229920000642 polymer Polymers 0.000 claims description 45
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 39
- 239000006229 carbon black Substances 0.000 claims description 38
- 239000003575 carbonaceous material Substances 0.000 claims description 36
- 239000000843 powder Substances 0.000 claims description 35
- 239000012752 auxiliary agent Substances 0.000 claims description 33
- RGTLAJIDOSPEDH-UHFFFAOYSA-N 3-methyl-1,3-thiazolidine-2-thione Chemical compound CN1CCSC1=S RGTLAJIDOSPEDH-UHFFFAOYSA-N 0.000 claims description 31
- 239000004215 Carbon black (E152) Substances 0.000 claims description 31
- 235000021355 Stearic acid Nutrition 0.000 claims description 31
- 229930195733 hydrocarbon Natural products 0.000 claims description 31
- 150000002430 hydrocarbons Chemical class 0.000 claims description 31
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 31
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims description 31
- 239000002904 solvent Substances 0.000 claims description 31
- 239000008117 stearic acid Substances 0.000 claims description 31
- 239000000463 material Substances 0.000 claims description 24
- 239000000395 magnesium oxide Substances 0.000 claims description 23
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims description 23
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims description 23
- 239000011787 zinc oxide Substances 0.000 claims description 23
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical group OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 22
- 238000005520 cutting process Methods 0.000 claims description 22
- 238000001035 drying Methods 0.000 claims description 20
- 239000002994 raw material Substances 0.000 claims description 20
- 229920001912 maleic anhydride grafted polyethylene Polymers 0.000 claims description 18
- 239000002245 particle Substances 0.000 claims description 17
- 229920001568 phenolic resin Polymers 0.000 claims description 15
- LZDOYVMSNJBLIM-UHFFFAOYSA-N 4-tert-butylphenol;formaldehyde Chemical compound O=C.CC(C)(C)C1=CC=C(O)C=C1 LZDOYVMSNJBLIM-UHFFFAOYSA-N 0.000 claims description 11
- 239000011248 coating agent Substances 0.000 claims description 11
- 238000000576 coating method Methods 0.000 claims description 11
- 125000000687 hydroquinonyl group Chemical group C1(O)=C(C=C(O)C=C1)* 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 9
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims description 5
- 239000005011 phenolic resin Substances 0.000 claims description 5
- 241000722946 Acanthocybium solandri Species 0.000 claims description 2
- 230000020477 pH reduction Effects 0.000 abstract description 25
- 229920003048 styrene butadiene rubber Polymers 0.000 abstract description 13
- 230000000694 effects Effects 0.000 abstract description 5
- 238000007654 immersion Methods 0.000 abstract description 5
- 238000005516 engineering process Methods 0.000 abstract description 4
- 230000009286 beneficial effect Effects 0.000 abstract description 3
- 238000011161 development Methods 0.000 abstract description 3
- 238000011031 large-scale manufacturing process Methods 0.000 abstract description 3
- 229920000181 Ethylene propylene rubber Polymers 0.000 abstract description 2
- 244000043261 Hevea brasiliensis Species 0.000 abstract description 2
- 229920005549 butyl rubber Polymers 0.000 abstract description 2
- 229920006235 chlorinated polyethylene elastomer Polymers 0.000 abstract description 2
- 229920001973 fluoroelastomer Polymers 0.000 abstract description 2
- 229920003052 natural elastomer Polymers 0.000 abstract description 2
- 229920001194 natural rubber Polymers 0.000 abstract description 2
- 238000002156 mixing Methods 0.000 description 55
- 229920001971 elastomer Polymers 0.000 description 35
- 239000005060 rubber Substances 0.000 description 35
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 27
- 239000000126 substance Substances 0.000 description 27
- 230000000052 comparative effect Effects 0.000 description 26
- 239000000203 mixture Substances 0.000 description 22
- 238000010074 rubber mixing Methods 0.000 description 21
- 238000003756 stirring Methods 0.000 description 20
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 description 18
- FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 17
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 14
- 239000002041 carbon nanotube Substances 0.000 description 14
- 229910021393 carbon nanotube Inorganic materials 0.000 description 14
- 238000002791 soaking Methods 0.000 description 14
- 238000007599 discharging Methods 0.000 description 13
- 238000006243 chemical reaction Methods 0.000 description 11
- 238000001816 cooling Methods 0.000 description 11
- 239000000498 cooling water Substances 0.000 description 11
- 239000011521 glass Substances 0.000 description 11
- 239000012046 mixed solvent Substances 0.000 description 11
- 238000005096 rolling process Methods 0.000 description 11
- 229920005989 resin Polymers 0.000 description 10
- 239000011347 resin Substances 0.000 description 10
- 238000005406 washing Methods 0.000 description 10
- QHPQWRBYOIRBIT-UHFFFAOYSA-N 4-tert-butylphenol Chemical compound CC(C)(C)C1=CC=C(O)C=C1 QHPQWRBYOIRBIT-UHFFFAOYSA-N 0.000 description 9
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 9
- 230000001458 anti-acid effect Effects 0.000 description 9
- 239000002086 nanomaterial Substances 0.000 description 9
- 229910017604 nitric acid Inorganic materials 0.000 description 9
- 229920003023 plastic Polymers 0.000 description 9
- 239000004033 plastic Substances 0.000 description 9
- 238000000967 suction filtration Methods 0.000 description 9
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 9
- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 description 9
- 238000009210 therapy by ultrasound Methods 0.000 description 9
- 229910052500 inorganic mineral Inorganic materials 0.000 description 8
- 239000011707 mineral Substances 0.000 description 8
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 230000035515 penetration Effects 0.000 description 5
- 229920000578 graft copolymer Polymers 0.000 description 4
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical group O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- 230000009471 action Effects 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- -1 Polyethylene Polymers 0.000 description 2
- 239000004698 Polyethylene Substances 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000004132 cross linking Methods 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 2
- 150000002989 phenols Chemical class 0.000 description 2
- 229920000573 polyethylene Polymers 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- XESZUVZBAMCAEJ-UHFFFAOYSA-N 4-tert-butylcatechol Chemical compound CC(C)(C)C1=CC=C(O)C(O)=C1 XESZUVZBAMCAEJ-UHFFFAOYSA-N 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 1
- 239000000292 calcium oxide Substances 0.000 description 1
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000013522 chelant Substances 0.000 description 1
- 230000009920 chelation Effects 0.000 description 1
- 230000006355 external stress Effects 0.000 description 1
- 238000005187 foaming Methods 0.000 description 1
- 239000003574 free electron Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 230000035882 stress Effects 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- CNHDIAIOKMXOLK-UHFFFAOYSA-N toluquinol Chemical compound CC1=CC(O)=CC=C1O CNHDIAIOKMXOLK-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/20—Adhesives in the form of films or foils characterised by their carriers
- C09J7/22—Plastics; Metallised plastics
- C09J7/24—Plastics; Metallised plastics based on macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- C09J7/245—Vinyl resins, e.g. polyvinyl chloride [PVC]
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J111/00—Adhesives based on homopolymers or copolymers of chloroprene
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J7/00—Adhesives in the form of films or foils
- C09J7/30—Adhesives in the form of films or foils characterised by the adhesive composition
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Description
项目 | 是否起泡 |
实施例1 | 否 |
实施例2 | 否 |
实施例3 | 否 |
对比例1 | 是 |
对比例2 | 是 |
对比例3 | 是 |
对比例4 | 是 |
对比例5 | 是 |
对比例6 | 是 |
项目 | 有残胶的玻璃块数 |
实施例1 | 0 |
实施例2 | 0 |
实施例3 | 0 |
对比例1 | 12 |
对比例2 | 7 |
对比例3 | 10 |
对比例4 | 8 |
对比例5 | 15 |
对比例6 | 8 |
项目 | 接触角 |
实施例1 | 128 |
实施例2 | 125 |
实施例3 | 126 |
对比例1 | 95 |
对比例2 | 97 |
对比例3 | 100 |
对比例4 | 199 |
对比例5 | 94 |
对比例6 | 93 |
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202110473363.7A CN113150704B (zh) | 2021-04-29 | 2021-04-29 | 一种稳定性好的抗酸膜及其制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202110473363.7A CN113150704B (zh) | 2021-04-29 | 2021-04-29 | 一种稳定性好的抗酸膜及其制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN113150704A CN113150704A (zh) | 2021-07-23 |
CN113150704B true CN113150704B (zh) | 2022-01-04 |
Family
ID=76872318
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN202110473363.7A Active CN113150704B (zh) | 2021-04-29 | 2021-04-29 | 一种稳定性好的抗酸膜及其制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN113150704B (zh) |
Family Cites Families (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103197797B (zh) * | 2013-04-02 | 2017-01-25 | 江西沃格光电股份有限公司 | 抗酸膜及其制备方法和应用 |
CN104004487B (zh) * | 2014-06-12 | 2016-06-01 | 哈尔滨理工大学 | 多壁碳纳米管改性醇溶型聚氨酯胶黏剂的制备方法 |
CN105585971A (zh) * | 2016-03-16 | 2016-05-18 | 苏州锦腾电子科技有限公司 | 一种耐酸碱腐蚀的电气用胶带及其制备方法 |
CN107746683A (zh) * | 2017-11-07 | 2018-03-02 | 张永宏 | 一种耐酸碱胶带 |
CN110484165B (zh) * | 2019-07-18 | 2021-09-24 | 南京利德东方橡塑科技有限公司 | 一种耐高、低温环保型氯丁橡胶胶粘剂及制备方法 |
-
2021
- 2021-04-29 CN CN202110473363.7A patent/CN113150704B/zh active Active
Also Published As
Publication number | Publication date |
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CN113150704A (zh) | 2021-07-23 |
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Address after: 512000 chlor alkali characteristic industrial base of hougongdu Economic Development Zone, Rucheng Town, Ruyuan County, Shaoguan City, Guangdong Province Patentee after: Guangdong Shuocheng Technology Co.,Ltd. Address before: 512000 chlor alkali characteristic industrial base of hougongdu Economic Development Zone, Rucheng Town, Ruyuan County, Shaoguan City, Guangdong Province Patentee before: GUANGDONG SHUOCHENG TECHNOLOGY Co.,Ltd. |
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Denomination of invention: The invention relates to an acid resistant film with good stability and a preparation method thereof Effective date of registration: 20220427 Granted publication date: 20220104 Pledgee: Guangdong Ruyuan Rural Commercial Bank Co.,Ltd. Pledgor: Guangdong Shuocheng Technology Co.,Ltd. Registration number: Y2022980004894 |
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Granted publication date: 20220104 Pledgee: Guangdong Ruyuan Rural Commercial Bank Co.,Ltd. Pledgor: Guangdong Shuocheng Technology Co.,Ltd. Registration number: Y2022980004894 |
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Denomination of invention: A stable acid resistant film and its preparation method Granted publication date: 20220104 Pledgee: Guangdong Ruyuan Rural Commercial Bank Co.,Ltd. Pledgor: Guangdong Shuocheng Technology Co.,Ltd. Registration number: Y2024980013062 |
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