CN113040297A - Environment-friendly fish feed additive and preparation method thereof - Google Patents
Environment-friendly fish feed additive and preparation method thereof Download PDFInfo
- Publication number
- CN113040297A CN113040297A CN202110462029.1A CN202110462029A CN113040297A CN 113040297 A CN113040297 A CN 113040297A CN 202110462029 A CN202110462029 A CN 202110462029A CN 113040297 A CN113040297 A CN 113040297A
- Authority
- CN
- China
- Prior art keywords
- parts
- mixture
- feed additive
- environment
- fish feed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K50/00—Feeding-stuffs specially adapted for particular animals
- A23K50/80—Feeding-stuffs specially adapted for particular animals for aquatic animals, e.g. fish, crustaceans or molluscs
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K10/00—Animal feeding-stuffs
- A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/105—Aliphatic or alicyclic compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/13—Amines
- A61K31/14—Quaternary ammonium compounds, e.g. edrophonium, choline
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/185—Acids; Anhydrides, halides or salts thereof, e.g. sulfur acids, imidic, hydrazonic or hydroximic acids
- A61K31/19—Carboxylic acids, e.g. valproic acid
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/21—Esters, e.g. nitroglycerine, selenocyanates
- A61K31/255—Esters, e.g. nitroglycerine, selenocyanates of sulfoxy acids or sulfur analogues thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/56—Compounds containing cyclopenta[a]hydrophenanthrene ring systems; Derivatives thereof, e.g. steroids
- A61K31/575—Compounds containing cyclopenta[a]hydrophenanthrene ring systems; Derivatives thereof, e.g. steroids substituted in position 17 beta by a chain of three or more carbon atoms, e.g. cholane, cholestane, ergosterol, sitosterol
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/02—Medicinal preparations containing materials or reaction products thereof with undetermined constitution from inanimate materials
- A61K35/10—Peat; Amber; Turf; Humus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/22—Anacardiaceae (Sumac family), e.g. smoketree, sumac or poison oak
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/48—Fabaceae or Leguminosae (Pea or Legume family); Caesalpiniaceae; Mimosaceae; Papilionaceae
- A61K36/484—Glycyrrhiza (licorice)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/70—Polygonaceae (Buckwheat family), e.g. spineflower or dock
- A61K36/708—Rheum (rhubarb)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/71—Ranunculaceae (Buttercup family), e.g. larkspur, hepatica, hydrastis, columbine or goldenseal
- A61K36/718—Coptis (goldthread)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/75—Rutaceae (Rue family)
- A61K36/758—Zanthoxylum, e.g. pricklyash
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
- A61P1/14—Prodigestives, e.g. acids, enzymes, appetite stimulants, antidyspeptics, tonics, antiflatulents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/331—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/33—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
- A61K2236/333—Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
Abstract
The invention discloses an environment-friendly fish feed additive and a preparation method thereof, and relates to the field of aquatic product cultivation, wherein the environment-friendly fish feed additive comprises the following components in parts by weight: 6-9 parts of rheum officinale, 10-20 parts of allicin, 10-15 parts of cornel, 20-30 parts of bile acid, 16-20 parts of fruit acid, 20-35 parts of sodium humate, 5-10 parts of liquorice, 5-8 parts of coptis chinensis, 7-12 parts of sumac and 22-28 parts of choline chloride. The additive is added with the fruit acid and the sodium humate, the ingestion frequency of the fish in sultry weather can be increased through the fruit acid, the effect of increasing appetite can be achieved, the sodium humate can improve the gastrointestinal function, promote gastric secretion, increase appetite, promote nutrient substances to enter organisms more quickly, stimulate the growth of beneficial bacteria in the gastrointestinal tract and inhibit the propagation of putrefying bacteria, and the sodium humate can promote digestion and absorption, so mineral elements in feed compatibility can be better absorbed and utilized.
Description
Technical Field
The invention relates to the field of aquatic product cultivation, in particular to an environment-friendly fish feed additive and a preparation method thereof.
Background
The fish products have higher nutritional value, are very important for improving dietary structure and improving human health level, and along with the increasing health consciousness, the consumption demand and quality requirements of consumers on the fish products are higher and higher, and carps, grass carps and the like are main freshwater cultured fishes in China and account for 33-40% of the total fish culture output.
Most of the existing fish feeds are high in protein and fat, and food which is eaten for a long time easily induces fat to accumulate in the liver for a long time to form fatty liver, damages liver function, causes metabolic disorder, causes large-area death due to liver and gall syndrome, simultaneously has short fish digestive tract and high emptying speed, discharges nutrient substances in the feed out of the body after being absorbed, reduces feed absorption rate, seriously pollutes aquaculture water due to nitrogen and phosphorus in fish discharge and has low aquaculture survival rate due to improper use of additives, and obviously reduces fish appetite in sultry weather, so that the fish growth speed is low.
Disclosure of Invention
The invention aims to: in order to solve the problem, an environment-friendly fish feed additive and a preparation method thereof are provided.
In order to achieve the purpose, the invention provides the following technical scheme: an environment-friendly fish feed additive comprises the following components in parts by weight: 6-9 parts of rheum officinale, 10-20 parts of allicin, 10-15 parts of cornel, 20-30 parts of bile acid, 16-20 parts of fruit acid, 20-35 parts of sodium humate, 5-10 parts of liquorice, 5-8 parts of coptis chinensis, 7-12 parts of sumac and 22-28 parts of choline chloride.
A preparation method of an environment-friendly fish feed additive comprises the following specific steps:
step 1: cleaning radix et rhizoma Rhei, fructus evodiae, Glycyrrhrizae radix, Coptidis rhizoma and folium Toxicodendri in proportion, air drying, and removing excessive water on surface;
step 2: mixing the dried rhubarb, the cornel, the liquorice, the coptis and the lacquer leaves, and then putting the mixture into a drying oven for drying to remove the internal water;
and step 3: pulverizing dried radix et rhizoma Rhei, fructus evodiae, Glycyrrhrizae radix, Coptidis rhizoma and folium Toxicodendri with plant pulverizer, and sieving with 50 mesh sieve to obtain Chinese medicinal mixture;
and 4, step 4: putting the traditional Chinese medicine mixture in the step 3 into ultrasonic extraction equipment, and adding an extraction solvent for extraction;
and 5: after the step 4 is finished, vacuum filtration is adopted to obtain filtrate and filter residue, the filtrate is concentrated to 1/5-1/6 of the original volume in vacuum, and the concentration temperature is 50-65 ℃;
step 6: then, the bile acid, the fruit acid, the allicin, the sodium humate and the choline chloride are added into a stirring reaction kettle one by one according to the proportion and are stirred uniformly, the stirring temperature is 40-50 ℃, and the temperature is kept for 1-1.5 hours after the stirring is finished;
and 7: and (3) adding the extract liquid obtained in the step (5) into the mixture obtained in the step (6), starting the stirring reaction kettle again to enable the extract liquid and the mixture to be uniformly stirred, and naturally cooling the mixture to normal temperature after the mixture is subjected to colloid milling to obtain the fish feed additive finished product.
Preferably, the extraction solvent in step 4 is one of ethanol, water or other organic solvents, and the amount of the extraction solvent is 9-12 times of the amount of the traditional Chinese medicine mixture.
Preferably, the extraction time in the step 5 is 40-50 minutes, and the ultrasonic power is 240-260W.
Preferably, the temperature of the drying oven in the step 2 is 70 ℃, and the drying time is 9 hours.
Preferably, the mixture preparation process in the step 7 is to stir at a constant temperature of 40-50 ℃ for 2-3 hours.
Preferably, the filter residue obtained in the step 5 is subjected to secondary extraction in the mode of the step 4.
Compared with the prior art, the invention has the beneficial effects that:
1. the additive is added with choline chloride and bile acid, and the choline chloride promotes the synthesis of liver lipoprotein, accelerates the transportation of fat in the liver to blood and can promote the recombination of amino acid; can improve the utilization rate of amino acid, especially essential amino acid methionine in vivo, and bile acid can improve lipase activity and promote fat digestion; the anti-oxidation capacity of an organism is improved, the utilization and conversion rate of the fish to fat in the feed are improved, the pollution of nitrogen and phosphorus in excrement of a culture object to a culture water body can be effectively reduced, the excessive accumulation of the fat in the liver and the abdominal cavity is reduced, the fatty liver of the fish is prevented, the liver cells and cell membranes are protected from oxidative damage, and meanwhile, the anti-liver injury and liver injury repairing effects are good, the liver and gall syndrome of the fish can be comprehensively and thoroughly solved, and the disease resistance of the organism is improved;
2. the additive is added with the fruit acid and the sodium humate, the ingestion frequency of the fish in sultry weather can be increased through the fruit acid, the effect of increasing appetite can be achieved, the sodium humate can improve the gastrointestinal function, promote gastric secretion, increase appetite, promote nutrient substances to enter organisms more quickly, stimulate the growth of beneficial bacteria in the gastrointestinal tract and inhibit the propagation of putrefying bacteria, and the sodium humate can promote digestion and absorption, so mineral elements of the feed can be better absorbed and utilized;
3. the fructus evodiae and the true sumac leaves are added into the additive, so that the additive has an insecticidal effect on fishes, the fructus evodiae can relieve the illness state of sick fishes, the food intake is increased, the resistance is improved, the rhubarb, the liquorice and the coptis chinensis are added, the effects of clearing heat and purging fire, cooling blood and detoxifying are achieved, the fat content of fish gland can be reduced, the fat degradation is promoted, the fat deposition in a body is inhibited, the Chinese herbal medicines are extracted by ultrasonic extraction equipment, the drug effect is more obvious than that of the Chinese herbal medicines which are directly added, useless components such as cellulose, wood and the like in the raw materials can be removed, the activity of the medicines in the Chinese herbal medicines is concentrated, the digestion and absorption of the fishes are facilitated, the survival rate is improved, and particularly, the additive has a good prevention and treatment effect.
Detailed Description
The first embodiment is as follows:
an environment-friendly fish feed additive comprises the following components in parts by weight: 6 parts of rhubarb, 10 parts of allicin, 10 parts of cornel, 20 parts of bile acid, 16 parts of fruit acid, 20 parts of sodium humate, 5 parts of liquorice, 5 parts of coptis chinensis, 7 parts of sumac and 22 parts of choline chloride.
A preparation method of an environment-friendly fish feed additive comprises the following specific steps:
step 1: cleaning radix et rhizoma Rhei, fructus evodiae, Glycyrrhrizae radix, Coptidis rhizoma and folium Toxicodendri in proportion, air drying, and removing excessive water on surface;
step 2: mixing the dried rhubarb, the cornel, the liquorice, the coptis and the lacquer leaves, and then putting the mixture into a drying oven for drying to remove the internal water;
and step 3: pulverizing dried radix et rhizoma Rhei, fructus evodiae, Glycyrrhrizae radix, Coptidis rhizoma and folium Toxicodendri with plant pulverizer, and sieving with 50 mesh sieve to obtain Chinese medicinal mixture;
and 4, step 4: putting the traditional Chinese medicine mixture in the step 3 into ultrasonic extraction equipment, and adding an extraction solvent for extraction;
and 5: after the step 4 is finished, vacuum filtration is adopted to obtain filtrate and filter residue, the filtrate is concentrated to 1/5 of the original volume in vacuum, and the concentration temperature is 50 ℃;
step 6: then, the bile acid, the fruit acid, the allicin, the sodium humate and the choline chloride are added into a stirring reaction kettle one by one according to the proportion and stirred uniformly, the stirring temperature is 40 ℃, and the temperature is kept for 1 hour after the stirring is finished;
and 7: and (3) adding the extract liquid obtained in the step (5) into the mixture obtained in the step (6), starting the stirring reaction kettle again to enable the extract liquid and the mixture to be uniformly stirred, and naturally cooling the mixture to normal temperature after the mixture is subjected to colloid milling to obtain the fish feed additive finished product.
In the invention, the solvent extracted in the step 4 is one of ethanol, water or other organic solvents, and the amount of the solvent is 9 times of that of the traditional Chinese medicine mixture.
In the invention, the extraction time in the step 5 is 40 minutes, and the ultrasonic power is 240W.
In the invention, the temperature of the drying box in the step 2 is 70 ℃, and the drying time is 9 hours.
In the invention, the preparation process of the mixture in the step 7 is obtained by stirring for 2 hours at a constant temperature of 40 ℃.
In the invention, the filter residue obtained in the step 5 is extracted for the second time in the mode of the step 4.
Example two:
an environment-friendly fish feed additive comprises the following components in parts by weight: 7 parts of rhubarb, 15 parts of allicin, 12 parts of cornel, 25 parts of bile acid, 18 parts of fruit acid, 25 parts of sodium humate, 7 parts of liquorice, 7 parts of coptis chinensis, 8 parts of lacquer leaves and 24 parts of choline chloride.
A preparation method of an environment-friendly fish feed additive comprises the following specific steps:
step 1: cleaning radix et rhizoma Rhei, fructus evodiae, Glycyrrhrizae radix, Coptidis rhizoma and folium Toxicodendri in proportion, air drying, and removing excessive water on surface;
step 2: mixing the dried rhubarb, the cornel, the liquorice, the coptis and the lacquer leaves, and then putting the mixture into a drying oven for drying to remove the internal water;
and step 3: pulverizing dried radix et rhizoma Rhei, fructus evodiae, Glycyrrhrizae radix, Coptidis rhizoma and folium Toxicodendri with plant pulverizer, and sieving with 50 mesh sieve to obtain Chinese medicinal mixture;
and 4, step 4: putting the traditional Chinese medicine mixture in the step 3 into ultrasonic extraction equipment, and adding an extraction solvent for extraction;
and 5: after the step 4 is finished, vacuum filtration is adopted to obtain filtrate and filter residue, the filtrate is concentrated to 1/6 of the original volume in vacuum, and the concentration temperature is 60 ℃;
step 6: then, the bile acid, the fruit acid, the allicin, the sodium humate and the choline chloride are added into the stirring reaction kettle one by one according to the proportion and are stirred uniformly, the stirring temperature is 58 ℃, and the temperature is kept for 1.5 hours after the stirring is finished;
and 7: and (3) adding the extract liquid obtained in the step (5) into the mixture obtained in the step (6), starting the stirring reaction kettle again to enable the extract liquid and the mixture to be uniformly stirred, and naturally cooling the mixture to normal temperature after the mixture is subjected to colloid milling to obtain the fish feed additive finished product.
In the invention, the solvent extracted in the step 4 is one of ethanol, water or other organic solvents, and the amount of the solvent is 10 times of that of the traditional Chinese medicine mixture.
In the invention, the extraction time in the step 5 is 40-50 minutes, and the ultrasonic power is 240-260W.
In the invention, the temperature of the drying box in the step 2 is 70 ℃, and the drying time is 9 hours.
In the invention, the preparation process of the mixture in the step 7 is obtained by stirring for 3 hours at a constant temperature of 48 ℃.
In the invention, the filter residue obtained in the step 5 is extracted for the second time in the mode of the step 4.
Example three:
an environment-friendly fish feed additive comprises the following components in parts by weight: 9 parts of rhubarb, 20 parts of allicin, 15 parts of cornel, 30 parts of bile acid, 20 parts of fruit acid, 35 parts of sodium humate, 10 parts of liquorice, 8 parts of coptis chinensis, 12 parts of sumac leaf and 28 parts of choline chloride.
A preparation method of an environment-friendly fish feed additive comprises the following specific steps:
step 1: cleaning radix et rhizoma Rhei, fructus evodiae, Glycyrrhrizae radix, Coptidis rhizoma and folium Toxicodendri in proportion, air drying, and removing excessive water on surface;
step 2: mixing the dried rhubarb, the cornel, the liquorice, the coptis and the lacquer leaves, and then putting the mixture into a drying oven for drying to remove the internal water;
and step 3: pulverizing dried radix et rhizoma Rhei, fructus evodiae, Glycyrrhrizae radix, Coptidis rhizoma and folium Toxicodendri with plant pulverizer, and sieving with 50 mesh sieve to obtain Chinese medicinal mixture;
and 4, step 4: putting the traditional Chinese medicine mixture in the step 3 into ultrasonic extraction equipment, and adding an extraction solvent for extraction;
and 5: after the step 4 is finished, vacuum filtration is adopted to obtain filtrate and filter residue, the filtrate is concentrated to 1/6 of the original volume in vacuum, and the concentration temperature is 65 ℃;
step 6: then, the bile acid, the fruit acid, the allicin, the sodium humate and the choline chloride are added into the stirring reaction kettle one by one according to the proportion and are stirred uniformly, the stirring temperature is 50 ℃, and the temperature is kept for 1.5 hours after the stirring is finished;
and 7: and (3) adding the extract liquid obtained in the step (5) into the mixture obtained in the step (6), starting the stirring reaction kettle again to enable the extract liquid and the mixture to be uniformly stirred, and naturally cooling the mixture to normal temperature after the mixture is subjected to colloid milling to obtain the fish feed additive finished product.
In the invention, the solvent extracted in the step 4 is one of ethanol, water or other organic solvents, and the amount of the solvent is 12 times of that of the traditional Chinese medicine mixture.
In the invention, the extraction time in the step 5 is 50 minutes, and the ultrasonic power is 260W.
In the invention, the temperature of the drying box in the step 2 is 70 ℃, and the drying time is 9 hours.
In the invention, the preparation process of the mixture in the step 7 is obtained by stirring for 3 hours at a constant temperature of 40-50 ℃.
In the invention, the filter residue obtained in the step 5 is extracted for the second time in the mode of the step 4.
Table 1 shows the water quality index and fish growth condition index of cultured grass carp
TABLE 1
As can be seen from the data in Table 1, compared with the traditional additive, the fish feed additive provided by the invention has the advantages that the fish feed additive obviously provides nutrition for fish, shortens the growth period of the fish and improves the survival rate of the fish, simultaneously improves the water cleanliness, finally achieves the purpose of ensuring the high-quality growth of the fish and avoiding pollution to a water body, and is a green fish culture product.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein.
Claims (7)
1. An environment-friendly fish feed additive comprises the following components in parts by weight: 6-9 parts of rheum officinale, 10-20 parts of allicin, 10-15 parts of cornel, 20-30 parts of bile acid, 16-20 parts of fruit acid, 20-35 parts of sodium humate, 5-10 parts of liquorice, 5-8 parts of coptis chinensis, 7-12 parts of sumac and 22-28 parts of choline chloride.
2. The preparation method of the environment-friendly fish feed additive according to claim 1, comprising the following specific steps:
step 1: cleaning radix et rhizoma Rhei, fructus evodiae, Glycyrrhrizae radix, Coptidis rhizoma and folium Toxicodendri in proportion, air drying, and removing excessive water on surface;
step 2: mixing the dried rhubarb, the cornel, the liquorice, the coptis and the lacquer leaves, and then putting the mixture into a drying oven for drying to remove the internal water;
and step 3: pulverizing dried radix et rhizoma Rhei, fructus evodiae, Glycyrrhrizae radix, Coptidis rhizoma and folium Toxicodendri with plant pulverizer, and sieving with 50 mesh sieve to obtain Chinese medicinal mixture;
and 4, step 4: putting the traditional Chinese medicine mixture in the step 3 into ultrasonic extraction equipment, and adding an extraction solvent for extraction;
and 5: after the step 4 is finished, vacuum filtration is adopted to obtain filtrate and filter residue, the filtrate is concentrated to 1/5-1/6 of the original volume in vacuum, and the concentration temperature is 50-65 ℃;
step 6: then, the bile acid, the fruit acid, the allicin, the sodium humate and the choline chloride are added into a stirring reaction kettle one by one according to the proportion and are stirred uniformly, the stirring temperature is 40-50 ℃, and the temperature is kept for 1-1.5 hours after the stirring is finished;
and 7: and (3) adding the extract liquid obtained in the step (5) into the mixture obtained in the step (6), starting the stirring reaction kettle again to enable the extract liquid and the mixture to be uniformly stirred, and naturally cooling the mixture to normal temperature after the mixture is subjected to colloid milling to obtain the fish feed additive finished product.
3. The method for preparing the environment-friendly fish feed additive according to claim 2, wherein the method comprises the following steps: the solvent extracted in step 4 is one of ethanol, water or other organic solvents, and the amount of the solvent is 9-12 times of that of the traditional Chinese medicine mixture.
4. The method for preparing the environment-friendly fish feed additive according to claim 2, wherein the method comprises the following steps: the extraction time in the step 5 is 40-50 minutes, and the ultrasonic power is 240-260W.
5. The method for preparing the environment-friendly fish feed additive according to claim 2, wherein the method comprises the following steps: and 2, the temperature of the drying box in the step 2 is 70 ℃, and the drying time is 9 hours.
6. The method for preparing the environment-friendly fish feed additive according to claim 2, wherein the method comprises the following steps: the preparation process of the mixture in the step 7 is to stir the mixture for 2 to 3 hours at a constant temperature of between 40 and 50 ℃.
7. The method for preparing the environment-friendly fish feed additive according to claim 2, wherein the method comprises the following steps: and (4) performing secondary extraction on the filter residue obtained in the step (5) by using the method in the step (4).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110462029.1A CN113040297A (en) | 2021-04-27 | 2021-04-27 | Environment-friendly fish feed additive and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110462029.1A CN113040297A (en) | 2021-04-27 | 2021-04-27 | Environment-friendly fish feed additive and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN113040297A true CN113040297A (en) | 2021-06-29 |
Family
ID=76517741
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202110462029.1A Pending CN113040297A (en) | 2021-04-27 | 2021-04-27 | Environment-friendly fish feed additive and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN113040297A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114601072A (en) * | 2022-03-25 | 2022-06-10 | 北京九州大地生物技术集团股份有限公司 | Feed composition for reducing heat stress of poultry and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101744122A (en) * | 2009-12-28 | 2010-06-23 | 浙江科盛饲料股份有限公司 | Feed additive, feed and preparation method thereof for preventing nutritional fatty liver of fish |
| CN107006538A (en) * | 2017-05-27 | 2017-08-04 | 明光市裕阳农业有限公司 | A kind of plant environment-friendly type bactericide used for aquiculture and preparation method thereof |
| CN108653515A (en) * | 2018-06-08 | 2018-10-16 | 天津市晨辉饲料有限公司 | A kind of feed addictive and preparation method thereof of prevention ornamental fish ich |
| CN111000036A (en) * | 2019-12-31 | 2020-04-14 | 福建天马科技集团股份有限公司 | Puffed pellet feed for rapid growth of east star spots and preparation method and equipment thereof |
| CN111802536A (en) * | 2020-07-31 | 2020-10-23 | 福建傲农生物科技集团股份有限公司 | Feed additive for large yellow croaker female fish and preparation method and application thereof |
-
2021
- 2021-04-27 CN CN202110462029.1A patent/CN113040297A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101744122A (en) * | 2009-12-28 | 2010-06-23 | 浙江科盛饲料股份有限公司 | Feed additive, feed and preparation method thereof for preventing nutritional fatty liver of fish |
| CN107006538A (en) * | 2017-05-27 | 2017-08-04 | 明光市裕阳农业有限公司 | A kind of plant environment-friendly type bactericide used for aquiculture and preparation method thereof |
| CN108653515A (en) * | 2018-06-08 | 2018-10-16 | 天津市晨辉饲料有限公司 | A kind of feed addictive and preparation method thereof of prevention ornamental fish ich |
| CN111000036A (en) * | 2019-12-31 | 2020-04-14 | 福建天马科技集团股份有限公司 | Puffed pellet feed for rapid growth of east star spots and preparation method and equipment thereof |
| CN111802536A (en) * | 2020-07-31 | 2020-10-23 | 福建傲农生物科技集团股份有限公司 | Feed additive for large yellow croaker female fish and preparation method and application thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114601072A (en) * | 2022-03-25 | 2022-06-10 | 北京九州大地生物技术集团股份有限公司 | Feed composition for reducing heat stress of poultry and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN112868888B (en) | Biological fermentation preparation and preparation method thereof | |
| CN103636991B (en) | A kind of fattening period pork pig feed containing traditional Chinese medicine ingredients | |
| CN1947549A (en) | Compound feed used for polyculture of freshwater shrimps and river crabs | |
| CN106213026A (en) | A kind of raising nutritive digestibility chicken feed addictive | |
| CN104054940B (en) | A kind of disease-resistant grass carp feed and preparation method thereof | |
| CN106615798A (en) | Lactating sow feed capable of increasing milk yield and preparation method thereof | |
| CN104522392A (en) | Preparation method of Chinese herbal medicine additive for pigs | |
| CN112167474A (en) | Micropterus salmoides expanded feed with ultrahigh digestibility and food calling performance and preparation method thereof | |
| CN107912646A (en) | A kind of largemouth bass compound feed for young | |
| CN113040297A (en) | Environment-friendly fish feed additive and preparation method thereof | |
| WO2019100540A1 (en) | Method for preparing litopenaeusvannamei feed additive | |
| CN104054939A (en) | Palatable feed for grass carp and preparation method of palatable feed | |
| CN114903128B (en) | Crayfish compound feed and preparation method thereof | |
| CN105146083A (en) | Chicken immunity enhancing feed additive prepared based on comprehensive utilization of coconut shells | |
| CN106306528A (en) | Chicken feed additive capable of increasing laying rate | |
| CN107691772A (en) | Swimming crab feed and preparation method thereof | |
| CN115024400A (en) | Livestock feed added with tea powder, preparation method and application thereof | |
| CN105192256A (en) | Chick feed additives comprehensively prepared from coconut shells and easy to digest and absorb | |
| CN105494939A (en) | Full nutritional feed for wild gooses in fattening period and preparation method thereof | |
| KR20210001465A (en) | Additives composition for pig feed containing moringa component | |
| CN110547359A (en) | Anti-vibrio enteron health care material for shrimps | |
| CN104543535A (en) | Health bamboo shoot shell fermented duck feed and preparing method thereof | |
| WO2020011128A1 (en) | Bile acid, preparation method thereof, and application of same in preparing animal feed additive | |
| CN101744113B (en) | Compound premix feed for improving animal meat quality and flavor and preparation method thereof | |
| CN117223802A (en) | Phagostimulant for mandarin fish feed and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20210629 |