CN112870421A - 一种无尘香及其制备工艺 - Google Patents
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Abstract
本发明属于熏香技术领域，具体涉及一种无尘香及其制备工艺，所述无尘香配方按重量份比例包括香料微胶囊10‑15份、木炭粉5‑10份、白芨粉4‑8份、茶油3‑5份。本发明所制备的无尘香，采用微胶囊技术将植物提取物以液体形式包裹在胶囊内，可延缓活性成分及香气的释放，同时植物提取物含有大部分挥发油，可燃性好，无粉尘；此外，将该无尘香制成中空型，进一步加大香料与空气的接触面积，使其燃烧更充分，无烟无尘。
Description
技术领域
本发明属于熏香技术领域，具体涉及一种无尘香及其制备工艺。
背景技术
微胶囊是指一种具有聚合物或无机物壁的微型容器或包装物。微胶囊造粒技术就是将固体、液体或气体包埋、封存在一种微型胶囊内成为一种固体微粒产品的技术，该技术已广泛应用于医药、农业、计算机、化学品、食品加工、化妆品等行业。
熏香一般采用纯天然植物制备而成，对人体有多重好处，不仅可以净化空气，使呼吸顺畅，调节生理机能，还能够舒缓神经压力，使人心旷神怡，宁心安神，在古代就有广泛的使用。但一般的熏香燃烧都会有大量的黑烟，而这些黑烟都是未燃烧充分的香料组分，随着烟气漂浮在空气中，形成粉尘，容易被吸入人体，影响呼吸道健康，长期使用这类熏香将会对人体产生不利效果。
发明内容
针对现有技术的不足，本发明的目的在于提供一种可燃性好、无烟无尘香。
本发明解决其技术问题所采用的技术方案是提供一种无尘香，配方按重量份比例包括香料微胶囊10-15份、木炭粉5-10份、白芨粉4-8份、茶油3-5份。
进一步的，所述香料微胶囊由芯材和壁材组成，所述芯材包括重量份柚子皮提取物8-12份、合欢花提取物5-9份、七里香提取物5-9份、灵香草提取物5-9份，所述壁材的原料包括糊精14-20份。
柚子皮性温，味苦、辛，有理气化痰、健脾消食、散寒燥湿的作用。柚皮的提取物成分具有抗氧化、抗微生物、抗癌、抑酶、抗衰老、降血糖、降血压以及预防动脉粥样硬化等活性。柚子皮含有挥发油，主要是柠檬酸和芳香醇，它能够散寒理气、燥湿化痰、消食，适用于一些风寒感冒咳嗽、喉痒痰多这一类的患者。
合欢花性味甘、性平，含有合欢甙，鞣质，具解郁安神，滋阴补阳，理气开胃，活络止痛，具有清热解暑，养颜祛斑解酒等功效。
七里香性味辛、微苦，性温，具通经络，行气，活血，散瘀，止痛，镇惊，消肿，解毒等功效。
灵香草，为报春花科植物灵香草的全草，其味辛、甘，性平，归肺、胃经，具有解表，止痛，行气，驱蛔的功效。
白芨为兰科多年生草本植物白芨的干燥块茎，其味苦、甘、涩，性微寒，归肺、肝、胃经。其粉末遇水膨胀，有显著粘滑感，粘性好。
进一步的，柚子皮提取物由下述方法制备而成：将柚子皮剪碎至2-3mm粒径，加6-10倍体积水蒸煮2-4h，过滤去除滤渣，得柚子皮提取物。
进一步的，合欢花提取物由下述方法制备而成：将合欢花破碎至1-2mm粒径，加入2-3倍体积的87％乙醇提取5-8h，得合欢花提取物。
进一步的，七里香提取物由下述方法制备而成：将七里香破碎至1-2mm粒径，加入2-3倍体积的87％乙醇提取5-8h，过滤去除滤渣，得七里香提取物。
进一步的，灵香草提取物由下述方法制备而成：将灵香草破碎至1-2mm粒径，加入2-3倍体积水，用超声波打匀，加入果胶酶进行酶解4-6h，将所得酶解液进行过滤，去除滤渣，得灵香草提取物。
进一步的，壁材由下述方法制备而成：取糊精，加入其10倍体积的55℃温水溶解并搅拌，过150目筛网，得壁材。
进一步的，香料微胶囊的制备工艺为：按配方称取柚子皮提取物、合欢花提取物、七里香提取物、灵香草提取物并混合，将混合液加入到均质机进行均质乳化，得乳化液；将刚制备好的壁材倒入搅拌装置搅拌，同时缓慢加入所得乳化液，600-800r/min持续搅拌2-3h，过120目筛网，静置并降温至室温，待微胶囊从溶液中析出后，抽滤，干燥，得香料微胶囊。
进一步的，上述均质压力为20-25MPa，温度为40-50℃。
本发明还提供上述无尘香的制备工艺，包括如下步骤：
1)按配方称取各原料待用；
2)取白芨粉加水糊化，再加入茶油，搅拌均匀，得混合溶液；
3)取香料微胶囊、木炭粉混合，加入步骤2)所得混合溶液，搅拌均匀得泥状物；
4)将步骤3)所得泥状物挤压成中空型盘式，自然干燥，得无尘香。
本发明具有的有益效果是：本发明所制备的无尘香，采用微胶囊技术将植物提取物以液体形式包裹在胶囊内，可延缓活性成分及香气的释放，同时植物提取物含有大部分挥发油，可燃性好，无粉尘；加入的茶油气味清香，除能抗菌、抗病毒及杀微菌，防治蚊虫叮咬外，其还具有助燃作用，能提高香料的燃烧性能；此外，将该无尘香制成中空型，进一步加大香料与空气的接触面积，使其燃烧更充分，无烟无尘。
具体实施方式
下述实施例中的实验方法，如无特别说明，均为常规方法。下述实施例涉及的原料若无特别说明，均为普通市售品，皆可通过市场购买获得。下面结合实施例对本发明作进一步详细描述：
实施例1
一种无尘香，配方按重量份比例包括香料微胶囊12份、木炭粉6份、白芨粉5份、茶油5份。
其制备工艺如下：
1)柚子皮提取物的制备：将柚子皮剪碎至2mm粒径，加8倍体积水蒸煮3h，过滤去除滤渣，得柚子皮提取物。
2)合欢花提取物的制备：将合欢花破碎至1mm粒径，加入3倍体积的87％乙醇提取5-8h，得合欢花提取物。
3)七里香提取物的制备：将七里香破碎至1mm粒径，加入3倍体积的87％乙醇提取5-8h，过滤去除滤渣，得七里香提取物。
4)灵香草提取物的制备：将灵香草破碎至1mm粒径，加入3倍体积水，用超声波打匀，加入果胶酶进行酶解5h，将所得酶解液进行过滤，去除滤渣，得灵香草提取物。
5)壁材的制备：取糊精16份，加入其10倍体积的55℃温水溶解并搅拌，过150目筛网，得壁材。
6)香料微胶囊的制备：称取柚子皮提取物10份、合欢花提取物8份、七里香提取物7份、灵香草提取物6份并混合均匀，将混合液加入到20MPa压力的均质机内进行均质乳化，得乳化液；将刚制备好的壁材倒入搅拌装置搅拌，同时缓慢加入所得乳化液，600-800r/min持续搅拌3h，过120目筛网，静置并降温至室温，待微胶囊从溶液中析出后，抽滤，干燥，得香料微胶囊。
7)无尘香的制备：
①按配方称取各原料待用；
②取白芨粉加水糊化，再加入茶油，搅拌均匀，得混合溶液；
③取香料微胶囊、木炭粉混合，加入步骤②所得混合溶液，搅拌均匀得泥状物；
④将步骤③所得泥状物挤压成中空型盘式，自然干燥，得无尘香。
实施例2
一种无尘香，配方按重量份比例包括香料微胶囊13份、木炭粉7份、白芨粉6份、茶油4份。
其制备工艺参照实施例1。
实施例3
一种无尘香，配方按重量份比例包括香料微胶囊14份、木炭粉8份、白芨粉7份、茶油3份。
其制备工艺参照实施例1。
对比例1
一种熏香，配方按重量份比例包括柚子皮10份、合欢花8份、七里香7份、灵香草6份、木炭粉7份、糯米粉6份。
其制备工艺如下：
①将上述原料烘干至水分低于3％，按配方称取各原料，并粉碎至120目，待用；
②取糯米粉加水，搅拌均匀，得糊化液；
③取称量好的柚子皮、合欢花、七里香、灵香草、木炭粉混合，加入步骤②所得糊化液，搅拌均匀得泥状物；
④将步骤③所得泥状物挤压成中空型盘式，自然干燥，得无尘香。
对比例2
一种熏香，配方按重量份比例包括柚子皮10份、合欢花8份、七里香7份、灵香草6份、木炭粉7份、糯米粉6份。
其制备工艺参照对比例2，但步骤④挤压成实芯盘式。
为了验证本发明方法制备获得的无尘香，进行了以下试验：
试验例1烟尘排放量试验
试验方法：根据国家环境保护行业标准HJ/T310-2006《环境标准产品技术要求盘式蚊香》中烟尘排放量要求测试，将实施例1和对比例1-2制备的盘式香点燃，用滤纸收集排出的全部烟尘，直到点燃完毕，收集到的烟尘重量，以mg/圈表示。
试验结果见表1：
从表1可以看出，本发明实施例1所制备的无尘香烟尘排放量比行业标准小很多，较比例1和对比例2也均要小，且远小于对比例2的烟尘排放量。
最后需要强调的是，以上所述仅为本发明的优选实施例，并不用于限制本发明，对于本领域的技术人员来说，本发明可以有各种变化和更改，凡在本发明的精神和原则之内，所做的任何修改、等同替换、改进等，均应包含在本发明的保护范围之内。
Claims (10)
1.一种无尘香，其特征在于，配方按重量份比例包括香料微胶囊10-15份、木炭粉5-10份、白芨粉4-8份、茶油3-5份。
2.根据权利要求1所述的无尘香，其特征在于，所述香料微胶囊由芯材和壁材组成，所述芯材包括重量份柚子皮提取物8-12份、合欢花提取物5-9份、七里香提取物5-9份、灵香草提取物5-9份，所述壁材的原料包括糊精14-20份。
3.根据权利要求2所述的无尘香，其特征在于，所述柚子皮提取物由下述方法制备而成：将柚子皮剪碎至2-3mm粒径，加6-10倍体积水蒸煮2-4h，过滤去除滤渣，得柚子皮提取物。
4.根据权利要求2所述的无尘香，其特征在于，所述合欢花提取物由下述方法制备而成：将合欢花破碎至1-2mm粒径，加入2-3倍体积的87％乙醇提取5-8h，得合欢花提取物。
5.根据权利要求2所述的无尘香，其特征在于，所述七里香提取物由下述方法制备而成：将七里香破碎至1-2mm粒径，加入2-3倍体积的87％乙醇提取5-8h，过滤去除滤渣，得七里香提取物。
6.根据权利要求2所述的无尘香，其特征在于，所述灵香草提取物由下述方法制备而成：将灵香草破碎至1-2mm粒径，加入2-3倍体积水，用超声波打匀，加入果胶酶进行酶解4-6h，将所得酶解液进行过滤，去除滤渣，得灵香草提取物。
7.根据权利要求2所述的无尘香，其特征在于，所述壁材由下述方法制备而成：取糊精，加入其10倍体积的55℃温水溶解并搅拌，过150目筛网，得壁材。
8.根据权利要求2所述的无尘香，其特征在于，所述香料微胶囊的制备工艺为：按配方称取柚子皮提取物、合欢花提取物、七里香提取物、灵香草提取物并混合，将混合液加入到均质机进行均质乳化，得乳化液；将刚制备好的壁材倒入搅拌装置搅拌，同时缓慢加入所得乳化液，600-800r/min持续搅拌2-3h，过120目筛网，静置并降温至室温，待微胶囊从溶液中析出后，抽滤，干燥，得香料微胶囊。
9.根据权利要求8所述的无尘香，其特征在于，所述均质压力为20-25MPa，温度为40-50℃。
10.根据权利要求1-9任一项所述无尘香的制备工艺，其特征在于，包括以下步骤：
1)按配方称取各原料待用；
2)取白芨粉加水糊化，再加入茶油，搅拌均匀，得混合溶液；
3)取香料微胶囊、木炭粉混合，加入步骤2)所得混合溶液，搅拌均匀得泥状物；
4)将步骤3)所得泥状物挤压成中空型盘式，自然干燥，得无尘香。
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