CN112870118A - Chinese herbal medicine shampoo and preparation method thereof - Google Patents
Chinese herbal medicine shampoo and preparation method thereof Download PDFInfo
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- CN112870118A CN112870118A CN202011640063.5A CN202011640063A CN112870118A CN 112870118 A CN112870118 A CN 112870118A CN 202011640063 A CN202011640063 A CN 202011640063A CN 112870118 A CN112870118 A CN 112870118A
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- shampoo
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- chinese herbal
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- GWLWWNLFFNJPDP-UHFFFAOYSA-M sodium;2-aminoethanesulfonate Chemical compound [Na+].NCCS([O-])(=O)=O GWLWWNLFFNJPDP-UHFFFAOYSA-M 0.000 description 1
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- 230000000475 sunscreen effect Effects 0.000 description 1
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- 229940082509 xanthan gum Drugs 0.000 description 1
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
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Images
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Abstract
The application provides a Chinese herbal medicine shampoo and a preparation method thereof. The Chinese herbal medicine shampoo comprises 10-30 parts of amino acid type surfactant, 1-5 parts of skin conditioner, 0.3-1 part of thickener, 0.5-5 parts of humectant, 0.02-0.08 part of chelating agent, 0.5-1 part of plant aromatic and 50-80 parts of solvent. The Chinese herbal medicine shampoo can nourish hair, has a protective effect on skin and is good in environmental protection.
Description
Technical Field
The invention relates to the technical field of daily necessities, in particular to Chinese herbal medicine shampoo and a preparation method thereof.
Background
The shampoo is also called shampoo, shampoo or shampoo, and is a basic care cosmetic applied to hair and scalp. Shampoos are classified into various types, and are suitable for dry hair, oily hair, and mixed hair. The shampoo is used for cleaning hair and scalp, and can be used for making foundation for hair styling, softening and nourishing hair, and preventing bifurcation. Along with the continuous improvement of living standard, the consciousness of pursuing health of people is also enhanced, and the most basic hair washing requirements are met, the attention to the hair quality maintenance is paid, and the effective shampoo capable of washing hair healthily is more used.
Shampoo on the market is various in types and different in functions, customers can select shampoo suitable for the customers according to the requirements of hair quality, but most of shampoo at present contains more or less chemical raw materials, and the chemical raw materials can play a basic role in removing dirt and dandruff, but still can initiate certain side effects on hair, and waste water and waste residues which are not beneficial to environmental protection can be generated in the processing process.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provides the Chinese herbal medicine shampoo which can nourish hair, has a protective effect on skin and is good in environmental protection and the preparation method thereof.
The purpose of the invention is realized by the following technical scheme:
a Chinese herbal medicine shampoo comprises the following components in parts by mass:
in one embodiment, the amino acid-type surfactant is at least one of cocoyl alanine TEA salt, sodium methylcocoyl taurate, cocamidopropyl hydroxysultaine, and cocoyl glutamic acid TEA salt.
In one embodiment, the skin conditioning agent is at least one of soapberry extract, eclipta prostrate extract, litchi chinensis fruit extract, glyceryl caprylate, glyceryl caprate, sodium dilinolamidopropyl PG-dimethyl ammonium chloride phosphate, lauroyl arginine ethyl ester hydrochloride, propylene glycol, sodium isostearoyl lactylate, lactic acid, and soy lecithin.
In one embodiment, the thickener is PEG-120 methyl glucose trioleate.
In one embodiment, the humectant is at least one of propylene glycol, caprylhydroxamic acid, glyceryl caprylate, and 1, 2-pentanediol.
In one embodiment, the chelating agent is sodium phytate.
In one embodiment, the botanical fragrance is at least one of neroli oil, geranium leaf oil, eucalyptus globulus leaf oil, and mugwort leaf oil.
In one embodiment, the Chinese herbal medicine shampoo further comprises the following components in parts by mass:
1-3 parts of hair conditioner.
In one embodiment, the Chinese herbal medicine shampoo further comprises the following components in parts by mass:
0.2 to 0.5 portion of pH regulator.
A preparation method of Chinese herbal medicine shampoo comprises the following steps:
sequentially adding an amino acid type surfactant, a first skin conditioner, a hair conditioner and a chelating agent into a reaction pot, and stirring for the first time at a first preset temperature to obtain a first mixture;
maintaining the reaction kettle at a first preset temperature state, adding a pH regulator into the first mixture, and carrying out second stirring operation to obtain a second mixture;
adding a thickening agent and a second skin conditioner into the second mixture, and carrying out stirring operation for the third time to obtain a third mixture;
cooling the reaction kettle to a second preset temperature, adding a solvent and a third skin conditioner into the third mixture, and stirring for the fourth time to obtain a fourth mixture;
cooling the reaction kettle to a third preset temperature, adding a fourth skin conditioner, a humectant and a plant aromatic into the fourth mixture, and performing fifth stirring operation to obtain a fifth mixture;
and cooling the reaction kettle to a fourth preset temperature, adding a fifth skin conditioner into the fifth mixture, stirring for the sixth time, and completely dissolving to obtain the Chinese herbal medicine shampoo.
Compared with the prior art, the invention has at least the following advantages:
1. the Chinese herbal medicine shampoo is prepared by adopting the amino acid type surfactant, the amino acid type surfactant has better foaming and dirt removing capability, the pH value of the amino acid type surfactant is close to that of human skin, the amino acid is a basic substance forming protein, the skin can be mild, and the irritation of the shampoo to the skin is smaller. Meanwhile, the Chinese herbal medicine shampoo prepared by the amino acid type surfactant has high biodegradability, and degradation products of the amino acid type surfactant are amino acid and fatty acid, so that the environment-friendly performance is better.
2. Due to the synergistic effect of the skin conditioner and the amino acid surfactant, the shampoo can remove dirt and dandruff without reducing the moisture of the stratum corneum of the skin, can further reduce the stimulation of the surfactant to the skin, and has a protective effect on the skin.
3. The Chinese herbal medicine shampoo adopts Chinese herbal medicine plant aromatic components, can replace components such as pigment, essence and the like, and takes the naturally extracted Chinese herbal medicine plant components as the aromatic, so that the irritation of the shampoo to the skin can be further reduced. Moreover, the Chinese herbal medicine components have better cleaning and antibacterial effects, such as the folium artemisiae argyi components, can relieve itching and deoiling, nourish the scalp and relieve alopecia.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings needed to be used in the embodiments will be briefly described below, it should be understood that the following drawings only illustrate some embodiments of the present invention and therefore should not be considered as limiting the scope, and for those skilled in the art, other related drawings can be obtained according to the drawings without inventive efforts.
Fig. 1 is a flow chart of a preparation method of a Chinese herbal medicine shampoo in an embodiment.
Detailed Description
To facilitate an understanding of the invention, the invention will now be described more fully with reference to the accompanying drawings. Preferred embodiments of the present invention are shown in the drawings. This invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete.
It will be understood that when an element is referred to as being "secured to" another element, it can be directly on the other element or intervening elements may also be present. When an element is referred to as being "connected" to another element, it can be directly connected to the other element or intervening elements may also be present. The terms "vertical," "horizontal," "left," "right," and the like as used herein are for illustrative purposes only and do not represent the only embodiments.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used herein in the description of the invention is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.
The application provides a Chinese herbal medicine shampoo. The Chinese herbal medicine shampoo comprises 10-30 parts of amino acid type surfactant, 1-5 parts of skin conditioner, 0.3-1 part of thickener, 0.5-5 parts of humectant, 0.02-0.08 part of chelating agent, 0.5-1 part of Chinese herbal medicine plant aromatic and 50-80 parts of solvent.
According to the Chinese herbal medicine shampoo, the amino acid type surfactant is prepared by adopting the amino acid type surfactant, the amino acid type surfactant has good foaming and dirt removing capabilities, the pH value of the amino acid type surfactant is close to that of human skin, amino acid is a basic substance forming protein, the skin can be mild, and the shampoo has small irritation to the skin. Meanwhile, the Chinese herbal medicine shampoo prepared by the amino acid type surfactant has high biodegradability, and degradation products of the amino acid type surfactant are amino acid and fatty acid, so that the environment-friendly performance is better. Furthermore, due to the synergistic effect of the skin conditioner and the amino acid surfactant, the shampoo can remove dirt and dandruff without reducing the moisture of the stratum corneum of the skin, can further reduce the stimulation of the surfactant to the skin, and has a protective effect on the skin. The Chinese herbal medicine shampoo adopts plant aromatic components, can replace components such as pigments and essences, and uses the naturally extracted Chinese herbal medicine plant components as the aromatic, so that the irritation of the shampoo to the skin can be further reduced. Moreover, the Chinese herbal medicine components have better cleaning and antibacterial effects, such as the folium artemisiae argyi components, can relieve itching and deoiling, nourish the scalp and relieve alopecia.
For better understanding of the herbal shampoo of the present invention, the following further explains the herbal shampoo of the present invention, and one embodiment of the herbal shampoo comprises 10 to 30 parts of amino acid type surfactant, 1 to 5 parts of skin conditioner, 0.3 to 1 part of thickener, 0.5 to 5 parts of humectant, 0.02 to 0.08 part of chelating agent, 0.5 to 1 part of plant fragrance, and 50 to 80 parts of solvent.
It will be appreciated that the amino acid surfactant is an amino acid salt of coconut oil, bay oil or palm oil having foaming detergency. The weakly acidic amino acid surfactant has a pH value close to that of human skin, and the amino acid is a basic substance for forming protein, so that the weak acidic amino acid surfactant can be used for mildly conditioning the skin and ensuring that the shampoo has small irritation to the skin. Meanwhile, the Chinese herbal medicine shampoo prepared by the amino acid type surfactant has high biodegradability, and degradation products of the amino acid type surfactant are amino acid and fatty acid, so that the environment-friendly performance is better. In the application, the skin conditioner refers to a component capable of improving skin conditions in Chinese herbal medicine hair washing, and due to the synergistic effect of the skin conditioner and the amino acid surfactant, the shampoo can remove dirt and dandruff without reducing the moisture of the stratum corneum of the skin, can further reduce the stimulation of the surface activity to the skin, and has a protective effect on the skin. The thickening agent can improve the viscosity of a system, so that the system is kept in a uniform and stable suspension state or an emulsion state, and meanwhile, the thickening agent also has an emulsifying effect. The humectant has low volatility, can retain water and be occluded on the surface of skin, and simultaneously, the humectant and other skin conditioners have synergistic effect to further improve the water retention of skin and hair and activate cell activity, so that the Chinese herbal medicine shampoo has the effects of keeping skin moist and smooth, and preventing hair from drying and darkening.
Further, the chelating agent is capable of causing a metal atom or ion to act as a ligand with two or more coordinated atoms to form a complex having a cyclic structure. The chelating agent is added into the Chinese herbal medicine shampoo, the chelating agent and salts of calcium, magnesium and iron can be utilized to generate water-soluble complex, the hard water resistance of the shampoo is further improved, and a calcium soap film and a magnesium soap film are prevented from being attached to hair when the fragrance on the hair is washed by hard water. In addition, the chelating agent and the Chinese herbal medicine components have synergistic effect, so that organic substances and antagonistic substances on the surface of the scalp can be effectively chelated, and the situation that the antagonistic substances are combined with active groups in the Chinese herbal medicine components to weaken the bactericidal effect of the Chinese herbal medicine components is avoided, so that the bactericidal effect of the Chinese herbal medicine components and the hair nourishing effect are effectively improved. Furthermore, the plant aromatic can replace components such as pigment, essence and the like, and the natural extracted Chinese herbal medicine plant components are used as the aromatic, so that the stimulation of the shampoo to the skin can be further reduced. Moreover, the Chinese herbal medicine components have better cleaning and antibacterial effects, such as the folium artemisiae argyi components, can relieve itching and deoiling, nourish the scalp and relieve alopecia.
To further enhance the mildness of the shampoo to the skin, in one embodiment the amino acid type surfactant is at least one of cocoyl alanine TEA salt, sodium methyl cocoyl taurate, cocamidopropyl hydroxysultaine, and cocoyl glutamic acid TEA salt. It will be appreciated that the amino acid surfactant is an amino acid salt of coconut oil, bay oil or palm oil having foaming detergency. The weakly acidic amino acid surfactant has a pH value close to that of human skin, and the amino acid is a basic substance for forming protein, so that the weak acidic amino acid surfactant can be used for mildly conditioning the skin and ensuring that the shampoo has small irritation to the skin. Meanwhile, the Chinese herbal medicine shampoo prepared by the amino acid type surfactant has high biodegradability, and degradation products of the amino acid type surfactant are amino acid and fatty acid, so that the environment-friendly performance is better. In this example, the amino acid type surfactant is at least one of cocoyl alanine TEA salt, sodium methylcocoyl taurate, cocamidopropyl hydroxysultaine, and cocoyl glutamic acid TEA salt. The TEA salt of cocoyl alanine is mild in nature and provides some cleansing and lathering benefits. The shampoo prepared from the cocoyl alanine TEA salt has good compatibility with skin, and has negligible irritation to skin and cornea. The sodium methyl cocoyl taurate is prepared by condensing natural fatty acid and sodium methyl taurate, makes foams rich, fine and stable under a wide pH value condition, and has very little irritation to skin due to the hydrophilic amino acid structure. The cocamidopropyl hydroxysulfobetaine is a zwitterionic surfactant with excellent solubility and compatibility, has excellent stability under acidic and alkaline conditions, respectively presents positive and negative ions, is often used together with anionic, cationic and nonionic surfactants, and has good compatibility. Besides the basic properties of emulsification, washing, dispersion, foaming, penetration, solubilization and dissolution of the surfactant, the TEA salt of cocoyl glutamic acid also has low irritation, low toxicity, softness, good biodegradability and good affinity to the human body.
In order to further improve the protective effect and the efficacy of the Chinese herbal medicine shampoo on the skin. In one embodiment, the skin conditioning agent is at least one of soapberry extract, eclipta prostrate extract, litchi chinensis fruit extract, glyceryl caprylate, glyceryl caprate, sodium dilinolamidopropyl PG-dimethyl ammonium chloride phosphate, lauroyl arginine ethyl ester hydrochloride, propylene glycol, sodium isostearoyl lactylate, lactic acid, and soy lecithin. It can be understood that the sapindus mukorossi extract contains a large amount of saponin components, and the saponin has physiological effects of antibacterial and antipruritic in addition to good foamability and detergency. The saponin is natural active substance, and does not cause chemical irritation or injury to skin. In addition, the soapberry is a traditional Chinese medicine component, has obvious curative effects on sebaceous gland metabolic diseases such as scalp, seborrheic dermatitis, acne and acne, and can also effectively prevent dandruff and prevent hair loss. The eclipta prostrata extract has effect in inhibiting reductase, relieving hair loss caused by high androgen, and stimulating hair growth. Meanwhile, the eclipta prostrata extract has an activation effect on tyrosinase, can increase the secretion of melanin, and is beneficial to the prevention and treatment of white hair. In addition, the snakehead intestine extract has good skin mildness and high safety factor, and can be used by special sensitive people such as pregnant women and children. The litchi fruit extract is beneficial to activating cathepsin, and the shampoo prepared by taking the litchi fruit extract as a main component can enhance the metabolism of a scalp area and has the effect of promoting hair growth. Is especially useful for relieving alopecia caused by high androgen. The shampoo prepared by using the glyceryl caprylate and the glyceryl caprate as main components can be suitable for sensitive people such as pregnant women, children and the like. The soybean lecithin is extracted from soybeans, is phospholipid forming a biological membrane, is easily absorbed by skin and hair of people, can promote the permeation of other nutrient substances, and has strong moisturizing performance; meanwhile, the soybean lecithin has strong emulsifying property and can stabilize emulsion. Further, in the embodiment, the skin conditioner is at least one of a soapberry extract, an eclipta prostrata extract and a litchi fruit extract, and the shampoo prepared by using the soapberry extract, the eclipta prostrata extract and the litchi fruit extract as main components can effectively nourish scalp and promote hair growth, is high in safety coefficient, and can be suitable for sensitive people such as pregnant women and children. And due to the synergistic effect of the skin conditioner and the amino acid surfactant, the shampoo can remove dirt and dandruff without reducing the moisture of the stratum corneum of the skin, can further reduce the stimulation of the surfactant to the skin, and has a protective effect on the skin.
In one embodiment, the thickener is PEG-120 methyl glucose trioleate. It can be understood that PEG-120 methyl glucose trioleate has good thickening effect and cleaning effect, and PEG-120 methyl glucose trioleate is added into a formula of the Chinese herbal medicine shampoo, so that the system viscosity of the Chinese herbal medicine shampoo can be effectively improved, and the system can be kept in a uniform and stable emulsion state. In the embodiment, the PEG-120 methyl glucose trioleate and the amino acid type surfactant act synergistically, so that the formulated shampoo not only has viscosity suitable for daily life, but also can mildly clean hair without stimulating and damaging scalp. In another embodiment, the thickener may also be at least one of natural plant starch, xanthan gum, gum arabic, guar gum, carrageenan, algin, propylene glycol, and glycerin.
In one embodiment, the humectant is at least one of propylene glycol, caprylhydroxamic acid, glyceryl caprylate, and 1, 2-pentanediol. It is understood that propylene glycol is one of the polyhydric alcohols, is almost colorless and odorless, has no greasy feeling, is completely dissolved in water, and also has preservative effect. The propylene glycol has strong permeability, and can help other components, such as Chinese herbal medicine components, disperse and permeate on the surface of the scalp, so that the nourishing effect of the Chinese herbal medicine shampoo on the scalp and hair roots is improved. The octanoyl hydroximic acid is an organic acid with an antibacterial effect, has high-efficiency and selective chelating capacity on ferrous ions and ferric ions, has limited growth of moulds in an environment with limited ferric ions, and has an optimal carbon chain length capable of promoting degradation of a cell membrane structure, so that the octanoyl hydroximic acid has high antibacterial capacity. The shampoo prepared by taking the caprylyl hydroximic acid as the main component not only has a good moisturizing effect, but also has strong antibacterial capability, and can well replace preservatives, so that the preservatives are prevented from causing damage to skin, especially sensitive skin. The 1, 2-pentanediol belongs to a micromolecule humectant, is a synthetic humectant, has the functions of water locking and antibiosis, and can improve the water resistance of a sunscreen product. In this embodiment, the moisturizer is at least one of propylene glycol, caprylyl hydroximic acid, glyceryl caprylate and 1, 2-pentanediol, and the moisturizer, in cooperation with other skin conditioners, can further improve the moisture retention and cell activation of skin and hair, so that the herbal shampoo has the effects of keeping skin moist and smooth, and preventing hair from drying and darkening. In addition, the humectant can enable the Chinese herbal medicine shampoo to have good antibacterial capacity, so that a preservative is further replaced, the Chinese herbal medicine shampoo does not need to be added with the preservative, and the Chinese herbal medicine shampoo has high safety and environmental friendliness.
In one embodiment, the chelating agent is sodium phytate. It can be understood that the sodium phytate has strong chelating effect with metal ions, has strong integration capability to the metal ions in a wide pH range, and particularly has large number constant to iron and copper ions, and the color effect of the metal ions, particularly the copper ions, can be effectively avoided by adding the sodium phytate into the Chinese herbal medicine shampoo. Sodium phytate is easily absorbed by skin and mucous membrane, is tonic nutritional agent, is helpful for enhancing skin function near scalp, and has hair growth stimulating effect. In this embodiment, sodium phytate is added to the herbal shampoo, and the sodium phytate and the salts of calcium, magnesium and iron can be used to form water-soluble complexes, thereby further improving the hard water resistance of the shampoo and preventing the calcium and magnesium soap film from adhering to the hair when the perfume on the hair is washed with hard water. In addition, the sodium phytate and the Chinese herbal medicine components have synergistic effect, so that organic substances and antagonistic substances on the surface of the scalp can be effectively chelated, and the situation that the antagonistic substances are combined with active groups in the Chinese herbal medicine components to weaken the bactericidal effect of the Chinese herbal medicine components is avoided, so that the bactericidal effect of the Chinese herbal medicine components and the nourishing effect on hair are effectively improved. In another embodiment, the chelating agent may also be disodium edetate.
In one embodiment, the plant fragrance is at least one of neroli oil, geranium oil, eucalyptus globulus oil, and mugwort oil. The bitter orange flower oil is derived from bitter orange petals, has sweet fragrance and bitter aftertaste, and has no toxicity or irritation. The bitter orange flower oil is added into the Chinese herbal medicine shampoo, so that the fragrance of the Chinese herbal medicine shampoo can be improved, the essence components in the existing shampoo are replaced, and the environmental protection performance of the Chinese herbal medicine shampoo is improved. In addition, the Chinese herbal medicine shampoo prepared by taking the neroli oil as the main component can promote the metabolism and cell regeneration functions of the scalp and the skin near the hair root, improve the water locking capacity of the skin and further be beneficial to nourishing the skin of the head. The geranium leaf oil has a rose-like fragrance, and is a pure natural substance, so that the geranium leaf oil can replace essence components in the existing shampoo, and the environmental protection performance of the Chinese herbal medicine shampoo is improved. In addition, the geranium leaf oil has an inhibiting effect on partial fungi, and can enable the Chinese herbal medicine shampoo to have antibacterial and acarid-removing effects. The geranium leaf oil also has an effect of eliminating partial free radicals, so that the Chinese herbal medicine shampoo has an antioxidant effect. The Eucalyptus globulus Labill oil has antibacterial and antiseptic effects, and no antiseptic is added into the shampoo. Furthermore, the eucalyptus globulus oil has an inhibition effect on histamine, so that the Chinese herbal medicine shampoo can have an anti-allergy effect. In addition, the eucalyptus globulus leaf oil also has the function of eliminating free radicals, so that the Chinese herbal medicine shampoo has the effect of antioxidation. The oleum folium Artemisiae Argyi has antibacterial and antiseptic effects, and no antiseptic is added into the herbal shampoo. Meanwhile, the Chinese herbal medicine shampoo prepared from the argy wormwood leaf oil can relieve itching and oil, nourish scalp and relieve alopecia. In this embodiment, the plant aromatic is at least one of neroli oil, geranium oil, eucalyptus globulus oil and argyi leaf oil, so that the plant aromatic can replace pigments, essences and other ingredients, and the stimulation of the shampoo to the skin can be further reduced by taking the naturally extracted Chinese herbal medicine plant ingredients as the aromatic.
Further, the plant aromatic is obtained by extracting in a low-temperature ultrasonic concentration mode. It is understood that the existing extraction of herbal plant components is generally carried out by soaking, boiling and heating, and the high-temperature extraction easily causes the active components of the herbal plant extract to lose efficacy. In this embodiment, the plant essential oil is extracted at a low temperature, and the plant cells are disrupted by an ultrasonic technique, so that the effective components of the herbal plant can be effectively extracted at a low temperature, and the efficacy of the active components of the herbal plant extract can be effectively ensured.
In one embodiment, the Chinese herbal medicine shampoo further comprises the following components in parts by mass: 1-3 parts of hair conditioner. It is understood that hair conditioners can improve the look and feel of hair, thicken or soften hair, facilitate hair styling, improve hair shine, and improve the texture of hair damaged by chemical or physical action.
Further, the hair conditioner is guar hydroxypropyl trimonium chloride. Guar gum hydroxypropyl trimethyl ammonium chloride is prepared with natural guar gum as material, and through removing the endosperm part containing galactose and mannose, drying, crushing, pressurized hydrolysis, deposition in 20% alcohol solution, centrifugal separation, drying and reaction with water-losing condensed glyceryl ether trimethyl ammonium chloride. The guar hydroxypropyl trimethyl ammonium chloride has high safety and environmental protection, and can be suitable for sensitive people such as pregnant women and children. In addition, guar gum hydroxypropyl trimethyl ammonium chloride is added into the Chinese herbal medicine shampoo, so that the Chinese herbal medicine shampoo has an antistatic effect.
In one embodiment, the Chinese herbal medicine shampoo further comprises the following components in parts by mass: 0.2 to 0.5 portion of pH regulator. It is understood that if the pH of the shampoo is too low, some anionic surfactants will hydrolyze, thereby affecting the safety of the product. If the pH value of the shampoo is too high, the swelling effect on the hair is obvious, and the luster and the strength of the hair are influenced. In this embodiment, the Chinese herbal medicine shampoo further comprises the following components in parts by mass: 0.2 to 0.5 portion of pH regulator. The pH value of the Chinese herbal medicine shampoo is regulated by the pH regulator, so that the safety and the environmental protection of the Chinese herbal medicine shampoo can be guaranteed, the inactivation of the surfactant can be prevented, the pH value can be regulated to a range suitable for the reaction of the surfactant, and the dirt removing and scurf removing capability of the surfactant is improved.
Further, the pH regulator is citric acid. It is understood that citric acid is extracted from lemon, which is one of the fruit acids. The citric acid is used as an acid-base regulator in the Chinese herbal medicine shampoo, can better regulate the pH value in the Chinese herbal medicine shampoo, belongs to a natural pH regulator, has small irritation to skin, and has better safety and environmental protection. Furthermore, the citric acid can also play a role of a natural preservative in the Chinese herbal medicine shampoo, so that the shelf life of the Chinese herbal medicine shampoo is effectively prolonged. In addition, citric acid is an important substance essential for citric acid circulation in human body, and can accelerate cutin renewal, help dirt and dandruff in scalp to fall off, and make the cleaning effect of the Chinese herbal medicine shampoo better.
In order to better understand the herbal shampoo, the application also provides a preparation method of the herbal shampoo, which comprises the following steps: sequentially adding an amino acid type surfactant, a first skin conditioner, a hair conditioner and a chelating agent into a reaction pot, and stirring for the first time at a first preset temperature to obtain a first mixture; keeping the reaction kettle in a first preset temperature state, adding a pH regulator into the first mixture, and carrying out second stirring operation to obtain a second mixture; adding the thickening agent and a second skin conditioner into the second mixture, and stirring for the third time to obtain a third mixture; cooling the reaction kettle to a second preset temperature, adding the solvent and a third skin conditioner into the third mixture, and performing fourth stirring operation to obtain a fourth mixture; cooling the reaction kettle to a third preset temperature, adding a fourth skin conditioner, a humectant and a plant aromatic into the fourth mixture, and performing fifth stirring operation to obtain a fifth mixture; and cooling the reaction kettle to a fourth preset temperature, adding a fifth skin conditioner into the fifth mixture, stirring for a sixth time, and completely dissolving to obtain the Chinese herbal medicine shampoo.
The preparation method of the Chinese herbal medicine shampoo is simple, easy to operate, mild in preparation conditions and good in environmental protection, and the prepared Chinese herbal medicine shampoo can nourish hair, has a protection effect on skin and is good in environmental protection.
S100, sequentially adding the amino acid type surfactant, the first skin conditioner, the hair conditioner and the chelating agent into a reaction pot, and stirring for the first time at a first preset temperature to obtain a first mixture.
In this embodiment, the amino acid type surfactant, the first skin conditioner, the hair conditioner, and the chelating agent are sequentially added to the reaction vessel, and the first stirring operation is performed at the first preset temperature, so that the amino acid type surfactant, the first skin conditioner, the hair conditioner, and the chelating agent are sufficiently and uniformly mixed together.
S200, keeping the reaction kettle in a first preset temperature state, adding the pH regulator into the first mixture, and carrying out second stirring operation to obtain a second mixture.
It can be understood that the basic components of the herbal shampoo are thoroughly and uniformly mixed after the first blending operation. In this embodiment, the reaction vessel is maintained at a first predetermined temperature state, the first mixture is adapted to the reaction conditions of the pH adjusting agent, and further, the pH adjusting agent is added to the first mixture and the second stirring operation is performed to obtain a second mixture. Through the addition of the pH regulator, the pH value of the first mixture can be regulated, so that the safety and the environmental friendliness of the Chinese herbal medicine shampoo can be guaranteed, the inactivation of the surfactant can be prevented, the pH value can be regulated to a range suitable for the reaction of the surfactant, and the dirt removing and scurf removing capacity of the surfactant is improved.
And S300, adding the thickening agent and the second skin conditioner into the second mixture, and stirring for the third time to obtain a third mixture.
In this embodiment, the thickener and the second skin conditioner are added to the second mixture, and a third stirring operation is performed to fully mix the thickener in the second mixture, so that the thickener and the amino acid type surfactant act synergistically, and the formulated shampoo not only has viscosity suitable for daily use, but also can mildly clean hair without stimulating and damaging scalp. Meanwhile, a second skin conditioner is added, so that the efficacy of the Chinese herbal medicine shampoo is further improved.
S400, cooling the reaction kettle to a second preset temperature, adding the solvent and the third skin conditioner into the third mixture, and stirring for the fourth time to obtain a fourth mixture.
In this embodiment, the reaction kettle is cooled to the second preset temperature, so that the solvent is conveniently added, the third mixture is sufficiently dissolved by the solvent, and meanwhile, the third skin conditioner is added, so that the efficacy of the Chinese herbal medicine shampoo is further improved. And then stirring for the fourth time in the reaction pot to fully dissolve and mix the third mixture, the solvent and the third skin conditioner.
And S500, cooling the reaction kettle to a third preset temperature, adding a fourth skin conditioner, a humectant and a plant aromatic into the fourth mixture, and performing fifth stirring operation to obtain a fifth mixture.
In this embodiment, the reaction kettle is cooled to a third preset temperature, so as to facilitate the addition of the humectant and the plant aroma, fully mix the humectant and the plant aroma in the fourth mixture, and ensure that the plant aroma does not lose activity due to an over-high temperature. Meanwhile, a fourth skin conditioner is added, so that the efficacy of the Chinese herbal medicine shampoo is further improved. And then stirring for the fifth time in the reaction pot to fully dissolve and mix the fourth mixture, the fourth skin conditioner, the humectant and the plant aromatic.
S600, cooling the reaction kettle to a fourth preset temperature, adding a fifth skin conditioner into the fifth mixture, stirring for a sixth time, and completely dissolving to obtain the Chinese herbal medicine shampoo.
In this embodiment, predetermine the temperature with the reaction kettle cooling to the fourth to conveniently mix fifth skin conditioner in the fifth mixture, convenient subsequent ejection of compact operation avoids the high temperature and influences ejection of compact operation simultaneously, improves discharging efficiency. And fully dissolving the fifth skin conditioner and mixing the fifth skin conditioner in the fifth mixture by stirring for the sixth time to obtain the Chinese herbal medicine shampoo.
In one of the embodiments, the amino acid-type surfactant is cocoyl alanine TEA salt, sodium methylcocoyl taurate, cocamidopropyl hydroxysultaine, and cocoyl glutamic acid TEA salt.
In one embodiment, the first skin conditioning agent is soapberry extract and snakehead gut extract.
In one embodiment, the hair conditioner is guar hydroxypropyltrimonium chloride.
In one embodiment, the chelating agent is sodium phytate.
In one embodiment, the first preset temperature is 80 ℃ to 90 ℃, so that the cocoyl alanine TEA salt, the methyl cocoyl sodium taurate, the cocamidopropyl hydroxysultaine, the cocoyl glutamic acid TEA salt, the soapberry extract, the eclipta prostrate extract, the guar hydroxypropyl trimonium chloride and the sodium phytate are fully stirred and mixed uniformly, and the activity of the amino acid type surfactant can be ensured.
Further, the stirring speed in the first stirring operation is 5r/min to 20 r/min. It can be understood that, when the first stirring operation is performed, the solvent is not added into the first mixture, and the components in the first mixture are stirred at a low stirring speed, so that the components in the first mixture can be sufficiently and uniformly mixed together, and the components in the first mixture can be prevented from being damaged due to the excessively high stirring speed, thereby ensuring the efficacy of the components in the first mixture. Furthermore, the first stirring operation adopts segmented stirring, the components in the first mixture are mixed together at a stirring speed of 8r/min, and then the components in the first mixture are further uniformly stirred at a stirring speed of 15 r/min.
In one embodiment, the pH adjusting agent is citric acid.
Further, the stirring speed in the second stirring operation is 10 r/min-20 r/min, so that the citric acid is more fully and uniformly mixed in the first mixture, and the preparation efficiency of the Chinese herbal medicine shampoo is improved.
In one embodiment, the second skin conditioning agent is glyceryl caprylate, glyceryl caprate, sodium dilinolamidopropyl PG-dimethyl ammonium chloride phosphate, and sodium isostearoyl lactylate.
In one embodiment, the thickener is PEG-120 methyl glucose trioleate.
In one embodiment, the stirring time of the second stirring operation is 10 minutes to 20 minutes.
In one embodiment, the solvent is deionized water.
In one embodiment, the third skin conditioning agent is soy lecithin.
In one embodiment, the second predetermined temperature is 45-55 ℃, so that the soybean lecithin and the third mixture are sufficiently dissolved together, and the efficacy of the soybean lecithin in the herbal shampoo is ensured.
In one embodiment, the fourth skin conditioning agent is lauroyl arginine ethyl ester hydrochloride and propylene glycol.
In one embodiment, the moisturizer is propylene glycol, caprylhydroxamic acid, glyceryl caprylate, and 1, 2-pentanediol.
In one embodiment, the botanical fragrance is neroli oil, geranium leaf oil, eucalyptus globulus leaf oil, and mugwort leaf oil.
In one embodiment, the third predetermined temperature is 40 ℃ to 50 ℃, so that the fourth skin conditioner, the humectant, the botanical aromatic and the fourth mixture are sufficiently dissolved together, and the efficacy of the botanical aromatic in the herbal shampoo is ensured.
In one embodiment, the fifth skin conditioning agent is lychee fruit extract and lactic acid.
In one embodiment, the fourth preset temperature is 35-45 ℃.
Further, the stirring speed of the third stirring operation, the stirring speed of the fourth stirring operation, the stirring speed of the fifth stirring operation, and the stirring speed of the sixth stirring operation are all the same as the stirring speed of the second stirring operation. Therefore, the uniformity of the mixture can be improved, the adjusting time of the stirring speed can be saved, and the production efficiency of the Chinese herbal medicine shampoo is further improved.
In one embodiment, after the step of cooling the reaction kettle to the fourth preset temperature, adding a fifth skin conditioner to the fifth mixture, and performing a sixth stirring operation, the method for preparing the Chinese herbal medicine shampoo further comprises the following steps: and a material pumping diaphragm pump is adopted for discharging. In this embodiment, the prepared Chinese herbal medicine shampoo is discharged by using a material pumping diaphragm pump, so that the Chinese herbal medicine shampoo is filtered to remove impurities in the preparation process of the Chinese herbal medicine shampoo, and the purity of the Chinese herbal medicine shampoo is improved. Furthermore, the material pumping diaphragm is filter cloth with 150-250 meshes, so that the purity of the Chinese herbal medicine shampoo is further improved.
Example 1
Accurately weighing various raw materials in the formula, placing the raw materials in a clean and sterilized container, and cleaning and sterilizing the main machine. The amino acid type surfactant, the first skin conditioner, the hair conditioner and the chelating agent are sequentially added into a reaction pot, firstly stirred at a stirring speed of 5r/min, then stirred at a stirring speed of 10r/min and heated to 80 ℃. Keeping the reaction kettle at 80 ℃, adding the pH regulator into the reaction kettle, uniformly stirring, wherein the stirring speed is 10r/min, after completely dissolving, adding the thickening agent and the second skin conditioner, keeping the temperature, stirring for 10 minutes, wherein the stirring speed is 10r/min, and after completely dissolving, cooling to 45 ℃. When the temperature of the reaction kettle is reduced to 45 ℃, adding the pre-treated solvent and the third skin conditioner, stirring at a stirring speed of 10r/min, and after complete dissolution, cooling to 40 ℃. When the temperature of the reaction kettle is reduced to 40 ℃, adding a fourth skin conditioner, a humectant and a plant aromatic, stirring at a stirring speed of 10r/min, and after complete dissolution, starting to reduce the temperature to 35 ℃. And when the temperature of the reaction kettle is reduced to 35 ℃, adding a fifth skin conditioner, stirring at the stirring speed of 10r/min, completely dissolving, filtering by using filter cloth of 150 meshes, and discharging to obtain the Chinese herbal medicine shampoo.
Example 2
Accurately weighing various raw materials in the formula, placing the raw materials in a clean and sterilized container, and cleaning and sterilizing the main machine. The amino acid type surfactant, the first skin conditioner, the hair conditioner and the chelating agent are sequentially added into a reaction pot, firstly stirring is carried out at a stirring speed of 10r/min, then stirring is carried out at a stirring speed of 20r/min, and the temperature is raised to 90 ℃. Keeping the reaction kettle at 90 ℃, adding the pH regulator into the reaction kettle, uniformly stirring, wherein the stirring speed is 20r/min, after completely dissolving, adding the thickening agent and the second skin conditioner, keeping the temperature, stirring for 20 minutes, wherein the stirring speed is 20r/min, and after completely dissolving, cooling to 55 ℃. When the temperature of the reaction kettle is reduced to 55 ℃, adding the pre-treated solvent and the third skin conditioner, stirring at the stirring speed of 20r/min, and after complete dissolution, starting to reduce the temperature to 50 ℃. When the temperature of the reaction kettle is reduced to 50 ℃, adding a fourth skin conditioner, a humectant and a plant aromatic, stirring at a stirring speed of 20r/min, and after complete dissolution, cooling to 45 ℃. And when the temperature of the reaction kettle is reduced to 45 ℃, adding a fifth skin conditioner, stirring at the stirring speed of 20r/min, completely dissolving, filtering by using filter cloth of 250 meshes, and discharging to obtain the Chinese herbal medicine shampoo.
Example 3
Accurately weighing various raw materials in the formula, placing the raw materials in a clean and sterilized container, and cleaning and sterilizing the main machine. The amino acid type surfactant, the first skin conditioner, the hair conditioner and the chelating agent are sequentially added into a reaction pot, the stirring speed is firstly 8r/min, then the stirring speed is 15r/min, and the temperature is increased to 85 ℃. Keeping the reaction kettle at 85 ℃, adding the pH regulator into the reaction kettle, uniformly stirring, wherein the stirring speed is 15r/min, after completely dissolving, adding the thickening agent and the second skin conditioner, keeping the temperature, stirring for 15 minutes, wherein the stirring speed is 15r/min, and after completely dissolving, cooling to 50 ℃. When the temperature of the reaction kettle is reduced to 50 ℃, adding the pre-treated solvent and the third skin conditioner, stirring at a stirring speed of 15r/min, and after complete dissolution, starting to reduce the temperature to 45 ℃. When the temperature of the reaction kettle is reduced to 45 ℃, adding a fourth skin conditioner, a humectant and a plant aromatic, stirring at a stirring speed of 15r/min, and after complete dissolution, cooling to 40 ℃. And when the temperature of the reaction kettle is reduced to 40 ℃, adding a fifth skin conditioner, stirring at the stirring speed of 15r/min, completely dissolving, filtering by using filter cloth of 200 meshes, and discharging to obtain the Chinese herbal medicine shampoo.
Example 4
Accurately weighing various raw materials in the formula, placing the raw materials in a clean and sterilized container, and cleaning and sterilizing the main machine. The amino acid type surfactant, the first skin conditioner, the hair conditioner and the chelating agent are sequentially added into a reaction pot, firstly stirring is carried out at a stirring speed of 6r/min, then stirring is carried out at a stirring speed of 18r/min, and the temperature is raised to 87 ℃. Keeping the reaction kettle at 87 ℃, adding the pH regulator into the reaction kettle, uniformly stirring, wherein the stirring speed is 18r/min, after completely dissolving, adding the thickening agent and the second skin conditioner, keeping the temperature, stirring for 16 minutes, wherein the stirring speed is 18r/min, and after completely dissolving, cooling to 52 ℃. When the temperature of the reaction kettle is reduced to 52 ℃, adding the pre-treated solvent and the third skin conditioner, stirring at the stirring speed of 18r/min, and after complete dissolution, starting to reduce the temperature to 49 ℃. When the temperature of the reaction kettle is reduced to 49 ℃, adding a fourth skin conditioner, a humectant and a plant aromatic, stirring at the stirring speed of 18r/min, and after the fourth skin conditioner, the humectant and the plant aromatic are completely dissolved, starting to reduce the temperature to 39 ℃. And when the temperature of the reaction kettle is reduced to 39 ℃, adding a fifth skin conditioner, stirring at the stirring speed of 18r/min, completely dissolving, filtering by using filter cloth of 200 meshes, and discharging to obtain the Chinese herbal medicine shampoo.
Compared with the prior art, the invention has at least the following advantages:
1. the Chinese herbal medicine shampoo is prepared by adopting the amino acid type surfactant, the amino acid type surfactant has better foaming and dirt removing capability, the pH value of the amino acid type surfactant is close to that of human skin, the amino acid is a basic substance forming protein, the skin can be mild, and the irritation of the shampoo to the skin is smaller. Meanwhile, the Chinese herbal medicine shampoo prepared by the amino acid type surfactant has high biodegradability, and degradation products of the amino acid type surfactant are amino acid and fatty acid, so that the environment-friendly performance is better.
2. Due to the synergistic effect of the skin conditioner and the amino acid surfactant, the shampoo can remove dirt and dandruff without reducing the moisture of the stratum corneum of the skin, can further reduce the stimulation of the surfactant to the skin, and has a protective effect on the skin.
3. The Chinese herbal medicine shampoo adopts plant aromatic components, can replace components such as pigment, essence and the like, and uses the natural extracted Chinese herbal medicine plant components as the aromatic, so that the stimulation of the shampoo to the skin can be further reduced. Moreover, the Chinese herbal medicine components have better cleaning and antibacterial effects, such as the folium artemisiae argyi components, can relieve itching and deoiling, nourish the scalp and relieve alopecia.
The above examples only show some embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.
Claims (10)
1. The Chinese herbal medicine shampoo is characterized by comprising the following components in parts by mass:
2. the herbal shampoo of claim 1, wherein the amino acid-type surfactant is at least one of cocoyl alanine (TEA) salt, sodium methyl cocoyl taurate, cocamidopropyl hydroxysultaine, and cocoyl glutamic acid (TEA) salt.
3. The herbal shampoo of claim 1, wherein the skin conditioner is at least one of soapberry extract, snakehead gut extract, litchi chinensis fruit extract, caprylic acid glyceride, capric acid ester, sodium dilinoleamidopropyl PG-dimethyl ammonium chloride phosphate, lauroyl arginine ethyl ester hydrochloride, propylene glycol, sodium isostearoyl lactylate, lactic acid, and soy lecithin.
4. The herbal shampoo as claimed in claim 1 wherein the thickener is PEG-120 methyl glucose trioleate.
5. The herbal shampoo as defined in claim 1 wherein the humectant is at least one of propylene glycol, caprylyl hydroxamic acid, caprylate and 1, 2-pentanediol.
6. The herbal shampoo as defined in claim 1 wherein the chelating agent is sodium phytate.
7. The herbal shampoo of claim 1, wherein the plant fragrance is at least one of neroli oil, geranium oil, eucalyptus globulus oil, and mugwort oil.
8. The Chinese herbal medicine shampoo as claimed in claim 1, wherein the Chinese herbal medicine shampoo further comprises the following components in parts by mass:
1-3 parts of hair conditioner.
9. The Chinese herbal medicine shampoo as claimed in claim 1, wherein the Chinese herbal medicine shampoo further comprises the following components in parts by mass:
0.2 to 0.5 portion of pH regulator.
10. The preparation method of the Chinese herbal medicine shampoo is characterized by comprising the following steps:
sequentially adding an amino acid type surfactant, a first skin conditioner, a hair conditioner and a chelating agent into a reaction pot, and stirring for the first time at a first preset temperature to obtain a first mixture;
maintaining the reaction kettle at a first preset temperature state, adding a pH regulator into the first mixture, and carrying out second stirring operation to obtain a second mixture;
adding a thickening agent and a second skin conditioner into the second mixture, and carrying out stirring operation for the third time to obtain a third mixture;
cooling the reaction kettle to a second preset temperature, adding a solvent and a third skin conditioner into the third mixture, and stirring for the fourth time to obtain a fourth mixture;
cooling the reaction kettle to a third preset temperature, adding a fourth skin conditioner, a humectant and a plant aromatic into the fourth mixture, and performing fifth stirring operation to obtain a fifth mixture;
and cooling the reaction kettle to a fourth preset temperature, adding a fifth skin conditioner into the fifth mixture, stirring for the sixth time, and completely dissolving to obtain the Chinese herbal medicine shampoo.
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| CN (1) | CN112870118A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106074252A (en) * | 2016-06-24 | 2016-11-09 | 杭州兰茜化妆品有限公司 | Shampoo |
| CN107536749A (en) * | 2017-08-23 | 2018-01-05 | 杭州兰茜化妆品有限公司 | Chinese medicine shampoo and its preparation technology |
| CN110302114A (en) * | 2019-08-08 | 2019-10-08 | 青龙高科技股份有限公司 | A kind of shampoo and preparation method thereof containing tea-seed oil and tea seed extract |
-
2020
- 2020-12-31 CN CN202011640063.5A patent/CN112870118A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106074252A (en) * | 2016-06-24 | 2016-11-09 | 杭州兰茜化妆品有限公司 | Shampoo |
| CN107536749A (en) * | 2017-08-23 | 2018-01-05 | 杭州兰茜化妆品有限公司 | Chinese medicine shampoo and its preparation technology |
| CN110302114A (en) * | 2019-08-08 | 2019-10-08 | 青龙高科技股份有限公司 | A kind of shampoo and preparation method thereof containing tea-seed oil and tea seed extract |
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| 吴久阳等: "中草药提取液在防脱生发洗发水中的应用", 《精细与专用化学品》 * |
| 李魁等: "一种中药组方育发液对小鼠毛发生长的影响", 《日用化学品科学》 * |
| 杨晓珊: "甲基椰油酰基牛磺酸钠的性能研究及在洗发水中的应用", 《日用化学品科学》 * |
| 覃勇荣等: "无患子总皂苷提取工艺条件优化及天然洗涤剂研制", 《北方园艺》 * |
| 龙致科等: "洗发水用表面活性剂的性能研究", 《中国洗涤用品工业》 * |
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