CN112763291A - 一种快速获取电池游离电解液的方法 - Google Patents
一种快速获取电池游离电解液的方法 Download PDFInfo
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- CN112763291A CN112763291A CN202011583616.8A CN202011583616A CN112763291A CN 112763291 A CN112763291 A CN 112763291A CN 202011583616 A CN202011583616 A CN 202011583616A CN 112763291 A CN112763291 A CN 112763291A
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- 239000003792 electrolyte Substances 0.000 title claims abstract description 108
- 238000000034 method Methods 0.000 title claims abstract description 54
- 238000002791 soaking Methods 0.000 claims abstract description 74
- 239000002904 solvent Substances 0.000 claims abstract description 69
- 238000012360 testing method Methods 0.000 claims abstract description 34
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims abstract description 24
- IEJIGPNLZYLLBP-UHFFFAOYSA-N dimethyl carbonate Chemical compound COC(=O)OC IEJIGPNLZYLLBP-UHFFFAOYSA-N 0.000 claims abstract description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 9
- 238000005406 washing Methods 0.000 claims abstract description 5
- 238000005070 sampling Methods 0.000 claims abstract description 3
- 239000011259 mixed solution Substances 0.000 claims description 7
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 claims description 5
- 230000008569 process Effects 0.000 abstract description 15
- 238000012512 characterization method Methods 0.000 abstract description 12
- 238000004458 analytical method Methods 0.000 abstract description 10
- 239000000463 material Substances 0.000 abstract description 6
- 238000013461 design Methods 0.000 abstract description 4
- 208000032953 Device battery issue Diseases 0.000 abstract description 2
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 14
- 229910001416 lithium ion Inorganic materials 0.000 description 12
- 230000000694 effects Effects 0.000 description 5
- 238000007654 immersion Methods 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 4
- 239000002184 metal Substances 0.000 description 4
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 3
- 230000008859 change Effects 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 239000008151 electrolyte solution Substances 0.000 description 3
- 239000010439 graphite Substances 0.000 description 3
- 229910002804 graphite Inorganic materials 0.000 description 3
- 229910052744 lithium Inorganic materials 0.000 description 3
- 231100000956 nontoxicity Toxicity 0.000 description 3
- 238000007789 sealing Methods 0.000 description 3
- 239000002699 waste material Substances 0.000 description 3
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- QSNQXZYQEIKDPU-UHFFFAOYSA-N [Li].[Fe] Chemical compound [Li].[Fe] QSNQXZYQEIKDPU-UHFFFAOYSA-N 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 229910001386 lithium phosphate Inorganic materials 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- 239000002985 plastic film Substances 0.000 description 2
- 229920006255 plastic film Polymers 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 238000011076 safety test Methods 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- TWQULNDIKKJZPH-UHFFFAOYSA-K trilithium;phosphate Chemical compound [Li+].[Li+].[Li+].[O-]P([O-])([O-])=O TWQULNDIKKJZPH-UHFFFAOYSA-K 0.000 description 2
- 230000002159 abnormal effect Effects 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
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- 239000000706 filtrate Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 231100000957 no side effect Toxicity 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
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- 238000005245 sintering Methods 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/04—Preparation or injection of sample to be analysed
- G01N30/06—Preparation
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/72—Mass spectrometers
- G01N30/7206—Mass spectrometers interfaced to gas chromatograph
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- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
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Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1888889A (zh) * | 2006-07-21 | 2007-01-03 | 天津力神电池股份有限公司 | 一种测定锂离子电池电解液中有机组分的方法 |
CN102610813A (zh) * | 2011-12-31 | 2012-07-25 | 华为技术有限公司 | 一种去除磷酸铁锂中杂质的方法及其电池 |
CN105355970A (zh) * | 2015-12-16 | 2016-02-24 | 东莞市杉杉电池材料有限公司 | 一种三元正极材料锂离子电池电解液及三元正极材料锂离子电池 |
CN105449297A (zh) * | 2015-12-28 | 2016-03-30 | 东莞新能源科技有限公司 | 电解液消耗量的定量分析方法 |
CN105720317A (zh) * | 2016-04-28 | 2016-06-29 | 深圳市力为锂能科技有限公司 | 一种废旧锂离子电池的回收方法及其装置 |
CN110797574A (zh) * | 2019-10-28 | 2020-02-14 | 桑顿新能源科技(长沙)有限公司 | 一种锂离子电池用非水电解液及其锂离子电池 |
CN110875499A (zh) * | 2018-08-31 | 2020-03-10 | 宁德时代新能源科技股份有限公司 | 电池补锂的方法 |
-
2020
- 2020-12-28 CN CN202011583616.8A patent/CN112763291A/zh active Pending
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1888889A (zh) * | 2006-07-21 | 2007-01-03 | 天津力神电池股份有限公司 | 一种测定锂离子电池电解液中有机组分的方法 |
CN102610813A (zh) * | 2011-12-31 | 2012-07-25 | 华为技术有限公司 | 一种去除磷酸铁锂中杂质的方法及其电池 |
CN105355970A (zh) * | 2015-12-16 | 2016-02-24 | 东莞市杉杉电池材料有限公司 | 一种三元正极材料锂离子电池电解液及三元正极材料锂离子电池 |
CN105449297A (zh) * | 2015-12-28 | 2016-03-30 | 东莞新能源科技有限公司 | 电解液消耗量的定量分析方法 |
CN105720317A (zh) * | 2016-04-28 | 2016-06-29 | 深圳市力为锂能科技有限公司 | 一种废旧锂离子电池的回收方法及其装置 |
CN110875499A (zh) * | 2018-08-31 | 2020-03-10 | 宁德时代新能源科技股份有限公司 | 电池补锂的方法 |
CN110797574A (zh) * | 2019-10-28 | 2020-02-14 | 桑顿新能源科技(长沙)有限公司 | 一种锂离子电池用非水电解液及其锂离子电池 |
Non-Patent Citations (2)
Title |
---|
孙顺: "磷酸铁锂电池循环性能衰减规律及加速寿命试验的研究", 《中国优秀博硕士学位论文全文数据库(博士) 工程科技Ⅱ辑》 * |
胡敏艺 等: "废旧锂离子电池电解液处理技术现状与展望", 《湖南有色金属》 * |
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Inventor after: Wu Zhengneng Inventor after: Hu Xueping Inventor after: Gao Fengjie Inventor after: Sun Qi Inventor after: Yang Qingheng Inventor before: Yuzhengri Inventor before: Liang Ting Inventor before: Xu Hui Inventor before: Deng Wei Inventor before: Yao Yao Inventor before: Liu Guangming Inventor before: Zhou Yong Inventor before: Hu Xueping Inventor before: Yang Qingheng |
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Application publication date: 20210507 |