CN112603869A - 一种美白淡斑霜及其制备方法 - Google Patents
一种美白淡斑霜及其制备方法 Download PDFInfo
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- CN112603869A CN112603869A CN202110018890.9A CN202110018890A CN112603869A CN 112603869 A CN112603869 A CN 112603869A CN 202110018890 A CN202110018890 A CN 202110018890A CN 112603869 A CN112603869 A CN 112603869A
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- Prior art keywords
- whitening
- spot
- extract
- phase
- cream
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Abstract
本发明涉及一种美白淡斑霜及其制备方法,该美白淡斑霜包括以下质量百分数的组分:4‑丁基间苯二酚3%;烟酰胺2%;生育酚1~3%;乙酰半胱氨酸0.5~1%;精氨酸阿魏酸盐0.3~0.5%;1‑甲基乙内酰脲‑2‑酰亚胺0.2~0.3%;甘油葡糖苷0.5~1%;润肤剂13.8~14.2%;保湿剂5.3~5.5%;皮肤调理剂0.875~0.95%;增稠剂6.3~6.5%;乳化剂5.7~6%;防腐剂0.6~0.8%;其他添加剂0.3~0.35%;余量为水。该美白淡斑淡斑霜能够有效地起到美白淡斑的效果,且稳定、不易变色、刺激性低。
Description
技术领域
本发明涉及化妆品领域,具体涉及一种美白淡斑霜及其制备方法。
背景技术
目前,市面上有很多美白化妆品,按剂型通常可以分为液体类、乳液类、霜类、膏类等。现有的美白淡斑化妆品没能达到相应的美白去斑效果,同等添加量下产品存在不安全、产生不良反应等问题,并且存在产品稳定性差的问题,在原料组合及制备方法方面都不够理想。如何降低美白淡斑化妆品的刺激性,提高化妆品的稳定,是目前美白淡斑化妆品面临的问题。
发明内容
针对现有技术的不足,本发明的第一目的是提供一种美白淡斑霜,该美白淡斑淡斑霜能够有效地起到美白淡斑的效果,且稳定、不易变色、刺激性低。
本发明的第二目的是提供一种美白淡斑霜的制备方法,该制备方法能够将各原料分散均匀,提高产品的稳定性,并且能够保持原料的活性。
为实现本发明的第一目的,本发明提供了一种美白淡斑霜,其包括以下质量百分数的组分:4-丁基间苯二酚3%;烟酰胺2%;生育酚1~3%;乙酰半胱氨酸0.5~1%;精氨酸阿魏酸盐0.3~0.5%;1-甲基乙内酰脲-2-酰亚胺0.2~0.3%;甘油葡糖苷0.5~1%;润肤剂13.8~14.2%;保湿剂5.3~5.5%;皮肤调理剂0.875~0.95%;增稠剂6.3~6.5%;乳化剂5.7~6%;防腐剂0.6~0.8%;其他添加剂0.3~0.35%;余量为水。
优选地,其他添加剂包括螯合剂,螯合剂为EDTA二钠;螯合剂在美白淡斑霜中的质量百分数为0.1%。
优选地,其他添加剂还包括抗氧化剂,抗氧化剂为焦亚硫酸钠;抗氧化剂在美白淡斑霜中的质量百分数为0.1~0.15%。
优选地,其他添加剂还包括芳香剂,芳香剂为香精;芳香剂在美白淡斑霜中的质量百分数为0.05~0.1%。
优选地,增稠剂包括蜂蜡、鲸蜡醇、硬脂醇和黄原胶;蜂蜡在美白淡斑霜中的质量百分数为3~3.2%;鲸蜡醇在美白淡斑霜中的质量百分数为1.8~2%;硬脂醇在美白淡斑霜中的质量百分数为1~1.2%;黄原胶在美白淡斑霜中的质量百分数为0.2~0.3%。
优选地,润肤剂包括甘油、棕榈酸乙基己酯、聚二甲基硅氧烷、三(辛基十二烷醇)柠檬酸酯、辛酸甘油三酯或癸酸甘油三酯和尿囊素;甘油在美白淡斑霜中的质量百分数为5~5.2%;棕榈酸乙基己酯在美白淡斑霜中的质量百分数为2.8~3%;聚二甲基硅氧烷在美白淡斑霜中的质量百分数为2~2.3%;三(辛基十二烷醇)柠檬酸酯在美白淡斑霜中的质量百分数为2~2.2%;辛酸甘油三酯或癸酸甘油三酯在美白淡斑霜中的质量百分数为2~2.2%;尿囊素在美白淡斑霜中的质量百分数为0.2~0.3%。
优选地,保湿剂为丁二醇;
优选地,皮肤调理剂包括茶叶提取物、光果甘草根提取物、虎杖根提取物、黄芩根提取物、积雪草根提取物、迷迭香花和/或叶和/或茎提取物、母菊花和/或叶和/或茎提取物、朝鲜当归根提取物、番石榴叶提取物、莲叶提取物和羧甲基壳多糖;茶叶提取物在美白淡斑霜中的质量百分数为0.1~0.12%光果甘草根提取物、虎杖根提取物、黄芩根提取物、积雪草根提取物、迷迭香花和/或叶和/或茎提取物、母菊花和/或叶和/或茎提取物在美白淡斑霜中的质量百分数分别为0.05~0.08%;朝鲜当归根提取物、番石榴叶提取物、莲叶提取物在美白淡斑霜中的质量百分数分别为0.02~0.025%;羧甲基壳多糖在美白淡斑霜中的质量百分数为0.08~0.1%。
优选地,乳化剂包括硬脂醇聚醚-2、硬脂醇聚醚-21、甘油硬脂酸酯、聚丙烯酸钠、C18~21烷和十三烷醇聚醚-6;硬脂醇聚醚-2在美白淡斑霜中的质量百分数为2~2.3%;硬脂醇聚醚-21在美白淡斑霜中的质量百分数为2~2.3%;甘油硬脂酸酯在美白淡斑霜中的质量百分数为0.8~1%;聚丙烯酸钠在美白淡斑霜中的质量百分数为0.21~0.22%;C18~21烷在美白淡斑霜中的质量百分数为0.34~0.35%;十三烷醇聚醚-6在美白淡斑霜中的质量百分数为0.14~0.15%;
优选地,防腐剂包括辛酰羟肟酸、乙基己基甘油、1,2-己二醇、丙二醇和羟苯甲酯;辛酰羟肟酸在美白淡斑霜中的质量百分数为0.24~0.26%;乙基己基甘油在美白淡斑霜中的质量百分数为0.28~0.3%;1,2-己二醇在美白淡斑霜中的质量百分数为0.02~0.03%;丙二醇在美白淡斑霜中的质量百分数为0.02~0.03%;羟苯甲酯在美白淡斑霜中的质量百分数为0.1~0.12%。
为实现本发明的第二目的,本发明提供了一种美白淡斑霜的制备方法,其包括以下步骤:
步骤一:分别准备A相、B相、C相、D相和E相的原料;A相的原料包括第一部分水、甘油、烟酰胺、乙酰半胱氨酸、黄原胶、1-甲基乙内酰脲-2-酰亚胺、精氨酸阿魏酸盐、焦亚硫酸钠、尿囊素、羟苯甲酯和EDTA二钠,A相的原料在≥75℃的条件下分散均匀;B相的原料包括蜂蜡、棕榈酸乙基己酯、鲸蜡醇、聚二甲基硅氧烷、三(辛基十二烷醇)柠檬酸酯、辛酸/癸酸甘油三酯、硬脂醇聚醚-2、硬脂醇聚醚-21、甘油硬脂酸酯、生育酚和硬脂醇,B相的原料在≥75℃的条件下分散均匀;C相的原料包括聚丙烯酸钠、C18~21烷和十三烷醇聚醚-6,C相的原料分散均匀;D相的原料包括第一部分丁二醇和4-丁基间苯二酚,D相的原料在温度≤45℃的条件下分散均匀;E相包括水茶叶提取物、光果甘草根提取物、虎杖根提取物、黄芩根提取物、积雪草根提取物、迷迭香花和/或叶和/或茎提取物、母菊花和/或叶和/或茎提取物、朝鲜当归根提取物、番石榴叶提取物、莲叶提取物、第二部分水、第二部分丁二醇、甘油葡糖苷、辛酰羟肟酸、乙基己基甘油、1,2-己二醇、丙二醇、羧甲基壳多糖和香精,E相的原料在温度≤45℃的条件下分散均匀;相对于美白淡斑霜的总质量,各原料的质量百分数如下:4-丁基间苯二酚3%;烟酰胺2%;生育酚1~3%;乙酰半胱氨酸0.5~1%;精氨酸阿魏酸盐0.3~0.5%;1-甲基乙内酰脲-2-酰亚胺0.2~0.3%;甘油葡糖苷0.5~1%;EDTA二钠0.1%;焦亚硫酸钠0.1~0.15%;香精0.05~0.1%;蜂蜡3~3.2%;鲸蜡醇1.8~2%;硬脂醇1~1.2%;黄原胶0.2~0.3%;甘油5~5.2%;棕榈酸乙基己酯2.8~3%;聚二甲基硅氧烷2~2.3%;三(辛基十二烷醇)柠檬酸酯2~2.2%;辛酸甘油三酯或癸酸甘油三酯2~2.2%;尿囊素0.2~0.3%;茶叶提取物0.1~0.12%;光果甘草根提取物0.05~0.08%;虎杖根提取物0.05~0.08%;黄芩根提取物0.05~0.08%;积雪草根提取物0.05~0.08%;迷迭香花和/或叶和/或茎提取物0.05~0.08%;母菊花和/或叶和/或茎提取物0.05~0.08%;朝鲜当归根提取物0.02~0.025%;番石榴叶提取物0.02~0.025%;莲叶提取物0.02~0.025%;羧甲基壳多糖0.08~0.1%;硬脂醇聚醚-2 2~2.3%;硬脂醇聚醚-21 2~2.3%;甘油硬脂酸酯0.8~1%;聚丙烯酸钠0.21~0.22%;C18~21烷0.34~0.35%;十三烷醇聚醚-6 0.14~0.15%;辛酰羟肟酸0.24~0.26%;乙基己基甘油0.28~0.3%;1,2-己二醇0.02~0.03%;丙二醇0.02~0.03%;羟苯甲酯0.1~0.12%;丁二醇5.3~5.5%;余量为水;
步骤二:将A相原料放入真空乳化搅拌机,再放入B相原料,搅拌均匀后,均质乳化3~5分钟后,加入C相的原料,均质并持续搅拌、抽真空,恒温静置10分钟以上;
步骤三:降温至40~45℃,加入D相的原料和E相的原料,充分搅拌均匀;
步骤四:降温至35~38℃,出料,静置。
优选地,在步骤一中,第一部分水和第二部分水的质量比为(25~30):1。
优选地,在步骤一中,分散A相的原料时,先将1-甲基乙内酰脲-2-酰亚胺和精氨酸阿魏酸盐混合均匀,再将所得的混合物与其他A相的原料混合;分散E相的原料时,先将第二部分水中的第三部分水、茶叶提取物、光果甘草根提取物、虎杖根提取物、黄芩根提取物、积雪草根提取物、迷迭香花和/或叶和/或茎提取物和母菊花和/或叶和/或茎提取物混合均匀,将第二部分水中的第四部分水水、第二部分丁二醇、朝鲜当归根提取物、番石榴叶提取物和莲叶提取物混合均匀,将辛酰羟肟酸、乙基己基甘油、1,2-己二醇和丙二醇混合均匀,再将所得的三个混合物与其他E相的原料混合。
与现有技术相比,本发明能够取得以下有益效果:
本发明的美白淡斑淡斑霜控制4-丁基间苯二酚的用量为3%,解决了使用4-丁基间苯二酚剂量过大容易引起刺激、产品外观粗糙、分层的问题,并且通过烟酰胺、乙酰半胱氨酸、1-甲基乙内酰脲-2-酰亚胺、精氨酸阿魏酸盐、甘油葡糖苷等配合4-丁基间苯二酚使用,提高4-丁基间苯二酚的美白淡斑效果,也不需要降低配方的pH值,减少刺激性,而且这些原料的配合还能解决4-丁基间苯二酚在配方中容易氧化变色的问题。此外,配方中还可以添加生育酚和螯合剂EDTA二钠,进一步增加配方的抗氧化能力,从而使4-丁基间苯二酚不易产生氧化,增加配方的稳定性。此外,本发明还利用了蜂蜡、硬脂醇聚醚-2、硬脂醇聚醚-21的耐离子性,使用膏体在制备后,耐寒耐热的稳定性更强,膏体细腻不粗糙。
本发明在制备过程中,将原料分为了A相、B相、C相、D相和E相,其中A相和B相的原料可以加热分散,使得原料充分溶解均匀,A相和B相的原料可以耐高温,不会因为温度过高而失活。C相是一个增稠剂,在A相与B相混合乳化后,再加入C相继续乳化,可以起到增稠和助乳化作用。D相是去斑美白的主要成分,要独立溶解,再低温加入料体。E相是活性添加剂,这类提取物含量高的,只能在料体低温的时候加入,这样才能保证活性。
具体实施方式
以下将结合具体实施例对本发明做进一步详细的说明。
实施例1
本实施例采用的原料及其含量、作用、混合过程所属组相如下表1所示。
表1实施例1的原料
本实施例的制备方法包括以下步骤:
1.将A相原料加入水相锅中,搅拌升温至80℃,充分搅拌均匀,保温备用;
2.将B相原料加入油相锅中,搅拌升温至75℃,充分搅拌均匀,保温备用;
3.先将A相原料先抽入真空乳化搅拌机,再将B相原料抽入,搅拌均匀后,均质乳化3分钟,加入C相,均质2分钟,持续搅拌,抽真空,恒温10分钟;
4.降温至45℃时,加入D相、E相原料,充分搅拌均匀;
5.降温至38℃时,出料、静置;
6.检验。
实施例2
本实施例采用的原料及其含量、作用、混合过程所属组相如下表2所示。
表2实施例2的原料
本实施例的制备方法包括以下步骤:
1.将A相原料加入水相锅中,搅拌升温至75℃,充分搅拌均匀,保温备用;
2.将B相原料加入油相锅中,搅拌升温至80℃,充分搅拌均匀,保温备用;
3.先将A相原料先抽入真空乳化搅拌机,再将B相原料抽入,搅拌均匀后,均质乳化5分钟,加入C相,均质3分钟,持续搅拌,抽真空,恒温10分钟;
4.降温至40℃时,加入D相、E相原料,充分搅拌均匀;
5.降温至35℃时,出料、静置;
6.检验。
对比例1
本对比例的配方以及制备方法与实施例1基本相同,区别在于部分原料的用量不同,具体如下表3所示。
表3对比例1和实施例1的原料用量区别
原料 | 对比例1 | 实施例1 |
生育酚 | 1.5% | 1% |
乙酰半胱氨酸 | 0.5% | 1% |
烟酰胺 | 1.5% | 2% |
甘油葡糖苷 | 1.5% | 1% |
4-丁基间苯二酚 | 4% | 3% |
蜂蜡 | 1% | 2% |
对比例2
本对比例的配方以及制备方法与实施例1基本相同,区别在于部分原料的用量不同,具体如下表4所示。
表4对比例2和实施例1的原料用量区别
原料 | 对比例2 | 实施例1 |
生育酚 | 0% | 1% |
乙酰半胱氨酸 | 0% | 1% |
烟酰胺 | 3% | 2% |
甘油葡糖苷 | 0.5% | 1% |
4-丁基间苯二酚 | 2% | 3% |
蜂蜡 | 3% | 2% |
A相中水 | 59.15% | 57.65% |
对比例3
本对比例的配方与实施例1相同,区别在于制备方法不同,对比例3不区分A相、B相、C相、D相和E相原料,对比例3的制备方法包括以下步骤:
1.将所有原料放入搅拌装置中,升温至45℃,充分搅拌均匀;
2.降温至38℃时,出料、静置;
3.检验。
以下对实施例以及对比例所得的美白淡斑霜进行性能测试,包括稳定性测试、过敏测试和祛斑霜效果测试。
(1)稳定性
结果如下表5所示。
表5稳定性测试结果
由上可见,本发明实施例1~2制备的美白淡斑霜具有稳定、不变色、不泛粗的优点,而对比例1中4-丁基间苯二酚过量,导致所得淡斑霜在略高的温度下容易变色;对比例3不采用本发明的制备方法,而采用全部原料混合的方法,所得的淡斑霜容易在离心和加热条件下容易分层;对比例2虽然4-丁基间苯二酚用量减少,但与之配合的生育酚、乙酰半胱氨酸、甘油葡糖苷等用量也少,导致了4-丁基间苯二酚仍然容易氧化。
(2)过敏测试
本测试对30人试用结果统计过敏数并计算过敏率。结果如下表6所示。
表6过敏测试结果
由上可见,相比于4-丁基间苯二酚用量过量的对比例1,本发明实施例1~2的过敏率较低,这是主要因为本发明降低了4-丁基间苯二酚的用量。
(3)祛斑效果测试
本测试对80人试用结果进行统计,其中雀斑35人,黄褐斑20人,晒斑23人,铅汞斑2人,每人每天使用量相同。对比未使用任何产品时的空白样来确定色素淡化率,结果如下表7所示。
表7祛斑效果测试结果(色素淡化率/%)
续表7:
由上可见,本发明的淡斑霜对雀斑、黄褐斑、晒斑和铅汞斑有良好的祛斑效果,尤其是对晒斑和雀斑。与对比例1相比,对比例1起始的祛斑效果较好,使用时间延长后本发明实施例与对比例1祛斑效果相当,而本发明实施例克服了对比例1刺激性强、易变色等缺点。与对比例2相比,对比例2的祛斑效果较差。
综上可见,本发明的美白淡斑霜稳定、不变色且低刺激性,具有较好的美白祛斑功效。
最后需要强调的是,以上所述仅为本发明的优选实施例,并不用于限制本发明。凡在本发明的精神和原则之内,所做的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。
Claims (10)
1.一种美白淡斑霜,其特征在于包括以下质量百分数的组分:4-丁基间苯二酚3%;烟酰胺2%;生育酚1~3%;乙酰半胱氨酸0.5~1%;精氨酸阿魏酸盐0.2~0.5%;1-甲基乙内酰脲-2-酰亚胺0.2~0.3%;甘油葡糖苷0.5~1%;润肤剂13.8~14.2%;保湿剂5.3~5.5%;皮肤调理剂0.875~0.95%;增稠剂6.3~6.5%;乳化剂5.7~6%;防腐剂0.6~0.8%;其他添加剂0.3~0.35%;余量为水。
2.根据权利要求1所述的美白淡斑霜,其特征在于:
所述其他添加剂包括螯合剂,所述螯合剂为EDTA二钠;所述螯合剂在所述美白淡斑霜中的质量百分数为0.1%。
3.根据权利要求2所述的美白淡斑霜,其特征在于:
所述其他添加剂还包括抗氧化剂,所述抗氧化剂为焦亚硫酸钠;所述抗氧化剂在所述美白淡斑霜中的质量百分数为0.1~0.15%。
4.根据权利要求3所述的美白淡斑霜,其特征在于:
所述其他添加剂还包括芳香剂,所述芳香剂为香精;所述芳香剂在所述美白淡斑霜中的质量百分数为0.05~0.1%。
5.根据权利要求1至4任一项所述的美白淡斑霜,其特征在于:
所述增稠剂包括蜂蜡、鲸蜡醇、硬脂醇和黄原胶;
所述蜂蜡在所述美白淡斑霜中的质量百分数为3~3.2%;
所述鲸蜡醇在所述美白淡斑霜中的质量百分数为1.8~2%;
所述硬脂醇在所述美白淡斑霜中的质量百分数为1~1.2%;
所述黄原胶在所述美白淡斑霜中的质量百分数为0.2~0.3%。
6.根据权利要求1至4任一项所述的美白淡斑霜,其特征在于:
所述润肤剂包括甘油、棕榈酸乙基己酯、聚二甲基硅氧烷、三(辛基十二烷醇)柠檬酸酯、辛酸甘油三酯或癸酸甘油三酯和尿囊素;
所述甘油在所述美白淡斑霜中的质量百分数为5~5.2%;
所述棕榈酸乙基己酯在所述美白淡斑霜中的质量百分数为2.8~3%;
所述聚二甲基硅氧烷在所述美白淡斑霜中的质量百分数为2~2.3%;
所述三(辛基十二烷醇)柠檬酸酯在所述美白淡斑霜中的质量百分数为2~2.2%;
所述辛酸甘油三酯或癸酸甘油三酯在所述美白淡斑霜中的质量百分数为2~2.2%
所述尿囊素在所述美白淡斑霜中的质量百分数为0.2~0.3%。
7.根据权利要求1至4任一项所述的美白淡斑霜,其特征在于:
所述保湿剂为丁二醇;
所述皮肤调理剂包括茶叶提取物、光果甘草根提取物、虎杖根提取物、黄芩根提取物、积雪草根提取物、迷迭香花和/或叶和/或茎提取物、母菊花和/或叶和/或茎提取物、朝鲜当归根提取物、番石榴叶提取物、莲叶提取物和羧甲基壳多糖;
所述茶叶提取物在所述美白淡斑霜中的质量百分数为0.1~0.12%
所述光果甘草根提取物、所述虎杖根提取物、所述黄芩根提取物、所述积雪草根提取物、所述迷迭香花和/或叶和/或茎提取物、所述母菊花和/或叶和/或茎提取物在所述美白淡斑霜中的质量百分数分别为0.05~0.08%;所述朝鲜当归根提取物、所述番石榴叶提取物、所述莲叶提取物在所述美白淡斑霜中的质量百分数分别为0.02~0.025%;
所述羧甲基壳多糖在所述美白淡斑霜中的质量百分数为0.08~0.1%。
8.根据权利要求1至4任一项所述的美白淡斑霜,其特征在于:
所述乳化剂包括硬脂醇聚醚-2、硬脂醇聚醚-21、甘油硬脂酸酯、聚丙烯酸钠、C18~21烷和十三烷醇聚醚-6;
所述硬脂醇聚醚-2在所述美白淡斑霜中的质量百分数为2~2.3%;
所述硬脂醇聚醚-21在所述美白淡斑霜中的质量百分数为2~2.3%;
所述甘油硬脂酸酯在所述美白淡斑霜中的质量百分数为0.8~1%;
所述聚丙烯酸钠在所述美白淡斑霜中的质量百分数为0.21~0.22%
所述C18~21烷在所述美白淡斑霜中的质量百分数为0.32~0.35%;
所述十三烷醇聚醚-6在所述美白淡斑霜中的质量百分数为0.14~0.16%;
所述防腐剂包括辛酰羟肟酸、乙基己基甘油、1,2-己二醇、丙二醇和羟苯甲酯;
所述辛酰羟肟酸在所述美白淡斑霜中的质量百分数为0.24~0.26%;
所述乙基己基甘油在所述美白淡斑霜中的质量百分数为0.28~0.3%;
所述1,2-己二醇在所述美白淡斑霜中的质量百分数为0.02~0.03%;
所述丙二醇在所述美白淡斑霜中的质量百分数为0.02~0.03%;
所述羟苯甲酯在所述美白淡斑霜中的质量百分数为0.1~0.12%。
9.一种美白淡斑霜的制备方法,其特征在于包括以下步骤:
步骤一:分别准备A相、B相、C相、D相和E相的原料;所述A相的原料包括第一部分水、甘油、烟酰胺、乙酰半胱氨酸、黄原胶、1-甲基乙内酰脲-2-酰亚胺、精氨酸阿魏酸盐、焦亚硫酸钠、尿囊素、羟苯甲酯和EDTA二钠,所述A相的原料在≥75℃的条件下分散均匀;所述B相的原料包括蜂蜡、棕榈酸乙基己酯、鲸蜡醇、聚二甲基硅氧烷、三(辛基十二烷醇)柠檬酸酯、辛酸/癸酸甘油三酯、硬脂醇聚醚-2、硬脂醇聚醚-21、甘油硬脂酸酯、生育酚和硬脂醇,所述B相的原料在≥75℃的条件下分散均匀;所述C相的原料包括聚丙烯酸钠、C18~21烷和十三烷醇聚醚-6,所述C相的原料分散均匀;所述D相的原料包括第一部分丁二醇和4-丁基间苯二酚,所述D相的原料在温度≤45℃的条件下分散均匀;所述E相包括水茶叶提取物、光果甘草根提取物、虎杖根提取物、黄芩根提取物、积雪草根提取物、迷迭香花和/或叶和/或茎提取物、母菊花和/或叶和/或茎提取物、朝鲜当归根提取物、番石榴叶提取物、莲叶提取物、第二部分水、第二部分丁二醇、甘油葡糖苷、辛酰羟肟酸、乙基己基甘油、1,2-己二醇、丙二醇、羧甲基壳多糖和香精,所述E相的原料在温度≤45℃的条件下分散均匀;相对于美白淡斑霜的总质量,各原料的质量百分数如下:4-丁基间苯二酚3%;烟酰胺2%;生育酚1~3%;乙酰半胱氨酸0.5~1%;精氨酸阿魏酸盐0.2~0.5%;1-甲基乙内酰脲-2-酰亚胺0.2~0.3%;甘油葡糖苷0.5~1%;EDTA二钠0.1%;焦亚硫酸钠0.1~0.15%;香精0.05~0.1%;蜂蜡3~3.2%;鲸蜡醇1.8~2%;硬脂醇1~1.2%;黄原胶0.2~0.3%;甘油5~5.2%;棕榈酸乙基己酯2.8~3%;聚二甲基硅氧烷2~2.3%;三(辛基十二烷醇)柠檬酸酯2~2.2%;辛酸甘油三酯或癸酸甘油三酯2~2.2%;尿囊素0.2~0.3%;茶叶提取物0.1~0.12%;光果甘草根提取物0.05~0.08%;虎杖根提取物0.05~0.08%;黄芩根提取物0.05~0.08%;积雪草根提取物0.05~0.08%;迷迭香花和/或叶和/或茎提取物0.05~0.08%;母菊花和/或叶和/或茎提取物0.05~0.08%;朝鲜当归根提取物0.02~0.025%;番石榴叶提取物0.02~0.025%;莲叶提取物0.02~0.025%;羧甲基壳多糖0.08~0.1%;硬脂醇聚醚-2 2~2.3%;硬脂醇聚醚-21 2~2.3%;甘油硬脂酸酯0.8~1%;聚丙烯酸钠0.21~0.22%;C18~21烷0.32~0.35%;十三烷醇聚醚-6 0.14~0.16%;辛酰羟肟酸0.24~0.26%;乙基己基甘油0.28~0.3%;1,2-己二醇0.02~0.03%;丙二醇0.02~0.03%;羟苯甲酯0.1~0.12%;丁二醇5.3~5.5%;余量为水;
步骤二:将所述A相原料放入真空乳化搅拌机,再放入所述B相原料,搅拌均匀后,均质乳化3~5分钟后,加入所述C相的原料,均质并持续搅拌、抽真空,恒温静置10分钟以上;
步骤三:降温至40~45℃,加入所述D相的原料和所述E相的原料,充分搅拌均匀;
步骤四:降温至35~38℃,出料,静置。
10.根据权利要求9所述的制备方法,其特征在于:
在所述步骤一中,所述第一部分水和所述第二部分水的质量比为(25~30):1;
在所述步骤一中,分散所述A相的原料时,先将1-甲基乙内酰脲-2-酰亚胺和精氨酸阿魏酸盐混合均匀,再将所得的混合物与其他A相的原料混合;分散所述E相的原料时,先将第二部分水中的第三部分水、茶叶提取物、光果甘草根提取物、虎杖根提取物、黄芩根提取物、积雪草根提取物、迷迭香花和/或叶和/或茎提取物和母菊花和/或叶和/或茎提取物混合均匀,将第二部分水中的第四部分水水、第二部分丁二醇、朝鲜当归根提取物、番石榴叶提取物和莲叶提取物混合均匀,将辛酰羟肟酸、乙基己基甘油、1,2-己二醇和丙二醇混合均匀,再将所得的三个混合物与其他E相的原料混合。
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