CN112535642A

CN112535642A - Moisturizing repair DIY soft film capable of making sound and using method thereof

Info

Publication number: CN112535642A
Application number: CN202011414244.6A
Authority: CN
Inventors: 刘润平; 丁淑兰; 方跃龙
Original assignee: Guangzhou Ryepeak Cosmetics Co ltd
Current assignee: Guangzhou Ryepeak Cosmetics Co ltd
Priority date: 2020-12-03
Filing date: 2020-12-03
Publication date: 2021-03-23
Anticipated expiration: 2040-12-03
Also published as: CN112535642B

Abstract

The application relates to the field of skin care, and particularly discloses a moisturizing and repairing DIY soft film capable of making sound and a using method thereof. The DIY soft film consists of a gel component and a powder component, wherein the weight ratio of the gel component to the oxygen injection component to the powder component is 40-50:18-22: 3; each part of gel component comprises the following raw materials in parts by weight: 7-50 parts of a humectant I, 1-5 parts of a film forming agent, 1-5 parts of an emulsifier, 1-5 parts of a humectant II and 23-87.78 parts of water; each part of oxygen injection component comprises the following raw materials in parts by weight: 80-120 parts of humectant III and 0.1-1.0 part of carbon dioxide, wherein each part of powder component comprises 60-150 parts of filling powder. According to the application, carbon dioxide is filled into the humectant IV, so that after the carbon dioxide reacts with water in the gel component, the carbon dioxide reacts with the water to form carbonic acid, and then the carbonic acid is used for promoting red blood cells in the skin to release oxygen, so that the oxygen content of the skin is improved, and the skin metabolism is promoted.

Description

Moisturizing repair DIY soft film capable of making sound and using method thereof

Technical Field

The application relates to the field of skin care products, in particular to a moisturizing and repairing DIY soft film capable of making sound and a using method thereof.

Background

The soft film is a facial mask containing powder, the soft film after being prepared and used keeps a wet state and is flexibly attached to the skin, but cannot be attached to the skin or combined with the skin too tightly, the skin cannot be pulled, pulled or pressed, and the use is comfortable, so that the soft film is widely applied to daily personal skin care and beauty salon skin care.

The gel component of the soft membrane keeps a wet state, so that the air permeability of the soft membrane is smaller than that of the sheet-shaped membrane, and the characteristic of small air permeability is utilized to heat the skin in the face applying process, so that the blood flow speed of the face is accelerated, and the absorption of nutrient components in the soft membrane is promoted. The existing soft membrane basically has a simple water replenishing and moisturizing function, or has the effects of relieving, resisting aging, whitening and the like, and with the inevitable contact of tail gas and dust in daily life of people and daily skin care and makeup, dust particles and makeup residues are easy to accumulate in pores to block the pores, so that the delivery of skin care nutrient substances to a skin bottom layer is influenced, the absorption degree of the skin on the nutrient substances is reduced, and even if the soft membrane prevents the skin from contacting with the outside to improve the absorption of the nutrient substances by the skin, the residual wastes in the skin pores also influence the permeation of the nutrient substances and the absorption degree of the skin.

In view of the above problems, the applicant believes that the degree of absorption of nutrients into the skin in daily skin care of a soft film still needs to be improved.

Disclosure of Invention

In order to solve the problem that the absorption degree of skin to nutrient components is low in the soft mask skin care, the application provides a moisturizing repair DIY soft mask capable of making a sound and a using method thereof.

In a first aspect, the application provides a moisturizing and repairing DIY soft membrane capable of making sound, which adopts the following technical scheme:

a DIY soft mask capable of producing sound and maintaining moisture is composed of a gel component and a powder component, wherein the weight ratio of the gel component to the powder component is 40-50: 22;

each part of the gel component comprises the following raw materials in parts by weight:

phase A: 7-50 parts of humectant I

1-5 parts of film forming agent

Phase B: 1-5 parts of emulsifier

1-5 parts of humectant II

And C phase: 23-87.78 parts of water;

each part of the powder particle component comprises the following raw materials in parts by weight:

phase D: 80-120 parts of humectant III

Phase E: 0.1-1.0 part of carbon dioxide;

each part of the powder particle component comprises 60 to 150 parts of filling powder.

By adopting the technical scheme, carbon dioxide is mixed into the oxygen injection component, when the oxygen injection component is mixed with the gel component, the carbon dioxide is contacted with water in the gel component to form a carbonic acid component, so that the carbon dioxide concentration of the soft membrane is higher, when the soft membrane is applied to the face, the carbon dioxide concentration on the surface of the skin is higher, the red blood cells in the skin are promoted to release oxygen, and the released oxygen reversely conveys oxygen to the skin, so that the oxygen content in the skin is improved, the generation of skin collagen is stimulated, the pore metabolism is accelerated, waste in the pores is eliminated, the pores are dredged, and the effects of repairing the skin and shrinking the pores can be simultaneously achieved. After the adopted film forming agent, the filling powder and the gel component are mixed, the film forming speed of the soft film can be accelerated, so that the soft film layer is formed on the skin, the skin is separated from the outside, and the skin is shielded and protected.

In addition, as the oxygen injection component is mixed with the gel component, carbon dioxide is released from the mixed system, air flow sound is generated in the process that carbon dioxide gas is released from the gel mixed system, and the air flow sound generated in the process of releasing carbon dioxide relieves the pressure of a user; specifically, a process of releasing carbon dioxide exists in the process of stirring and mixing the oxygen injection component and the gel component, airflow sound is generated, carbon dioxide is continuously released in the process of applying the dough after uniform stirring, the airflow sound is continuously generated, and the amount of the carbon dioxide is controlled so that the process of generating the airflow sound lasts for 20-30 min.

In addition, the oxygen injection component and the powder component can be respectively used as two dosage forms and respectively packaged, namely, the gel component mixed with the phase A, the phase B and the phase C is used as a first dosage form, the oxygen injection component mixed with the phase D and the phase E is used as a second dosage form, the powder component is used as a third dosage form to form a DIY soft film of the three dosage forms, the two dosage forms and the third dosage form are respectively packaged, and the second dosage form and the third dosage form are added into the first dosage form to be mixed to form the soft film and are applied on the surface.

Alternatively, the oxygen injection component and the powder component are blended to form a dosage form for packaging, namely the gel component is used as a first dosage form, the oxygen injection component and the powder component are mixed to form a second dosage form, DIY soft films of the two dosage forms are formed and packaged respectively, and the second dosage form is added into the first dosage form and mixed to form a soft film when in use, and then the soft film is applied on the face for use. The mode of adopting two dosage forms can reduce the cost rising problem that leads to because three dosage forms package, can improve the mixing convenience when using simultaneously, and it is convenient to use.

The mode of adopting two dosage forms or three dosage forms of the soft film is in the protection scope of the application, and the blending of materials can be realized.

Preferably, in the phase A, the humectant I comprises the following raw materials in parts by weight:

the moisturizing agent can permeate into the inner layer of the skin, and the moisturizing performance of the soft membrane on the skin is improved, wherein the glycerin is mixed with the hydrolyzed sodium hyaluronate and the hyaluronic acid to absorb moisture in the air into the soft membrane, so that the soft membrane absorbs the moisture in the air after being applied to the skin, the soft state of the soft membrane is kept, and the moisturizing effect is performed on the skin.

The adopted glycerin has a soft and lubricating effect on the skin, but when the addition amount of the glycerin is high, the sticky feeling is easy to appear in a semi-dry state, and the use feeling is reduced, so that the addition amount of the glycerin polyether-26 is reduced, the moisturizing effect of a small amount of the glycerin polyether-26 is stronger than that of the glycerin, and the sticky feeling of the soft membrane in the semi-dry state caused by the glycerin can be reduced. The adopted hydrolyzed sodium hyaluronate can repair damaged cells and remove free radicals, thereby being beneficial to improving the activity of the cells; the sodium hyaluronate can soften stratum corneum, has strong affinity to skin, and can be firmly kept on the surface of skin, so that water is not easy to evaporate from the skin, and the water replenishing and retaining effects of the soft membrane on the skin can be improved; the sodium hyaluronate cross-linked polymer can absorb a large amount of water so as to achieve the effects of moisturizing water and preventing water loss, has transdermal property, can improve skin nutrition metabolism, and promotes a soft membrane to metabolize and remove residues in pores; the hyaluronic acid is used together with the hydrolyzed sodium hyaluronate, the acetylated sodium hyaluronate and the sodium hyaluronate cross-linked polymer, so that the water replenishing and locking effects of the gel components can be improved, the skin metabolism is promoted, residues in pores are discharged, the absorption of nutrient substances is promoted, and the soft membrane simultaneously achieves the effects of promoting the metabolism and supplementing nutrition.

The adopted panthenol has small molecular weight, can effectively permeate into the horny layer to soften the horny layer, further promotes the absorption of skin to nutrient components, and improves the moisture retention and absorption promotion effects of the soft membrane; the adopted polyglycerol-10 contains a large amount of hydroxyl groups, and can form a strong hydrogen bond effect with water molecules, so that the moisturizing effect of the soft film is improved; the adopted potassium chloride is mixed with water to form a saline state, so that the skin pores can be cleaned, the metabolism of skin is promoted, the pores are dredged, and the absorption of moisture-keeping components and nutrient components in the soft membrane is increased by cleaning the pores; the adopted Chondrus crispus, glucomannan and propylene glycol have moisturizing effect, and act together with the hyaluronic acid substances and panthenol to improve the moisturizing and water locking effects of the soft film.

Preferably, in phase a, the film forming agent is sodium alginate; in the phase B, the emulsifier is glycerol hard acid ester, and the humectant II is phytosterol oleate.

The sodium alginate is mixed with the powder components to promote the curing of the soft film and the emulsion film forming efficiency so as to form a film state, and the degree of adhesion with the skin is high; on the other hand, the sodium alginate can increase the moisture retention and water locking property, the tightness and the elasticity of the skin, enhance the immunity and the repair effect of the skin, improve the grease secretion of dry and oily skin, promote pore shrinkage, improve the problem of large pores, and enable the soft membrane to play the roles of promoting metabolism and supplementing water and repairing the skin under the condition of isolating the outside.

The adopted hard glyceride has higher emulsification effect and excellent dispersibility and permeability, so that the A phase, the B phase and the C phase are fully dispersed and emulsified after being mixed to form a stable gel emulsification system, the gel component has high stability, and the penetration and moisture retention performance to skin are good after being mixed with the particle component to form a soft membrane. The adopted phytosterol oleate improves the softness and moisture retention of the gel component.

Preferably, the B phase also comprises 1-5 parts of caprylic/capric triglyceride.

The adopted caprylic/capric triglyceride is compatible with human skin, has fresh texture and is odorless, so that the gel component has the effects of lubricating and softening the skin, promotes the penetration of nutrient components and effective components, and improves the penetration and absorption of nutrient components such as moisture components in the gel component.

Preferably, the gel component is prepared by the following steps:

step one, adding the phase C into an emulsifying device, heating to 80-85 ℃, stirring, then sequentially adding the humectant I and the film forming agent, uniformly stirring and dispersing, then preserving heat at 80-85 ℃, and continuously stirring to obtain a mixture;

step two, heating the phase B to 65-75 ℃, stirring and melting, then adding the phase B into the mixture prepared in the step one, homogenizing and stirring, cooling after complete emulsification, cooling to below 38 ℃, and filtering to obtain a gel component.

By adopting the technical scheme, the moisturizing component is added into water, the temperature is controlled, the stirring is carried out, the solubility of the phase A component in the water is promoted, and a stable water phase is formed; and adding the phase B of the oil phase into the water phase, homogenizing and emulsifying at high temperature to form a stable emulsifying system, and finally cooling and discharging, wherein the lower the temperature, the higher the viscosity, so as to form a stable gel component with certain viscosity.

Preferably, each portion of the gel component further comprises phases F and G:

and (3) phase F: 1-5 parts of humectant IV

0.1 to 0.5 portion of chelating agent

0.1-0.5 part of emollient

Phase G: 0.01-0.5 part of skin conditioner I

0.01-0.5 part of essence I;

in the phase F, the humectant IV is propylene glycol, the chelating agent is p-hydroxyacetophenone, and the emollient is hexanediol;

in phase G, the skin conditioner I is carnosine.

In the phase F, propylene glycol is used as a moisturizing component, and hexylene glycol is used as a moisturizing component, so that the phase F has good transdermal property, and the phase A moisturizing agent I and the phase B moisturizing agent II are promoted to permeate into the skin, so that the moisturizing effect is effectively achieved. The adopted p-hydroxyacetophenone has activity stability, is chelated with external dust particles after the soft film is coated, reduces the functional components of the soft film polluted by external substances, and can also improve the storage, preservation and quality guarantee performance of the gel component.

The carnosine adopted by the G phase can promote skin metabolism, assist in chelating metal ions and discharging the metal ions out of the skin, accelerate the discharge of skin metabolites, purify the skin, maintain the normal internal circulation of the skin, protect lipid components of cell membranes, prevent the damage of free radicals, play a role in resisting aging and oxidation, improve the metabolism promotion effect of the soft membrane on the skin and better absorb nutrient components under the clean state of the skin.

Preferably, the gel component added with the F phase and the G phase is prepared by the following steps:

adding the phase C into an emulsifying device, heating to 80-85 ℃, stirring, sequentially adding the humectant I and the film-forming agent, uniformly stirring and dispersing, and then keeping the temperature at 80-85 ℃ and continuously stirring to obtain a mixture;

step (2), heating the phase B to 65-75 ℃, stirring and melting, then adding the phase B into the mixture prepared in the step (1), homogenizing and stirring, cooling after complete emulsification, adding the pre-mixed and dissolved phase F when the temperature is reduced to 45-50 ℃, stirring uniformly, and continuing cooling; cooling to below 40 deg.C, adding the pre-mixed and dissolved G phase, stirring, cooling to below 38 deg.C, and filtering to obtain gel component.

By adopting the technical scheme, the humectant I and the film forming agent are added into water, the temperature is controlled, the mixture is stirred, and the solubility of the phase A component in the water is promoted to form a stable water phase; adding phase B of the oil phase into the water phase, homogenizing and emulsifying at high temperature to form a stable emulsifying system, finally cooling and discharging, sequentially adding phase F and phase G in the cooling process, wherein the lower the temperature is, the higher the viscosity is due to the fact that the adding of the substance accelerates the cooling of the system, the generation of the gel component is promoted, and meanwhile, the phase F contains alcohol which can play a certain diluting role in the gel component, so that the phase F and the phase G can be uniformly dispersed, the problem that the materials are added in the process of viscosity rising and are not uniformly dispersed is solved, and the stable gel component with certain viscosity is formed.

Preferably, in phase D, the humectant III comprises the following raw materials in parts by weight: 40-60 parts of white granulated sugar, 20-30 parts of lactose and 20-30 parts of maltose syrup;

the carbon dioxide gas is mainly pressed into the humectant III, after the humectant III is mixed with water in the gel component, white granulated sugar, lactose and maltose syrup are dissolved, the carbon dioxide pressed into the humectant III is released due to the dissolution of the humectant III, the released carbon dioxide is mixed with the water in the gel component to form a carbonic acid component, and the carbonic acid component reacts with the skin under the shielding external action of the soft membrane, the carbonic acid enters the skin to promote the red blood cells in the skin to release oxygen, the released oxygen is used for the skin again, the oxygen content of the skin is improved, the generation of skin collagen is stimulated, pores are promoted to be dredged, pore waste is discharged, and the skin metabolism is accelerated; the purified skin has improved absorption of humectant, antiaging and antioxidant components. And airflow sound is generated in the release process of the carbon dioxide, so that the pressure of the human body is relieved in the process of preparing and using the soft membrane.

Preferably, the filling powder material comprises the following raw materials in parts by weight:

20-50 parts of nacre shell powder

20-50 parts of hydroxypropyl starch sodium phosphate

20-50 parts of shell hard protein powder.

By adopting the filling powder, on one hand, the nacre shell powder and the conch hard protein powder play a role in filling the gel component, so that the viscosity of the gel component is increased, the gel component is easy to coat on skin and is difficult to flow, and a solidified soft membrane state is formed; on the other hand, the hydroxypropyl starch sodium phosphate and the gel component are mixed to play roles of thickening and emulsifying, the attaching degree of the soft film after coating is improved, the soft film component is not easy to flow, and the soft film component is acted with the film forming agent to promote the curing and film forming of the soft film; on the other hand, after the conchiolin powder and the water phase in the gel component act, conchiolin hydrolysate has good permeability on the skin, can assist the permeation and absorption of other active ingredients, has the effects of moistening and moistening the skin, can inhibit skin allergy caused by histamine, and has good repairing effect on the skin.

Preferably, in the phase D, 0.0002-0.002 part of skin conditioner II, 0.1-0.5 part of essence II and 0.0001-0.001 part of pigment are also included, wherein the skin conditioner II comprises 0.0001-0.001 part of carnosine and 0.0001-0.001 part of avenin;

each part of the powder component also comprises 0.001-0.05 part of a skin conditioner III, and the skin conditioner III is ceramide.

The utility model provides an activity that the oat peptide that this application adopted can restrain protease, has anti-oxidant effect, and can condition the skin, high efficiency is moisturized, reduce the roughness of skin, the osmosis is had simultaneously, act on in the mantle, can help skin to absorb other nutrients better in the face applying in-process, and act on mutually with carnosine, carnosine promotes skin metabolism in order to discharge metabolite on the one hand, purify skin, on the other hand oat peptide then promotes the effective component and permeates to the skin in, promote the skin that has purified to the absorption of nutrient substance, make the mantle act on the skin and play the effect of promoting metabolism discharge metabolic waste, promote the absorption nutrient substance simultaneously.

The ceramide is mixed with the gel component to form a soft membrane and acts on the skin, and contacts with the stratum corneum at the outermost layer of the skin in the face application process, so that the ceramide content of the stratum corneum of the skin is improved, and the ceramide has strong ability of associating with water molecules and can form a net structure, so that the stratum corneum can effectively lock the moisture in the skin, keep the normal water content in the skin, moisten and preserve moisture, and reduce the loss of the moisture in the skin, thereby playing the effects of locking the moisture, repairing the skin barrier, resisting aging and the like.

Preferably, the oxygen injection component is prepared by the following steps: mixing the D phase, and charging the E phase carbon dioxide to obtain the oxygen injection component.

By adopting the technical scheme, carbon dioxide is pressed into the phase D, specifically is pressed into the humectant III, after the humectant III is mixed with water in the gel component, white granulated sugar, lactose and maltose syrup are dissolved, the carbon dioxide pressed into the humectant III is released due to the dissolution of the humectant III, and the released carbon dioxide is mixed with the water in the gel component to form a carbonic acid component, so that carbon dioxide is mixed in a soft membrane system, the carbon dioxide concentration on the surface layer of skin is higher during membrane application, the release of oxygen from erythrocytes is promoted, and the oxygen content of the skin is improved; and the sound generated during the outward release of carbon dioxide is continuously generated during the mixing of the soft films and the application of the face, thereby reducing the pressure of the human body through the DIY soft film mixing and the application process.

Preferably, the powder particle component is prepared by the following steps: mixing the materials to prepare powder components;

the powder components are prepared by directly mixing the powder materials, and the method is simple and convenient to operate and easy to control.

In a second aspect, the application provides a method for using a moisturizing and repairing DIY film capable of making sound, which adopts the following technical scheme:

when the soft membrane adopts three dosage forms, the gel component is used as a first dosage form, the oxygen injection component is used as a second dosage form, and the powder component is used as a third dosage form, and the use method of the moisturizing repair DIY soft membrane capable of emitting sound comprises the following steps: adding the oxygen injection component and the powder component into the gel component according to the weight ratio, uniformly stirring, then coating on the skin, naturally coagulating to form a soft membrane, preferably applying the soft membrane for 15-20min, and then removing the coagulated soft membrane to finish the membrane application process.

Or, when the soft membrane adopts two dosage forms, the gel component is used as a first dosage form, the oxygen injection component and the powder particle component are mixed to be used as a second dosage form, and the use method of the moisturizing repair DIY soft membrane capable of emitting sound comprises the following steps: adding the powder component into the gel component according to the weight ratio, stirring uniformly, then coating on skin, naturally coagulating to form soft membrane, preferably applying for 15-20min, and then removing coagulated soft membrane to complete the process of applying membrane.

By adopting the two technical schemes, the oxygen injection component and the powder particle component can be added into the gel component to be mixed and stirred so as to fill the gel component to form a soft film with certain viscosity, and then the soft film is coated on the surface of the skin and isolated from the outside of the skin, thereby playing the roles of promoting penetration, moisturizing and repairing the skin; the whole using process is convenient to operate and easy to prepare, and the air flow sound is generated due to the release of carbon dioxide in the preparing process and the film coating process, so that the pressure of a human body is relieved.

In summary, the present application has the following beneficial effects:

1. in the oxygen injection component, carbon dioxide is filled into white granulated sugar, lactose and maltose, so that after the oxygen injection component is mixed with the gel component, the white granulated sugar, the lactose and the maltose are dissolved in water of the gel component, the injected carbon dioxide is released, and air flow sound is generated in the releasing process; and the carbonic acid formed by the action of the released carbon dioxide and water acts on the skin to promote the red blood cells to release oxygen so as to improve the oxygen content of the skin, stimulate the production of skin collagen, dredge pores, discharge pore wastes, accelerate skin metabolism and repair the skin.

2. In the gel component of this application, add the oil phase material to the aqueous phase material to the emulsification forms the gel state, adds F looks and G looks while cooling at the ejection of compact in-process of cooling down, in order to form the gel component of certain viscosity, stability is high.

3. In the powder component, the oat peptide and the carnosine are adopted to act, so that the permeation and absorption of the carnosine and other nutrient components are improved under the effects of promoting metabolism and purifying the skin by the oat peptide and the carbonic acid, and the absorption effect of the skin on the nutrient components is improved.

4. The application method of the DIY soft film is easy to operate, the powder component is added into the gel component to form a stable soft film state, a user can prepare the DIY to form the soft film by himself and apply the film by himself, and the operability is high.

Detailed Description

The present application is further described in detail in connection with the following examples.

In the following examples and comparative examples, the sodium hyaluronate cross-linked polymer was selected from sodium hyaluronate cross-linked polymer of superior pure GR from Wang Biotech, Inc., Henan kang;

the glucomannan is selected from glucomannan of Shanxi Hunengda Biotech limited with product number HM 20110202;

the hard glyceride is selected from Henan Ruoren bioengineering Co;

the phytosterol oleate is selected from HSF LowChol phytosterol oleate of Seisalsf Biotech Co., Ltd;

carnosine is selected from Guangdong Gaoyang science and technology limited;

the oat peptide is selected from the oat peptide of Shaanxi Sinot biotechnology limited with the product number of 20201117;

the ceramide is selected from ceramide of Sianeborne biotechnology limited with the code BL-2019112702.

Examples

Example 1

A DIY soft mask capable of producing sound and maintaining moisture is composed of a gel component, an oxygen injection component and a powder component, wherein the weight ratio of the gel component to the oxygen injection component to the powder component is 40:22: 3;

the gel component is prepared by the following steps:

adding 23 parts of water into an emulsifying device, heating to 80 ℃ and stirring, then sequentially adding 1 part of glycerol, 1 part of glyceryl polyether-26, 1 part of hydrolyzed sodium hyaluronate, 1 part of acetylated sodium hyaluronate, 1 part of sodium hyaluronate cross-linked polymer, 1 part of hyaluronic acid, 1 part of silanetriol, 5 parts of panthenol, 0.3 part of crinkle moss, 0.4 part of glucomannan, 0.3 part of potassium chloride, 1 part of propylene glycol, 5 parts of polyglycerol-10 and 1 part of sodium alginate, stirring and dispersing uniformly, then preserving heat at 80 ℃ and continuing stirring to prepare a mixture;

and step two, mixing 5 parts of glycerol hard acid ester and 1 part of phytosterol oleate, heating to 65 ℃, stirring for melting, then adding into the mixture prepared in the step one, homogenizing and stirring, cooling after complete emulsification, cooling to below 38 ℃, and filtering to obtain the gel component.

The oxygen injection component is prepared by the following steps: mixing 40 parts of white granulated sugar, 30 parts of lactose and 30 parts of maltose syrup according to the parts by weight, and then charging 0.1 part of carbon dioxide to prepare the oxygen injection component.

The powder component is prepared by the following steps: according to the weight portion, 20 portions of nacre shell powder, 20 portions of hydroxypropyl starch sodium phosphate and 50 portions of conch hard protein powder are evenly mixed to prepare the powder component.

The use method of the moisturizing and repairing DIY soft film capable of making sound comprises the following specific steps: adding the oxygen injection component and the powder component into the gel component, stirring, uniformly coating on skin, naturally coagulating to form soft membrane, applying for 20min, and taking off the coagulated soft membrane to complete one-time application.

Example 2

This embodiment differs from embodiment 1 described above in that: the amount of the materials used was varied, see table 1 below;

in addition, in the preparation of the gel component of this example, the stirring temperature in the first step was 83 ℃, and the heating temperature after mixing the diglycerol hard acid ester and the phytosterol oleate in the second step was 70 ℃.

Example 3

in addition, in the preparation of the gel component of this example, the stirring temperature in the first step was 85 ℃, and the heating temperature after mixing the diglycerol hard acid ester and the phytosterol oleate was 75 ℃.

TABLE 1 Material usage data sheet for examples 1-3

Example 4

This embodiment differs from embodiment 2 described above in that: the gel component also comprises an F phase and a G phase, and is prepared by the following steps:

adding 56 parts of water into an emulsifying device, heating to 83 ℃ and stirring, then sequentially adding 5 parts of glycerol, 3 parts of glyceryl polyether-26, 0.5 part of hydrolyzed sodium hyaluronate, 0.5 part of acetylated sodium hyaluronate, 0.5 part of sodium hyaluronate cross-linked polymer, 0.5 part of hyaluronic acid, 0.5 part of silanetriol, 3 parts of panthenol, 1.0 part of crinkle carrageenan, 1 part of glucomannan, 1.0 part of potassium chloride, 5 parts of propylene glycol, 3 parts of polyglycerol-10 and 3 parts of sodium alginate, stirring and dispersing uniformly, then preserving heat at 80 ℃ and continuing stirring to prepare a mixture;

step two, mixing 3 parts of glycerol hard acid ester and 3 parts of phytosterol oleate, heating to 70 ℃, stirring and melting, then adding into the mixture prepared in the step one, homogenizing and stirring, and cooling after complete emulsification; cooling to 45 deg.C, adding 1 part propylene glycol, 0.5 part p-hydroxyacetophenone and 0.5 part hexanediol, stirring, and cooling; cooling to below 40 deg.C, adding 0.5 part of mixed and dissolved carnosine and 0.01 part of essence I, stirring, cooling to below 38 deg.C, and filtering to obtain gel component.

Example 5

This embodiment differs from embodiment 4 described above in that: the material dosage of the F phase and the G phase is different, and the material dosage is specifically shown in the following table 2;

in addition, in the preparation of the gel component in this embodiment, in the cooling process of step two, the pre-mixed and dissolved F phase is added when the temperature is reduced to 48 ℃.

Example 6

This embodiment differs from embodiment 4 described above in that: the amount of the materials used was varied, see table 1 below;

in addition, in the preparation of the gel component in this embodiment, in the cooling process of the second step, the pre-mixed and dissolved F phase is added when the temperature is reduced to 50 ℃.

Table 2 table of material usage data for examples 4-6

Example 7

This embodiment differs from embodiment 5 described above in that: phase B also included 1 part caprylic/capric triglyceride and was added with 3 parts glyceryl stearate and 3 parts phytosterol oleate at step two of the gel component preparation process.

Example 8

This embodiment differs from embodiment 5 described above in that: phase B also included 3 parts caprylic/capric triglyceride and was added with 3 parts glyceryl stearate and 3 parts phytosterol oleate during step two of the gel component preparation process.

Example 9

This embodiment differs from embodiment 5 described above in that: phase B also included 5 parts caprylic/capric triglyceride and was added with 3 parts glyceryl stearate and 3 parts phytosterol oleate during step two of the gel component preparation process.

Example 10

This embodiment differs from embodiment 8 described above in that:

in phase D, also include 0.0001 parts carnosine, 0.001 parts oat peptide, 0.1-0.5 parts essence II and 0.0001 parts pigment;

in the preparation step of the oxygen injection component, carnosine, oat peptide and essence II are mixed with 50 parts of white granulated sugar, 25 parts of lactose and 25 parts of maltose syrup, and then 0.5 part of carbon dioxide is charged to prepare the oxygen injection component.

Example 11

This embodiment differs from embodiment 10 described above in that: the amounts of carnosine, avenin and essence ii also included in phase D were varied, as shown in table 3 below.

Example 12

Example 13

This embodiment differs from embodiment 12 described above in that:

0.001 part of ceramide is also included in each part of the powder particle component.

Example 14

This embodiment differs from embodiment 12 described above in that:

each part of the powder particle component also comprises 0.03 part of ceramide.

Example 15

This embodiment differs from embodiment 12 described above in that:

0.05 part of ceramide is also included in each part of the powder particle component.

TABLE 3 data Table for material quantities of examples 10-15

Example 16

This embodiment differs from embodiment 14 described above in that: in phase D, equal amounts of carnosine were used instead of avenin.

Example 17

This embodiment differs from embodiment 14 described above in that: in phase D, equal amounts of avenin were used instead of carnosine.

Comparative example

Comparative example 1

This embodiment differs from embodiment 14 described above in that:

and removing carbon dioxide in the phase E, adding 0.5 part of carbon dioxide into the gel component, specifically, in the second gel preparation step, cooling to below 38 ℃, filling carbon dioxide, and filtering to obtain the gel component.

Comparative example 2

This embodiment differs from embodiment 14 described above in that:

and replacing carbon dioxide in the phase E with equal amount of sodium carbonate, and adding sodium carbonate into carnosine, oat peptide, essence II, white granulated sugar, lactose and maltose syrup, and mixing to obtain oxygen injection component.

Comparative example 3

This embodiment differs from embodiment 14 described above in that:

and removing carbon dioxide in the phase E, adding 0.5 part of sodium carbonate into the phase B of the gel component, cooling to below 38 ℃ in the second step of preparing the gel, adding the sodium carbonate, and filtering to obtain the gel component.

Comparative example 4

This embodiment differs from embodiment 14 described above in that:

carbon dioxide in phase E was removed and an equal amount of water was added to the gel component.

Physical and chemical Property test of Performance test

In examples 1 to 17 and comparative examples 1 to 4, the gel component, the oxygen injection component, and the powder component were mixed and stirred at a weight ratio to prepare a soft film to be coated, the soft film to be coated was subjected to viscosity and pH measurement, and at the same time, the soft film was subjected to centrifugation (3000rpm, 30min), and the delamination phenomenon after the centrifugation was observed.

TABLE 4 Soft film physico-chemical Properties of examples 1-17 and comparative examples 1-4

As can be seen from the above table 4, the soft film material of the present application has the advantages of uniform dispersion, stable performance, no delamination, weak acidity and moderate viscosity. The F phase and the G phase are increased from the examples 4-6 to the example 2, and the propylene glycol and the hexanediol are included, and the viscosity of the soft film is reduced compared with the example 2; in examples 7-9, caprylic/capric triglyceride was added to the composition of example 5, so that the oil phase components were slightly increased and the viscosity of the soft film was slightly reduced compared to example 5; in examples 10-12, carnosine, avenin, essence II and pigment were added as compared with example 8, and in examples 13-15, ceramide was added as compared with example 11, and the viscosity of the soft membrane was increased.

Comparative example 1 carbon dioxide was injected into the gel component without significant change in the pH of the film product; in comparative examples 2 to 3, the pH of the soft film was raised from example 14 by using sodium carbonate instead of injecting carbon dioxide, because the pH of the soft film was raised by hydrolysis of carbonate ions generated by mixing water in the sodium carbonate gel component. In contrast, comparative example 4, in which the same amount of water was used instead of carbon dioxide, showed a significant increase in pH as compared to example 14, probably because there was no carbon dioxide component and thus no generation of carbonic acid component, so that the pH of the soft film was close to neutral.

(II) Metabolic competence and radical scavenging Performance test

1. Metabolic capacity test

The XTT colorimetric method is adopted to detect the activity of the cells and reflect the metabolic capability of the cells. When the XTT and the electronic coupling agent Phenazine Methosulfate (PMS) are used together, the XTT and the electronic coupling agent phenazine methosulfate can be reduced by living cell mitochondrial dehydrogenase to form a water-soluble brown-yellow formazan product, the generation amount of the formazan product is in positive correlation with the number of the living cells, and the metabolic capacity of the cells is further reflected.

Inoculating human immortalized keratinocyte (HaCaT) cells in a limiting keratinocyte serum-free medium (DK-SFM) at 37 deg.C in CO₂Culturing in a constant temperature incubator with volume fraction of 5% for 5 days until cells are fused, and changing culture solution every other day. For the experiment, the cell culture flask was taken out, HaCaT cells were digested with trypsin for 4min, and then the cells were inoculated and incubated with 96-well plates for 24 h.

Respectively mixing and stirring the gel component, the oxygen injection component and the powder component according to the weight ratio of the examples 1-17 and the comparative examples 1-4 to prepare a soft film to be coated; the to-be-coated flexible membrane was diluted with DK-SFM culture medium to a concentration of 0.1mg/mL, added to a well plate at 200 μ L per well, and assayed after 48h in an incubator.

Preparing a reagent: (1) XTT is prepared into a solution with the concentration of 0.2g/L by using a 60 ℃ preheated culture solution, and is subjected to filtration sterilization and fresh preparation; (2) PMS is dissolved in PBS with pH of 7.2, the ionic strength I is 0.15mol/kg, the concentration is 5mmol/L, and the PMS is stored in dark for 20 days and is used up; (3) the volume ratio of XTT/PMS of the chromogenic working solution is 200/l.

The cell culture medium in the 96-well plate was removed, and after adding the chromogenic working solution XTT/PMS (200:1) to each well, the plates were incubated at 37 deg.CCulturing for 2h under the condition, measuring the light absorption value OD at the wavelength of 450nm on a microplate reader, and taking the light absorption value 0D measured in comparative example 4₀As a reference value, the absorbance measured for each test sample was divided by the absorbance of comparative example 4 and multiplied by 100% to obtain the mitochondrial activity ratio OD/0D₀。

Meanwhile, the light absorption value 0D of the comparative example 4 is subtracted from the light absorption value measured by each sample to be measured₀And obtaining an improved value, dividing the improved value by the light absorption value 0D measured by each sample to be detected, and multiplying by 100% to obtain the mitochondrial activity improvement ratio.

2. DPPH radical scavenging Rate test

S1, preparing a DPPH-anhydrous methanol stock solution: weighing 3.5mgDPPH reagent, using absolute ethyl alcohol solvent, quantitatively transferring into a 10mL volumetric flask, using absolute ethyl alcohol to fix the volume to a scale, taking 2mL to 100mL volumetric flask, fixing the volume, and shaking up to obtain DPPH-absolute methyl alcohol stock solution with the concentration of 0.0178 mmol/L;

s2, preparing a test solution: respectively mixing and stirring the gel component, the oxygen injection component and the powder component according to the weight ratio of the examples 1-17 and the comparative examples 1-4 to prepare a soft film to be coated; weighing 5mg of the soft membrane to be coated, dissolving the soft membrane with absolute ethyl alcohol, quantitatively transferring the soft membrane to a 50mL volumetric flask, quantitatively measuring the soft membrane to a scale with the absolute ethyl alcohol, taking the soft membrane from 10mL to 100mL volumetric flask, and uniformly shaking to prepare a liquid to be tested;

s3, determination of DPPH free radical clearance: sequentially adding 4.0mL of DPPH-absolute methanol stock solution and 4.0mL of to-be-tested solution into a 10mL colorimetric tube, adding absolute ethanol to fix the volume to a scale, uniformly mixing, immediately measuring a light absorption value (A) at a wavelength of 517nm by using a 1cm cuvette, and marking the light absorption value as Ai; then, storing the mixture in a dark place in a greenhouse for 30min, and then measuring the light absorption value again, wherein the light absorption value is recorded as Aj; and only adding DPPH-absolute methanol stock solution into the blank control group, and recording the light absorption value as Ac. Finally, the DPPH free radical clearance rate is calculated according to the following formula: DPPH radical clearance (%) [1- (Ai-Aj)/Ac ] × 100%, averaged over three measurements, see table 5 below for specific test results.

TABLE 5 membrana metabolizing ability and radical scavenging Properties of examples 1 to 17 and comparative examples 1 to 4

As can be seen from table 5, the soft mask prepared by the present application has excellent effects of promoting skin metabolism and scavenging DPPH free radicals, and the oxygen injection component contains carbon dioxide, and forms carbonic acid after being mixed with water in the gel component, and the carbonic acid acts on the skin to promote skin metabolism, discharge skin metabolites, clean the skin, and further promote absorption of antioxidant and anti-aging components such as avenin, ceramide, and the like.

In examples 4 to 6, the F phase and the G phase were added to example 2, and the propylene glycol and the hexylene glycol were included, the mitochondrial activity ratio and the mitochondrial activity improvement ratio were both increased, and the DPPH radical clearance rate was not significantly changed, because the propylene glycol and the hexylene glycol were both transdermal, the permeation of the generated carbonic acid component into the skin was promoted, the skin cell metabolism was promoted, and the mitochondrial activity was further increased than that of example 2.

In examples 7 to 9, caprylic/capric triglyceride is added, compared with example 5, the mitochondrial activity ratio, the mitochondrial activity improvement ratio and the DPPH free radical clearance are slightly increased, but the increase is not obvious, because caprylic/capric triglyceride mainly plays a role in softening and lubricating the skin, does not play a very obvious role in promoting metabolism or oxidation resistance, but promotes the penetration of ingredients in the soft membrane to a certain extent through the soft skin surface layer, further improves the absorption degree of the skin on nutrients, and improves the oxidation resistance to a certain extent.

In examples 10 to 12, compared with example 8, carnosine, avenin, essence ii and pigment are added, so that the mitochondrial activity ratio, the mitochondrial activity increase ratio and the DPPH free radical clearance rate are all significantly increased, which may be due to the compounding effect of carnosine and avenin, carnosine promotes skin metabolism to discharge metabolites, purifies the skin, increases the mitochondrial activity ratio and the mitochondrial activity increase ratio, and avenin promotes the penetration of functional components into the skin, and avenin has the effects of repairing and resisting aging on the skin, thereby increasing the DPPH free radical clearance rate.

For the compounding effect of carnosine and oat peptide, the same amount of carnosine is used for replacing oat peptide in example 16, and the same amount of oat peptide is used for replacing carnosine in example 17, wherein the DPPH free radical clearance rate of example 16 is obviously reduced, and the mitochondrial activity ratio and the mitochondrial activity improvement ratio are increased compared with example 14, because the reduction of oat peptide may cause the reduction of antioxidant and anti-aging performance of a soft membrane, the DPPH free radical clearance rate is reduced, the content of carnosine is increased, the metabolic capacity of skin cells is increased, and the mitochondrial activity is increased; the reason why the mitochondrial activity ratio, the mitochondrial activity improvement ratio and the DPPH free radical clearance of example 17 are all reduced compared with example 14 is that the decrease of the carnosine content may reduce the metabolic capability of skin cells, and the decrease of the metabolic capability affects the absorption degree of the skin cells to the nutrient components, so that the ability of absorbing the components with the repairing and anti-aging effects, such as avenin, ceramide and the like, is reduced, and the DPPH free radical clearance is reduced. In example 14, carnosine and avenin are used in combination to make the pia mater have the balance of metabolism promotion, anti-aging and anti-oxidation.

Compared with the embodiment 11, the embodiment 13-15 is added with the ceramide, so that the DPPH free radical clearance rate is obviously increased, and the reason is probably that the ceramide can be stably attached to the surface of the skin, not only can the stable network structure be used for improving the water locking effect, but also the repairing and anti-aging effects on the skin can be realized, and further, the DPPH free radical clearance rate is increased.

In comparative example 1, the injection of carbon dioxide into the gel component significantly reduced the mitochondrial activity ratio and the mitochondrial activity increase ratio compared to example 14, probably because the injected carbon dioxide was mixed with water in the gel component prematurely to form carbonic acid prematurely, while carbonic acid formed by dissolving carbon dioxide in water was unstable and the reaction was reversible, so that carbonic acid was likely to decompose reversely to produce carbon dioxide and water, carbon dioxide was discharged to volatilize, so that the concentration of carbon dioxide in the soft membrane acting on the skin was reduced, the ability to promote oxygen production in the skin was reduced, the ability to promote metabolism was reduced, and the mitochondrial activity ratio and the mitochondrial activity increase ratio were reduced.

In contrast, in comparative example 2, the carbon dioxide injected in phase E was replaced with the same amount of sodium carbonate, in comparative example 3, no carbon dioxide was added to phase E, and the same amount of sodium carbonate was added to phase B of the gel component, and the mitochondrial activity ratio and the mitochondrial activity improvement ratio of comparative examples 2 to 3 were significantly reduced as compared to example 14, probably because sodium carbonate, even though it was hydrolyzed by mixing with water in the gel component, did not produce carbon dioxide but produced carbonate and did not function to increase the concentration of carbon dioxide on the skin surface to promote the generation of oxygen, the metabolizing promoting ability of sodium carbonate was inferior to that of carbon dioxide, and the metabolizing absorption promoting degree was not obvious as in example 14.

In contrast, in comparative example 4, no carbon dioxide is added to phase E, and equal amount of water is added to phase B of the gel component, that is, equal amount of water replaces carbon dioxide, the mitochondrial activity ratio and the mitochondrial activity improvement ratio of the soft membrane in comparative example 4 are obviously inferior to those in example 14, probably because carbonic acid is not generated in the soft membrane, and thus the metabolism and absorption promoting effects on the skin are not achieved.

(III) application Effect test

In examples 1 to 16 and comparative examples 1 to 4 described above, the gel component, the oxygen injection component and the powder component were mixed and stirred in the weight ratio to prepare a soft film to be coated.

80 healthy skin women aged 30 years are selected as volunteer testers, divided into 4 groups of 20 persons, and skin moisture value and skin elasticity value of the left half face are tested by a German DJM skin tester before film application test.

And then cleaning the left half face of each group of volunteer testees, coating the soft film to be coated, and leaving the right half face as a blank group without any substance. Taking off the soft membrane after applying the membrane for 20min, cleaning the residual soft membrane on the face, and testing the skin moisture value and the skin elasticity value of the left half face after applying the membrane by using a German DJM skin tester.

In addition, the left half face of each group of volunteer testers is continuously coated with the film for eight weeks, the film is coated once every seven days, the film is coated for 20min every time, the left half face and the right half face are kept for daily skin care, only the right half face is not coated with the film, the skin moisture value and the skin elasticity value of the left half face are tested every two weeks, and the average value is calculated.

The test results are shown below:

TABLE 6 average skin moisture values before and after application of examples 1-17 and comparative examples 1-4

TABLE 7 average values of skin elasticity before and after application for examples 1-17 and comparative examples 1-4

As can be seen from tables 6 and 7, the moisture value and elasticity of the skin of the soft mask prepared by the present application are increased, which indicates that the soft mask of the present application can moisturize the skin, the skin moisture is increased, the elasticity is increased, and the adopted oat peptide, ceramide and other components can repair and resist aging. The test data shows that the moisture value and the elasticity value after the first film application are obviously increased, the moisture value and the elasticity value tested after two weeks of the regular film application are reduced to some extent compared with the first film application, the moisture value and the elasticity value gradually increase after 6-8 weeks of the regular film application, the moisture-preserving effect on the skin can be well achieved and the instant moisture-preserving effect can be achieved when the film application is carried out for the first time, and the high moisture state of the skin can be maintained only when the skin is continuously protected after the skin is continuously protected.

Wherein, the phases F and G are added in examples 4-6 compared with the phase G in example 2, and the water content and the elasticity measured after the first film application and the regular film application are both higher than those of example 2, probably because the propylene glycol and the hexylene glycol have transdermal property, and the moisturizing agent I of the phase A and the moisturizing agent II of the phase B are promoted to permeate into the skin to effectively play a moisturizing role; and the moisture value and the elasticity value after 8 weeks of regular film application basically exceed the moisture value and the elasticity value after the first film application, probably because the added G phase contains carnosine, the metabolism of the skin is promoted, and the added G phase helps to chelate metal ions in the skin and discharge the metal ions out of the skin, so that the skin is purified, the skin can more effectively absorb the nutrient components in the soft film in a clean state, the nutrient components are continuously purified and absorbed, and the moisture value and the elasticity value of the skin are effectively improved.

In examples 7 to 9, caprylic/capric triglyceride is added compared with example 5, and the moisture value and elasticity value measured after the first application and the regular application of the film are both increased compared with example 5, probably because the caprylic/capric triglyceride has the effects of softening and lubricating the skin, further promoting the penetration of ingredients, improving the absorption degree of the skin and further improving the moisture value and elasticity value of the skin.

In examples 10 to 12, carnosine, oat peptide, essence II and pigment are added in comparison with example 8, the moisture value and the elasticity value measured after the first and the regular film application are both increased in comparison with example 8, and the increase of the moisture value is larger than that of example 8 in comparison with example 5, probably because the carnosine and the oat peptide are compounded, the carnosine promotes the skin metabolism to discharge metabolites and purify the skin, the oat peptide promotes the functional components to permeate into the skin and promote the purified skin to absorb nutrients, and the synergistic effect of the carnosine and the oat peptide simultaneously promotes the metabolism and the absorption when the soft film is applied to the skin, so that the absorption of the nutrients by the skin is improved, and the moisture value and the elasticity value are obviously increased.

And for the combination effect of carnosine and avenin, the same amount of carnosine is used for replacing avenin in example 16, the same amount of avenin is used for replacing the avenin in example 17, and compared with example 14, the moisture value and the elasticity value after the first membrane application are not increased to a high degree in example 17, the moisture value and the elasticity value after the regular membrane application for 8 weeks are equivalent to those after the first membrane application and are not increased obviously, in particular, the moisture value after the membrane application for 8 weeks is lower than those after the first membrane application in example 17, probably because the D phase of example 17 does not contain carnosine, the content of carnosine in the gel component is lower than that of example 14, so that the metabolism promoting effect on the skin is reduced periodically, and the regular membrane application can promote the metabolism of the skin, but the content of the carnosine is reduced, so that the metabolism promoting capability on the skin is reduced, and further partial waste is accumulated in the skin, no obvious increase of the moisture value after the regular film application is caused; in example 16, although the content of carnosine is higher than that of example 14, oat peptide is not contained, so that the skin absorbs less nutrition, and the elasticity value and the moisture value are not increased to a high degree in example 14; meanwhile, the carnosine and the oat peptide are probably compounded and used in a certain dosage, so that the metabolism and absorption promoting effect of the pellicles on the skin can be obviously improved, and the moisture value and the elasticity value of the skin are improved.

Compared with the embodiment 11, the embodiments 13-15 are added with ceramide, and the moisture value and the elasticity value are obviously improved compared with the embodiment 11, probably because after the soft membrane is attached to the skin, the ceramide is contacted with the surface stratum corneum of the skin, the ceramide content of the stratum corneum is improved, and water molecules can be associated to form a net structure, so that the water locking effect of the stratum corneum is improved, the evaporation of water in the skin is reduced, and the moisture value and the elasticity value of the skin after the first membrane application and the periodical membrane application are obviously improved.

In comparative example 1, carbon dioxide was injected into the gel composition, and the moisture value and elasticity value of the skin after the initial application and the regular application were both lower than those of example 14, because the injected carbon dioxide was mixed with water in the gel composition too early to form carbonic acid too early, and the carbonic acid formed by dissolving carbon dioxide in water was unstable and reversibly reacted, so that carbonic acid might be decomposed reversely to produce carbon dioxide and water, carbon dioxide was discharged and volatilized, the carbon dioxide concentration in the soft membrane applied to the skin was decreased, the ability to promote oxygen generation in the skin was decreased, the ability to promote metabolism was decreased, and the degree of absorption of nutrients was decreased, and the moisture value and elasticity value after the application were both lower than those of example 14.

In contrast, in comparative example 2, the carbon dioxide injected in phase E was replaced by the same amount of sodium carbonate, in comparative example 3, the carbon dioxide was not added in phase E, and the same amount of sodium carbonate was added in phase B of the gel composition, and the moisture value and the elasticity value of the soft film of comparative examples 2-3 were increased after the first application, but the moisture value and the elasticity value were not improved as compared with those of the first application, and the moisture value and the elasticity value were not improved as in example 14, because the moisture-retaining component in the soft film could increase the moisture value and the elasticity value of the skin just after the first application, but the sodium carbonate was hydrolyzed without generating carbon dioxide and carbonate, which did not increase the carbon dioxide concentration on the skin surface to promote the generation of oxygen, the metabolism-promoting ability of sodium carbonate was inferior to carbon dioxide, the metabolism-promoting absorption-promoting degree was not obvious as in example 14, so that the skin was protected with a partial waste accumulation, the moisture and elasticity values were not as significant as in example 14.

In contrast, in comparative example 4, no carbon dioxide was added to phase E and equal amounts of water were added to phase B of the gel component, i.e., equal amounts of water replaced carbon dioxide, the moisture and elasticity values of the film of comparative example 4 increased after the initial application, but the moisture and elasticity values were not as good as those of the film of example 14 after the periodic application, possibly because no carbonic acid was generated in the film and no metabolism and absorption promoting effect was exerted on the skin, so that the moisture and elasticity values of the skin after application were not as good as those of example 14.

The present embodiment is only for explaining the present application, and it is not limited to the present application, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present application.

Claims

1. A moisturizing and repairing DIY film capable of making sound is characterized in that: the DIY soft film consists of a gel component, an oxygen injection component and a powder component, wherein the weight ratio of the gel component to the oxygen injection component to the powder component is 40-50:18-22: 3;

phase A: 7-50 parts of humectant I

1-5 parts of film forming agent

Phase B: 1-5 parts of emulsifier

1-5 parts of humectant II

And C phase: 23-87.78 parts of water;

each part of the oxygen injection component comprises the following raw materials in parts by weight:

phase D: 80-120 parts of humectant III

Phase E: 0.1-1.0 part of carbon dioxide;

2. The sound-emitting, moisturizing, repair DIY film of claim 1, wherein: in the phase A, the humectant I comprises the following raw materials in parts by weight:

1-10 parts of glycerol

Glyceryl polyether-261-5 parts

0.2 to 1 portion of hydrolyzed sodium hyaluronate

0.2 to 1 portion of acetylated sodium hyaluronate

0.2-1 part of sodium hyaluronate cross-linked polymer

Hyaluronic acid 0.2-1 part

0.2-1 part of silanetriol

1-5 parts of panthenol

0.3 to 1.5 portions of crinkle-wave carrageen

0.4 to 2 portions of glucomannan

0.3 to 1.5 portions of potassium chloride

1-10 parts of propylene glycol

101-5 parts of polyglycerol.

3. The sound-emitting, moisturizing, repair DIY film of claim 1, wherein: in phase A, the film forming agent is sodium alginate; in the phase B, the emulsifier is glycerol hard acid ester, and the humectant II is phytosterol oleate.

4. A moisturizing repair DIY film according to any of claims 1-3, wherein: the gel component is prepared by the following steps:

5. A moisturizing repair DIY film according to any of claims 1-3, wherein: each of the gel components further includes a phase F and a phase G:

and (3) phase F: 1-5 parts of humectant IV

0.1 to 0.5 portion of chelating agent

0.1-0.5 part of emollient

Phase G: 0.01-0.5 part of skin conditioner I

0.01-0.5 part of essence I;

in phase G, the skin conditioner I is carnosine.

6. The sound-emitting, moisturizing, repair DIY film of claim 5, wherein: the gel component is prepared by the following steps:

7. The sound-emitting, moisturizing, repair DIY film of claim 1, wherein: in the phase D, the humectant III comprises the following raw materials in parts by weight: 40-60 parts of white granulated sugar, 20-30 parts of lactose and 20-30 parts of maltose syrup;

the filling powder comprises the following raw materials in parts by weight:

20-50 parts of nacre shell powder

20-50 parts of hydroxypropyl starch sodium phosphate

20-50 parts of shell hard protein powder.

8. The sound-emitting, moisturizing, repair DIY film of claim 7, wherein: in phase D, 0.0002-0.002 part of skin conditioner II, 0.1-0.5 part of essence II and 0.0001-0.001 part of pigment are also included, wherein the skin conditioner II comprises 0.0001-0.001 part of carnosine and 0.0001-0.001 part of oat peptide;

9. The sound-emitting, moisturizing, repair DIY film of claim 1, wherein: the oxygen injection component is prepared by the following steps: mixing the phases D and then charging carbon dioxide of the phase E to prepare an oxygen injection component;

the powder particle component is prepared by the following steps: mixing the materials to obtain the powder component.

10. A method of using a sound-emitting moisturizing repair DIY film according to any of claims 1-9, wherein: the method comprises the following steps: adding the oxygen injection component and the powder component into the gel component according to the weight ratio, stirring uniformly, then coating on the skin, and naturally coagulating to form a soft membrane.