CN107569419A - A kind of preparation method of moisturizing emulsion - Google Patents
A kind of preparation method of moisturizing emulsion Download PDFInfo
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- CN107569419A CN107569419A CN201710835797.0A CN201710835797A CN107569419A CN 107569419 A CN107569419 A CN 107569419A CN 201710835797 A CN201710835797 A CN 201710835797A CN 107569419 A CN107569419 A CN 107569419A
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Abstract
The invention belongs to cosmetic technical field, and in particular to a kind of preparation method of moisturizing emulsion.The present invention passes through the extraction to lotus leaf and herba fibraureae recisae fruit, obtain wherein natural alkaloid and alcohols material, the lipid and cutin of human skin are modified by alkaloid and alcohols, reduce its obstructing capacity to water, increase the ability that hydrophilic molecule is absorbed by organisms, also the skin ill symptomses such as inflammation of skin surface are administered by extract simultaneously, skin is supplemented using the nutriment of extract China, keep the activity of skin, the effect of long-term is made it have to the parcel beneficial to thing by alginic acid simultaneously.
Description
Technical field
The invention belongs to cosmetic technical field, and in particular to a kind of preparation method of moisturizing emulsion.
Background technology
Skin cell tissue's moisture is easily lost in, and lack of moisture can cause xerosis cutis, dimness, produces scurf, wrinkle.
Replenishing water and preserving moisture is the essential link of daily skin maintenance.The replenishing water and preserving moisture cosmetics of specialty, being capable of deep layer, effective benefit
Water, nourish moist skin.Generally, due to the presence of the lipid and cuticula of skin, hydrophilic molecule are difficult to pass through
Skin barrier and be absorbed by organisms.The characteristic of active matter molecule, such as molecular size and lipophilicity, instrument is carried, such as formulation and rush
Saturating agent, and the tissue of application site, can cutaneous assimilation effect.
Chinese patent 201410268341.7 discloses a kind of skin whitening, moisturizing tencel facial mask essence containing lecithin, with
EDTA-2Na, lecithin/C12-16 alcohol/palmitic acid compound, glycerine, 1,3-PD, hyaluronic acid, hydroxyethyl cellulose etc.
For raw material, the skin whitening, moisturizing Essence containing lecithin is stored in tencel facial mask cloth, obtained facial mask is more docile, soft
Soft, ventilative and comfortable, skin whitening, moisturizing is better, but general facial mask cloth only carries nutrient solution, and its Transdermal absorption effect need
Discuss.
Moisturizing emulsion contains a certain amount of water at present simultaneously, can be kept the skin wet for skin, and emulsion also contains a small amount of oil,
Again can be with skin care.But traditional emulsion is typically all the grease using chemical synthesis, fat content is unreasonable, it is not easy to
It is absorbed by the skin, lacks and nourish composition, the moistening effect duration is short.
The content of the invention
The technical problems to be solved by the invention：It is typically all the oil using chemical synthesis for emulsion traditional at present
Fat, fat content are unreasonable, it is not easy to are absorbed by the skin, lack and nourish composition, the problem of moistening effect duration is short, this hair
It is bright to provide a kind of preparation method of moisturizing emulsion.
In order to solve the above technical problems, the present invention is using technical scheme as described below：
A kind of preparation method of moisturizing emulsion, the preparation method comprise the following steps：
（1）Take lotus leaf, Freamine Ⅲ and HCA to be put into mixer to be stirred, collect stirring mixture, stirring is mixed
Compound carries out ultrasonic oscillation, collects concussion mixture；
（2）Concussion mixture, bacterium powder and chrysanthemum are well mixed, is put into fermentation tank and is fermented, collects fermenting mixture, then
It is put into smash to pieces in tank and is smashed to pieces, mixture is smashed in collection to pieces；
（3）Mixture will be smashed to pieces to be mixed with ethanol solution, then carry out supercritical carbon dioxide extracting, collect extract, will
Extract is filtered, and collects filtered fluid, and filtered fluid is mixed with activated carbon, is stood, is distilled, and reclaims ethanol, is collected
Distill residue；
（4）Count in parts by weight, take 60~65 portions of distillation residues, 15~18 parts of hydrosol water, 3~5 parts of Tea Polyphenols, 2~4 portions of reeds
Luxuriant growth glue and 1~3 part of alginic acid, stir, and carry out sterilizing, filtering, collect filtrate, produce moisturizing emulsion.
The step（1）The mass ratio of lotus leaf, Freamine Ⅲ and HCA is 4:7~11:3.
The step（2）The mass ratio for shaking mixture, bacterium powder and chrysanthemum is 9:1~3:3, bacterium powder is lactic acid bacteria powder.
The step（3）The mass ratio for smashing mixture and ethanol solution to pieces is 2:5~7, the quality of filtered fluid and activated carbon
Than for 7:2~3.
Compared with other method, advantageous effects are the present invention：
The present invention obtains wherein natural alkaloid and alcohols material, passes through alkaloid by the extraction to lotus leaf and herba fibraureae recisae fruit
And alcohols is modified to the lipid and cutin of human skin, its obstructing capacity to water is reduced, increases hydrophilic point
The ability that son is absorbed by organisms, while also the skin ill symptomses such as inflammation of skin surface are administered by extract, make
Skin is supplemented with the nutriment of extract China, keeps the activity of skin, while by alginic acid to beneficial to thing
Parcel, makes it have the effect of long-term.
Embodiment
Bacterium powder selection is lactic acid bacteria powder.
A kind of preparation method of moisturizing emulsion, the preparation method comprise the following steps：
（1）It is 4 in mass ratio:7~11:3, take lotus leaf, 1.6mol/L Freamine Ⅲs and HCA to be put into mixer, with
300r/min is stirred 20~30min, collects stirring mixture, and stirring mixture is put into ultrasonic oscillation device, with
1.2MHz carries out 10~15min of ultrasonic oscillation, collects concussion mixture；
（2）In mass ratio 9:1~3:3, concussion mixture, bacterium powder and chrysanthemum are well mixed, is put into fermentation tank, uses dioxy
Change carbon to discharge the gas in fermentation tank, fermentation is stirred 1~3 day with 150r/min at 30~35 DEG C, it is mixed to collect fermentation
Compound, place into smash to pieces in tank and smashed to pieces with 12000r/min, mixture is smashed in collection to pieces；
（3）It is 2 in mass ratio:5~7, mixture will be smashed to pieces and mixed with 1.3mol/L ethanol solutions, then carry out overcritical two
Carbonoxide extracts, and extraction conditions be 14~16MPa of pressure, and temperature is 35~40 DEG C, carbon dioxide flow 22kg/h, during extraction
Between be 1~2h, collect extract, extract is filtered, collect filtered fluid, and in mass ratio be 7:2~3, by filtered fluid
Mixed with activated carbon, stand 30min, then distilled, reclaim ethanol, collect distillation residue；
（4）Count in parts by weight, take 60~65 portions of distillation residues, 15~18 parts of hydrosol water, 3~5 parts of Tea Polyphenols, 2~4 portions of reeds
Luxuriant growth glue and 1~3 part of alginic acid, stir, and carry out sterilizing, filtering, collect filtrate, produce moisturizing emulsion.
Example 1
Bacterium powder selection is lactic acid bacteria powder.
A kind of preparation method of moisturizing emulsion, the preparation method comprise the following steps：
（1）It is 4 in mass ratio:9:3, take lotus leaf, 1.6mol/L Freamine Ⅲs and HCA to be put into mixer, with 300r/
Min is stirred 25min, collects stirring mixture, and stirring mixture is put into ultrasonic oscillation device, surpassed with 1.2MHz
Sound wave shock 13min, collect concussion mixture；
（2）In mass ratio 9:2:3, concussion mixture, bacterium powder and chrysanthemum are well mixed, is put into fermentation tank, uses titanium dioxide
Carbon discharges the gas in fermentation tank, and fermentation 2 days is stirred with 150r/min at 33 DEG C, collects fermenting mixture, then put
Enter to smash to pieces in tank and smashed to pieces with 12000r/min, mixture is smashed in collection to pieces；
（3）It is 2 in mass ratio:6, mixture will be smashed to pieces and mixed with 1.3mol/L ethanol solutions, then carry out overcritical dioxy
Change carbon extraction, extraction conditions is pressure 15MPa, and temperature is 38 DEG C, carbon dioxide flow 22kg/h, extraction time 2h, is received
Collect extract, extract is filtered, collect filtered fluid, and be 7 in mass ratio:2, filtered fluid is mixed with activated carbon, it is quiet
30min is put, then is distilled, reclaims ethanol, collects distillation residue；
（4）Count in parts by weight, take 63 parts of distillation residues, 17 parts of hydrosol water, 4 parts of Tea Polyphenols, 3 parts of Aloe Vera Gels and 2 portions of marine algas
Acid, stir, and carry out sterilizing, filter, collect filtrate, produce moisturizing emulsion.
Example 2
Bacterium powder selection is lactic acid bacteria powder.
A kind of preparation method of moisturizing emulsion, the preparation method comprise the following steps：
（1）It is 4 in mass ratio: 11:3, take lotus leaf, 1.6mol/L Freamine Ⅲs and HCA to be put into mixer, with
300r/min is stirred 30min, collects stirring mixture, stirring mixture is put into ultrasonic oscillation device, with 1.2MHz
Ultrasonic oscillation 15min is carried out, collects concussion mixture；
（2）In mass ratio 9: 3:3, concussion mixture, bacterium powder and chrysanthemum are well mixed, is put into fermentation tank, uses titanium dioxide
Carbon discharges the gas in fermentation tank, and fermentation 3 days is stirred with 150r/min at 35 DEG C, collects fermenting mixture, then put
Enter to smash to pieces in tank and smashed to pieces with 12000r/min, mixture is smashed in collection to pieces；
（3）It is 2 in mass ratio:7, mixture will be smashed to pieces and mixed with 1.3mol/L ethanol solutions, then carry out overcritical dioxy
Change carbon extraction, extraction conditions is pressure 16MPa, and temperature is 40 DEG C, carbon dioxide flow 22kg/h, extraction time 2h, is received
Collect extract, extract is filtered, collect filtered fluid, and be 7 in mass ratio:3, filtered fluid is mixed with activated carbon, it is quiet
30min is put, then is distilled, reclaims ethanol, collects distillation residue；
（4）Count in parts by weight, take 65 parts of distillation residues, 18 parts of hydrosol water, 5 parts of Tea Polyphenols, 4 parts of Aloe Vera Gels and 3 portions of marine algas
Acid, stir, and carry out sterilizing, filter, collect filtrate, produce moisturizing emulsion.
Example 3
Bacterium powder selection is lactic acid bacteria powder.
A kind of preparation method of moisturizing emulsion, the preparation method comprise the following steps：
（1）It is 4 in mass ratio:7:3, take lotus leaf, 1.6mol/L Freamine Ⅲs and HCA to be put into mixer, with 300r/
Min is stirred 20min, collects stirring mixture, and stirring mixture is put into ultrasonic oscillation device, surpassed with 1.2MHz
Sound wave shock 10min, collect concussion mixture；
（2）In mass ratio 9:1:3, concussion mixture, bacterium powder and chrysanthemum are well mixed, is put into fermentation tank, uses titanium dioxide
Carbon discharges the gas in fermentation tank, and fermentation 1 day is stirred with 150r/min at 30 DEG C, collects fermenting mixture, then put
Enter to smash to pieces in tank and smashed to pieces with 12000r/min, mixture is smashed in collection to pieces；
（3）It is 2 in mass ratio:5, mixture will be smashed to pieces and mixed with 1.3mol/L ethanol solutions, then carry out overcritical dioxy
Change carbon extraction, extraction conditions is pressure 14MPa, and temperature is 35 DEG C, carbon dioxide flow 22kg/h, extraction time 1h, is received
Collect extract, extract is filtered, collect filtered fluid, and be 7 in mass ratio:2, filtered fluid is mixed with activated carbon, it is quiet
30min is put, then is distilled, reclaims ethanol, collects distillation residue；
（4）Count in parts by weight, take 60 parts of distillation residues, 15 parts of hydrosol water, 3 parts of Tea Polyphenols, 2 parts of Aloe Vera Gels and 1 portion of marine alga
Acid, stir, and carry out sterilizing, filter, collect filtrate, produce moisturizing emulsion.
Reference examples：The moisturizing emulsion of company of Suzhou City production.
Moisturizing emulsion obtained by examples detailed above and the moisturizing emulsion of reference examples are detected, specific detection is as follows：
According to light industry standard QB/T4256-2011 cosmetics moisture-keeping efficacy evaluation guides, the moisturizing of measure embodiment preparation
The moistening effect of emulsion and reference examples.Moisture using capacitance method measure human skin keratinocyte's layer is based on water and other things
The difference in dielectric constant of matter is notable, and according to the difference of keratoderma moisture, the capacitance of the skin measured is different, and it is joined
Number can represent skin moisture content.Healthy volunteer 30 is chosen, male 10, women 20, the age is 25-50 year.In perseverance
Warm environment（20~22℃）, relative humidity 50 ± 10%, after 1 hour of resting, the sample that embodiment and reference examples is respectively adopted applies
In subject's left hand inner forearm（3cm×3cm）With right forearm inner side（3cm×3cm）Test simultaneously.It is being painted with sample respectively
The hydrauture state of skin is tested after 1 hour and 6 hours.Testing result such as table 1.
Table 1：
Summary, moisturizing emulsion moistening effect of the invention is more preferable and the moisturizing duration is grown, and is worth of widely use.
Claims (4)
1. a kind of preparation method of moisturizing emulsion, it is characterised in that the preparation method comprises the following steps：
（1）Take lotus leaf, Freamine Ⅲ and HCA to be put into mixer to be stirred, collect stirring mixture, stirring is mixed
Compound carries out ultrasonic oscillation, collects concussion mixture；
（2）Concussion mixture, bacterium powder and chrysanthemum are well mixed, is put into fermentation tank and is fermented, collects fermenting mixture, then
It is put into smash to pieces in tank and is smashed to pieces, mixture is smashed in collection to pieces；
（3）Mixture will be smashed to pieces to be mixed with ethanol solution, then carry out supercritical carbon dioxide extracting, collect extract, will
Extract is filtered, and collects filtered fluid, and filtered fluid is mixed with activated carbon, is stood, is distilled, and reclaims ethanol, is collected
Distill residue；
（4）Count in parts by weight, take 60~65 portions of distillation residues, 15~18 parts of hydrosol water, 3~5 parts of lecithin, 2~4 portions of reeds
Luxuriant growth glue and 1~3 part of alginic acid, stir, and carry out sterilizing, filtering, collect filtrate, produce moisturizing emulsion.
2. the preparation method of moisturizing emulsion according to claim 1, it is characterised in that the step（1）Lotus leaf, amino acid are molten
The mass ratio of liquid and HCA is 4:7~11:3.
3. the preparation method of moisturizing emulsion according to claim 1, it is characterised in that the step（2）Shake mixture, bacterium
The mass ratio of powder and chrysanthemum is 9:1~3:3, bacterium powder is lactic acid bacteria powder.
4. the preparation method of moisturizing emulsion according to claim 1, it is characterised in that the step（3）Smash to pieces mixture with
The mass ratio of ethanol solution is 2:5~7, the mass ratio of filtered fluid and activated carbon is 7:2~3.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113143836A (en) * | 2020-12-30 | 2021-07-23 | 广州丹葶日用品实业有限公司 | Coated body lotion based on calamine extract and preparation method thereof |
| CN113425652A (en) * | 2021-08-18 | 2021-09-24 | 胡宗义 | Method for extracting Garcinia cambogia extract and cosmetic containing extract |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102018640A (en) * | 2009-09-21 | 2011-04-20 | 刘秀英 | Whitening, face thinning and moisturizing essence emulsion |
| CN103284933A (en) * | 2013-05-13 | 2013-09-11 | 张娟 | Preparation process of beauty fluid with lotus leaf powder |
| CN105267084A (en) * | 2015-09-23 | 2016-01-27 | 嘉兴市蝶柔化妆品有限公司 | Moisturizer |
-
2017
- 2017-09-16 CN CN201710835797.0A patent/CN107569419A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102018640A (en) * | 2009-09-21 | 2011-04-20 | 刘秀英 | Whitening, face thinning and moisturizing essence emulsion |
| CN103284933A (en) * | 2013-05-13 | 2013-09-11 | 张娟 | Preparation process of beauty fluid with lotus leaf powder |
| CN105267084A (en) * | 2015-09-23 | 2016-01-27 | 嘉兴市蝶柔化妆品有限公司 | Moisturizer |
Non-Patent Citations (1)
| Title |
|---|
| 国家食品药品监督管理总局: ""化妆品中禁用植物组分"", 《化妆品安全技术规范》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113143836A (en) * | 2020-12-30 | 2021-07-23 | 广州丹葶日用品实业有限公司 | Coated body lotion based on calamine extract and preparation method thereof |
| CN113425652A (en) * | 2021-08-18 | 2021-09-24 | 胡宗义 | Method for extracting Garcinia cambogia extract and cosmetic containing extract |
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Application publication date: 20180112 |