CN112534249A - 聚合物的无定形含量的测定 - Google Patents

聚合物的无定形含量的测定 Download PDF

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Publication number
CN112534249A
CN112534249A CN201980051817.2A CN201980051817A CN112534249A CN 112534249 A CN112534249 A CN 112534249A CN 201980051817 A CN201980051817 A CN 201980051817A CN 112534249 A CN112534249 A CN 112534249A
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China
Prior art keywords
olefin
particles
based polymer
elution
polymer
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Pending
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CN201980051817.2A
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English (en)
Chinese (zh)
Inventor
丛蓉娟
K·L·贝利
V·里卡
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Dow Global Technologies LLC
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Dow Global Technologies LLC
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Publication of CN112534249A publication Critical patent/CN112534249A/zh
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/86Signal analysis
    • G01N30/8675Evaluation, i.e. decoding of the signal into analytical information
    • G01N30/8679Target compound analysis, i.e. whereby a limited number of peaks is analysed
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/50Conditioning of the sorbent material or stationary liquid
    • G01N30/52Physical parameters
    • G01N30/54Temperature
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/26Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/34Size selective separation, e.g. size exclusion chromatography, gel filtration, permeation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D15/00Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08Selective adsorption, e.g. chromatography
    • B01D15/26Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/38Selective adsorption, e.g. chromatography characterised by the separation mechanism involving specific interaction not covered by one or more of groups B01D15/265 - B01D15/36
    • B01D15/3861Selective adsorption, e.g. chromatography characterised by the separation mechanism involving specific interaction not covered by one or more of groups B01D15/265 - B01D15/36 using an external stimulus
    • B01D15/3876Selective adsorption, e.g. chromatography characterised by the separation mechanism involving specific interaction not covered by one or more of groups B01D15/265 - B01D15/36 using an external stimulus modifying the temperature
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N2030/0075Separation due to differential desorption
    • G01N2030/008Thermal desorption
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N30/00Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
    • G01N30/02Column chromatography
    • G01N30/88Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
    • G01N2030/8809Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
    • G01N2030/884Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds
    • G01N2030/885Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds involving polymers
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/44Resins; Plastics; Rubber; Leather
    • G01N33/442Resins; Plastics

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Immunology (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Pathology (AREA)
  • Engineering & Computer Science (AREA)
  • Library & Information Science (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Chemical Kinetics & Catalysis (AREA)
CN201980051817.2A 2018-06-29 2019-06-25 聚合物的无定形含量的测定 Pending CN112534249A (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201862691733P 2018-06-29 2018-06-29
US62/691733 2018-06-29
PCT/US2019/039003 WO2020005953A1 (en) 2018-06-29 2019-06-25 Determination of the amorphous content of polymers

Publications (1)

Publication Number Publication Date
CN112534249A true CN112534249A (zh) 2021-03-19

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CN201980051817.2A Pending CN112534249A (zh) 2018-06-29 2019-06-25 聚合物的无定形含量的测定

Country Status (9)

Country Link
US (1) US11988650B2 (ko)
EP (1) EP3814761B1 (ko)
JP (1) JP7386820B2 (ko)
KR (1) KR20210027418A (ko)
CN (1) CN112534249A (ko)
BR (1) BR112020026888A2 (ko)
SG (1) SG11202013153SA (ko)
TW (1) TW202000288A (ko)
WO (1) WO2020005953A1 (ko)

Citations (4)

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WO2015115631A1 (ja) * 2014-01-29 2015-08-06 サン・トックス株式会社 ポリオレフィン系無延伸多層フィルム
CN105001584A (zh) * 2008-01-30 2015-10-28 陶氏环球技术有限责任公司 乙烯/α-烯烃嵌段互聚物
CN106817902A (zh) * 2014-08-21 2017-06-09 陶氏环球技术有限责任公司 借助嵌段复合物成核剂的成核
CN107923883A (zh) * 2015-08-28 2018-04-17 陶氏环球技术有限责任公司 具有减少的共结晶的聚合物的色谱法

Family Cites Families (13)

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NL254972A (ko) * 1960-06-21
US5222390A (en) 1991-09-20 1993-06-29 The Dow Chemical Company Crystallization analysis fractionization
RU2178422C2 (ru) 1996-03-27 2002-01-20 Дзе Дау Кемикал Компани Активатор катализаторов полимеризации олефинов, каталитическая система и способ полимеризации
JP4204676B2 (ja) * 1998-02-23 2009-01-07 出光興産株式会社 プロピレン系樹脂並びにそれを用いたフィルム及び積層体
WO2006081116A1 (en) 2005-01-24 2006-08-03 Dow Global Technologies, Inc. Apparatus for method for polymer characterization
EA200870112A1 (ru) 2005-12-23 2009-12-30 СОЛВЕЙ ЭДВАНСТ ПОЛИМЕРС, Эл.Эл.Си. Новое применение полибифенилэфирсульфонов
US8071714B2 (en) 2006-03-15 2011-12-06 Polymer Characterization, S.A. Method for separating and purifying crystallisable organic compounds
EP2483348B2 (en) 2009-10-02 2019-11-27 Dow Global Technologies LLC Block composites and impact modified compositions
US8318896B2 (en) * 2009-12-21 2012-11-27 Dow Global Technologies Llc Chromatography of polyolefin polymers
ES2973122T3 (es) 2013-07-09 2024-06-18 Dow Global Technologies Llc Interpolímeros de etileno/alfa-olefina con fluidez de gránulos mejorada
JP7237101B2 (ja) 2018-06-29 2023-03-10 ダウ グローバル テクノロジーズ エルエルシー 発泡ビーズ及び焼結発泡構造体
KR102601945B1 (ko) 2018-06-29 2023-11-16 다우 글로벌 테크놀로지스 엘엘씨 폼 비드 및 소결된 폼 구조물
US11912842B2 (en) 2018-06-29 2024-02-27 Dow Global Technologies Llc Foam bead and sintered foam structure

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105001584A (zh) * 2008-01-30 2015-10-28 陶氏环球技术有限责任公司 乙烯/α-烯烃嵌段互聚物
WO2015115631A1 (ja) * 2014-01-29 2015-08-06 サン・トックス株式会社 ポリオレフィン系無延伸多層フィルム
CN106817902A (zh) * 2014-08-21 2017-06-09 陶氏环球技术有限责任公司 借助嵌段复合物成核剂的成核
CN107923883A (zh) * 2015-08-28 2018-04-17 陶氏环球技术有限责任公司 具有减少的共结晶的聚合物的色谱法

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
L. WILD ET AL,: "DETERMINATION OF BRANCHING DISTRIBUTIONS IN POLYETHYLENE AND ETHYLENE COPOLYMERS", JOURNAL OF POLYMER SCIENCE PART B:POLYMER PHYSICS, vol. 20, pages 441 - 45 *
WEIFENG LIU ET AL,: "Structure analysis of ethylene/1-octene copolymers synthesized from living coordination polymerization", EUROPEAN POLYMER JOURNAL, no. 54, pages 160 - 171, XP028847988, DOI: 10.1016/j.eurpolymj.2014.03.010 *

Also Published As

Publication number Publication date
TW202000288A (zh) 2020-01-01
WO2020005953A1 (en) 2020-01-02
JP2021528660A (ja) 2021-10-21
US20210132011A1 (en) 2021-05-06
EP3814761A1 (en) 2021-05-05
BR112020026888A2 (pt) 2021-03-30
SG11202013153SA (en) 2021-01-28
KR20210027418A (ko) 2021-03-10
EP3814761B1 (en) 2024-03-27
US11988650B2 (en) 2024-05-21
JP7386820B2 (ja) 2023-11-27

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