CN112494364B - Smoothie makeup removing cream capable of quickly melting makeup and preparation method thereof - Google Patents
Smoothie makeup removing cream capable of quickly melting makeup and preparation method thereof Download PDFInfo
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- CN112494364B CN112494364B CN202011567446.4A CN202011567446A CN112494364B CN 112494364 B CN112494364 B CN 112494364B CN 202011567446 A CN202011567446 A CN 202011567446A CN 112494364 B CN112494364 B CN 112494364B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8105—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- A61K8/8111—Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
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- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
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Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to a smoothie makeup removing cream capable of quickly melting makeup and a preparation method thereof. The makeup removing cream is prepared by matching Fischer-Tropsch synthetic wax X, fischer-Tropsch synthetic wax Y and hyperbranched polyolefin synthetic wax Z with other components, can be quickly melted when in use, promotes the whole makeup removing cream to be attached to skin, and greatly shortens the makeup removing time; meanwhile, the integral stability of the makeup removing cream can be ensured, so that the makeup removing cream can keep higher stability under high-temperature or low-temperature conditions; in addition, the makeup removing cream has beautiful sand-coagulated appearance and is favored by consumers. The preparation method is simple and is suitable for large-scale industrial production.
Description
Technical Field
The invention belongs to the technical field of cosmetics. More particularly, relates to a smoothie makeup removing cream for quickly removing makeup and a preparation method thereof.
Background
With the increasing improvement of living standard of people, cosmetics become a part of daily life of people. As a result, post-makeup cleansing becomes a crucial step in skin care. If the cleansing is not thorough, the residual cosmetics can cause the pores of the facial skin to be blocked, so that the oil and water secretion of the skin is disordered, and the troublesome skin problems of acne, blackheads and the like are caused. Even if the residual cosmetics enter hair follicles along with the respiration of pores, cysts are formed, and the residual cosmetics are difficult to clean in the surface layer of the skin for a long time.
Currently, the makeup removing cosmetics generally used mainly comprise products such as makeup removing water or makeup removing oil. The makeup remover oil is an oily flowable liquid formed by mixing oil ester and an oil-in-water self-emulsifying agent, and by utilizing the characteristic of similar intermiscibility of the oil ester, oil between an oil-soluble film forming agent and a pigment contained in makeup and oil secreted by human skin are dissolved and dispersed in cleaning water and removed, so that the effects of makeup removal and cleaning are achieved, but the makeup remover oil is a flowable liquid, has low viscosity and is inconvenient to use. In order to solve the problems, the Chinese patent application CN105581939A discloses a massage makeup-removing cleansing cream which is mainly prepared from grease, a nonionic surfactant, a thickening agent and other components, wherein the thickening agent is polyethylene wax, the grease is ethylhexyl palmitate, mineral oil, cetyl ethylhexyl ester, olive oil, jojoba seed oil and the like, the cleansing cream has certain viscosity and shape, is convenient to use, can improve blood circulation, muscle tension and the like, and solves the problems of dull complexion and the like. However, in actual use, the melting point of the polyethylene wax added into the product is higher (85-120 ℃), and the problems of low makeup melting speed, long makeup removing time and the like exist; the cleaning agent is not easy to wash and is too greasy, so that the use experience is poor; and if the thickener with low melting point is adopted, the problems that the makeup removing paste is difficult to form, the thermal stability is poor and the like can be caused.
Therefore, the makeup removing cream which can quickly remove makeup, has high thermal stability and is good in use experience is urgently needed.
Disclosure of Invention
The technical problem to be solved by the invention is to overcome the defects and shortcomings of low makeup-removing speed, long makeup-removing time, difficult washing, excessive greasiness, poor experience and poor thermal stability of the existing makeup-removing cream, and provide the smoothie makeup-removing cream which is quick in makeup-removing, high in thermal stability and good in use experience.
The invention aims to provide a smoothie makeup removing paste capable of quickly melting makeup.
The invention also aims to provide a preparation method of the smoothie makeup removing cream.
The above purpose of the invention is realized by the following technical scheme:
the smoothie makeup removing cream capable of quickly melting makeup comprises the following components in parts by weight:
the component A comprises: 13 to 18 portions of polysorbate-81, 2 to 5 portions of ceteareth-20, 15 to 20 portions of ethylhexyl palmitate, 15 to 20 portions of decyl oleate, 10 to 15 portions of isohexadecane, 2 to 3 portions of synthetic wax X, 8 to 12 portions of synthetic wax Y and 2.5 to 4.5 portions of synthetic wax Z;
and the component B comprises: 1-4 parts of silica;
wherein the synthetic wax X is CH 3 -(CH 2 )n-CH 3 The molecular weight of the long straight chain alkane is 300-500 daltons; the synthetic wax Y is CH 3 -(CH 2 )n-CH 3 The molecular weight of the long straight chain alkane is 500-1000 dalton; the synthetic wax Z is hyperbranched polyolefin, and the number average molecular weight Mn =1800.
Preferably, the composition comprises the following components in parts by weight:
and (2) component A: 14 to 16 portions of polysorbate-81, 3.5 to 4.5 portions of ceteareth-20, 15.5 to 17 portions of ethylhexyl palmitate, 15.5 to 17 portions of decyl oleate, 10.5 to 12 portions of isohexadecane, 2.2 to 2.8 portions of synthetic wax X, 9 to 11 portions of synthetic wax Y and 2.8 to 3.8 portions of synthetic wax Z;
and the component B comprises: 2-3 parts of silica.
More preferably, the composition comprises the following components in parts by weight:
and (2) component A: 15 parts of polysorbate-81, 4 parts of ceteareth-20, 16 parts of ethylhexyl palmitate, 16 parts of decyl oleate, 11 parts of isohexadecane, 2.5 parts of synthetic wax X, 10 parts of synthetic wax Y and 3 parts of synthetic wax Z;
and B component: silica 2.5 parts.
Preferably, the molecular weight of the synthetic wax X is in the range of 300 to 400 daltons.
Preferably, the molecular weight of the synthetic wax Y is between 600 and 1000 daltons.
Preferably, the melting point of the synthetic wax X is 61 to 67 ℃.
Preferably, the melting point of the synthetic wax Y is 80 to 85 ℃.
Preferably, the melting point of the synthetic wax Z is 32 to 50 ℃.
The synthetic wax X and the synthetic wax Y are both Fischer-Tropsch synthetic wax, and the synthetic wax Z is hyperbranched polyolefin synthetic wax and has the advantage of narrow melting range; the three materials have different structures and melting points, and are mixed and matched according to a certain proportion, so that when the cleansing cream is used, after the cleansing cream is contacted with the skin of a human body, the synthetic wax Z with the melting point close to the body temperature of the human body can be quickly melted, the whole cleansing cream is promoted to be attached to the skin, and the cleansing time is greatly shortened; meanwhile, the combination of other two synthetic waxes X and Y with higher melting points can improve the overall stability of the makeup removing cream, so that the makeup removing cream can keep higher stability under high-temperature or low-temperature conditions. On the other hand, the inventors have found creatively in practice that a makeup remover having a frosty appearance can be prepared by adding other raw materials to a combination of a synthetic wax X, a synthetic wax Y and a synthetic wax Z at a predetermined ratio, and the makeup remover can be more easily appreciated by consumers.
In addition, the invention also provides a preparation method of the smoothie cleansing cream, which comprises the following steps:
uniformly mixing the raw materials of the component A, heating to 85-90 ℃, stirring for dissolving, adding the component B, stirring for homogenizing, keeping the temperature and stirring for 5-8 minutes after the powder is completely dispersed, cooling, filling, standing and cooling to room temperature to obtain the product.
Further, the temperature of the cooling filling is 70-75 ℃.
The invention has the following beneficial effects:
the smoothie makeup removing cream capable of quickly melting the makeup quickly disclosed by the invention is characterized in that the Fischer-Tropsch synthetic wax X, the Fischer-Tropsch synthetic wax Y and the hyperbranched polyolefin synthetic wax Z are matched with other components, so that the smoothie makeup removing cream can be quickly melted when in use, the whole makeup removing cream is promoted to be attached to the skin, and the makeup removing time is greatly shortened; meanwhile, the integral stability of the makeup removing cream can be ensured, so that the makeup removing cream can keep higher stability under high-temperature or low-temperature conditions; in addition, the makeup removing cream has beautiful sand-coagulated appearance and is favored by consumers. The preparation method is simple and suitable for large-scale industrial production.
Detailed Description
The present invention is further illustrated by the following specific examples, which are not intended to limit the invention in any way. Reagents, methods and apparatus used in the present invention are conventional in the art unless otherwise indicated.
Unless otherwise indicated, reagents and materials used in the following examples are commercially available.
Examples 1 to 5 quick makeup-melting smoothie makeup remover
The smoothie cleansing cream capable of quickly melting the makeup is prepared according to the components in the table 1.
Table 1 examples 1 to 5 smoothie makeup remover cream for quick makeup melting
Wherein the synthetic wax X is CH 3 -(CH 2 )n-CH 3 The long straight chain alkane has the molecular weight of 300-400 daltons and the melting point of 61-67 ℃; the synthetic wax Y is CH 3 -(CH 2 )n-CH 3 The long straight chain alkane has the molecular weight of 600-1000 daltons and the melting point of 80-85 ℃; the synthetic wax Z is hyperbranched polyolefin, the number average molecular weight Mn =1800 and the melting point is 32-50 ℃.
The preparation method comprises the following steps:
uniformly mixing the raw materials of the component A, heating to 85 ℃, stirring for dissolving for 5 minutes, and uniformly stirring; adding the component B, stirring and homogenizing for 1 minute to completely disperse the powder uniformly, then keeping the temperature and stirring for 8 minutes, stirring, cooling to 75 ℃, filling, standing and cooling to room temperature to obtain the product.
Comparative examples 1 to 6 cleansing cream
The makeup removing cream was prepared according to the components in table 2.
Table 2 comparative examples 1 to 6 smoothie cleansing cream for quick makeup melting
The preparation method comprises the following steps: reference is made to the preparation of examples 1 to 5.
Experimental example 1 cleansing cream appearance and solidification temperature
The appearance and the solidification temperature of the makeup removing pastes obtained in the examples and comparative examples were measured, and the measurement results are shown in table 3.
TABLE 3 appearance of makeup remover and measurement results of solidification temperature
| Group of | Appearance of the product | Onset of coagulation temperature/. Degree.C |
| Example 1 | Paste with sand-coagulated appearance | 71.5 |
| Example 2 | Paste with sand-setting appearance | 69.3 |
| Example 3 | Paste with sand-coagulated appearance | 70.3 |
| Example 4 | Paste with sand-coagulated appearance | 70.8 |
| Example 5 | Paste with sand-coagulated appearance | 70.5 |
| Comparative example 1 | Paste with sand-coagulated appearance | 68.1 |
| Comparative example 2 | Common paste | 64.6 |
| Comparative example 3 | Paste with sand-setting appearance | 69.6 |
| Comparative example 4 | Common paste | 64.3 |
| Comparative example 5 | Common paste | 40.5 |
| Comparative example 6 | Common paste | 73.4 |
As can be seen from Table 3, the makeup removing pastes prepared in examples 1 to 5 of the present invention all had a beautiful cream-like appearance of coagulated sand, and the temperature at which solidification starts was about 70 ℃; the makeup removing pastes prepared in comparative examples 2, 4 and 6 are only common pastes, and have low solidification temperature and stability easily affected by temperature rise.
Experimental example 2 cleansing cream stability test
The stability of the makeup removing pastes obtained in examples and comparative examples was measured, and the appearance of the makeup removing pastes was observed by placing the pastes at 50 ℃ for one month at 4 ℃ and 18 ℃ for one month or at 50 ℃ for 24 hours at 18 ℃ for 24 hours and circulating at high and low temperatures for 6 times, respectively, and the results are shown in Table 4.
Table 4 cleansing cream stability measurement results
As can be seen from Table 4, the makeup removing pastes prepared in examples 1 to 5 of the present invention can maintain a normal state even after being left at 50 ℃ and 4 ℃ to 18 ℃ for one month, and can maintain their original states even under high and low temperature cycle conditions, and thus have good stability. While comparative example 1 has no appearance of the sand at a higher temperature of 50 ℃, comparative example 1 and comparative example 3 can not keep good morphological appearance under high and low temperature circulation conditions, and the stability is poor.
Experimental example 3 Consumer experience test of cleansing cream
Test objects: 44 female volunteers aged 20-30 years are selected, wherein 22 skins are dry skins, and the other 22 skins are oily skins, and are not patients with severe system diseases, immunodeficiency or autoimmune diseases, no active allergic diseases, no physique hypersensitiveness and no hormone drugs or immunosuppressants used in the last month.
The test method comprises the following steps: each sample correspondingly selects 2 female volunteers with dry skin and oily skin, the female volunteers are used for three times, the female volunteers are used once a day for 3 days, the face of the volunteer is the tested part, and the makeup removing test is carried out after the volunteers use the same cosmetics for makeup application. The melting rate, the easy washing degree, the use freshness, the makeup removing strength and the mildness are respectively scored (1-5 points, the 1 point is the worst, and the 5 points are the best), and the results are averaged and shown in table 5.
TABLE 5 cleansing cream Consumer experience scoring results
As can be seen from table 5, the makeup removing pastes prepared in the embodiments 1 to 5 of the present invention have high scores in the aspects of makeup removing speed, easy rinsing degree, use freshness, makeup removing power, mildness and the like, and are good in use experience, and the comprehensive score is more than 4 points, so that the makeup removing pastes are highly popular with volunteers.
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such modifications are intended to be included in the scope of the present invention.
Claims (7)
1. The smoothie makeup removing cream capable of quickly melting makeup is characterized by comprising the following components in parts by weight:
the component A comprises: 13 to 18 portions of polysorbate-81, 2 to 5 portions of ceteareth-20, 15 to 20 portions of ethylhexyl palmitate, 15 to 20 portions of decyl oleate, 10 to 15 portions of isohexadecane, 2 to 3 portions of synthetic wax X, 8 to 12 portions of synthetic wax Y and 2.5 to 4.5 portions of synthetic wax Z;
and the component B comprises: 1-4 parts of silica;
wherein the synthetic wax X is CH 3 -(CH 2 )n-CH 3 The long straight chain alkane has the molecular weight of 300-500 daltons and the melting point of 61-67 ℃; the synthetic wax Y is CH 3 -(CH 2 )n-CH 3 The long straight chain alkane has the molecular weight of 500-1000 daltons and the melting point of 80-85 ℃; the synthetic wax Z is hyperbranched polyolefin, the number average molecular weight Mn =1800 and the melting point is 32-50 ℃.
2. The smoothie makeup removing cream as claimed in claim 1, which is characterized by comprising the following components in parts by weight:
the component A comprises: 14 to 16 portions of polysorbate-81, 3.5 to 4.5 portions of cetearyl alcohol polyether-20, 15.5 to 17 portions of ethylhexyl palmitate, 15.5 to 17 portions of decyl oleate, 10.5 to 12 portions of isohexadecane, 2.2 to 2.8 portions of synthetic wax X, 9 to 11 portions of synthetic wax Y and 2.8 to 3.8 portions of synthetic wax Z;
and B component: 2-3 parts of silica.
3. The smoothie makeup removing cream according to claim 2, which is characterized by comprising the following components in parts by weight:
the component A comprises: polysorbate-81 parts, ceteareth-20 parts, ethylhexyl palmitate 16 parts, decyl oleate 16 parts, isohexadecane 11 parts, synthetic wax X2.5 parts, synthetic wax Y10 parts, and synthetic wax Z3 parts;
and B component: 2.5 parts of silica.
4. The quick-makeup-melting smoothie makeup removing cream according to claim 1, wherein the molecular weight of said synthetic wax X is 300 to 400 daltons.
5. The quick-makeup-melting smoothie makeup removing cream according to claim 1, wherein the molecular weight of the synthetic wax Y is 600 to 1000 daltons.
6. A method for preparing the smoothie makeup removing cream as claimed in any one of claims 1 to 5, characterized by comprising the steps of:
uniformly mixing the raw materials of the component A, heating to 85-90 ℃, stirring for dissolving, adding the component B, stirring for homogenizing, keeping the temperature and stirring for 5-8 minutes after completely dispersing the powder, cooling, filling, standing and cooling to room temperature to obtain the composition.
7. The method according to claim 6, wherein the temperature of the cooling and filling is 70-75 ℃.
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| JP2017206450A (en) * | 2016-05-17 | 2017-11-24 | 株式会社ファンケル | Oily cleansing cosmetic |
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| WO2009086513A1 (en) * | 2007-12-28 | 2009-07-09 | L'oreal S.A. | Cosmetic composition containing a polar modified wax and a low melting point polyolefin wax |
| US9278060B2 (en) * | 2007-12-28 | 2016-03-08 | L'oreal | Composition containing a polar modified polymer |
| EP3572462A1 (en) * | 2018-05-25 | 2019-11-27 | Sasol Wax GmbH | Wax composition comprising linear hydrocarbons, branched hydrocarbons and oxidized hydrocarbons, aqueous dispersion thereof, method to produce such wax composition and dispersion and use thereof as carnauba wax replacement |
| CN110433091A (en) * | 2019-09-09 | 2019-11-12 | 杭州千岛湖蓝色天使实业有限公司 | A kind of eye make-up remover and preparation method thereof |
| CN111603414A (en) * | 2020-06-12 | 2020-09-01 | 成都律恩泽雅科技有限公司 | Makeup removing cream and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2016074638A (en) * | 2014-10-08 | 2016-05-12 | クラシエホームプロダクツ株式会社 | Pasty cleansing cosmetic |
| CN105534755A (en) * | 2016-01-13 | 2016-05-04 | 广州丹奇日用化工厂有限公司 | Refreshing mild cleansing cream and preparation method thereof |
| JP2017206450A (en) * | 2016-05-17 | 2017-11-24 | 株式会社ファンケル | Oily cleansing cosmetic |
| CN106491461A (en) * | 2016-12-24 | 2017-03-15 | 严志海 | A kind of make-up remover and preparation method thereof |
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