CN112402306A - Soapberry emulsion type shampoo and preparation method thereof - Google Patents
Soapberry emulsion type shampoo and preparation method thereof Download PDFInfo
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- CN112402306A CN112402306A CN202011171557.3A CN202011171557A CN112402306A CN 112402306 A CN112402306 A CN 112402306A CN 202011171557 A CN202011171557 A CN 202011171557A CN 112402306 A CN112402306 A CN 112402306A
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- 240000003377 Shepherdia canadensis Species 0.000 title claims abstract description 72
- 235000018324 Shepherdia canadensis Nutrition 0.000 title claims abstract description 72
- 239000002453 shampoo Substances 0.000 title claims abstract description 64
- 239000000839 emulsion Substances 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title abstract description 16
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 84
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 60
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 40
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims abstract description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- -1 alkyl glycoside Chemical class 0.000 claims abstract description 24
- 239000004354 Hydroxyethyl cellulose Substances 0.000 claims abstract description 22
- 229920000663 Hydroxyethyl cellulose Polymers 0.000 claims abstract description 22
- 229930182470 glycoside Natural products 0.000 claims abstract description 22
- 235000019447 hydroxyethyl cellulose Nutrition 0.000 claims abstract description 22
- 229940048842 sodium xylenesulfonate Drugs 0.000 claims abstract description 22
- QUCDWLYKDRVKMI-UHFFFAOYSA-M sodium;3,4-dimethylbenzenesulfonate Chemical compound [Na+].CC1=CC=C(S([O-])(=O)=O)C=C1C QUCDWLYKDRVKMI-UHFFFAOYSA-M 0.000 claims abstract description 22
- 229920002907 Guar gum Polymers 0.000 claims abstract description 21
- 150000005690 diesters Chemical class 0.000 claims abstract description 21
- 239000012153 distilled water Substances 0.000 claims abstract description 21
- 239000000665 guar gum Substances 0.000 claims abstract description 21
- 235000010417 guar gum Nutrition 0.000 claims abstract description 21
- 229960002154 guar gum Drugs 0.000 claims abstract description 21
- 244000060011 Cocos nucifera Species 0.000 claims abstract description 20
- 235000013162 Cocos nucifera Nutrition 0.000 claims abstract description 20
- 239000011780 sodium chloride Substances 0.000 claims abstract description 20
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 claims abstract description 13
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 claims abstract description 13
- 229960002216 methylparaben Drugs 0.000 claims abstract description 13
- 239000000047 product Substances 0.000 claims description 93
- 238000002156 mixing Methods 0.000 claims description 46
- 238000003756 stirring Methods 0.000 claims description 11
- 238000010438 heat treatment Methods 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 9
- 238000007599 discharging Methods 0.000 claims description 8
- 239000012467 final product Substances 0.000 claims description 8
- 238000001816 cooling Methods 0.000 claims description 7
- 239000000243 solution Substances 0.000 claims description 7
- 239000003755 preservative agent Substances 0.000 claims 3
- 230000002335 preservative effect Effects 0.000 claims 3
- 208000003251 Pruritus Diseases 0.000 abstract description 10
- 230000007803 itching Effects 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 7
- 238000005187 foaming Methods 0.000 abstract description 7
- 230000003656 anti-hair-loss Effects 0.000 abstract description 3
- 230000009286 beneficial effect Effects 0.000 abstract description 3
- MRUAUOIMASANKQ-UHFFFAOYSA-N cocamidopropyl betaine Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC([O-])=O MRUAUOIMASANKQ-UHFFFAOYSA-N 0.000 description 18
- 239000000463 material Substances 0.000 description 18
- 235000011187 glycerol Nutrition 0.000 description 17
- 239000000126 substance Substances 0.000 description 15
- 238000012360 testing method Methods 0.000 description 15
- 238000011156 evaluation Methods 0.000 description 10
- 239000006260 foam Substances 0.000 description 7
- 238000005406 washing Methods 0.000 description 7
- 241000580955 Sapindus mukorossi Species 0.000 description 6
- 210000003128 head Anatomy 0.000 description 6
- 230000001953 sensory effect Effects 0.000 description 6
- 238000007792 addition Methods 0.000 description 5
- 239000000523 sample Substances 0.000 description 5
- 208000001840 Dandruff Diseases 0.000 description 4
- AOMUHOFOVNGZAN-UHFFFAOYSA-N N,N-bis(2-hydroxyethyl)dodecanamide Chemical compound CCCCCCCCCCCC(=O)N(CCO)CCO AOMUHOFOVNGZAN-UHFFFAOYSA-N 0.000 description 4
- 238000002474 experimental method Methods 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- GLDOVTGHNKAZLK-UHFFFAOYSA-N octadecan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCO GLDOVTGHNKAZLK-UHFFFAOYSA-N 0.000 description 4
- 230000003068 static effect Effects 0.000 description 4
- 238000004458 analytical method Methods 0.000 description 3
- 238000013461 design Methods 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- BOUCRWJEKAGKKG-UHFFFAOYSA-N n-[3-(diethylaminomethyl)-4-hydroxyphenyl]acetamide Chemical compound CCN(CC)CC1=CC(NC(C)=O)=CC=C1O BOUCRWJEKAGKKG-UHFFFAOYSA-N 0.000 description 3
- 229930182490 saponin Natural products 0.000 description 3
- 150000007949 saponins Chemical class 0.000 description 3
- 235000017709 saponins Nutrition 0.000 description 3
- LDVVTQMJQSCDMK-UHFFFAOYSA-N 1,3-dihydroxypropan-2-yl formate Chemical compound OCC(CO)OC=O LDVVTQMJQSCDMK-UHFFFAOYSA-N 0.000 description 2
- 201000004384 Alopecia Diseases 0.000 description 2
- 239000004166 Lanolin Substances 0.000 description 2
- 239000004698 Polyethylene Substances 0.000 description 2
- 231100000360 alopecia Toxicity 0.000 description 2
- 125000002091 cationic group Chemical group 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- 230000032798 delamination Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 229940039717 lanolin Drugs 0.000 description 2
- 235000019388 lanolin Nutrition 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000002398 materia medica Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000005457 optimization Methods 0.000 description 2
- 229920000573 polyethylene Polymers 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 239000012488 sample solution Substances 0.000 description 2
- 238000004088 simulation Methods 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- 230000000007 visual effect Effects 0.000 description 2
- MIJYXULNPSFWEK-GTOFXWBISA-N 3beta-hydroxyolean-12-en-28-oic acid Chemical compound C1C[C@H](O)C(C)(C)[C@@H]2CC[C@@]3(C)[C@]4(C)CC[C@@]5(C(O)=O)CCC(C)(C)C[C@H]5C4=CC[C@@H]3[C@]21C MIJYXULNPSFWEK-GTOFXWBISA-N 0.000 description 1
- 244000303965 Cyamopsis psoralioides Species 0.000 description 1
- 240000001008 Dimocarpus longan Species 0.000 description 1
- JKLISIRFYWXLQG-UHFFFAOYSA-N Epioleonolsaeure Natural products C1CC(O)C(C)(C)C2CCC3(C)C4(C)CCC5(C(O)=O)CCC(C)(C)CC5C4CCC3C21C JKLISIRFYWXLQG-UHFFFAOYSA-N 0.000 description 1
- 235000000235 Euphoria longan Nutrition 0.000 description 1
- 240000001080 Grifola frondosa Species 0.000 description 1
- 235000007710 Grifola frondosa Nutrition 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 206010028980 Neoplasm Diseases 0.000 description 1
- YBRJHZPWOMJYKQ-UHFFFAOYSA-N Oleanolic acid Natural products CC1(C)CC2C3=CCC4C5(C)CCC(O)C(C)(C)C5CCC4(C)C3(C)CCC2(C1)C(=O)O YBRJHZPWOMJYKQ-UHFFFAOYSA-N 0.000 description 1
- MIJYXULNPSFWEK-UHFFFAOYSA-N Oleanolinsaeure Natural products C1CC(O)C(C)(C)C2CCC3(C)C4(C)CCC5(C(O)=O)CCC(C)(C)CC5C4=CCC3C21C MIJYXULNPSFWEK-UHFFFAOYSA-N 0.000 description 1
- 229920001214 Polysorbate 60 Polymers 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 238000007664 blowing Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 230000003750 conditioning effect Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 239000006071 cream Substances 0.000 description 1
- 238000007405 data analysis Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005485 electric heating Methods 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 230000004438 eyesight Effects 0.000 description 1
- 210000001061 forehead Anatomy 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 231100000989 no adverse effect Toxicity 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 238000010606 normalization Methods 0.000 description 1
- 230000000474 nursing effect Effects 0.000 description 1
- 229940100243 oleanolic acid Drugs 0.000 description 1
- 244000045947 parasite Species 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 239000006187 pill Substances 0.000 description 1
- 229920000136 polysorbate Polymers 0.000 description 1
- HZLWUYJLOIAQFC-UHFFFAOYSA-N prosapogenin PS-A Natural products C12CC(C)(C)CCC2(C(O)=O)CCC(C2(CCC3C4(C)C)C)(C)C1=CCC2C3(C)CCC4OC1OCC(O)C(O)C1O HZLWUYJLOIAQFC-UHFFFAOYSA-N 0.000 description 1
- 239000001397 quillaja saponaria molina bark Substances 0.000 description 1
- 238000000611 regression analysis Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 238000007665 sagging Methods 0.000 description 1
- 229940095673 shampoo product Drugs 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 150000008130 triterpenoid saponins Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/604—Alkylpolyglycosides; Derivatives thereof, e.g. esters
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/737—Galactomannans, e.g. guar; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/04—Antipruritics
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q7/00—Preparations for affecting hair growth
Abstract
The invention discloses a soapberry emulsion shampoo and a preparation method thereof. Is prepared from 40-46 parts of distilled water, 0.7-1.3 parts of sodium chloride, 2.5-3.5 parts of glycerol, 0.2-0.6 part of methyl paraben, 4-6 parts of cocoanut diethanolamide (6501), 1.5-2.5 parts of polyquaternium-7, 4-6 parts of alkyl glycoside, 6-10 parts of CAB, 1-3 parts of sodium xylene sulfonate, 0.2-0.6 part of pearlescent diester, 15-23 parts of AES, 15-30 parts of soapberry extract, 0.14-0.22 part of guar gum and 0.2-0.4 part of hydroxyethyl cellulose, and then adding citric acid to adjust the pH value to 6-7. The soapberry emulsion shampoo prepared by the invention has the advantages of good detergency, better foaming performance, combing performance, stability, itching relieving and other performances, and has certain anti-hair loss effect and the beneficial effect of keeping hair smooth.
Description
Technical Field
The invention relates to a soapberry emulsion type shampoo, in particular to a soapberry emulsion type shampoo and a preparation method thereof.
Background
Sapindus mukorossi Gaertn, bitter, slightly pungent and cold. Has little toxicity. Clear heat and dispel phlegm, eliminate stagnation and kill parasites. Alias: sapindus mukorossi (compendium of materia medica), oil lodes, fructus hordei zizaniae, other names of places: rubbing eyes, false longan, grifola frondosa and the like. The compendium of materia medica records that the soapberry can remove head wind (dandruff) for improving eyesight by washing hair, whiten and remove spots by washing face, the soapberry (soapberry) is collected for … … October, cooked and mashed, and the white face and various fragrances are used as pills, the body and the face are bathed, and the soapberry is better than the soapberry in terms of scaling and greasiness. Sapindus mukorossi, also known as soapberry, contains abundant Sapindus mukorossi saponins in the peel, mainly comprises oleanolic acid type triterpenoid saponins, is collectively called Sapindus mukorossi total saponins, is a natural nonionic surfactant, and has biological activities of sterilization, itching relieving, tumor resisting, blood pressure and blood fat reducing and the like.
At present, soapberry is applied to washing and protecting products, but the optimization research on the prescription is few, sensory evaluation, foamability, stability and low-temperature flowing evaluation of the shampoo are used as indexes, the prescription of the shampoo is optimized by adopting a material mixing and homogenizing method, and an experimental basis is provided for the development and utilization of the soapberry emulsion type shampoo.
Disclosure of Invention
The invention aims to provide a soapberry emulsion shampoo and a preparation method thereof. The soapberry emulsion shampoo prepared by the invention has the characteristics of good detergency, better foaming performance, combing performance, stability, itching relieving and the like, and has certain anti-hair loss effect and can keep hair smooth.
The technical scheme of the invention is as follows: a soapberry emulsion shampoo and a preparation method thereof are disclosed, wherein the soapberry emulsion shampoo is prepared from 40-46 parts of distilled water, 0.7-1.3 parts of sodium chloride, 2.5-3.5 parts of glycerol, 0.2-0.6 part of methyl paraben, 4-6 parts of cocoanut diethanolamide, 1.5-2.5 parts of polyquaternium-7, 4-6 parts of alkyl glycoside, 6-10 parts of CAB, 1-3 parts of sodium xylene sulfonate, 0.2-0.6 part of pearlescent diester, 15-23 parts of AES, 15-30 parts of soapberry extract, 0.14-0.22 part of guar gum and 0.2-0.4 part of hydroxyethyl cellulose by weight, and then citric acid is added to adjust the pH value to 6-7.
The soapberry emulsion shampoo is prepared from 42-44 parts by weight of distilled water, 0.8-1.2 parts by weight of sodium chloride, 2.7-3.3 parts by weight of glycerol, 0.3-0.5 part by weight of methyl paraben, 4.5-5.5 parts by weight of coconut diethanolamide, 1.7-2.3 parts by weight of polyquaternium-7, 4.5-5.5 parts by weight of alkyl glycoside, 7-9 parts by weight of CAB, 1.5-2.5 parts by weight of sodium xylene sulfonate, 0.3-0.5 part by weight of pearlescent diester, 17-21 parts by weight of AES, 18-25 parts by weight of soapberry extract, 0.16-0.2 part by weight of guar gum and 0.25-0.35 part by weight of hydroxyethyl cellulose, and then citric acid is added to adjust the pH to 6-7.
The soapberry emulsion shampoo is prepared from 42.7 parts by weight of distilled water, 0.98 part by weight of sodium chloride, 2.95 parts by weight of glycerol, 0.4 part by weight of methyl paraben, 5.01 parts by weight of coconut diethanolamide, 2 parts by weight of polyquaternium-7, 4.96 parts by weight of alkyl glycoside, 8 parts by weight of CAB, 2.01 parts by weight of sodium xylene sulfonate, 0.48 part by weight of pearlescent diester, 18.59 parts by weight of AES, 20 parts by weight of soapberry extract, 0.18 part by weight of guar gum and 0.32 part by weight of hydroxyethyl cellulose, and then citric acid is added to adjust the pH to be 6-7.
The preparation method of the soapberry emulsion shampoo comprises the following steps:
(1) mixing distilled water, sodium chloride, glycerol, methyl hydroxybenzoate and citric acid to obtain product A;
(2) mixing coconut diethanolamide (6501), polyquaternium-7, alkyl glycoside, CAB, sodium xylene sulfonate and pearlescent diester uniformly to obtain product B;
(3) AES is product C;
(4) mixing fructus Sapindi Mukouossi extractive solution, guar gum and hydroxyethyl cellulose uniformly to obtain product D;
(5) adding product A into product D, and mixing to obtain product E;
(6) adding product B into product C at 70-80 deg.C, and mixing to obtain product F;
(7) adding the product E into the product F at 45-50 deg.C, mixing, adjusting pH to 6-7 with citric acid, stopping heating, stirring, cooling, and discharging to obtain the final product.
In the above preparation method of the soapberry emulsion shampoo, in the step (6), the product B is added to the product C at 75 ℃ and mixed uniformly.
Compared with the prior art, the invention has the following beneficial effects:
the auxiliary material type of the soapberry emulsion type shampoo is determined according to a shampoo ingredient principle and a pre-experimental result, sensory evaluation, foamability, stability and low-temperature flowability evaluation of the shampoo are used as indexes, and a mixing uniformity test is adopted to optimize the prescription of the soapberry emulsion type shampoo; and (4) obtaining a result: the prepared soapberry emulsion shampoo has the advantages of being good in detergency, good in foaming performance, good in combing performance, good in stability, good in itching relieving performance and the like, having a certain alopecia prevention effect, and being capable of keeping hair smooth.
Experiments prove that
1 Material
1.1 reagents
Soapberry extract (prepared by laboratories); ALES (ammonium laureth sulfate) (batch No. 20180607, Shandong Yousio chemical science and technology Co., Ltd.); cocodiethanolamide (6501) (cocodiethanolamide) (batch No. 20180521, Shandong Yousio chemical science and technology Limited); alkyl glycoside (batch No. 20180613, Shandong Youso chemical science and technology Co., Ltd.); CAB (Cocoamidopropyl betaine) (batch No. 20180904, Shandong Yousol chemical science and technology Co., Ltd.); sodium xylene sulfonate (batch No. 20181104, Shandong Yousio chemical science and technology Limited); polyquaternium-7 (batch No. 20180604, Shandong Yousio chemical science and technology Limited Co., Ltd.); NaCl (batch No. 2018121059, Tianjin chemical three factories, Ltd.); cationic guar (batch No. 20181107, Shandong Youso chemical science and technology Co., Ltd.); glycerol (batch No. 20171025, Tanskin Seiyuan Chemicals, Inc.); hydroxyethyl cellulose (Shankou No. 20180524, Tokyo chemical science and technology Co., Ltd.); pearlescent grease (batch No. 20180406, Shandong Youso chemical science and technology Co., Ltd.); distilled water; tween 60 batch No.: 20180521, Shandong Youso chemical science and technology Co., Ltd.); lanolin batch number: (20180521, Shandong Yousol chemical science and technology Co., Ltd.); monoglyceride (20190521, Shandong Youthol chemical technology Co., Ltd.); octadecanol (2010607, Shandong Yousio chemical science and technology Co., Ltd.).
1.2 instruments
A microcomputer type acidimeter; BSM-220-4 type electronic balance (limited electronics science, shanghai zhuojing); SB-4200D ultrasonic cleaner (Ningbo New Art ultrasonic Equipment Limited company); GZX-9240MBE electric heating blowing dry box (Shanghai Bochen industry Co., Ltd.) medical equipment factory; BCD-240SDPN refrigerator (Qingdao Haier Co., Ltd.); HH-4 digital display constant temperature water bath (Changzhou Ouhua Instrument Co., Ltd.)
Prescription of 2 soapberry emulsion type shampoo and preparation process
The main principle of shampoo preparation is as follows: the cleaning power is moderate, and the foam is rich, uniform and fine; secondly, the appearance is pleasant, the pearl effect is achieved, and the fragrance is pleasant; moderate consistency; the product is slightly acidic, the pH value is controlled to be 6-7, the pH value is close to that of the skin, and the product has no irritation to the skin; fifthly, has the efficacy of removing dandruff, relieving itching, protecting hair, nourishing hair and the like; sixthly, the conditioning and nursing performance is good, and the hair is smooth and soft and is easy to comb; the moisture retention performance is good, and the hair is prevented from drying.
2.1 establishment of evaluation method for emulsion type shampoo of Sapindus mukorossi
2.1.1 sensory Scoring
The color, appearance and smell of the shampoo and the fineness of the paste are taken as indexes, and each index accounts for 5 points, and 20 points in total.
Color: the degree of uniformity of the color of the formed shampoo was scored between 0 and 5, visually observed at room temperature and in the absence of sunlight.
Appearance: at room temperature and in non-sunlight, the formed shampoo is observed by naked eyes to have 0 minute of foreign matters and no 5 minutes of foreign matters.
Odor: the evaluation is carried out according to the existence of peculiar smell, the peculiar smell is not found for 5 points, and the peculiar smell is found for 0 point.
The paste fineness is as follows: the degree of fineness of the cream of the shampoo was scored between 0 and 5 at room temperature and in the absence of sunlight.
2.1.2 measurement of foamability (waring-Blender method)
Heating and emulsifying lanolin 2%, monoglyceride 0.15%, octadecanol 0.15%, tween 601% and water by a conventional method to uniformly mix, cleaning and drying the real hair and false head, uniformly spraying 10g of prepared emulsion on the top of the real hair and false head by a sprayer, after drying, dissolving 2g of a shampoo sample in 20g of warm water, pouring the sample solution on the top of the false head, rubbing and kneading the sample solution for 100 times in a fixed hair washing mode, then combing 20 times from the forehead root of the false head by fingers, collecting foam on the false head by a 500ml measuring cylinder, and measuring the volume (ml) of the foam. (Total score 20 points, scored by foam volume)
2.1.3 stability assay
Heat resistance: according to the heat-resisting (shampoo) test method of physicochemical indexes of shampoo and paste shampoo (GB/T29679-2013), the samples are respectively poured into 2 test tubes with the diameter of 20mm multiplied by 120mm, the liquid level is about 80mm, and clean plugs are plugged. One test tube to be tested is placed in a constant temperature box which is adjusted to 40 ℃ in advance, taken out after 24 hours, restored to the room temperature and compared with the other test tube in a visual mode. (No delamination 10 minutes after recovery from room temperature and 0 minute)
Cold resistance: according to the cold-resistant (shampoo) test method of the physicochemical indexes of shampoo and paste shampoo (GB/T29679-2013), samples are respectively poured into 2 test tubes with the diameter of 20mm multiplied by 120mm, the liquid level is about 80mm, and clean plugs are plugged. One test tube to be tested is placed in a refrigerator which is pre-adjusted to-8 ℃, taken out after 24 hours, restored to the room temperature and compared with a sample of the other test tube by visual observation. (No delamination 10 minutes after recovery from room temperature and 0 minute)
2.1.4 measurement of Low temperature sag
10g of soapberry emulsion shampoo samples were accurately weighed into polyethylene tubes. The polyethylene tube with the sample is sealed and then vertically fixed in a refrigerator at 2 ℃ for 24 h. The stored sample was removed and the nozzle was held down on a 30 ° ramp, with the flow time(s) immediately timed to the time tSF when the sample flowed to the nozzle. (the total score is 20 points and is scored according to the tSF value; 0 point: more than 30s, 1-20 points: less than or equal to 30s)
2.2 blend uniformity design optimization of the formulation of the soapberry emulsion shampoo
In the case of fixing the soapberry extract, taking ALES, cocoanut diethanolamide (6501), alkyl glycoside, CAB, sodium xylene sulfonate, polyquaternium-7, NaCl, cationic guar gum, glycerol, hydroxyethyl cellulose, pearlescent diester and water, and taking the percentage content of the variables as independent variables, respectively setting the independent variables as X1,X2,X3,X4,X5,X6,X7,X8,X9,X10,X11,X12And (4) optimizing the formula, and determining the composition range of independent variables through a single factor test. Meanwhile, considering a normalization condition, providing a constraint limiting condition for uniform mixed material design:
(1)12.5％≤X1≤25％、5％≤X2≤6.25％、6.25％≤X3≤7.5％、 1％≤X4≤1.25％、2.5％≤X5≤3.75％、1.25％≤X6≤2.5％、1.25％≤ X7≤3.75％、0.125％≤X8≤0.5％、0.1875％≤X9≤3.75％、0.375％≤ X10≤3.75％、0.375％≤X11≤0.625％、30.25％≤X12≤58.5％；
(2)X1+X2+X3+X4+X5+X6+X7+X8+X9+X10+X11+X12＝100％
the 12-factor uniform mixing Design is carried out under the limiting condition, the Design-Expert 8.0.6 uniform Design software is used for arranging experiments, and the evaluation indexes are as follows: composite score Y ═ Y1+Y2+Y3+Y4，Y1、Y2、Y3、Y4The sensory score, foamability (simulation) score, stability (heat resistance, cold resistance) score, and low-temperature static sagging score of the soapberry emulsion shampoo were respectively shown. The factor level is shown in table 1, the shampoo formula is shown in table 2, and the test result is shown in table 3;
table 1 mixing uniformity test factor level table
TABLE 2 shampoo prescription Table
TABLE 3 test results
2.3 data analysis
With X1-X12And (3) taking the comprehensive score Y as a dependent variable, and performing quadratic polynomial regression analysis on the test data by using DPS7.05 uniform experiment software to obtain a quadratic polynomial regression equation:
y ═ 110.8852586+224.29663883X9-3922.577647X 1X 10+ 607.5647584X 2X 9-1582.1652605X 3X 12-9255.682845X 4X 9-43201.008716X 5X 7+144.38962876X 6X 10+133294.750720X 6X 11+4246.047720X 7X 10+275960.994350X 9X 11(r ═ 1.0000, P ═ 0.0035<0.05), the results of the quadratic polynomial stepwise analysis between the composite score Y and the independent variables are shown in tables 2-4:
TABLE 4 results of two-term multiple stepwise analysis
According to the analysis result of the mixed material uniformity test, the formula of the soapberry emulsion shampoo is obtained as follows:
the method comprises the following steps: 42.7 percent of distilled water (mass fraction, the same below), 0.98 percent of sodium chloride, 2.95 percent of glycerin, a proper amount of citric acid and 0.4 percent of methyl paraben
Secondly, the step of: 5.01 percent of coconut diethanolamide (6501), 2 percent of polyquaternium-7, 4.96 percent of alkyl glycoside, 8 percent of CAB, 2.01 percent of sodium xylene sulfonate and 0.48 percent of pearlescent diester
③: AES is 18.59%
Fourthly, the method comprises the following steps: 20 percent of soapberry extract, 0.18 percent of guar gum and 0.32 percent of hydroxyethyl cellulose, and the preparation process comprises the following steps: uniformly stirring the materials, pouring the materials into the swelled materials, adding the materials into the materials after the materials are completely dissolved at 75 ℃, uniformly stirring the materials, finally pouring the materials into the materials when the temperature is kept between 45 and 50 ℃, uniformly stirring the materials, adjusting the pH value to be between 6 and 7 by using citric acid, stopping heating, stirring the materials until the materials are cooled, and discharging the materials.
2.4 investigating the influence of the addition of the soapberry extract on the shampooing performance
TABLE 5 odor, color, foam, pH, heat resistance and cold resistance of various soapberry extract additions
Note: the foamability is detected by a simulation method; the pH was measured using a microcomputer type acidimeter.
As can be seen from Table 5, the color of the final product gradually deepens with the increase of the added amount of the soapberry extract, the unique faint scent of the soapberry gradually becomes rich, the fluctuation of the pH and low-temperature static flowability is reduced, the heat resistance and the cold resistance are stable, and the fluctuation of the foam height is increased. And when the low-temperature static flowing property is less than 30s, the shampoo is easily accepted by consumers. Therefore, the soapberry extract has the advantages of low addition amount of less than 10 percent (containing 10 percent), poor low-temperature flowability and high low-temperature static flowability of more than 15 percent (containing 15 percent). It can be seen that the soapberry extract has no adverse effect on the shampoo and has good compatibility with other components.
By adopting a sensory evaluation method, various performances such as foaming performance, combing performance, stability, itching stopping and the like of the soapberry emulsion type shampoo are tested by taking a shampoo product (regarded as a reference 1) which is popular in the market as a reference, a test subject uses the reference 1 and the test product respectively to comprehensively grade the various effects such as combing performance, itching stopping and the like according to the self feeling, and the evaluation grades are set to be 6-very good, 5-good, 4-good, 3-common, 2-poor and 1-poor grades and 6 grades.
Table 6 average score of sensory evaluation of subjects
From Table 6, it can be seen that the highest comprehensive score is obtained when the addition amount of the extract is 20%, 25%, 30%, but the indexes are better when the addition amount of the extract is 20% based on the principle of "cost saving".
Conclusion and discussion
In the world trend of "returning to nature", natural medicines are giving off a great vitality, and more consumers tend to use natural products when selecting washing products. Soapberry is a traditional natural washing and protecting precious fruit of Chinese nationality since ancient times, and the water decoction of the soapberry can be used for washing hair, can prevent dandruff and has the efficacy of removing dandruff and relieving itching. The total saponin in the soapberry extract is a pure natural surfactant, the foaming performance is good, the foam hand feeling is fine and smooth, the dirt-removing capability is strong, and the prepared shampoo has the advantages of nature and no pollution and has great development potential. The shampoo prescription optimized in the experiment has multiple performances of better foaming performance, combing performance, stability, itching relieving and the like, and has a certain anti-hair loss effect. The experiment is expected to provide experimental basis for developing the soapberry emulsion shampoo.
In conclusion, the soapberry emulsion shampoo prepared by the invention has the advantages of good detergency, better foaming performance, combing performance, stability, itching relieving and the like, and has the beneficial effects of certain alopecia prevention effect and hair smoothness maintenance.
Detailed Description
The present invention is further illustrated by the following examples, which are not to be construed as limiting the invention.
Example 1: a soapberry emulsion shampoo is prepared from 40kg of distilled water, 0.7kg of sodium chloride, 2.5kg of glycerin, 0.2kg of methyl paraben, 4kg of coconut diethanolamide (6501), 1.5kg of polyquaternium-7, 4kg of alkyl glycoside, 6kg of CAB, 1kg of sodium xylene sulfonate, 0.2kg of pearlescent diester, 15kg of AES, 15kg of soapberry extract, 0.14kg of guar gum and 0.2kg of hydroxyethyl cellulose, and then citric acid is added to adjust the pH to 6-7.
The preparation method of the soapberry emulsion type shampoo comprises the following steps:
(1) mixing distilled water, sodium chloride, glycerol, methyl hydroxybenzoate and citric acid to obtain product A;
(2) mixing coconut diethanolamide (6501), polyquaternium-7, alkyl glycoside, CAB, sodium xylene sulfonate and pearlescent diester uniformly to obtain product B;
(3) AES is product C;
(4) mixing fructus Sapindi Mukouossi extractive solution, guar gum and hydroxyethyl cellulose uniformly to obtain product D;
(5) adding product A into product D, and mixing to obtain product E;
(6) adding product B into product C at 70 deg.C, and mixing to obtain product F;
(7) adding the product E into the product F at 45 deg.C, mixing, adjusting pH to 6-7 with citric acid, stopping heating, stirring, cooling, and discharging to obtain the final product.
Example 2: a soapberry emulsion shampoo is prepared from 42kg of distilled water, 1kg of sodium chloride, 3kg of glycerin, 0.3kg of methyl paraben, 5kg of cocodiethanolamide (6501), 2kg of polyquaternium-7, 5kg of alkyl glycoside, 8kg of CAB, 2kg of sodium xylene sulfonate, 0.4kg of pearlescent diester, 18kg of AES, 25kg of soapberry extract, 0.18kg of guar gum and 0.3kg of hydroxyethyl cellulose, and then citric acid is added to adjust the pH to 6-7.
The preparation method of the soapberry emulsion type shampoo comprises the following steps:
(1) mixing distilled water, sodium chloride, glycerol, methyl hydroxybenzoate and citric acid to obtain product A;
(2) mixing coconut diethanolamide (6501), polyquaternium-7, alkyl glycoside, CAB, sodium xylene sulfonate and pearlescent diester uniformly to obtain product B;
(3) AES is product C;
(4) mixing fructus Sapindi Mukouossi extractive solution, guar gum and hydroxyethyl cellulose uniformly to obtain product D;
(5) adding product A into product D, and mixing to obtain product E;
(6) adding product B into product C at 75 deg.C, and mixing to obtain product F;
(7) adding the product E into the product F at 48 deg.C, mixing, adjusting pH to 6-7 with citric acid, stopping heating, stirring, cooling, and discharging to obtain the final product.
Example 3: a soapberry emulsion shampoo is prepared from 43kg of distilled water, 1.2kg of sodium chloride, 3.3kg of glycerin, 0.5kg of methyl paraben, 5.5kg of coconut diethanolamide (6501), 2.3kg of polyquaternium-7, 4.5kg of alkyl glycoside, 9kg of CAB, 2.5kg of sodium xylene sulfonate, 0.5kg of pearlescent diester, 20kg of AES, 28kg of soapberry extract, 0.19kg of guar gum and 0.35kg of hydroxyethyl cellulose, and then citric acid is added to adjust the pH to 6-7.
The preparation method of the soapberry emulsion type shampoo comprises the following steps:
(1) mixing distilled water, sodium chloride, glycerol, methyl hydroxybenzoate and citric acid to obtain product A;
(2) mixing coconut diethanolamide (6501), polyquaternium-7, alkyl glycoside, CAB, sodium xylene sulfonate and pearlescent diester uniformly to obtain product B;
(3) AES is product C;
(4) mixing fructus Sapindi Mukouossi extractive solution, guar gum and hydroxyethyl cellulose uniformly to obtain product D;
(5) adding product A into product D, and mixing to obtain product E;
(6) adding product B into product C at 80 deg.C, and mixing to obtain product F;
(7) adding the product E into the product F at 50 deg.C, mixing, adjusting pH to 6-7 with citric acid, stopping heating, stirring, cooling, and discharging to obtain the final product.
Example 4: a soapberry emulsion shampoo is prepared from 42.7kg of distilled water, 0.98kg of sodium chloride, 2.95kg of glycerin, 0.4kg of methyl paraben, 5.01kg of coconut diethanolamide (6501), 2kg of polyquaternium-7, 4.96kg of alkyl glycoside, 8kg of CAB, 2.01kg of sodium xylene sulfonate, 0.48kg of pearlescent diester, 18.59kg of AES, 20kg of soapberry extract, 0.18kg of guar gum and 0.32kg of hydroxyethyl cellulose, and then citric acid is added to adjust the pH to 6-7.
The preparation method of the soapberry emulsion type shampoo comprises the following steps:
(1) mixing distilled water, sodium chloride, glycerol, methyl hydroxybenzoate and citric acid to obtain product A;
(2) mixing coconut diethanolamide (6501), polyquaternium-7, alkyl glycoside, CAB, sodium xylene sulfonate and pearlescent diester uniformly to obtain product B;
(3) AES is product C;
(4) mixing fructus Sapindi Mukouossi extractive solution, guar gum and hydroxyethyl cellulose uniformly to obtain product D;
(5) adding product A into product D, and mixing to obtain product E;
(6) adding product B into product C at 75 deg.C, and mixing to obtain product F;
(7) adding the product E into the product F at 48 deg.C, mixing, adjusting pH to 6-7 with citric acid, stopping heating, stirring, cooling, and discharging to obtain the final product.
Example 5: a soapberry emulsion shampoo is prepared from 46kg of distilled water, 1.3kg of sodium chloride, 3.5kg of glycerin, 0.6kg of methyl paraben, 6kg of coconut diethanolamide (6501), 2.5kg of polyquaternium-7, 6kg of alkyl glycoside, 10kg of CAB, 3kg of sodium xylene sulfonate, 0.6kg of pearlescent diester, 23kg of AES, 30kg of soapberry extract, 0.22kg of guar gum and 0.4kg of hydroxyethyl cellulose, and then citric acid is added to adjust the pH to 6-7.
The preparation method of the soapberry emulsion type shampoo comprises the following steps:
(1) mixing distilled water, sodium chloride, glycerol, methyl hydroxybenzoate and citric acid to obtain product A;
(2) mixing coconut diethanolamide (6501), polyquaternium-7, alkyl glycoside, CAB, sodium xylene sulfonate and pearlescent diester uniformly to obtain product B;
(3) AES is product C;
(4) mixing fructus Sapindi Mukouossi extractive solution, guar gum and hydroxyethyl cellulose uniformly to obtain product D;
(5) adding product A into product D, and mixing to obtain product E;
(6) adding product B into product C at 80 deg.C, and mixing to obtain product F;
(7) adding the product E into the product F at 50 deg.C, mixing, adjusting pH to 6-7 with citric acid, stopping heating, stirring, cooling, and discharging to obtain the final product.
Claims (5)
1. A soapberry emulsion shampoo is characterized in that: the preservative is prepared from 40-46 parts by weight of distilled water, 0.7-1.3 parts by weight of sodium chloride, 2.5-3.5 parts by weight of glycerol, 0.2-0.6 part by weight of methyl paraben, 4-6 parts by weight of cocoanut diethanolamide, 1.5-2.5 parts by weight of polyquaternium-7, 4-6 parts by weight of alkyl glycoside, 6-10 parts by weight of CAB, 1-3 parts by weight of sodium xylene sulfonate, 0.2-0.6 part by weight of pearlescent diester, 15-23 parts by weight of AES, 15-30 parts by weight of soapberry extract, 0.14-0.22 part by weight of guar gum and 0.2-0.4 part by weight of hydroxyethyl cellulose, and then citric acid is added to adjust the pH to 6-7.
2. The soapberry emulsion type shampoo according to claim 1, characterized in that: the preservative is prepared from 42-44 parts by weight of distilled water, 0.8-1.2 parts by weight of sodium chloride, 2.7-3.3 parts by weight of glycerol, 0.3-0.5 part by weight of methyl paraben, 4.5-5.5 parts by weight of cocoanut diethanolamide, 1.7-2.3 parts by weight of polyquaternium-7, 4.5-5.5 parts by weight of alkyl glycoside, 7-9 parts by weight of CAB, 1.5-2.5 parts by weight of sodium xylene sulfonate, 0.3-0.5 part by weight of pearlescent diester, 17-21 parts by weight of AES, 18-25 parts by weight of soapberry extract, 0.16-0.2 part by weight of guar gum and 0.25-0.35 part by weight of hydroxyethyl cellulose, and then adding citric acid to adjust the pH to 6-7.
3. The soapberry emulsion type shampoo according to claim 2, characterized in that: the preservative is prepared from 42.7 parts by weight of distilled water, 0.98 part by weight of sodium chloride, 2.95 parts by weight of glycerol, 0.4 part by weight of methyl paraben, 5.01 parts by weight of coconut diethanolamide, 2 parts by weight of polyquaternium-7, 4.96 parts by weight of alkyl glycoside, 8 parts by weight of CAB, 2.01 parts by weight of sodium xylene sulfonate, 0.48 part by weight of pearlescent diester, 18.59 parts by weight of AES, 20 parts by weight of soapberry extract, 0.18 part by weight of guar gum and 0.32 part by weight of hydroxyethyl cellulose, and then citric acid is added to adjust the pH value to 6-7.
4. The method for preparing the soapberry emulsion type shampoo according to any one of claims 1 to 3, characterized in that: the method comprises the following steps:
(1) mixing distilled water, sodium chloride, glycerol, methyl hydroxybenzoate and citric acid to obtain product A;
(2) mixing coconut diethanolamide, polyquaternium-7, alkyl glycoside, CAB, sodium xylene sulfonate and pearlescent diester uniformly to obtain product B;
(3) AES is product C;
(4) mixing fructus Sapindi Mukouossi extractive solution, guar gum and hydroxyethyl cellulose uniformly to obtain product D;
(5) adding product A into product D, and mixing to obtain product E;
(6) adding product B into product C at 70-80 deg.C, and mixing to obtain product F;
(7) adding the product E into the product F at 45-50 deg.C, mixing, adjusting pH to 6-7 with citric acid, stopping heating, stirring, cooling, and discharging to obtain the final product.
5. The method for preparing the soapberry emulsion type shampoo according to claim 4, wherein the method comprises the following steps: in the step (6), the B product is added into the C product at the temperature of 75 ℃ and uniformly mixed.
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| CN104688634A (en) * | 2015-04-03 | 2015-06-10 | 泉州市奈斯材料科技有限公司 | Soapberry scurf-removing itching-relieving shampoo |
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