CN112300876A - Making process of peel essential oil soap - Google Patents
Making process of peel essential oil soap Download PDFInfo
- Publication number
- CN112300876A CN112300876A CN202011191541.9A CN202011191541A CN112300876A CN 112300876 A CN112300876 A CN 112300876A CN 202011191541 A CN202011191541 A CN 202011191541A CN 112300876 A CN112300876 A CN 112300876A
- Authority
- CN
- China
- Prior art keywords
- essential oil
- soap
- peel
- pericarp
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F5/00—Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
- C05F5/006—Waste from chemical processing of material, e.g. diestillation, roasting, cooking
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/10—Mixing; Kneading
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D13/00—Making of soap or soap solutions in general; Apparatus therefor
- C11D13/14—Shaping
- C11D13/16—Shaping in moulds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/20—Fertilizers of biological origin, e.g. guano or fertilizers made from animal corpses
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Botany (AREA)
- Environmental & Geological Engineering (AREA)
- Detergent Compositions (AREA)
Abstract
The invention relates to a process for preparing a peel essential oil soap, which comprises the steps of removing useless parts of peel, crushing, distilling and extracting at the temperature of 95-100 ℃ to obtain essential oil, uniformly cutting a soap base, melting in a water bath, mixing the essential oil and additives thereof, finally putting into a mold for condensation, and demolding to obtain the essential oil soap. The essential oil soap is simple in manufacturing process and capable of being industrially produced in batch, natural pollution is caused by the essential oil soap prepared by the method, soap liquid is not coked in the manufacturing process, essential oil components in peel can be effectively extracted, the extraction rate of the essential oil reaches 45-65%, and the extraction rate of the essential oil is high; in addition, the invention utilizes the waste pericarp, effectively improves the utilization rate of resources, reduces the waste of pericarp materials, and can directly use the pericarp dregs after being air-dried, thereby not polluting the air and the environment.
Description
Technical Field
The invention relates to the field of soap preparation, in particular to a process for preparing a peel essential oil soap.
Background
The kitchen waste is a domestic waste formed in the process of domestic consumption of residents, is extremely easy to rot and deteriorate, emits foul smell and spreads bacteria and viruses. The melon and fruit peel accounts for a large part of the kitchen waste. But kitchen waste is not always available. The national committee for improvement, the jurissin, the chief deputy, indicates that the kitchen waste has the characteristics of wastes and resources, and is a typical 'resource which is misplaced'. In particular various types of pericarp containing essential oils, such as: orange, lemon, grapefruit, etc. Essential oil soaps, soaps containing vegetable essential oils, known as essential oil soaps. The essential oil is a volatile aromatic substance extracted from flowers, leaves, stems, roots or fruits of plants by a steam distillation method, an extrusion method, a cold soaking method or a solvent extraction method, and consists of 250 molecules, and the essential oil has the functions of preventing infectious diseases, resisting bacteria, viruses and molds, preventing inflammation, preventing spasm, promoting cell metabolism and regenerating cells.
Disclosure of Invention
The invention provides a manufacturing process of a peel essential oil soap, which aims to solve the problems of waste and environmental pollution caused by the waste of the conventional peel.
The invention adopts the following technical scheme:
the manufacturing process of the peel essential oil soap comprises the following steps in sequence:
A. collecting pericarp (such as fresh lemon peel, fresh orange peel, fresh shaddock peel, and lemon food residue), cleaning pericarp, and removing the part of the inner surface of pericarp which does not contain essential oil;
B. crushing the peel by using a wall breaking machine, transferring the crushed peel into a distillation device, and distilling at the temperature of 95-100 ℃;
C. collecting the condensate volatilized by the peel and condensed on the distillation cover, standing and cooling for 25-45 min; after standing, sucking an essential oil layer on the upper layer in the condensate to obtain essential oil;
D. taking a soap base, cutting to obtain soap base particles with similar particle sizes, heating and melting the soap base particles in a water bath at 65-80 ℃ to obtain a soap solution, adding the essential oil prepared in the step C, and uniformly mixing, wherein the essential oil accounts for 2-5% of the weight of the soap solution;
E. and (3) putting the soap solution into a mold, standing at room temperature for 50-75 min, or refrigerating for 15-20 min, condensing and solidifying the soap solution, and demolding to obtain the essential oil soap.
In a further improvement, in the step D, the essential oil is added when the temperature of the soap solution is 60-63 ℃.
In a further improvement, in the step D, petals or/and strand-shaped or granular peel with the weight percentage of 4-7% of uniformly mixed soap liquid are also added into the soap liquid; the addition of the petals or/and the peel can improve the hardness of the essential oil soap after the soap liquid is condensed, so that the essential oil soap is not easily scratched when being demoulded.
In a further improvement, in the step D, a pigment which is uniformly mixed and accounts for 0.05-0.08% of the soap solution in weight percent is added into the soap solution for coloring.
In a further improvement, in the step E, a silica gel mold is used; the silicon gel mold is used, so that the demolding of the essential oil soap is easier, and the damage probability of the appearance of the essential oil soap is lower.
As can be seen from the above description of the present invention, compared with the prior art, the present invention has the following advantages: the essential oil soap is simple in manufacturing process and capable of being industrially produced in batch, natural pollution is caused by the essential oil soap prepared by the method, soap liquid is not coked in the manufacturing process, essential oil components in peel can be effectively extracted, the extraction rate of the essential oil reaches 0.1-1.0%, and the extraction rate of the essential oil is high; in addition, the invention utilizes the waste pericarp, effectively improves the utilization rate of resources, reduces the waste of pericarp materials, and can directly use the pericarp dregs after being air-dried, thereby not polluting the air and the environment.
Detailed Description
Implementation mode one
The manufacturing process of the peel essential oil soap comprises the following steps in sequence:
A. collecting pericarp (such as fresh lemon peel, fresh orange peel, fresh shaddock peel, and lemon food residue), cleaning pericarp, and removing the part of the inner surface of pericarp which does not contain essential oil;
B. crushing the peel by using a wall breaking machine, transferring the crushed peel into a distillation device, and distilling at the temperature of 95-100 ℃;
C. collecting the condensate volatilized by the peel and condensed on the distillation cover, standing and cooling for 25-45 min; after standing, sucking an essential oil layer on the upper layer in the condensate to obtain essential oil;
D. taking soap base, cutting to obtain soap base particles with similar particle sizes, improving the melting speed of the soap base particles and melting more uniformly, and heating and melting by using a water bath at 65-75 ℃ to obtain soap liquid; the purpose of water bath heating is to prevent the soap base from being burnt, if the soap base is directly heated, the fire needs to be adjusted to be very small, the burning is prevented at any time, when the soap base is heated, only a small fire needs to be used, the water temperature does not need to be too high, if the water begins to bubble or even boils, the water temperature is indicated to be too high, and the fire needs to be adjusted to be small or temporarily closed quickly; adding the essential oil prepared in the step C when the temperature of the soap solution is reduced to 60-63 ℃ so as to avoid waste caused by rapid volatilization of the essential oil due to too high temperature; uniformly mixing, wherein the essential oil accounts for 2-5% of the weight of the soap liquid;
the soap base is transparent soap base, and the preparation method of the transparent soap base comprises the following steps:
(1) mixing water, grease and alkali liquor at about 55 ℃ to obtain a melanized mixture;
(2) adding glycerol, and heating with medium fire;
(3) heating until the soap base is gelatinized, stopping heating, and adding alcohol;
(4) continuously heating with medium fire, and mixing continuously;
(5) adding the granulated sugar water mixed solution after 10 minutes;
(6) heating with middle fire again, adding essential oil or other materials after the soap base is formed into syrup;
(7) pouring into a mold;
(8) and (5) ventilating and drying for 2-3 weeks.
Preparing the essential oil soap:
a. the cold preparation method comprises the following steps: slowly pouring water into a big cup filled with sodium hydroxide, slowly stirring to be uniform, stirring to dissipate heat to enable the temperature of the sodium hydroxide solution in the cup to rise, weighing the grease and heating to about 70 ℃, mixing an oil phase and an alkali liquor when the temperature of the oil phase and the alkali liquor are about 70 ℃, slowly pouring the alkali liquor into the grease, continuously stirring for 30-40 minutes at a high stirring speed, adding the essential oil prepared in the step C, continuously stirring until the oil phase and the alkali liquor become thick, covering a preservative film, and placing for at least more than one month.
b. A cooked preparation method comprises the following steps: and D, boiling the essential oil soap liquid prepared in the step D on a furnace to accelerate the reaction speed of the soap, so that the essential oil soap can be used immediately after being saponified for hours.
c. Melting and re-preparing method: the soap base is prepared by melting the ready-made soap base and adding color and taste, most of the soap base is transparent soap, and through a comparison test, the soap base can be used as the soap base as follows: transparent glycerin soap base, white glycerin soap base, coconut oil soap base. The saponification time of the essential oil soap prepared by the method is 1 hour, and the essential oil soap can be used immediately.
d. The soap is prepared by adding water or milk to melt after the existing soap is sliced, and the saponification time of the method is several weeks.
Experimental data sheet (average value of 5 groups of experiments with coconut oil)
| Method of producing a composite material | Cold production method | Cooking method | Melting and recycling method | Regeneration process |
| Time of manufacture | 3.2 hours | 2.4 hours | 1 hour | 0.5 hour |
| Time of saponification | 840 hours | 0.6 hour | 0.01 hour | 72. Hour(s) |
E. Putting the soap solution into a mold, and using a silica gel mold, wherein the mold must be cleaned and dried in advance; the silicon gel mold is used, so that the demolding of the essential oil soap is easier, and the damage probability of the appearance of the essential oil soap is lower; standing at room temperature for 50-75 min, or refrigerating for 15-20 min, condensing and solidifying the soap liquid, and demolding to obtain the essential oil soap.
The essential oil soap prepared by the embodiment has natural pollution, does not generate soap liquid coking in the preparation process, can effectively extract essential oil components in peel, and has the advantages that the extraction rate of the essential oil reaches 45-65%, and the extraction rate of the essential oil is high; in addition, the embodiment utilizes the waste pericarp, effectively improves the utilization rate of resources, reduces the waste of pericarp materials, and can be directly used as fertilizer after the pericarp broken slag treated by the embodiment is air-dried, thereby not polluting the air and the environment.
Second embodiment
The manufacturing process of the peel essential oil soap comprises the following steps in sequence:
A. collecting pericarp (such as fresh lemon peel, fresh orange peel, fresh shaddock peel, and lemon food residue), cleaning pericarp, and removing the part of the inner surface of pericarp which does not contain essential oil;
B. crushing the peel by using a wall breaking machine, transferring the crushed peel into a distillation device, and distilling at the temperature of 95-100 ℃;
C. collecting the condensate volatilized by the peel and condensed on the distillation cover, standing and cooling for 25-45 min; after standing, sucking an essential oil layer on the upper layer in the condensate to obtain essential oil;
D. taking a soap base, cutting to obtain soap base particles with similar particle sizes, improving the melting speed of the soap base particles and melting more uniformly, and heating and melting by using a water bath at 73-80 ℃ to obtain a soap solution; the purpose of water bath heating is to prevent the soap base from being burnt, if the soap base is directly heated, the fire needs to be adjusted to be very small, the burning is prevented at any time, when the soap base is heated, only a small fire needs to be used, the water temperature does not need to be too high, if the water begins to bubble or even boils, the water temperature is indicated to be too high, and the fire needs to be adjusted to be small or temporarily closed quickly; c, when the temperature of the soap liquid is reduced to 60-63 ℃, adding the essential oil prepared in the step C, and uniformly mixing, wherein the essential oil accounts for 2-5% of the weight of the soap liquid; adding petals or/and strand-shaped or granular peel with the weight percentage of 4-7% and pigment with the weight percentage of 0.05-0.08% into the soap solution for coloring, wherein the petals or/and the strand-shaped or granular peel are uniformly mixed with the soap solution; the addition of the petals or/and the peel can improve the hardness of the essential oil soap after the soap liquid is condensed, so that the essential oil soap is not easily scratched when being demoulded;
E. putting the soap solution into a mold, and using a silica gel mold, wherein the mold must be cleaned and dried in advance; the silicon gel mold is used, so that the demolding of the essential oil soap is easier, and the damage probability of the appearance of the essential oil soap is lower; standing at room temperature for 50-75 min, or refrigerating for 15-20 min, condensing and solidifying the soap liquid, and demolding to obtain the essential oil soap.
The essential oil soap prepared by the embodiment has natural pollution, does not generate soap liquid coking in the preparation process, can effectively extract essential oil components in peel, and has the advantages that the extraction rate of the essential oil reaches 45-65%, and the extraction rate of the essential oil is high; in addition, the embodiment utilizes the waste pericarp, effectively improves the utilization rate of resources, reduces the waste of pericarp materials, and can be directly used as fertilizer after the pericarp broken slag treated by the embodiment is air-dried, thereby not polluting the air and the environment.
The above description is only an embodiment of the present invention, but the design concept of the present invention is not limited thereto, and any insubstantial modifications made by using the design concept should fall within the scope of infringing the present invention.
Claims (5)
1. The manufacturing process of the peel essential oil soap is characterized by comprising the following steps in sequence:
A. collecting pericarp, cleaning pericarp, and removing the part of the inner surface of pericarp which does not contain essential oil;
B. crushing the peel by using a wall breaking machine, transferring the crushed peel into a distillation device, and distilling at the temperature of 95-100 ℃;
C. collecting the condensate volatilized by the peel and condensed on the distillation cover, standing and cooling for 25-45 min; after standing, sucking an essential oil layer on the upper layer in the condensate to obtain essential oil;
D. taking a soap base, cutting to obtain soap base particles with similar particle sizes, heating and melting the soap base particles in a water bath at 65-80 ℃ to obtain a soap solution, adding the essential oil prepared in the step C, and uniformly mixing, wherein the essential oil accounts for 2-5% of the weight of the soap solution;
E. and (3) putting the soap solution into a mold, standing at room temperature for 50-75 min, or refrigerating for 15-20 min, condensing and solidifying the soap solution, and demolding to obtain the essential oil soap.
2. The process for making the peel essential oil soap of claim 1, wherein: and D, adding the essential oil when the temperature of the soap solution is 60-63 ℃.
3. The process for making the peel essential oil soap of claim 1, wherein: and D, adding petals or/and strand-shaped or granular peel, which are 4-7% of the soap liquid in weight percentage and are uniformly mixed, into the soap liquid.
4. The process for making the peel essential oil soap of claim 1, wherein: and D, adding a pigment with the weight percentage of 0.05-0.08% into the soap liquid, wherein the pigment is uniformly mixed with the soap liquid.
5. The process for making the peel essential oil soap of claim 1, wherein: in step E, a silicone mold was used.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011191541.9A CN112300876A (en) | 2020-10-30 | 2020-10-30 | Making process of peel essential oil soap |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011191541.9A CN112300876A (en) | 2020-10-30 | 2020-10-30 | Making process of peel essential oil soap |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN112300876A true CN112300876A (en) | 2021-02-02 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011191541.9A Pending CN112300876A (en) | 2020-10-30 | 2020-10-30 | Making process of peel essential oil soap |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101050404A (en) * | 2007-05-16 | 2007-10-10 | 徐海波 | Soap with fragrant of ginseng flower for protecting skin, and fabricating technique |
| CN104031773A (en) * | 2014-06-04 | 2014-09-10 | 韩城市司马迁旅游文化发展有限公司 | Method for preparing pepper volatile oil fragrant skin care soap |
| CN106350229A (en) * | 2016-10-31 | 2017-01-25 | 劳炳凤 | Method for extracting lemon essential oil from fruit peels |
| CN106893651A (en) * | 2017-03-07 | 2017-06-27 | 钟浪雅 | One kind removal cock skin skin fancy soap formula and its compounding method |
| CN108277114A (en) * | 2018-03-30 | 2018-07-13 | 福建生物工程职业技术学院 | A kind of production method of the handmade soap containing tangerine oil |
| CN111196954A (en) * | 2018-11-18 | 2020-05-26 | 南京艾蒙利特生物科技有限公司 | Preparation method of glycerin soap with citrus fragrance |
-
2020
- 2020-10-30 CN CN202011191541.9A patent/CN112300876A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101050404A (en) * | 2007-05-16 | 2007-10-10 | 徐海波 | Soap with fragrant of ginseng flower for protecting skin, and fabricating technique |
| CN104031773A (en) * | 2014-06-04 | 2014-09-10 | 韩城市司马迁旅游文化发展有限公司 | Method for preparing pepper volatile oil fragrant skin care soap |
| CN106350229A (en) * | 2016-10-31 | 2017-01-25 | 劳炳凤 | Method for extracting lemon essential oil from fruit peels |
| CN106893651A (en) * | 2017-03-07 | 2017-06-27 | 钟浪雅 | One kind removal cock skin skin fancy soap formula and its compounding method |
| CN108277114A (en) * | 2018-03-30 | 2018-07-13 | 福建生物工程职业技术学院 | A kind of production method of the handmade soap containing tangerine oil |
| CN111196954A (en) * | 2018-11-18 | 2020-05-26 | 南京艾蒙利特生物科技有限公司 | Preparation method of glycerin soap with citrus fragrance |
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Application publication date: 20210202 |