CN107384633A - A kind of preparation method of the skin repair soap of the collagen containing sashimi - Google Patents
A kind of preparation method of the skin repair soap of the collagen containing sashimi Download PDFInfo
- Publication number
- CN107384633A CN107384633A CN201710568456.1A CN201710568456A CN107384633A CN 107384633 A CN107384633 A CN 107384633A CN 201710568456 A CN201710568456 A CN 201710568456A CN 107384633 A CN107384633 A CN 107384633A
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- CN
- China
- Prior art keywords
- sashimi
- collagen
- soap
- oil
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K38/00—Medicinal preparations containing peptides
- A61K38/01—Hydrolysed proteins; Derivatives thereof
- A61K38/012—Hydrolysed proteins; Derivatives thereof from animals
- A61K38/014—Hydrolysed proteins; Derivatives thereof from animals from connective tissue peptides, e.g. gelatin, collagen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/48—Medical, disinfecting agents, disinfecting, antibacterial, germicidal or antimicrobial compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/225—Polymers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Veterinary Medicine (AREA)
- Medicinal Chemistry (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Pharmacology & Pharmacy (AREA)
- Immunology (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Zoology (AREA)
- Biomedical Technology (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
A kind of preparation method of the skin repair soap of the collagen containing sashimi, including sashimi collagen is prepared, soap is prepared using animal fat 50g, vegetable fat 72g, NaOH10g, water 32g, sashimi collagen 5g, essential oil 1g.The soap addition sashimi collagen of the present invention, sashimi collagen is as a kind of natural polymeric biomaterial, with relatively low immunogenicity, excellent biocompatibility and biological degradability, bootable regeneration, promote the characteristics such as the growth of cell propagation and anastalsis.Using plant and animal grease, without syntheticses such as paraffin, stearic agent, injury will not be produced to skin, and it is more degradable, pollution will not be produced to environment.
Description
Technical field
The present invention relates to soap preparing technical field, and in particular to a kind of skin repair soap of collagen containing sashimi
Preparation method.
Background technology
The making of general soap is mainly formed by grease, strong base substance and water through saponification, and add using paraffin,
The syntheticses such as stearic agent are to increase the hardness of soap, and these syntheticses can cause some skin problems, and due to
The degradability of synthetics is poor, also easily causes the pollution to environment.Meanwhile the pH value of the soap produced is too high, if
For cleaning skin and inappropriate, or even disease of skin can be produced due to too strong alkalescence, be not suitable for skin wound person and use.
The content of the invention
According to problems of the prior art, the invention provides one kind suitable various skins, especially surface of a wound skin
The preparation method of the skin repair soap for the collagen containing sashimi that patient uses.
The present invention uses following technical scheme：
A kind of preparation method of the skin repair soap of collagen containing sashimi, comprises the following steps：
Step 1：Dry stichopus japonicus 50g is weighed, 60 DEG C of water are sent out two days, water are changed daily 3 times, 40 DEG C in 500mL absolute ethyl alcohols
Lower continuous extraction two days, changes 1 ethanol, is most dried after under normal temperature daily；
Step 2：Take the stichopus japonicus after drying superoxide dismutase act on enzyme digestion reaction 4h, superoxide dismutase with
Substrate mass ratio is 1:6th, pH6.5, temperature 45 C, after the completion of reaction, 5min enzyme deactivations are boiled, and are rapidly cooled to room temperature,
2000r/min centrifugal treating 30min, supernatant is taken to add 200mL absolute ethyl alcohol precipitates overnights, then 3000r/min centrifugal treatings
30min, 40 DEG C of rotary evaporation 1h of supernatant are taken, obtain sashimi collagen；
Step 3：Weigh animal fat 50g, vegetable fat 72g, NaOH10g, water 32g, sashimi collagen 5g, essential oil
1g；
Step 4：NaOH is slowly dissolved in the water and stirred, the NaOH aqueous solution is made；
Step 5：Animal fat, vegetable fat, sashimi collagen, essential oil are well mixed, and be heated in a water bath
After 50 DEG C, in the NaOH aqueous solution is poured slowly under conditions of being stirred continuously, keeping temperature is 50 DEG C, stirring reaction 4h；
Step 6：When reactant mixture changes into ivory-white stringy liquid, natural cooling in mould is poured into, is placed
At shady and cool ventilation, soap can be stripped into after 2-3 weeks.
Preferably, described animal fat is the one or more in lard, sheep oil, butter.
Preferably, the one or more in described vegetable fat coconut oil, palm oil, olive oil, castor oil.
The beneficial effects of the present invention are：
1) sashimi collagen is added, sashimi collagen has relatively low as a kind of natural polymeric biomaterial
Immunogenicity, excellent biocompatibility and biological degradability, bootable regeneration, promote cell propagation growth and hemostasis
The characteristics such as effect.
2) plant and animal grease is used, without syntheticses such as paraffin, stearic agent, injury will not be produced to skin,
And it is more degradable, pollution will not be produced to environment.
Embodiment
With reference to embodiment, the present invention will be further described.
Embodiment 1
A kind of preparation method of the skin repair soap of collagen containing sashimi, comprises the following steps：
Step 1：Dry stichopus japonicus 50g is weighed, 60 DEG C of water are sent out two days, water are changed daily 3 times, 40 DEG C in 500mL absolute ethyl alcohols
Lower continuous extraction two days, changes 1 ethanol, is most dried after under normal temperature daily；
Step 2：Take the stichopus japonicus after drying superoxide dismutase act on enzyme digestion reaction 4h, superoxide dismutase with
Substrate mass ratio is 1:6th, pH6.5, temperature 45 C, after the completion of reaction, 5min enzyme deactivations are boiled, and are rapidly cooled to room temperature,
2000r/min centrifugal treating 30min, supernatant is taken to add 200mL absolute ethyl alcohol precipitates overnights, then 3000r/min centrifugal treatings
30min, 40 DEG C of rotary evaporation 1h of supernatant are taken, obtain sashimi collagen；
Step 3：Weigh animal fat 50g, vegetable fat 72g, NaOH10g, water 32g, sashimi collagen 5g, essential oil
1g；
Step 4：NaOH is slowly dissolved in the water and stirred, the NaOH aqueous solution is made；
Step 5：Animal fat, vegetable fat, sashimi collagen, essential oil are well mixed, and be heated in a water bath
After 50 DEG C, in the NaOH aqueous solution is poured slowly under conditions of being stirred continuously, keeping temperature is 50 DEG C, stirring reaction 4h；
Step 6：When reactant mixture changes into ivory-white stringy liquid, natural cooling in mould is poured into, is placed
At shady and cool ventilation, soap can be stripped into after 2-3 weeks.
Described animal fat is the one or more in lard, sheep oil, butter.
One or more in described vegetable fat coconut oil, palm oil, olive oil, castor oil.
By soap made from the embodiment of the present invention 1 and skin effect (the equal area surface of a wound of same type soap on the market
Recovery extent) comparing result see the table below 1.
Table 1
| Project | Skin effect |
| Embodiment 1 | Well |
| Same type soap | To no effect |
Claims (3)
1. the preparation method of the skin repair soap of a kind of collagen containing sashimi, it is characterised in that comprise the following steps：
Step 1：Dry stichopus japonicus 50g is weighed, 60 DEG C of water are sent out two days, change water daily 3 times, connect at 40 DEG C in 500mL absolute ethyl alcohols
Continuous extraction two days, changes 1 ethanol, is most dried after under normal temperature daily；
Step 2：The stichopus japonicus after drying is taken to act on enzyme digestion reaction 4h, superoxide dismutase and substrate in superoxide dismutase
Mass ratio is 1:6th, pH6.5, temperature 45 C, after the completion of reaction, 5min enzyme deactivations are boiled, and is rapidly cooled to room temperature, 2000r/min
Centrifugal treating 30min, take supernatant to add 200mL absolute ethyl alcohol precipitates overnights, then 3000r/min centrifugal treating 30min, take supernatant
40 DEG C of rotary evaporation 1h of liquid, obtain sashimi collagen；
Step 3：Weigh animal fat 50g, vegetable fat 72g, NaOH10g, water 32g, sashimi collagen 5g, essential oil 1g；
Step 4：NaOH is slowly dissolved in the water and stirred, the NaOH aqueous solution is made；
Step 5：Animal fat, vegetable fat, sashimi collagen, essential oil are well mixed, and are heated to 50 DEG C in a water bath
Afterwards, in the NaOH aqueous solution is poured slowly under conditions of being stirred continuously, keeping temperature is 50 DEG C, stirring reaction 4h；
Step 6：When reactant mixture changes into ivory-white stringy liquid, natural cooling in mould is poured into, is placed shady and cool
Ventilation, soap can be stripped into after 2-3 weeks.
2. a kind of preparation method of the skin repair soap of collagen containing sashimi according to claim 1, its feature exist
In：Described animal fat is the one or more in lard, sheep oil, butter.
3. a kind of preparation method of the skin repair soap of collagen containing sashimi according to claim 1, its feature exist
In：One or more in described vegetable fat coconut oil, palm oil, olive oil, castor oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710568456.1A CN107384633A (en) | 2017-07-13 | 2017-07-13 | A kind of preparation method of the skin repair soap of the collagen containing sashimi |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710568456.1A CN107384633A (en) | 2017-07-13 | 2017-07-13 | A kind of preparation method of the skin repair soap of the collagen containing sashimi |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107384633A true CN107384633A (en) | 2017-11-24 |
Family
ID=60340538
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710568456.1A Withdrawn CN107384633A (en) | 2017-07-13 | 2017-07-13 | A kind of preparation method of the skin repair soap of the collagen containing sashimi |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107384633A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108998302A (en) * | 2018-08-02 | 2018-12-14 | 辽宁中医药大学 | A kind of Elsholtzia cilita essential oil antibacterial soap and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101343653A (en) * | 2008-08-22 | 2009-01-14 | 中国海洋大学 | Preparation method for holothurian collagen active peptide and application thereof |
| CN102512351A (en) * | 2011-12-30 | 2012-06-27 | 曲少男 | Sea cucumber extract used for skin care cosmetics and processing method |
| CN103045408A (en) * | 2013-01-15 | 2013-04-17 | 刘晓伟 | Method for preparing body cleaning soap with gardenia fragrance |
| CN106265413A (en) * | 2016-08-09 | 2017-01-04 | 谭攸恒 | A kind of Stichopus japonicus boiling liquid and goods application in cosmetics, articles for washing and article of everyday use thereof |
-
2017
- 2017-07-13 CN CN201710568456.1A patent/CN107384633A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101343653A (en) * | 2008-08-22 | 2009-01-14 | 中国海洋大学 | Preparation method for holothurian collagen active peptide and application thereof |
| CN102512351A (en) * | 2011-12-30 | 2012-06-27 | 曲少男 | Sea cucumber extract used for skin care cosmetics and processing method |
| CN103045408A (en) * | 2013-01-15 | 2013-04-17 | 刘晓伟 | Method for preparing body cleaning soap with gardenia fragrance |
| CN106265413A (en) * | 2016-08-09 | 2017-01-04 | 谭攸恒 | A kind of Stichopus japonicus boiling liquid and goods application in cosmetics, articles for washing and article of everyday use thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108998302A (en) * | 2018-08-02 | 2018-12-14 | 辽宁中医药大学 | A kind of Elsholtzia cilita essential oil antibacterial soap and preparation method thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20171124 |