CN106350229A - Method for extracting lemon essential oil from fruit peels - Google Patents
Method for extracting lemon essential oil from fruit peels Download PDFInfo
- Publication number
- CN106350229A CN106350229A CN201610967612.7A CN201610967612A CN106350229A CN 106350229 A CN106350229 A CN 106350229A CN 201610967612 A CN201610967612 A CN 201610967612A CN 106350229 A CN106350229 A CN 106350229A
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- CN
- China
- Prior art keywords
- lemon
- fructus citri
- citri limoniae
- fresh
- peels
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a method for extracting lemon essential oil from fruit peels. The method is characterized by comprising the following steps: 1, preparing required raw materials including fresh lemon peels, fresh orange peels, fresh grapefruit peels and lemon food residues; 2, preparing making machines including a pounding machine, a squeezer, a centrifugal machine and a distillation tower; 3, pounding the fresh lemon peels, the fresh orange peels and the fresh grapefruit peels into pieces by using the pounding machine at first, and then squeezing the peels twice by using the low-temperature squeezer to obtain lemon residues and lemon squeezed liquid, wherein the squeezing temperature is 1-10 DEG C; 4, putting the squeezed liquid into the centrifugal machine to perform centrifugal clarification, and then performing filtration to obtain primary lemon liquid; 5, putting the lemon residues obtained by squeezing and lemon residues generated during food processing into the distillation tower to perform steam distillation so as to obtain primary lemon essential oil; and 6, mixing the prepared primary lemon liquid and the primary lemon essential oil together, performing extraction by using dichloromethane as an extracting agent, and boiling off the dichloromethane to obtain the lemon essential oil.
Description
Technical field
The present invention relates to the method extracting Fructus Citri Limoniae quintessence oil from Fericarpium Citri Limoniae, belong to industrial technical field.
Background technology
The pure and fresh fragrance of Fructus Citri Limoniae, can help spirit of refreshing oneself, and alleviate irritated, lemon essence quintessence oil, also have for skin and body
Much positive opsonic actions.It is rich in abundant vitamin c in Limon pulp, but Fructus Citri Limoniae quintessence oil does not have vitamin, Fructus Citri Limoniae quintessence oil
In limonene be particularly useful for whitening, convergence, Bergamot Mint Extract, the treatment oily skin symptom such as comedo.Aromatic odor:
Weak yellow liquid, the fragrance of citruss is salubrious and fresh.Match quintessence oil therewith: Benzoinum, Fructus Amomi Rotunduss, eucalyptus globoluss, Olibanum, India
Certain herbaceous plants with big flowers, jasmine, gin, Garden lavender, Lignum Santali Albi, red Citrus chachiensis Hort., Cananga odorata, Flos Matricariae chamomillae, coriander.
Fructus Citri Limoniae quintessence oil abnormal smells from the patient is strong, pure and fresh, chlorine, water quality viscosity.If being used for aromatotherapy, Fructus Citri Limoniae quintessence oil
Shelf-life is only 8 ~ 10 months, but after having spent the shelf-life, still can be used for aroma-therapeutic, such as vaporizastion.Volatility: fast.
Main component: limonene, citral, (Niu Biao) gemic acid, citronella oil, lauro lene.Lemon originates in India, and this is a kind of evergreen
Plant, can grow to 6m height, blade blackish green, avette, boundary zone sawtooth, pattern pink colour or white, aromatic flavor.Tree belt pierces,
Ripening of fruits, by green flavescence.
The English word " lemon " of Fructus Citri Limoniae, from Arabic " laimun " or Persian human speech " limun ", this tree
It is that Europe is brought in medieval times by Crusader.Its fruit contains abundant vitamin a, b, c, in Royal Navy
In, drink 1 ounce of Fructus Citri Limoniae juice for each person every day, to prevent vitamin C deficiency and other avitaminosis.
Fructus Citri Limoniae quintessence oil can improve circulatory function, including blood circulation promoting, to reduce blood pressure, only nose bleeding.It is permissible
Strengthen immune system, purify body, improve digestive system function, the group of reducing fat, treatment dyspepsia and constipation.
Fructus Citri Limoniae quintessence oil has the effect consoling and alleviating headache and migraine, by the acidic materials in general physical, right
Treatment of arthritis and rheumatism are also helpful.Additionally aid cleaning acne, cleaning Greasy Skin and hair, and it is thin to remove dead bark
Born of the same parents.
Instill several Fructus Citri Limoniae quintessence oil in the hot water of foot bath, the purpose that can reach promoting blood circulation meridians is moreover it is possible to reach removal foot
The effect of gas foot odor.
Fructus Citri Limoniae oil can remove old dead cell, the bright colour of skin, consolidation blood capillary, promotes collagen protein to produce, desalinates melanin,
There is purification to greasy skin of sending out, causes scar tissue can be softened；Improve oily skin, have clean skin, convergence, Sage Extract to divide
Secrete, the effect of skin whitening；For removing clavuss, verruca plana and general wart all very effectively it is also possible to soften causes scar tissue, prevention
Fingernail trouble is split.The gentle whitening of skin care, prevents wrinkle from producing, increases skin gloss, desalinate freckle, helps oily skin to reduce
Sebum secretion, except clavuss, wart tumor etc..
Fructus Citri Limoniae oil is the excellent tonic of blood circulation, makes unblocked blood flowing, mitigates the pressure at varicosis position；Can recover
Erythrocytic vigor.Fructus Citri Limoniae oil can mitigate the phenomenon of anemia, stimulate leukocyte simultaneously, helps the communicable disease of body resistance
Disease；The function of facilitating digestion system.Stimulate leukocyte, all kinds of knife injury or wound are all suitable for, hemostasis, help wound healing, adjust
Along whole digestive system, there is certain curative effect to gastropathy, gastric ulcer etc..Conditioning blood circulation, is particularly suitable for treating varicosis, right
Hypertension is also suitable, and preventing cold, brings down a fever, and slows down skin aging, helps digest, and bursts in mosquito-proof insect stingss, various focusing depths represented, oral cavity
Infectionss.
The effect of Fructus Citri Limoniae quintessence oil；The effect of Fructus Citri Limoniae quintessence oil is very many, especially anti-corruption, and antibacterial and deodouring aspect is optimal, so
A lot of people's Fructus Citri Limoniae quintessence oil are called super depurator.Fructus Citri Limoniae, except also can purifying human body with environment purification, even more nourishes lymphatic system
The good medicine of system, it can help want that the people losing weight exclude unnecessary body fluid, promote circulation, prevent and improve varicosis,
Body metabolism fat can be helped, be the fat-reducing indispensable good friend of personage.
The processing of Fructus Citri Limoniae is mainly used in Food ＆ Drink, and food processing Fructus Citri Limoniae only takes its internal juice, and its skin is worked as mostly
Rubbish discards.But the Fructus Citri Limoniae quintessence oil that contains in Fericarpium Citri Limoniae is most.
Content of the invention
Fructus Citri Limoniae quintessence oil in order to extract one stream meets the requirement of society, causes also for overcoming normal food processing Fructus Citri Limoniae
The waste of Fericarpium Citri Limoniae, a kind of method extracting Fructus Citri Limoniae quintessence oil from Fericarpium Citri Limoniae of my invention, this method be suitable in food plus
The Fericarpium Citri Limoniae producing in the flow process of work carries out instant processing and produces Fructus Citri Limoniae quintessence oil.
A kind of method solve problem extracting Fructus Citri Limoniae quintessence oil from peel is adopted the technical scheme that by below step
Carry out: one, raw material used: lemon skin, fresh Pericarpium citri sinensiss, fresh pomelo peel, Fructus Citri Limoniae food slag；2nd, production machinery: bruisher,
Squeezer, centrifuge, distillation column；3rd, first lemon skin, fresh Pericarpium citri sinensiss, fresh Fructus Citri grandiss are smashed to pieces with bruisher, then by each skin
Squeeze to obtain lemon dregs and Fructus Citri Limoniae pressed liquor through low temperature pressing machine twice, pressing temperature: 1 DEG C ~ 10 DEG C；4th, pressed liquor is put into
Centrifuge is filtrated to get primary lemon fluid after carrying out centrifugal clarification；5th, by the above-mentioned lemon dregs squeezing and food processing process
The lemon dregs of middle generation are put distillation column into and are carried out steam distillation and obtain primary Fructus Citri Limoniae quintessence oil；6th, by above-mentioned prepared primary Fructus Citri Limoniae
Liquid and primary Fructus Citri Limoniae oil dichloromethane admixed together are extracted as extractant, obtain lemon extract after steaming vibrating dichloromethane
Oil.
A kind of beneficial effect of the method extracting Fructus Citri Limoniae quintessence oil from peel is: a kind of extraction Fructus Citri Limoniae quintessence oil from peel
Method can be squeezed the slag charge after extracting juice and be made using the Fericarpium Citri Limoniae producing in food processing process, Pericarpium citri sinensiss, pomelo peel and food
It is processed extracting Fructus Citri Limoniae quintessence oil for raw material, by smashing to pieces, squeeze twice, be centrifuged the primary lemon fluid of acquisition, then passing through the way of distillation
Obtain primary Fructus Citri Limoniae quintessence oil from food slag, carry out extraction by the use of dichloromethane as extractant and obtain Fructus Citri Limoniae quintessence oil, overcome one
As food processing Fructus Citri Limoniae cause the waste of Fericarpium Citri Limoniae, the Fructus Citri Limoniae quintessence oil of high-quality is provided for fields such as medical treatment, health cares.
Specific embodiment
Embodiment: a kind of method solve problem extracting Fructus Citri Limoniae quintessence oil from peel is adopted the technical scheme that by following
Step carry out: one, raw material used: lemon skin, fresh Pericarpium citri sinensiss, fresh pomelo peel, Fructus Citri Limoniae food slag；2nd, production machinery: smash
Broken machine, squeezer, centrifuge, distillation column；3rd, first lemon skin, fresh Pericarpium citri sinensiss, fresh Fructus Citri grandiss are smashed to pieces with bruisher, then
Each skin is squeezed to obtain lemon dregs and Fructus Citri Limoniae pressed liquor twice through low temperature pressing machine, pressing temperature: 1 DEG C ~ 10 DEG C；4th, will squeeze
Liquid is put into after centrifuge carries out centrifugal clarification and is filtrated to get primary lemon fluid；5th, the above-mentioned lemon dregs squeezing and food are added
The lemon dregs producing during work are put distillation column into and are carried out steam distillation and obtain primary Fructus Citri Limoniae quintessence oil；6th, by above-mentioned prepared just
Level lemon fluid and primary Fructus Citri Limoniae oil dichloromethane admixed together are extracted as extractant, obtain after steaming vibrating dichloromethane
Fructus Citri Limoniae quintessence oil.
Claims (1)
1. a kind of method extracting Fructus Citri Limoniae quintessence oil from peel, is characterized in that carrying out by below step: one, raw material used:
Lemon skin, fresh Pericarpium citri sinensiss, fresh pomelo peel, Fructus Citri Limoniae food slag；2nd, production machinery: bruisher, squeezer, centrifuge, distillation
Tower；3rd, first lemon skin, fresh Pericarpium citri sinensiss, fresh Fructus Citri grandiss are smashed to pieces with bruisher, then by each skin through low temperature pressing machine twice
Squeeze to obtain lemon dregs and Fructus Citri Limoniae pressed liquor, pressing temperature: 1 DEG C ~ 10 DEG C；4th, pressed liquor is put into centrifuge and carry out centrifugal clarification
After be filtrated to get primary lemon fluid；5th, the lemon dregs producing in the above-mentioned lemon dregs squeezing and food processing process are put into
Distillation column carries out steam distillation and obtains primary Fructus Citri Limoniae quintessence oil；6th, by above-mentioned prepared primary lemon fluid and primary Fructus Citri Limoniae oil mixing
Reinstate dichloromethane to one to be extracted as extractant, after steaming vibrating dichloromethane, obtain Fructus Citri Limoniae quintessence oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610967612.7A CN106350229A (en) | 2016-10-31 | 2016-10-31 | Method for extracting lemon essential oil from fruit peels |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610967612.7A CN106350229A (en) | 2016-10-31 | 2016-10-31 | Method for extracting lemon essential oil from fruit peels |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106350229A true CN106350229A (en) | 2017-01-25 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201610967612.7A Withdrawn CN106350229A (en) | 2016-10-31 | 2016-10-31 | Method for extracting lemon essential oil from fruit peels |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108440266A (en) * | 2018-04-12 | 2018-08-24 | 江苏耐雀生物工程技术有限公司 | A method of preparing citral from the grey seed in mountain |
| CN112006946A (en) * | 2020-09-28 | 2020-12-01 | 宁波捷通机械有限公司 | Preparation process of skin care product lemon essential oil |
| CN112300876A (en) * | 2020-10-30 | 2021-02-02 | 石狮市明德培训学校 | Making process of peel essential oil soap |
| CN112315852A (en) * | 2020-11-03 | 2021-02-05 | 宁波鼎科新材料科技有限公司 | Preparation method of cosmetic plant extraction additive |
| CN112940837A (en) * | 2021-03-23 | 2021-06-11 | 康洛信(广东)生物科技有限公司 | Method for extracting finger lemon essential oil |
| CN113332179A (en) * | 2021-05-11 | 2021-09-03 | 广州明创生物科技有限公司 | Antibacterial essential oil for skin |
| CN115029186A (en) * | 2022-06-08 | 2022-09-09 | 深圳市复绿生物环保科技有限公司 | Volatile organic compound remover, preparation method and removing equipment |
| CN115444135A (en) * | 2022-06-07 | 2022-12-09 | 木由子(上海)生物科技有限公司 | Shaddock peel extraction process and shaddock peel extract |
| CN115486529A (en) * | 2022-06-30 | 2022-12-20 | 广西桂腰食品有限公司 | Preparation method of flavored cashew nuts based on lemon extract |
Citations (3)
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| CN103897806A (en) * | 2014-04-03 | 2014-07-02 | 广东添乐化妆品有限公司 | Microwave assisted extraction method of lemon essential oil |
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Patent Citations (3)
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| CN103897806A (en) * | 2014-04-03 | 2014-07-02 | 广东添乐化妆品有限公司 | Microwave assisted extraction method of lemon essential oil |
| CN104815100A (en) * | 2015-05-15 | 2015-08-05 | 成都市康飞药业有限公司 | Composition with effects of refreshing and restoring consciousness and application thereof |
| CN105748321A (en) * | 2016-02-25 | 2016-07-13 | 刘忠波 | Mosquito-proof itching relieving liquid and preparation method thereof |
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| X76610: "从橙皮中提取柠檬精油", 《豆丁网》 * |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108440266A (en) * | 2018-04-12 | 2018-08-24 | 江苏耐雀生物工程技术有限公司 | A method of preparing citral from the grey seed in mountain |
| CN112006946A (en) * | 2020-09-28 | 2020-12-01 | 宁波捷通机械有限公司 | Preparation process of skin care product lemon essential oil |
| CN112300876A (en) * | 2020-10-30 | 2021-02-02 | 石狮市明德培训学校 | Making process of peel essential oil soap |
| CN112315852A (en) * | 2020-11-03 | 2021-02-05 | 宁波鼎科新材料科技有限公司 | Preparation method of cosmetic plant extraction additive |
| CN112940837A (en) * | 2021-03-23 | 2021-06-11 | 康洛信(广东)生物科技有限公司 | Method for extracting finger lemon essential oil |
| CN113332179A (en) * | 2021-05-11 | 2021-09-03 | 广州明创生物科技有限公司 | Antibacterial essential oil for skin |
| CN115444135A (en) * | 2022-06-07 | 2022-12-09 | 木由子(上海)生物科技有限公司 | Shaddock peel extraction process and shaddock peel extract |
| CN115029186A (en) * | 2022-06-08 | 2022-09-09 | 深圳市复绿生物环保科技有限公司 | Volatile organic compound remover, preparation method and removing equipment |
| CN115029186B (en) * | 2022-06-08 | 2023-12-22 | 深圳市复绿生物环保科技有限公司 | Volatile organic compound remover, preparation method and removing equipment |
| CN115486529A (en) * | 2022-06-30 | 2022-12-20 | 广西桂腰食品有限公司 | Preparation method of flavored cashew nuts based on lemon extract |
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| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20170125 |