CN112245313A - Moisturizing and repairing composition and preparation method thereof - Google Patents
Moisturizing and repairing composition and preparation method thereof Download PDFInfo
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- CN112245313A CN112245313A CN202011117748.1A CN202011117748A CN112245313A CN 112245313 A CN112245313 A CN 112245313A CN 202011117748 A CN202011117748 A CN 202011117748A CN 112245313 A CN112245313 A CN 112245313A
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- 230000003020 moisturizing effect Effects 0.000 title claims abstract description 52
- 239000000203 mixture Substances 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title claims abstract description 35
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims abstract description 101
- 229940038481 bee pollen Drugs 0.000 claims abstract description 57
- 241000246358 Thymus Species 0.000 claims abstract description 48
- 235000007303 Thymus vulgaris Nutrition 0.000 claims abstract description 48
- 239000001585 thymus vulgaris Substances 0.000 claims abstract description 48
- 239000004408 titanium dioxide Substances 0.000 claims abstract description 47
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 46
- 241001166194 Geranium wilfordii Species 0.000 claims abstract description 41
- 230000002745 absorbent Effects 0.000 claims abstract description 30
- 239000002250 absorbent Substances 0.000 claims abstract description 30
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 29
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 claims abstract description 28
- 229920002674 hyaluronan Polymers 0.000 claims abstract description 28
- 229960003160 hyaluronic acid Drugs 0.000 claims abstract description 28
- 239000004519 grease Substances 0.000 claims abstract description 27
- 229920002385 Sodium hyaluronate Polymers 0.000 claims abstract description 25
- 229940010747 sodium hyaluronate Drugs 0.000 claims abstract description 25
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims abstract description 25
- 108010020346 Polyglutamic Acid Proteins 0.000 claims abstract description 22
- 229920002643 polyglutamic acid Polymers 0.000 claims abstract description 22
- 239000008367 deionised water Substances 0.000 claims abstract description 21
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 21
- 239000000230 xanthan gum Substances 0.000 claims abstract description 21
- 229920001285 xanthan gum Polymers 0.000 claims abstract description 21
- 229940082509 xanthan gum Drugs 0.000 claims abstract description 21
- 235000010493 xanthan gum Nutrition 0.000 claims abstract description 21
- DXGLGDHPHMLXJC-UHFFFAOYSA-N oxybenzone Chemical compound OC1=CC(OC)=CC=C1C(=O)C1=CC=CC=C1 DXGLGDHPHMLXJC-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229960001173 oxybenzone Drugs 0.000 claims abstract description 17
- 239000002994 raw material Substances 0.000 claims abstract description 11
- 239000011259 mixed solution Substances 0.000 claims description 74
- 239000000243 solution Substances 0.000 claims description 63
- 239000000047 product Substances 0.000 claims description 43
- 238000003756 stirring Methods 0.000 claims description 42
- 238000002156 mixing Methods 0.000 claims description 31
- 238000005485 electric heating Methods 0.000 claims description 28
- 239000000706 filtrate Substances 0.000 claims description 24
- 238000001914 filtration Methods 0.000 claims description 24
- 238000010298 pulverizing process Methods 0.000 claims description 24
- 238000009210 therapy by ultrasound Methods 0.000 claims description 24
- 239000007788 liquid Substances 0.000 claims description 17
- VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 claims description 16
- 229940075529 glyceryl stearate Drugs 0.000 claims description 16
- 229950008882 polysorbate Drugs 0.000 claims description 16
- 229920000136 polysorbate Polymers 0.000 claims description 16
- 238000010992 reflux Methods 0.000 claims description 16
- 238000000605 extraction Methods 0.000 claims description 15
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims description 15
- 239000002245 particle Substances 0.000 claims description 9
- 229960005196 titanium dioxide Drugs 0.000 claims description 7
- CMDKPGRTAQVGFQ-UHFFFAOYSA-N 2-ethoxyethyl 3-(4-methoxyphenyl)prop-2-enoate Chemical compound CCOCCOC(=O)C=CC1=CC=C(OC)C=C1 CMDKPGRTAQVGFQ-UHFFFAOYSA-N 0.000 claims description 4
- 238000000034 method Methods 0.000 claims 3
- 230000035876 healing Effects 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 7
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 230000008929 regeneration Effects 0.000 abstract description 2
- 238000011069 regeneration method Methods 0.000 abstract description 2
- 230000002195 synergetic effect Effects 0.000 abstract description 2
- OSJVRHJQUTTZIN-UHFFFAOYSA-N 2-ethoxyethyl 2-methoxy-3-phenylprop-2-enoate Chemical compound CCOCCOC(=O)C(OC)=CC1=CC=CC=C1 OSJVRHJQUTTZIN-UHFFFAOYSA-N 0.000 abstract 1
- 210000003491 skin Anatomy 0.000 description 24
- -1 dimethyl siloxane Chemical class 0.000 description 12
- 241000208152 Geranium Species 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 7
- 239000004615 ingredient Substances 0.000 description 6
- AFDXODALSZRGIH-UHFFFAOYSA-N p-coumaric acid methyl ether Natural products COC1=CC=C(C=CC(O)=O)C=C1 AFDXODALSZRGIH-UHFFFAOYSA-N 0.000 description 5
- 239000002537 cosmetic Substances 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 3
- 230000018109 developmental process Effects 0.000 description 3
- 238000010998 test method Methods 0.000 description 3
- 102000008186 Collagen Human genes 0.000 description 2
- 108010035532 Collagen Proteins 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 230000003712 anti-aging effect Effects 0.000 description 2
- 229920001436 collagen Polymers 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 238000011895 specific detection Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- YBGZDTIWKVFICR-JLHYYAGUSA-N Octyl 4-methoxycinnamic acid Chemical compound CCCCC(CC)COC(=O)\C=C\C1=CC=C(OC)C=C1 YBGZDTIWKVFICR-JLHYYAGUSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 239000013522 chelant Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 230000002500 effect on skin Effects 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- DHNGCHLFKUPGPX-RMKNXTFCSA-N ethyl trans-p-methoxycinnamate Chemical compound CCOC(=O)\C=C\C1=CC=C(OC)C=C1 DHNGCHLFKUPGPX-RMKNXTFCSA-N 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 238000000338 in vitro Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 210000002510 keratinocyte Anatomy 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 125000004433 nitrogen atom Chemical group N* 0.000 description 1
- 229960001679 octinoxate Drugs 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 125000004430 oxygen atom Chemical group O* 0.000 description 1
- 238000007539 photo-oxidation reaction Methods 0.000 description 1
- 230000035755 proliferation Effects 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 230000009759 skin aging Effects 0.000 description 1
- 230000008591 skin barrier function Effects 0.000 description 1
- 125000001424 substituent group Chemical group 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 235000013619 trace mineral Nutrition 0.000 description 1
- 239000011573 trace mineral Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/88—Polyamides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a moisturizing repair composition and a preparation method thereof in the technical field of moisturizing repair, wherein the moisturizing repair composition comprises the following raw materials in parts by weight: 12-15 parts of grease, 3-4 parts of thyme extracting solution, 5-7 parts of geranium wilfordii extracting solution, 3-4 parts of bee pollen extracting solution, 10-12 parts of emulsifier, 2-3 parts of absorbent, 2-3 parts of hyaluronic acid, 3-4 parts of sodium hyaluronate, 5-8 parts of titanium dioxide, 1-2 parts of polyglutamic acid, 1-3 parts of xanthan gum and 50-60 parts of deionized water; the ultraviolet-proof moisturizing repair composition is added with the absorbent and the titanium dioxide, so that the ultraviolet-proof performance of the moisturizing repair composition is improved, the titanium dioxide in the moisturizing repair composition mainly reflects and scatters ultraviolet rays, the ethoxyethyl methoxycinnamate and the oxybenzone mainly absorb ultraviolet rays which cannot be reflected and scattered and convert the ultraviolet rays into heat energy to be released, the hyaluronic acid and the sodium hyaluronate mainly promote the repair and regeneration of skin, and the three components have synergistic effect, so that the ultraviolet-proof moisturizing repair composition is beneficial to improving the ultraviolet-proof effect.
Description
Technical Field
The invention relates to the technical field of moisturizing repair, in particular to a moisturizing repair composition and a preparation method thereof.
Background
According to the regulations on the management of cosmetic identification published by the national quality inspection administration of 27.8.2007, cosmetics refer to chemical industry products or fine chemical products which are applied, sprayed or the like to any part of the surface of a human body, such as skin, hair, nails, lips and teeth, to achieve the purposes of cleaning, maintaining, beautifying, modifying and changing the appearance, or correcting the odor of the human body and maintaining a good state, and the development of modern cosmetics can be divided into two times.
The age of natural ingredients, starting from the 80 s of the last century, skin experts found: various natural raw materials are added into the skin care product, so that the skin care product has a certain moistening effect on the skin. This time the large scale natural extraction and separation industry has matured and since then natural ingredients that are slowly found in skin care compositions on the market! From land to sea, and from plants to animals, various natural ingredients should be present. Some people even go to places where people are rarely seen, try to find special raw materials and create peculiar skin care traces, including tropical rainforests, and some companies can completely abandon the original industrial production line, produce purely natural things and slowly form some top-grade very-focused brands. In the zero-load era, before 2010, zero-load products begin to be popular in taiwan in europe and america, plants are excessively pursued in the past, natural skin care products are increasingly provided with various additives due to social development and the requirement of meeting more people on special skin, and therefore, a plurality of skin care products are natural and actually not natural. The natural ingredients are used, and the mineral ingredients are more in ingredients, so that unnecessary damage and even allergy are caused to the skin, and the alarm clock is sounded to the skin care industry, and zero pursuit of burden is about to become the most substantial change in the current skin care development history. After 2010, zero-load products are produced, a batch of zero-load products mainly reduce unnecessary chemical components and increase pure skin care components, and bring brand-new innovation to women who use frequent cosmetics, and the zero-load products are mainly characterized in that a plurality of useless components are drastically reduced, skin care components such as hyaluronic acid and collagen are used actively and are directly absorbed by skin, the product performance is extremely mild, and even fragile skin is used properly and generally has no problem, so that the skin can be made up to the maximum extent without damage.
At present, most of moisturizing repair emulsions achieve water locking, moisturizing and repairing by adding hyaluronic acid and grease, but the repairing effect is relatively common, and in addition, the effect of shielding ultraviolet rays only through hyaluronic acid is relatively common.
Moisturizing repair compositions have therefore been proposed to solve the above problems.
Disclosure of Invention
The invention aims to provide a moisturizing repair composition and a preparation method thereof, so as to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following scheme to realize the following steps: the moisturizing and repairing composition comprises the following raw materials in parts by weight: 12-15 parts of grease, 3-4 parts of thyme extracting solution, 5-7 parts of geranium wilfordii extracting solution, 3-4 parts of bee pollen extracting solution, 10-12 parts of emulsifying agent, 2-3 parts of absorbent, 2-3 parts of hyaluronic acid, 3-4 parts of sodium hyaluronate, 5-8 parts of titanium dioxide, 1-2 parts of polyglutamic acid, 1-3 parts of xanthan gum and 50-60 parts of deionized water.
Preferably, the oil and fat comprises 13-15 parts of oil and fat, 3.2-3.8 parts of thyme extract, 5.5-6.5 parts of geranium wilfordii extract, 3.4-3.6 parts of bee pollen extract, 11-12 parts of emulsifier, 2-2.8 parts of absorbent, 2.5-3 parts of hyaluronic acid, 3.5-4 parts of sodium hyaluronate, 6-8 parts of titanium dioxide, 1-1.8 parts of polyglutamic acid, 1-2 parts of xanthan gum and 52-58 parts of deionized water.
Preferably, the oil and fat comprises 14 parts of oil and fat, 3.5 parts of thyme extracting solution, 6 parts of geranium wilfordii extracting solution, 3.5 parts of bee pollen extracting solution, 12 parts of emulsifying agent, 2.5 parts of absorbent, 2.8 parts of hyaluronic acid, 3.7 parts of sodium hyaluronate, 7 parts of titanium dioxide, 1.5 parts of polyglutamic acid, 1.5 parts of xanthan gum and 55 parts of deionized water.
Preferably, the preparation method of the thyme extracting solution comprises the following steps: pulverizing thyme, mixing with water according to the material-liquid ratio of 1:20, performing ultrasonic treatment to obtain thyme mixed solution, extracting the thyme mixed solution under reflux for 2 times, and filtering to obtain filtrate, namely a target product; the preparation method of the geranium wilfordii extractive solution comprises the following steps: pulverizing the fine geranium wilfordii, adding water according to the material-liquid ratio of 3:20, mixing, performing ultrasonic treatment to obtain a fine geranium wilfordii mixed solution, performing reflux extraction on the fine geranium wilfordii mixed solution for 2 times, and filtering to obtain a filtrate, namely a target product; the preparation method of the bee pollen extracting solution comprises the following steps: pulverizing bee pollen, mixing with water at a ratio of 1:15, performing ultrasonic treatment to obtain bee pollen mixed solution, reflux-extracting the bee pollen mixed solution for 3 times, and filtering to obtain filtrate as target product.
Preferably, the grease comprises pentaerythritol tetraester, hydrogenated polydecene and cyclopentadimethylsiloxane which are mixed according to a mass ratio of 1:1: 1.
Preferably, the emulsifier comprises polysorbate and glyceryl stearate, and the polysorbate and the glyceryl stearate are mixed in a mass ratio of 2: 1.
Preferably, the absorbent comprises ethoxyethyl p-methoxycinnamate and oxybenzone, and the ethoxyethyl p-methoxycinnamate and the oxybenzone are mixed according to the mass ratio of 1: 2.
Preferably, the titanium dioxide is rutile type titanium dioxide, and the particle size of the titanium dioxide is 40-50 nm.
The invention also provides a preparation method of the moisturizing and repairing composition, which comprises the following steps:
(1) the grease and the emulsifier are put into a first electric heating stirrer to be stirred for 15-20min at the rotating speed of 1200-1500r/min, and the stirring temperature is kept at 60-70 ℃ to obtain a mixed solution A;
(2) placing the absorbent, hyaluronic acid, sodium hyaluronate, titanium dioxide, polyglutamic acid and deionized water into a second electric heating stirrer, stirring for 20-25min at the rotating speed of 1500-1800r/min, and keeping the stirring temperature at 50-60 ℃ to obtain a mixed solution B;
(3) adding the mixed solution A into a second electric-heating stirrer, mixing with the mixed solution B, adding herba Thymi extract, herba Erodii seu Geranii extract, bee pollen extract and xanthan gum into the second electric-heating stirrer, and stirring for 40-50min to obtain the target product.
Preferably, the stirring speed in the step (3) is 2500-.
The invention has the beneficial effects that:
according to the invention, the thyme extracting solution, the geranium tenue extracting solution and the bee pollen extracting solution are added, wherein the geranium tenue plays a role in deep skin to repair the substrate, so that the elasticity of the skin is favorably restored, and the skin is firmer; the thyme extract can eliminate free radicals, and has antiaging effect; the bee pollen extracting solution contains various trace elements and also has the anti-aging effect, and the thyme extracting solution and the bee pollen extracting solution act together to further delay the skin aging;
the invention adds absorbent and titanium dioxide, improve the anti-ultraviolet performance of the moisturizing repair composition, firstly, the added titanium dioxide with the particle size of 40-50nm has small particle size and high activity, can reflect and scatter ultraviolet rays and absorb ultraviolet rays, thereby having stronger blocking capability to the ultraviolet rays, secondly, the added ethyoxyl ethyl methoxycinnamate and oxybenzone have ortho-hydroxyphenyl substituent groups, after being irradiated by the ultraviolet rays, hydrogen bonds are destroyed, and chelate rings formed by the ortho-hydroxyl and nitrogen atoms or oxygen atoms are opened, thereby changing the ultraviolet rays which can not be successfully blocked by the titanium dioxide into heat energy to be released, further shielding the ultraviolet rays, furthermore, hyaluronic acid and sodium hyaluronate can promote the proliferation of cells, and can clear oxygen free radicals, prevent the photo-oxidation reaction from proceeding, and protect the skin; the titanium dioxide in the moisturizing repair composition mainly reflects and scatters ultraviolet rays, the ethyoxyl methoxycinnamate and the oxybenzone mainly absorb ultraviolet rays which cannot be reflected and scattered and convert the ultraviolet rays into heat energy to be released, the hyaluronic acid and the sodium hyaluronate mainly promote the repair and regeneration of skin, and the three components have synergistic effect with each other, so that the ultraviolet shielding effect is improved;
according to the invention, by adding thyme extract, geranium tenuifolia extract, bee pollen extract, hyaluronic acid, sodium hyaluronate and polyglutamic acid, the water-locking and moisturizing effect is improved, and the repairing effect on skin is also improved.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1
The moisturizing and repairing composition comprises the following raw materials in parts by weight: 12 parts of grease, 3 parts of thyme extracting solution, 5 parts of geranium wilfordii extracting solution, 3 parts of bee pollen extracting solution, 10 parts of emulsifier, 2 parts of absorbent, 2 parts of hyaluronic acid, 3 parts of sodium hyaluronate, 5 parts of titanium dioxide, 1 part of polyglutamic acid, 1 part of xanthan gum and 50 parts of deionized water.
The preparation method of the thyme extracting solution comprises the following steps: pulverizing thyme, adding water according to the material-liquid ratio of 1:20, mixing, performing ultrasonic treatment to obtain thyme mixed solution, performing reflux extraction for 2 times, and filtering to obtain filtrate, namely a target product; the preparation method of the geranium wilfordii extractive solution comprises the following steps: pulverizing the fine geranium wilfordii, adding water according to the material-liquid ratio of 3:20, mixing, performing ultrasonic treatment to obtain a fine geranium wilfordii mixed solution, performing reflux extraction on the fine geranium wilfordii mixed solution for 2 times, and filtering to obtain a filtrate, namely a target product; the preparation method of the bee pollen extracting solution comprises the following steps: pulverizing bee pollen, mixing with water at a ratio of 1:15, performing ultrasonic treatment to obtain bee pollen mixed solution, reflux-extracting the bee pollen mixed solution for 3 times, and filtering to obtain filtrate as target product.
The grease comprises pentaerythritol tetraester, hydrogenated polydecene and cyclopenta dimethyl siloxane, wherein the pentaerythritol tetraester, the hydrogenated polydecene and the cyclopenta dimethyl siloxane are mixed according to the mass ratio of 1:1: 1; the emulsifier comprises polysorbate and glyceryl stearate, and the polysorbate and the glyceryl stearate are mixed according to the mass ratio of 2: 1; the absorbent comprises p-methoxycinnamic acid ethoxy ethyl ester and oxybenzone, and the methoxy cinnamic acid ethoxy ethyl ester and the oxybenzone are mixed according to the mass ratio of 1: 2; the titanium dioxide is rutile type titanium dioxide, and the particle size of the titanium dioxide is 40-50 nm.
The preparation method of the moisturizing and repairing composition specifically comprises the following steps:
(1) putting the grease and the emulsifier into a first electric stirrer, stirring for 15min at the rotating speed of 1200r/min, and keeping the stirring temperature at 60 ℃ to obtain a mixed solution A;
(2) placing the absorbent, hyaluronic acid, sodium hyaluronate, titanium dioxide, polyglutamic acid and deionized water into a second electric heating stirrer, stirring for 20min at a rotating speed of 1500r/min, and keeping the stirring temperature at 50 ℃ to obtain a mixed solution B;
(3) adding the mixed solution A into a second electric heating stirrer, mixing with the mixed solution B, adding thyme extract, Geranium tenuifolium extract, bee pollen extract and xanthan gum into the second electric heating stirrer, stirring at 2500r/min, and stirring for 40min to obtain the target product.
Example 2
The moisturizing and repairing composition comprises the following raw materials in parts by weight: 13 parts of grease, 3.2 parts of thyme extracting solution, 5.5 parts of fine geranium extracting solution, 3.4 parts of bee pollen extracting solution, 11 parts of emulsifier, 2 parts of absorbent, 2.5 parts of hyaluronic acid, 3.5 parts of sodium hyaluronate, 6 parts of titanium dioxide, 1 part of polyglutamic acid, 1 part of xanthan gum and 53 parts of deionized water.
The preparation method of the thyme extracting solution comprises the following steps: pulverizing thyme, adding water according to the material-liquid ratio of 1:20, mixing, performing ultrasonic treatment to obtain thyme mixed solution, performing reflux extraction for 2 times, and filtering to obtain filtrate, namely a target product; the preparation method of the geranium wilfordii extractive solution comprises the following steps: pulverizing the fine geranium wilfordii, adding water according to the material-liquid ratio of 3:20, mixing, performing ultrasonic treatment to obtain a fine geranium wilfordii mixed solution, performing reflux extraction on the fine geranium wilfordii mixed solution for 2 times, and filtering to obtain a filtrate, namely a target product; the preparation method of the bee pollen extracting solution comprises the following steps: pulverizing bee pollen, mixing with water at a ratio of 1:15, performing ultrasonic treatment to obtain bee pollen mixed solution, reflux-extracting the bee pollen mixed solution for 3 times, and filtering to obtain filtrate as target product.
The grease comprises pentaerythritol tetraester, hydrogenated polydecene and cyclopenta dimethyl siloxane, wherein the pentaerythritol tetraester, the hydrogenated polydecene and the cyclopenta dimethyl siloxane are mixed according to the mass ratio of 1:1: 1; the emulsifier comprises polysorbate and glyceryl stearate, and the polysorbate and the glyceryl stearate are mixed according to the mass ratio of 2: 1; the absorbent comprises p-methoxycinnamic acid ethoxy ethyl ester and oxybenzone, and the methoxy cinnamic acid ethoxy ethyl ester and the oxybenzone are mixed according to the mass ratio of 1: 2; the titanium dioxide is rutile type titanium dioxide, and the particle size of the titanium dioxide is 40-50 nm.
The preparation method of the moisturizing and repairing composition specifically comprises the following steps:
(1) placing the grease and the emulsifier into a first electric stirrer, stirring for 16min at the rotating speed of 1300r/min, and keeping the stirring temperature at 65 ℃ to obtain a mixed solution A;
(2) placing the absorbent, hyaluronic acid, sodium hyaluronate, titanium dioxide, polyglutamic acid and deionized water into a second electric heating stirrer, stirring for 22min at a rotating speed of 1600r/min, and keeping the stirring temperature at 55 ℃ to obtain a mixed solution B;
(3) adding the mixed solution A into a second electric heating stirrer to be mixed with the mixed solution B, continuously adding thyme extract, geranium tenuifolium extract, bee pollen extract and xanthan gum into the second electric heating stirrer, stirring at 2700r/min, and stirring for 45min to obtain the target product.
Example 3
The moisturizing and repairing composition comprises the following raw materials in parts by weight: 14 parts of grease, 3.5 parts of thyme extracting solution, 6 parts of fine geranium extracting solution, 3.5 parts of bee pollen extracting solution, 12 parts of emulsifying agent, 2.5 parts of absorbent, 2.8 parts of hyaluronic acid, 3.7 parts of sodium hyaluronate, 7 parts of titanium dioxide, 1.5 parts of polyglutamic acid, 1.5 parts of xanthan gum and 55 parts of deionized water.
The preparation method of the thyme extracting solution comprises the following steps: pulverizing thyme, adding water according to the material-liquid ratio of 1:20, mixing, performing ultrasonic treatment to obtain thyme mixed solution, performing reflux extraction for 2 times, and filtering to obtain filtrate, namely a target product; the preparation method of the geranium wilfordii extractive solution comprises the following steps: pulverizing the fine geranium wilfordii, adding water according to the material-liquid ratio of 3:20, mixing, performing ultrasonic treatment to obtain a fine geranium wilfordii mixed solution, performing reflux extraction on the fine geranium wilfordii mixed solution for 2 times, and filtering to obtain a filtrate, namely a target product; the preparation method of the bee pollen extracting solution comprises the following steps: pulverizing bee pollen, mixing with water at a ratio of 1:15, performing ultrasonic treatment to obtain bee pollen mixed solution, reflux-extracting the bee pollen mixed solution for 3 times, and filtering to obtain filtrate as target product.
The grease comprises pentaerythritol tetraester, hydrogenated polydecene and cyclopenta dimethyl siloxane, wherein the pentaerythritol tetraester, the hydrogenated polydecene and the cyclopenta dimethyl siloxane are mixed according to the mass ratio of 1:1: 1; the emulsifier comprises polysorbate and glyceryl stearate, and the polysorbate and the glyceryl stearate are mixed according to the mass ratio of 2: 1; the absorbent comprises p-methoxycinnamic acid ethoxy ethyl ester and oxybenzone, and the methoxy cinnamic acid ethoxy ethyl ester and the oxybenzone are mixed according to the mass ratio of 1: 2; the titanium dioxide is rutile type titanium dioxide, and the particle size of the titanium dioxide is 40-50 nm.
The preparation method of the moisturizing and repairing composition specifically comprises the following steps:
(1) putting the grease and the emulsifier into a first electric heating stirrer, stirring for 18min at the rotating speed of 1400r/min, and keeping the stirring temperature at 65 ℃ to obtain a mixed solution A;
(2) placing the absorbent, hyaluronic acid, sodium hyaluronate, titanium dioxide, polyglutamic acid and deionized water into a second electric heating stirrer, stirring for 22min at a rotating speed of 1600r/min, and keeping the stirring temperature at 55 ℃ to obtain a mixed solution B;
(3) adding the mixed solution A into a second electric heating stirrer, mixing with the mixed solution B, adding thyme extractive solution, herba Erodii seu Geranii extractive solution, bee pollen extractive solution and xanthan gum into the second electric heating stirrer at 2900r/min, and stirring for 45min to obtain the target product.
Example 4
The moisturizing and repairing composition comprises the following raw materials in parts by weight: 14 parts of grease, 3.8 parts of thyme extracting solution, 6.5 parts of fine geranium extracting solution, 3.6 parts of bee pollen extracting solution, 12 parts of emulsifying agent, 2.5 parts of absorbent, 3 parts of hyaluronic acid, 4 parts of sodium hyaluronate, 7 parts of titanium dioxide, 1.5 parts of polyglutamic acid, 1.5 parts of xanthan gum and 58 parts of deionized water.
The preparation method of the thyme extracting solution comprises the following steps: pulverizing thyme, adding water according to the material-liquid ratio of 1:20, mixing, performing ultrasonic treatment to obtain thyme mixed solution, performing reflux extraction for 2 times, and filtering to obtain filtrate, namely a target product; the preparation method of the geranium wilfordii extractive solution comprises the following steps: pulverizing the fine geranium wilfordii, adding water according to the material-liquid ratio of 3:20, mixing, performing ultrasonic treatment to obtain a fine geranium wilfordii mixed solution, performing reflux extraction on the fine geranium wilfordii mixed solution for 2 times, and filtering to obtain a filtrate, namely a target product; the preparation method of the bee pollen extracting solution comprises the following steps: pulverizing bee pollen, mixing with water at a ratio of 1:15, performing ultrasonic treatment to obtain bee pollen mixed solution, reflux-extracting the bee pollen mixed solution for 3 times, and filtering to obtain filtrate as target product.
The grease comprises pentaerythritol tetraester, hydrogenated polydecene and cyclopenta dimethyl siloxane, wherein the pentaerythritol tetraester, the hydrogenated polydecene and the cyclopenta dimethyl siloxane are mixed according to the mass ratio of 1:1: 1; the emulsifier comprises polysorbate and glyceryl stearate, and the polysorbate and the glyceryl stearate are mixed according to the mass ratio of 2: 1; the absorbent comprises p-methoxycinnamic acid ethoxy ethyl ester and oxybenzone, and the methoxy cinnamic acid ethoxy ethyl ester and the oxybenzone are mixed according to the mass ratio of 1: 2; the titanium dioxide is rutile type titanium dioxide, and the particle size of the titanium dioxide is 40-50 nm.
The preparation method of the moisturizing and repairing composition specifically comprises the following steps:
(1) putting the grease and the emulsifier into a first electric stirrer, stirring for 18min at a rotating speed of 1500r/min, and keeping the stirring temperature at 68 ℃ to obtain a mixed solution A;
(2) placing the absorbent, hyaluronic acid, sodium hyaluronate, titanium dioxide, polyglutamic acid and deionized water into a second electric heating stirrer, stirring for 22min at a rotating speed of 1700r/min, and keeping the stirring temperature at 57 ℃ to obtain a mixed solution B;
(3) adding the mixed solution A into a second electric heating stirrer, mixing with the mixed solution B, adding thyme extract, Geranium tenuifolium extract, bee pollen extract and xanthan gum into the second electric heating stirrer at 3100r/min, and stirring for 48min to obtain the target product.
Example 5
The moisturizing and repairing composition comprises the following raw materials in parts by weight: 15 parts of grease, 4 parts of thyme extracting solution, 7 parts of geranium wilfordii extracting solution, 4 parts of bee pollen extracting solution, 12 parts of emulsifier, 3 parts of absorbent, 3 parts of hyaluronic acid, 4 parts of sodium hyaluronate, 8 parts of titanium dioxide, 2 parts of polyglutamic acid, 3 parts of xanthan gum and 60 parts of deionized water.
The preparation method of the thyme extracting solution comprises the following steps: pulverizing thyme, adding water according to the material-liquid ratio of 1:20, mixing, performing ultrasonic treatment to obtain thyme mixed solution, performing reflux extraction for 2 times, and filtering to obtain filtrate, namely a target product; the preparation method of the geranium wilfordii extractive solution comprises the following steps: pulverizing the fine geranium wilfordii, adding water according to the material-liquid ratio of 3:20, mixing, performing ultrasonic treatment to obtain a fine geranium wilfordii mixed solution, performing reflux extraction on the fine geranium wilfordii mixed solution for 2 times, and filtering to obtain a filtrate, namely a target product; the preparation method of the bee pollen extracting solution comprises the following steps: pulverizing bee pollen, mixing with water at a ratio of 1:15, performing ultrasonic treatment to obtain bee pollen mixed solution, reflux-extracting the bee pollen mixed solution for 3 times, and filtering to obtain filtrate as target product.
The grease comprises pentaerythritol tetraester, hydrogenated polydecene and cyclopenta dimethyl siloxane, wherein the pentaerythritol tetraester, the hydrogenated polydecene and the cyclopenta dimethyl siloxane are mixed according to the mass ratio of 1:1: 1; the emulsifier comprises polysorbate and glyceryl stearate, and the polysorbate and the glyceryl stearate are mixed according to the mass ratio of 2: 1; the absorbent comprises p-methoxycinnamic acid ethoxy ethyl ester and oxybenzone, and the methoxy cinnamic acid ethoxy ethyl ester and the oxybenzone are mixed according to the mass ratio of 1: 2; the titanium dioxide is rutile type titanium dioxide, and the particle size of the titanium dioxide is 40-50 nm.
The preparation method of the moisturizing and repairing composition specifically comprises the following steps:
(1) putting the grease and the emulsifier into a first electric stirrer, stirring for 18min at a rotating speed of 1500r/min, and keeping the stirring temperature at 70 ℃ to obtain a mixed solution A;
(2) placing the absorbent, hyaluronic acid, sodium hyaluronate, titanium dioxide, polyglutamic acid and deionized water into a second electric heating stirrer, stirring for 25min at the rotating speed of 1800r/min, and keeping the stirring temperature at 60 ℃ to obtain a mixed solution B;
(3) adding the mixed solution A into a second electric heating stirrer, mixing with the mixed solution B, adding herba Thymi extract, herba Erodii seu Geranii extract, bee pollen extract and xanthan gum into the second electric heating stirrer at 3500r/min, and stirring for 50min to obtain the target product.
Comparative example
The moisturizing and repairing composition comprises the following raw materials in parts by weight: 14 parts of grease, 3.5 parts of thyme extracting solution, 6 parts of fine geranium extracting solution, 3.5 parts of bee pollen extracting solution, 12 parts of emulsifying agent, 2.8 parts of hyaluronic acid, 3.7 parts of sodium hyaluronate, 1.5 parts of polyglutamic acid, 1.5 parts of xanthan gum and 55 parts of deionized water.
The preparation method of the thyme extracting solution comprises the following steps: pulverizing thyme, adding water according to the material-liquid ratio of 1:20, mixing, performing ultrasonic treatment to obtain thyme mixed solution, performing reflux extraction for 2 times, and filtering to obtain filtrate, namely a target product; the preparation method of the geranium wilfordii extractive solution comprises the following steps: pulverizing the fine geranium wilfordii, adding water according to the material-liquid ratio of 3:20, mixing, performing ultrasonic treatment to obtain a fine geranium wilfordii mixed solution, performing reflux extraction on the fine geranium wilfordii mixed solution for 2 times, and filtering to obtain a filtrate, namely a target product; the preparation method of the bee pollen extracting solution comprises the following steps: pulverizing bee pollen, mixing with water at a ratio of 1:15, performing ultrasonic treatment to obtain bee pollen mixed solution, reflux-extracting the bee pollen mixed solution for 3 times, and filtering to obtain filtrate as target product.
The grease comprises pentaerythritol tetraester, hydrogenated polydecene and cyclopenta dimethyl siloxane, wherein the pentaerythritol tetraester, the hydrogenated polydecene and the cyclopenta dimethyl siloxane are mixed according to the mass ratio of 1:1: 1; the emulsifier comprises polysorbate and glyceryl stearate, and the polysorbate and the glyceryl stearate are mixed according to the mass ratio of 2: 1;
the preparation method of the moisturizing and repairing composition specifically comprises the following steps:
(1) putting the grease and the emulsifier into a first electric heating stirrer, stirring for 18min at the rotating speed of 1400r/min, and keeping the stirring temperature at 65 ℃ to obtain a mixed solution A;
(2) putting hyaluronic acid, sodium hyaluronate, polyglutamic acid and deionized water into a second electric heating stirrer, stirring for 22min at a rotating speed of 1600r/min, and keeping the stirring temperature at 55 ℃ to obtain a mixed solution B;
(3) adding the mixed solution A into a second electric heating stirrer, mixing with the mixed solution B, adding thyme extractive solution, herba Erodii seu Geranii extractive solution, bee pollen extractive solution and xanthan gum into the second electric heating stirrer at 2900r/min, and stirring for 45min to obtain the target product.
Result detection
1. The test method comprises the following steps: human keratinocytes are cultured in a gas-liquid medium on a collagen matrix to form an in vitro reconstructed human epidermal model. The moisturizing repair compositions obtained in examples 1 to 5 and comparative example were applied to the surface of an artificial skin model, and the results were observed after 15min, and the relative moisturizing rate was measured using a skin barrier capacity test method. Specific detection results are shown in table 1.
TABLE 1 relative moisturizing percentage
| Group of | Relative moisture retention/% |
| Example 1 | 197.2 |
| Example 2 | 198.7 |
| Example 3 | 199.7 |
| Example 4 | 198.2 |
| Example 5 | 197.9 |
| Comparative example | 196.6 |
2. The test method comprises the following steps: in the test, an equal amount of the moisturizing repair composition prepared in examples 1 to 5 and comparative example was uniformly applied to a glass slide with a medical tape, and after scanning a base line, the average value of the ultraviolet absorption of each test sample in different bands of ultraviolet rays was scanned. Specific detection results are shown in table 1.
TABLE 1 ultraviolet absorption
The comparative example is based on the example and reduces the absorbent and titanium dioxide.
As can be seen from table 1, the moisturizing repair composition in the embodiment of the invention has high relative moisturizing rate and good water-locking and moisturizing effects, and the relative moisturizing rate in the comparative example is not much different from that in the embodiment;
as can be seen from table 2, the ultraviolet absorption values (UVA, UVB, and UVC) in the examples of the present invention are all higher than those in the comparative examples, which indicates that the addition of the absorbent and titanium dioxide in the present invention certainly improves the ultraviolet shielding effect of the moisturizing repair composition, and the three cooperate with each other to better shield ultraviolet.
In the description herein, references to the description of "one embodiment," "an example," "a specific example" or the like are intended to mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.
The preferred embodiments of the invention disclosed above are intended to be illustrative only. The preferred embodiments are not exhaustive and do not limit the method of making a high strength caliper seal to the specific embodiments described. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and the practical application, to thereby enable others skilled in the art to best utilize the invention. The invention is limited only by the claims and their full scope and equivalents.
Claims (10)
1. The moisturizing and repairing composition is characterized by comprising the following raw materials in parts by weight: 12-15 parts of grease, 3-4 parts of thyme extracting solution, 5-7 parts of geranium wilfordii extracting solution, 3-4 parts of bee pollen extracting solution, 10-12 parts of emulsifying agent, 2-3 parts of absorbent, 2-3 parts of hyaluronic acid, 3-4 parts of sodium hyaluronate, 5-8 parts of titanium dioxide, 1-2 parts of polyglutamic acid, 1-3 parts of xanthan gum and 50-60 parts of deionized water.
2. The moisturizing and repairing composition as claimed in claim 1, wherein the moisturizing and repairing composition comprises 13-15 parts of grease, 3.2-3.8 parts of thyme extract, 5.5-6.5 parts of geranium wilfordii extract, 3.4-3.6 parts of bee pollen extract, 11-12 parts of emulsifier, 2-2.8 parts of absorbent, 2.5-3 parts of hyaluronic acid, 3.5-4 parts of sodium hyaluronate, 6-8 parts of titanium dioxide, 1-1.8 parts of polyglutamic acid, 1-2 parts of xanthan gum and 52-58 parts of deionized water.
3. The moisturizing and repairing composition as claimed in claim 1, wherein the oil is 14 parts, the thyme extract is 3.5 parts, the geranium wilfordii extract is 6 parts, the bee pollen extract is 3.5 parts, the emulsifier is 12 parts, the absorbent is 2.5 parts, the hyaluronic acid is 2.8 parts, the sodium hyaluronate is 3.7 parts, the titanium dioxide is 7 parts, the polyglutamic acid is 1.5 parts, the xanthan gum is 1.5 parts, and the deionized water is 55 parts.
4. The moisturizing and healing composition according to claim 1, wherein the thyme extract is prepared by a method comprising: pulverizing thyme, mixing with water according to the material-liquid ratio of 1:20, performing ultrasonic treatment to obtain thyme mixed solution, extracting the thyme mixed solution under reflux for 2 times, and filtering to obtain filtrate, namely a target product; the preparation method of the geranium wilfordii extractive solution comprises the following steps: pulverizing the fine geranium wilfordii, adding water according to the material-liquid ratio of 3:20, mixing, performing ultrasonic treatment to obtain a fine geranium wilfordii mixed solution, performing reflux extraction on the fine geranium wilfordii mixed solution for 2 times, and filtering to obtain a filtrate, namely a target product; the preparation method of the bee pollen extracting solution comprises the following steps: pulverizing bee pollen, mixing with water at a ratio of 1:15, performing ultrasonic treatment to obtain bee pollen mixed solution, reflux-extracting the bee pollen mixed solution for 3 times, and filtering to obtain filtrate as target product.
5. The moisturizing repair composition of claim 1, wherein the grease comprises pentaerythritol tetraester, hydrogenated polydecene, and cyclopentadimethicone, the pentaerythritol tetraester, the hydrogenated polydecene, and the cyclopentadimethicone being mixed in a mass ratio of 1:1: 1.
6. The moisturizing repair composition of claim 1, wherein the emulsifier comprises polysorbate and glyceryl stearate, and the polysorbate and the glyceryl stearate are mixed in a mass ratio of 2: 1.
7. The moisturizing repair composition of claim 1, wherein the absorbent comprises ethoxyethyl p-methoxycinnamate and oxybenzone, and the ethoxyethyl p-methoxycinnamate and oxybenzone are mixed in a mass ratio of 1: 2.
8. The moisturizing repair composition of claim 1, wherein the titanium dioxide is rutile titanium dioxide and the titanium dioxide has a particle size of 40-50 nm.
9. A method of preparing a moisturizing repair composition according to any one of claims 1-8, comprising the steps of:
(1) the grease and the emulsifier are put into a first electric heating stirrer to be stirred for 15-20min at the rotating speed of 1200-1500r/min, and the stirring temperature is kept at 60-70 ℃ to obtain a mixed solution A;
(2) placing the absorbent, hyaluronic acid, sodium hyaluronate, titanium dioxide, polyglutamic acid and deionized water into a second electric heating stirrer, stirring for 20-25min at the rotating speed of 1500-1800r/min, and keeping the stirring temperature at 50-60 ℃ to obtain a mixed solution B;
(3) adding the mixed solution A into a second electric-heating stirrer, mixing with the mixed solution B, adding herba Thymi extract, herba Erodii seu Geranii extract, bee pollen extract and xanthan gum into the second electric-heating stirrer, and stirring for 40-50min to obtain the target product.
10. The method for preparing a moisturizing repair composition according to claim 9, wherein the stirring speed in step (3) is 2500-.
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| CN115040935A (en) * | 2022-06-20 | 2022-09-13 | 湖州西岭科技有限公司 | Ultraviolet sterilization resistant electrostatic filtering material and preparation method and application thereof |
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