CN112022772A - Vitis davidii willd plant essence rich in veratryl alcohol and preparation method thereof - Google Patents
Vitis davidii willd plant essence rich in veratryl alcohol and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
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- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9771—Ginkgophyta, e.g. Ginkgoaceae [Ginkgo family]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses a veratryl alcohol-rich vitis davidii plant essence and a preparation method thereof, wherein the veratryl alcohol-rich vitis davidii plant essence is prepared from the following raw materials in parts by weight: 40-60 parts of distilled water, 5-12 parts of collagen powder, 50-65 parts of spiny grape seed powder, 10-15 parts of resveratrol powder, 10-14 parts of ginkgo leaf extract, 2-6 parts of lycopene, 3-8 parts of magnolia flower oil, 1-3 parts of vitamin C, 1-3 parts of catechin, 1-2 parts of arbutin, 1-3 parts of allicin, 5-12 parts of uric acid and 0.5-1.5 parts of hydrophilic antibacterial agent. The veratryl alcohol-rich Vitis davidii plant essence disclosed by the invention has multiple nutritional ingredients and antioxidant active ingredients, and the preparation method strictly controls the temperature and the sequence of adding various components, so that the product stability and consistency of the essence are better.
Description
Technical Field
The invention relates to the technical field of plant extraction, and particularly relates to a veratryl alcohol-rich vitis davidii plant essence and a preparation method thereof.
Background
With the stimulation of factors such as modern life rhythm acceleration, climatic environment and the like, such as ultraviolet rays, sunlight, air pollution, human body organism and the like, skin problems are continuous, and the skin cells are damaged by excessive free radicals, so that the problems of dry skin, color spots, pigment deposition and the like are caused. The emergence of new resveratrol products is a good medicine for solving the problem. As a pure natural product, the resveratrol has no toxic or side effect, and can effectively eliminate redundant free radicals of a human body and improve the synthesis and metabolism of collagen so as to effectively improve the skin. The resveratrol can also inhibit tyrosinase activity from various signal paths by reducing the expression of MCR1 and reducing the expression of genes such as KIT and the like, block the generation and the transportation of melanin and brighten skin color. At present, resveratrol is applied to many occasions, most of the resveratrol is taken as health-care food, and the value of the resveratrol in beautifying and protecting skin, particularly in whitening, cannot be fully embodied.
The essence is an extreme product in skin care products, has delicate components, strong efficacy and obvious effect, and always keeps the nobility and mystery of the essence. The essence contains microelements, collagen and serum, has the functions of anti-aging, anti-wrinkle, moisturizing, whitening, freckle removing and the like, and is a water-separating agent and an oil agent of the essence, wherein high-nutrient substances are extracted and concentrated. However, the essence in the existing market is complex in components and single in function, and the essence in the prior art is added with some heavy metal elements unintentionally due to the components and the preparation process.
Disclosure of Invention
Based on the situation, the invention aims to provide the vitis amurensis plant essence rich in veratryl alcohol and the preparation method thereof, which can effectively solve the problems.
In order to solve the technical problems, the technical scheme provided by the invention is as follows:
the Vitis davidii willd plant essence rich in veratryl alcohol is prepared from the following raw materials in parts by weight: 40-60 parts of distilled water, 5-12 parts of collagen powder, 50-65 parts of spiny grape seed powder, 10-15 parts of resveratrol powder, 10-14 parts of ginkgo leaf extract, 2-6 parts of lycopene, 3-8 parts of magnolia flower oil, 1-3 parts of vitamin C, 1-3 parts of catechin, 1-2 parts of arbutin, 1-3 parts of allicin, 5-12 parts of uric acid and 0.5-1.5 parts of hydrophilic antibacterial agent.
Preferably, the veratryl alcohol-rich vitis davidii plant essence consists of the following raw materials in parts by weight: 60 parts of distilled water, 10 parts of collagen powder, 60 parts of spiny grape seed powder, 12 parts of resveratrol powder, 13 parts of ginkgo leaf extract, 5 parts of lycopene, 6 parts of magnolia flower oil, 2 parts of vitamin C, 2 parts of catechin, 1 part of arbutin, 2 parts of allicin, 10 parts of hyaluronic acid and 1.0 part of hydrophilic antibacterial agent.
Preferably, the veratryl alcohol-rich vitis davidii plant essence consists of the following raw materials in parts by weight: 50 parts of distilled water, 5 parts of collagen powder, 50 parts of spiny grape seed powder, 10 parts of resveratrol powder, 10 parts of ginkgo leaf extract, 3 parts of lycopene, 5 parts of magnolia flower oil, 1 part of vitamin C, 3 parts of catechin, 2 parts of arbutin, 1 part of allicin, 12 parts of hyaluronic acid and 1.5 parts of hydrophilic antibacterial agent.
The invention also provides a preparation method of the vitis amurensis plant essence rich in veratryl alcohol, which comprises the following steps:
(1) cleaning fresh folium Ginkgo, air drying, drying at 60-75 deg.C for 8-9 hr, pulverizing, soaking in ethanol solution, heating in water bath at 60-70 deg.C for 3-4 hr, vacuum filtering, concentrating the filtrate to obtain extract, and vacuum drying at 60-75 deg.C to obtain folium Ginkgo extract;
(2) cleaning fresh magnolia flower, drying in air, placing in a vacuum oven, drying, crushing to 80-100 meshes, placing the crushed raw materials in an extraction kettle, and extracting to obtain magnolia flower oil for later use;
(3) according to the formula of the raw materials, distilled water is taken, and the spiny grape seed powder, the resveratrol powder, the ginkgo leaf extract, the catechin, the arbutin and the allicin in the raw materials are sequentially added to the distilled water and fully stirred and mixed to obtain a base solution;
(4) sequentially adding collagen powder, lycopene, hyaluronic acid and hydrophilic antibacterial agent in the raw materials into the base solution, stirring uniformly, heating in water bath at 35-38 deg.C for 20-40min, naturally cooling to room temperature, adding flos Magnoliae oil and vitamin C, and stirring uniformly to obtain the final product.
In the step (1), the ethanol solution accounts for 60% by mass, the heating is carried out for three times during water bath heating, the heating is carried out for 1-2h each time, gauze is used for filtering after each heating, an appropriate amount of ethanol is added into the filtrate to continue the next heating, and the filtrate is obtained after the third heating is finished and is subjected to suction filtration.
Wherein, in the step (2), the extraction process comprises the following steps: extracting at 25-30 deg.C and 40-55MPa for 2-4 hr, wherein the temperature of the first stage of separation is: 30-45 ℃ and 20-25 MPa; temperature in the separation stage: 20-35 ℃ and 10-15 MPa.
Wherein, the resveratrol powder in the step (3) is prepared by the following process: taking resveratrol solid, and mixing the resveratrol solid with the mixture according to the weight ratio of 1 g: (50-55) mL, adding the resveratrol solid into a 90-95% ethanol solution, adding the solution into hydroxypropyl-beta-cyclodextrin, evaporating to remove ethanol, and spray-freeze drying to obtain resveratrol powder.
Wherein, the spiny grape seed powder in the step (3) is prepared by the following process: putting the spiny grape seed material into an extraction kettle, adding a tetrafluoroethane solution until the spiny grape seed material is submerged, starting extraction, wherein the extraction temperature is 30-40 ℃, the extraction pressure is 20-30MPa, the extraction time is 10-30min, then separating in a separation kettle, the separation temperature is 30-45 ℃, the separation pressure is 10-15MPa, the separation time is 30-60min, obtaining oil in the separation kettle, adding the extraction liquid without the oil into a molecular distiller, setting the vacuum degree in the molecular distiller to be 1.0-2.0Pa, the temperature to be 120-150 ℃ and the rotating speed of a rotary brush membrane to be 1200r/min until the oil is completely collected by a heavy phase collection tank and a light phase collection tank, obtaining an extraction liquid, and carrying out spray drying to obtain the spiny grape seed powder.
Compared with the prior art, the invention has the following beneficial effects:
according to the invention, by adding the natural plants of the magnolia oil, the ginkgo leaf extract and the thorn grape seed powder, the essence has the characteristics of good permeability and easy absorption, and the plant essence can effectively enter the skin, increase the metabolism of the skin and supplement nutrition while permeating.
In the first step, ethanol is adopted for soaking and extracting, so that bacteria are prevented from being generated in the extraction process, and the water bath temperature is low, so that the effective components in the extract cannot be damaged. The ginkgo leaf extract is added, so that the ginkgo leaf extract is rich in ginkgolides, vitamins, flavonoids and the like, and the irritation of the essence on the skin of a human body can be reduced when the essence is used for protecting the skin; the flavone component contained in folium Ginkgo can inhibit formation and deposition of pigment in dermis, and the microelements such as manganese and molybdenum in folium Ginkgo, in addition to flavone, also can remove oxygen free radical and inhibit melanin growth, can reduce chloasma and freckle caused by ultraviolet irradiation, and also has effects of keeping moisture and keeping moisture. The flavone in folium Ginkgo extract is free radical scavenger, and has effects of protecting dermal layer cells, improving blood circulation, and preventing cell oxidation and wrinkle generation.
The vitamin C is an antioxidant with strong effect, but is easy to be oxidized and lose efficacy, and the lycopene, the catechin, the arbutin and the garlicin are added into the essence disclosed by the invention, so that the vitamin C and an oxidizing substance can be blocked from carrying out electron exchange, the stability of the vitamin C is kept, and the essence has strong antioxidant and whitening effects. The collagen powder is added into the preparation, so that the preparation has the anti-aging function, has the effect of improving the skin elasticity, and also has the help effect on the recovery of the operation wound. By adding vitamin C, catechin, lycopene and allicin, the essence disclosed by the invention has excellent antioxidant performance, so that the essence has an anti-aging function, good skin elasticity improving effect and excellent cold and hot stability. The essence disclosed by the invention has various nutritional ingredients and antioxidant active ingredients, and the preparation method strictly controls the temperature and the sequence of adding various components, so that the product stability and consistency of the essence are better.
Detailed Description
In order that those skilled in the art will better understand the technical solutions of the present invention, the following description of the preferred embodiments of the present invention is provided in connection with specific examples, which should not be construed as limiting the present patent.
The test methods or test methods described in the following examples are conventional methods unless otherwise specified; the reagents and materials, unless otherwise indicated, are conventionally obtained commercially or prepared by conventional methods.
Example 1:
the Vitis davidii willd plant essence rich in veratryl alcohol is prepared from the following raw materials in parts by weight: 60 parts of distilled water, 10 parts of collagen powder, 60 parts of spiny grape seed powder, 12 parts of resveratrol powder, 13 parts of ginkgo leaf extract, 5 parts of lycopene, 6 parts of magnolia flower oil, 2 parts of vitamin C, 2 parts of catechin, 1 part of arbutin, 2 parts of allicin, 10 parts of hyaluronic acid and 1.0 part of hydrophilic antibacterial agent.
Wherein the particle size of lycopene is 20-25 nm.
The embodiment also provides a preparation method of the vitis amurensis plant essence rich in veratryl alcohol, which comprises the following steps:
(1) cleaning fresh folium Ginkgo, air drying, oven drying at 68 deg.C for 8 hr, pulverizing, soaking in ethanol solution, heating in water bath at 60 deg.C for 3.5 hr, vacuum filtering to obtain filtrate, distilling and concentrating the filtrate to obtain extract, and vacuum drying at 70 deg.C to obtain folium Ginkgo extract;
(2) cleaning fresh magnolia flower, drying in air, placing in a vacuum oven, drying, crushing to 80-100 meshes, placing the crushed raw materials in an extraction kettle, and extracting to obtain magnolia flower oil for later use;
(3) according to the formula of the raw materials, distilled water is taken, and the spiny grape seed powder, the resveratrol powder, the ginkgo leaf extract, the catechin, the arbutin and the allicin in the raw materials are sequentially added to the distilled water and fully stirred and mixed to obtain a base solution;
(4) sequentially adding collagen powder, lycopene, hyaluronic acid and hydrophilic antibacterial agent in the raw materials into the base solution, stirring uniformly, heating in water bath at 36.3 deg.C for 30min, naturally cooling to room temperature, adding flos Magnoliae oil and vitamin C, and stirring uniformly to obtain the Vitis davidii extract rich in veratryl alcohol.
In the step (1), the ethanol solution accounts for 60% by mass, the ethanol solution is heated for three times in a water bath heating process, the heating is carried out for 1-2 hours each time, gauze is used for filtering after each heating, an appropriate amount of ethanol is added into the filtrate to continue the next heating, and the filtrate is obtained after the third heating is finished and is subjected to suction filtration.
In the step (2), the extraction process comprises the following steps: extraction was carried out at 25 ℃ and 55MPa for 3h, with the separation stage temperature: at 45 ℃, the pressure is 20 MPa; temperature in the separation stage: 20 ℃ and 15 MPa.
The resveratrol powder in the step (3) is prepared by the following process: taking resveratrol solid, and mixing the resveratrol solid with the mixture according to the weight ratio of 1 g: adding the solid resveratrol into a 90% ethanol solution according to the proportion of 52mL, then adding the solution into hydroxypropyl-beta-cyclodextrin, evaporating to remove ethanol, and carrying out spray freeze drying to obtain resveratrol powder.
The spiny grape seed powder in the step (3) is prepared by the following process: putting the spiny grape seed material into an extraction kettle, adding a tetrafluoroethane solution until the spiny grape seed material is submerged, starting extraction, wherein the extraction temperature is 40 ℃, the extraction pressure is 20MPa, the extraction time is 30min, then separating in a separation kettle, the separation temperature is 40 ℃, the separation pressure is 10MPa, the separation time is 50min, obtaining oil in the separation kettle, adding an extract liquid without the oil into a molecular distiller, setting the vacuum degree in the molecular distiller to be 2.0Pa, the temperature to be 120 ℃, and the rotating speed of a rotary brush membrane to be 1200r/min until the oil is completely collected by a heavy phase collection tank and a light phase collection tank to obtain an extracting solution, and carrying out spray drying to obtain the spiny grape seed powder.
Example 2:
the Vitis davidii willd plant essence rich in veratryl alcohol is prepared from the following raw materials in parts by weight: 50 parts of distilled water, 5 parts of collagen powder, 50 parts of spiny grape seed powder, 10 parts of resveratrol powder, 10 parts of ginkgo leaf extract, 3 parts of lycopene, 5 parts of magnolia flower oil, 1 parts of vitamin C, 3 parts of catechin, 2 parts of arbutin, 1 part of allicin, 12 parts of hyaluronic acid and 1.5 parts of hydrophilic antibacterial agent.
The embodiment also provides a preparation method of the vitis amurensis plant essence rich in veratryl alcohol, which comprises the following steps:
(1) cleaning fresh folium Ginkgo, air drying, oven drying at 60 deg.C for 9 hr, pulverizing, soaking in ethanol solution, heating in 70 deg.C water bath for 3 hr, vacuum filtering to obtain filtrate, distilling and concentrating the filtrate to obtain extract, and vacuum drying at 63 deg.C to obtain folium Ginkgo extract;
(2) cleaning fresh magnolia flower, drying in air, placing in a vacuum oven, drying, crushing to 80-100 meshes, placing the crushed raw materials in an extraction kettle, and extracting to obtain magnolia flower oil for later use;
(3) according to the formula of the raw materials, distilled water is taken, and the spiny grape seed powder, the resveratrol powder, the ginkgo leaf extract, the catechin, the arbutin and the allicin in the raw materials are sequentially added to the distilled water and fully stirred and mixed to obtain a base solution;
(4) sequentially adding collagen powder, lycopene, hyaluronic acid and hydrophilic antibacterial agent in the raw materials into the base solution, stirring uniformly, heating in water bath at 35 deg.C for 40min, naturally cooling to room temperature, adding flos Magnoliae oil and vitamin C, and stirring uniformly to obtain the Vitis davidii extract rich in veratryl alcohol.
In the step (1), the ethanol solution accounts for 60% by mass, the ethanol solution is heated for three times in a water bath heating process, the heating is carried out for 1-2 hours each time, gauze is used for filtering after each heating, an appropriate amount of ethanol is added into the filtrate to continue the next heating, and the filtrate is obtained after the third heating is finished and is subjected to suction filtration.
In the step (2), the extraction process comprises the following steps: extraction was carried out at 30 ℃ and 40MPa pressure for 2h, wherein the separation stage temperature: 30 ℃ and 25 MPa; temperature in the separation stage: 35 ℃ and the pressure is 10 MPa.
The resveratrol powder in the step (3) is prepared by the following process: taking resveratrol solid, and mixing the resveratrol solid with the mixture according to the weight ratio of 1 g: adding the solid resveratrol into a 90% ethanol solution according to the proportion of 55mL, then adding the solution into hydroxypropyl-beta-cyclodextrin, evaporating to remove ethanol, and carrying out spray freeze drying to obtain resveratrol powder.
The spiny grape seed powder in the step (3) is prepared by the following process: putting the spiny grape seed material into an extraction kettle, adding a tetrafluoroethane solution until the spiny grape seed material is submerged, starting extraction, wherein the extraction temperature is 30 ℃, the extraction pressure is 30MPa, the extraction time is 25min, then separating in a separation kettle, the separation temperature is 30 ℃, the separation pressure is 15MPa, the separation time is 45min, obtaining oil in the separation kettle, adding an extract liquid without the oil into a molecular distiller, setting the vacuum degree in the molecular distiller to be 1.0Pa, the temperature to be 140 ℃, and the rotating speed of a rotary brush membrane to be 1200r/min until the oil is completely collected by a heavy phase collection tank and a light phase collection tank to obtain an extracting solution, and carrying out spray drying to obtain the spiny grape seed powder.
Example 3:
the Vitis davidii willd plant essence rich in veratryl alcohol is prepared from the following raw materials in parts by weight: 40 parts of distilled water, 12 parts of collagen powder, 65 parts of spiny grape seed powder, 15 parts of resveratrol powder, 14 parts of ginkgo leaf extract, 6 parts of lycopene, 8 parts of magnolia flower oil, 3 parts of vitamin C, 1 part of catechin, 1.5 parts of arbutin, 3 parts of allicin and 5 parts of hyaluronic acid
And 1.2 parts of hydrophilic antibacterial agent.
The embodiment also provides a preparation method of the vitis amurensis plant essence rich in veratryl alcohol, which comprises the following steps:
(1) cleaning fresh folium Ginkgo, air drying, oven drying at 75 deg.C for 8.5 hr, pulverizing, soaking in ethanol solution, heating in 62 deg.C water bath for 4 hr, vacuum filtering to obtain filtrate, distilling and concentrating the filtrate to obtain extract, and vacuum drying at 65 deg.C to obtain folium Ginkgo extract;
(2) cleaning fresh magnolia flower, drying in air, placing in a vacuum oven, drying, crushing to 80-100 meshes, placing the crushed raw materials in an extraction kettle, and extracting to obtain magnolia flower oil for later use;
(3) according to the formula of the raw materials, distilled water is taken, and the spiny grape seed powder, the resveratrol powder, the ginkgo leaf extract, the catechin, the arbutin and the allicin in the raw materials are sequentially added to the distilled water and fully stirred and mixed to obtain a base solution;
(4) sequentially adding collagen powder, lycopene, hyaluronic acid and hydrophilic antibacterial agent in the raw materials into the base solution, stirring uniformly, heating in water bath at 38 deg.C for 20min, naturally cooling to room temperature, adding flos Magnoliae oil and vitamin C, and stirring uniformly to obtain the Vitis davidii extract rich in veratryl alcohol.
In the step (1), the ethanol solution accounts for 60% by mass, the ethanol solution is heated for three times in a water bath heating process, the heating is carried out for 1-2 hours each time, gauze is used for filtering after each heating, an appropriate amount of ethanol is added into the filtrate to continue the next heating, and the filtrate is obtained after the third heating is finished and is subjected to suction filtration.
In the step (2), the extraction process comprises the following steps: extraction was carried out at 27 ℃ under a pressure of 50MPa for 4h, with separation of the temperature of the first stage: at 40 ℃, the pressure is 22 MPa; temperature in the separation stage: 30 ℃ and the pressure of 13 MPa.
The resveratrol powder in the step (3) is prepared by the following process: taking resveratrol solid, and mixing the resveratrol solid with the mixture according to the weight ratio of 1 g: adding the solid resveratrol into a 95% ethanol solution according to the proportion of 50mL, then adding the solution into hydroxypropyl-beta-cyclodextrin, evaporating to remove ethanol, and carrying out spray freeze drying to obtain resveratrol powder.
The spiny grape seed powder in the step (3) is prepared by the following process: putting the spiny grape seed material into an extraction kettle, adding a tetrafluoroethane solution until the spiny grape seed material is submerged, starting extraction, wherein the extraction temperature is 38 ℃, the extraction pressure is 25MPa, the extraction time is 20min, then separating in a separation kettle, the separation temperature is 45 ℃, the separation pressure is 10MPa, the separation time is 60min, obtaining oil in the separation kettle, adding an extract liquid without the oil into a molecular distiller, setting the vacuum degree in the molecular distiller to be 2.0Pa, the temperature to be 120 ℃, and the rotating speed of a rotary brush membrane to be 1200r/min until the oil is completely collected by a heavy phase collection tank and a light phase collection tank to obtain an extracting solution, and carrying out spray drying to obtain the spiny grape seed powder.
The effect test was performed on the essences prepared in examples 1 to 3, in which 120 healthy women, aged 30 to 60 years, with an average age of 45 ± 10.2, were randomly divided into the first group to the fourth group, corresponding to example 1, design example 2, example 3, and comparative example, were selected, the subjects applied the essences on the face after cleaning the face with warm water every day, the comparative example used the essence of plant wisdom-based elegance white essence, commercial number 65231918304, test period thirty days, skin elasticity change was examined by testing the magnitude of rebound deformation of the skin using MPA580 elasticity tester, and the test results are shown in table 1 below.
TABLE 1
As can be seen from table 1, the essence of the present invention has a significant effect of improving skin elasticity, and the effect is greater than that of commercially available essences. Meanwhile, the part from the eye to the canthus is selected as an experimental object, the wrinkle numbers before and after the essence is used are observed visually and organoleptically, and the result shows that: the first group showed significant wrinkle removal after 30 days of use, the second and third groups showed significant wrinkle removal after 30 days of use, and the fourth group showed insignificant wrinkle removal after 30 days of use. The product of the invention has very good effect on reducing facial wrinkles.
The above is only a preferred embodiment of the present invention, and it should be noted that the above preferred embodiment should not be considered as limiting the present invention, and the protection scope of the present invention should be subject to the scope defined by the claims. It will be apparent to those skilled in the art that various modifications and variations can be made in the present invention without departing from the spirit or scope of the invention, and these modifications and variations should also be considered as within the scope of the invention.
Claims (8)
1. The vitis amurensis plant essence rich in veratryl alcohol is characterized by comprising the following raw materials in parts by weight: 40-60 parts of distilled water, 5-12 parts of collagen powder, 50-65 parts of spiny grape seed powder, 10-15 parts of resveratrol powder, 10-14 parts of ginkgo leaf extract, 2-6 parts of lycopene, 3-8 parts of magnolia flower oil, 1-3 parts of vitamin C, 1-3 parts of catechin, 1-2 parts of arbutin, 1-3 parts of allicin, 5-12 parts of uric acid and 0.5-1.5 parts of hydrophilic antibacterial agent.
2. The veratryl alcohol-rich Vitis davidii plant essence according to claim 1, comprising the following raw materials in parts by weight: 60 parts of distilled water, 10 parts of collagen powder, 60 parts of spiny grape seed powder, 12 parts of resveratrol powder, 13 parts of ginkgo leaf extract, 5 parts of lycopene, 6 parts of magnolia flower oil, 2 parts of vitamin C, 2 parts of catechin, 1 part of arbutin, 2 parts of allicin, 10 parts of hyaluronic acid and 1.0 part of hydrophilic antibacterial agent.
3. The veratryl alcohol-rich Vitis davidii plant essence according to claim 1, comprising the following raw materials in parts by weight: 50 parts of distilled water, 5 parts of collagen powder, 50 parts of spiny grape seed powder, 10 parts of resveratrol powder, 10 parts of ginkgo leaf extract, 3 parts of lycopene, 5 parts of magnolia flower oil, 1 part of vitamin C, 3 parts of catechin, 2 parts of arbutin, 1 part of allicin, 12 parts of hyaluronic acid and 1.5 parts of hydrophilic antibacterial agent.
4. The method of preparing the veratryl alcohol-rich Vitis davidii botanical essence of claim 1, comprising the steps of:
(1) cleaning fresh folium Ginkgo, air drying, drying at 60-75 deg.C for 8-9 hr, pulverizing, soaking in ethanol solution, heating in water bath at 60-70 deg.C for 3-4 hr, vacuum filtering, concentrating the filtrate to obtain extract, and vacuum drying at 60-75 deg.C to obtain folium Ginkgo extract;
(2) cleaning fresh magnolia flower, drying in air, placing in a vacuum oven, drying, crushing to 80-100 meshes, placing the crushed raw materials in an extraction kettle, and extracting to obtain magnolia flower oil for later use;
(3) according to the formula of the raw materials, distilled water is taken, and the spiny grape seed powder, the resveratrol powder, the ginkgo leaf extract, the catechin, the arbutin and the allicin in the raw materials are sequentially added to the distilled water and fully stirred and mixed to obtain a base solution;
(4) sequentially adding collagen powder, lycopene, hyaluronic acid and hydrophilic antibacterial agent in the raw materials into the base solution, stirring uniformly, heating in water bath at 35-38 deg.C for 20-40min, naturally cooling to room temperature, adding flos Magnoliae oil and vitamin C, and stirring uniformly to obtain the final product.
5. The method of claim 4, wherein the veratryl alcohol-rich Vitis davidii Murr plant essence comprises: in the step (1), the ethanol solution accounts for 60% by mass, the ethanol solution is heated for three times in a water bath heating process, the heating is carried out for 1-2 hours each time, gauze is used for filtering after each heating, an appropriate amount of ethanol is added into the filtrate to continue the next heating, and the filtrate is obtained after the third heating is finished and is subjected to suction filtration.
6. The method of claim 4, wherein the veratryl alcohol-rich Vitis davidii Murr plant essence comprises: in the step (2), the extraction process comprises the following steps: extracting at 25-30 deg.C and 40-55MPa for 2-4 hr, wherein the temperature of the first stage of separation is: 30-45 ℃ and 20-25 MPa; temperature in the separation stage: 20-35 ℃ and 10-15 MPa.
7. The method of claim 4, wherein the veratryl alcohol-rich Vitis davidii Murr plant essence comprises: the resveratrol powder in the step (3) is prepared by the following process: taking resveratrol solid, and mixing the resveratrol solid with the mixture according to the weight ratio of 1 g: (50-55) mL, adding the resveratrol solid into a 90-95% ethanol solution, adding the solution into hydroxypropyl-beta-cyclodextrin, evaporating to remove ethanol, and spray-freeze drying to obtain resveratrol powder.
8. The method of claim 4, wherein the veratryl alcohol-rich Vitis davidii Murr plant essence comprises: the spiny grape seed powder in the step (3) is prepared by the following process: putting the spiny grape seed material into an extraction kettle, adding a tetrafluoroethane solution until the spiny grape seed material is submerged, starting extraction, wherein the extraction temperature is 30-40 ℃, the extraction pressure is 20-30MPa, the extraction time is 10-30min, then separating in a separation kettle, the separation temperature is 30-45 ℃, the separation pressure is 10-15MPa, the separation time is 30-60min, obtaining oil in the separation kettle, adding the extraction liquid without the oil into a molecular distiller, setting the vacuum degree in the molecular distiller to be 1.0-2.0Pa, the temperature to be 120-150 ℃ and the rotating speed of a rotary brush membrane to be 1200r/min until the oil is completely collected by a heavy phase collection tank and a light phase collection tank, obtaining an extraction liquid, and carrying out spray drying to obtain the spiny grape seed powder.
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