CN111714428B - Whitening and moisturizing composition and whitening and moisturizing skin care product containing natural plant extracts - Google Patents
Whitening and moisturizing composition and whitening and moisturizing skin care product containing natural plant extracts Download PDFInfo
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- CN111714428B CN111714428B CN202010562498.6A CN202010562498A CN111714428B CN 111714428 B CN111714428 B CN 111714428B CN 202010562498 A CN202010562498 A CN 202010562498A CN 111714428 B CN111714428 B CN 111714428B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses a whitening and moisturizing composition and a whitening and moisturizing skin care product containing natural plant extracts, and relates to the field of cosmetics. The whitening and moisturizing composition disclosed by the invention comprises a clivia extract, a winter jasmine extract and a florist extract. The whitening and moisturizing composition contains the extract of natural plant sources, has tyrosinase inhibitory activity, and can be prepared into skin care products, so that the whitening and moisturizing functions of skin can be improved, and the skin has luster and elasticity.
Description
Technical Field
The invention relates to the field of cosmetics, in particular to a whitening and moisturizing composition containing natural plant extracts and a whitening and moisturizing skin care product.
Background
Skin is an important part of the human body and covers the surface of the human body. The skin is a natural barrier between the external environment and the body, protecting the organs in the body from temperature and humidity changes. The outermost layer of the skin is the stratum corneum, which maintains a certain moisture content due to the water absorption and barrier functions of the stratum corneum itself and the actions of amino acids, lactate, saccharides and the like which are natural moisturizing factors contained in the stratum corneum, and thus the skin is kept moist. However, with age, the skin is also subject to problems such as weakening of metabolism, poor blood circulation, poor nutrients, etc., which easily cause accumulation of melanin on the skin, and further cause darkness, slackening, wrinkles, color spots, etc.
The whitening and moisturizing skin care product containing the natural plant extract is more and more focused by consumers due to the advantages of active ingredients of natural sources, wide sources and the like. Natural plant whitening, moisturizing and skin care products with stronger whitening and moisturizing functions are becoming research hot spots.
In view of this, the present invention has been made.
Disclosure of Invention
The invention aims to provide a whitening and moisturizing composition containing natural plant extracts, which has tyrosinase inhibitory activity and can be used for preparing whitening and moisturizing skin care products.
Another object of the present invention is to provide the use of the above-mentioned whitening and moisturizing composition in whitening and moisturizing.
The invention further aims to provide a whitening and moisturizing skin care product which has good whitening and moisturizing functions, can reduce melanin of skin and enables the skin to have high moisture content.
The invention further aims at providing a method for preparing the whitening and moisturizing skin care product.
The invention is realized in the following way:
in a first aspect, the present invention provides a whitening and moisturizing composition comprising natural plant extracts, comprising the following extracts: extract of Clivia, extract of flos Helianthi, and extract of flos Lupuli.
According to the invention, researches show that the extract of clivia miniata, the extract of winter jasmine and the extract of Fulu coo have tyrosinase inhibitory activity, and the extract of clivia miniata, the extract of winter jasmine and the extract of Fulu coo have whitening and moisturizing functions when used in skin care products, so that the skin has luster and elasticity.
Further experimental study shows that compared with the combination of single or two, the combination of the three extracts of the clivia extract, the winter jasmine extract and the floras extract has more prominent tyrosinase inhibition activity.
Further, in a preferred embodiment, the clivia extract and the flos verrucae vulnifoliae extract are both aqueous extracts, and the florus extract is an alcoholic extract.
Further, in a preferred embodiment, the mass ratio of the clivia extract, the spring-welcoming extract and the floret extract is 1:1:1.
When the mass ratio of the clivia extract to the winter jasmine extract to the floras extract is 1:1:1, the three extracts have a certain synergistic effect, so that the tyrosine inhibition activity of the composition is greatly improved.
Further, in a preferred embodiment, the clivia extract or the verruca ushi extract is prepared by the following method:
soaking clivia leaves or winter jasmine leaves in water, performing first ultrasonic extraction, heating and boiling, filtering, taking filtrate, and decolorizing to obtain the clivia flower extract or winter jasmine extract.
Further, in a preferred embodiment, the mass to volume ratio of the clivia petals or the winter jasmine petals to water is 1:30-50.
Further, in a preferred embodiment, wherein the mass to volume ratio of the clivia petals or the winter jasmine petals to water is 1:40.
Further, in a preferred embodiment, the first ultrasonic extraction is performed at a power of 100-600w for a time of 60-120min.
Further, in a preferred embodiment, the power at which the first ultrasonic extraction is performed is 400w and the extraction time is 120min.
Further, in a preferred embodiment, the time of heating to boil is 10-15 minutes.
Further, in a preferred embodiment, the time of heating to boil is 10 minutes.
The preparation methods of the clivia miniata extract and the winter jasmine extract are the same, and the clivia miniata extract and the winter jasmine extract prepared by adopting the water extraction method have tyrosinase inhibitory activity and can be used for whitening and moisturizing.
Further, in a preferred embodiment, the extract of the florfenicol is prepared by the following method:
mixing the dried Fulu-colestuary petals with ethanol, performing second ultrasonic extraction, filtering, concentrating to obtain extract, and dissolving the extract with water to obtain the Fulu-colestuary flower extract.
The study of the present invention shows that, in comparison with the aqueous extraction method, the obtained extract of the floras has tyrosinase inhibitory activity, which is unexpected to those skilled in the art.
Further, in a preferred embodiment, the concentration of the ethanol is 70% -80%, and the mass-volume ratio of the ethanol to the ethanol is 1:10-15.
Further, in a preferred embodiment, the concentration of the ethanol is 70%, and the mass-to-volume ratio of the ethanol to the ethanol is 1:12.
Further, in a preferred embodiment, the second ultrasonic extraction is performed at a power of 200-300w for a time of 30-60 minutes.
Further, in a preferred embodiment, the second ultrasonic extraction is performed at a power of 300w for a time of 60 minutes.
Further, in a preferred embodiment, the conditions of concentration are concentration to a density of 1.1-1.2.
Further, in a preferred embodiment, the conditions of concentration are concentration to a density of 1.1.
Further, in a preferred embodiment, the mass to volume ratio of the extract to the water is 1:1-2.
Further, in a preferred embodiment, the mass to volume ratio of the extract to the water is 1:2.
In a second aspect, the invention provides an application of the whitening and moisturizing composition in preparing a whitening and moisturizing skin care product.
In a third aspect, the invention provides a whitening and moisturizing skin care product, which comprises the whitening and moisturizing composition as described in any one of the above raw materials.
The whitening and moisturizing skin care product provided by the invention has the whitening and moisturizing functions, and can keep the skin in the whitening and moisturizing state for a long time after being used.
Further, in a preferred embodiment, the feedstock further comprises: propylene glycol, carbomer, glycerol stearate, talcum powder, neutralizer, sodium benzoate and essence.
Further, in a preferred embodiment, the raw materials include, in parts by weight: 12-25 parts of propylene glycol, 2-6 parts of carbomer, 5-10 parts of glycerol stearate, 5-10 parts of talcum powder, 1-5 parts of neutralizer, 1-5 parts of sodium benzoate, 1-2 parts of essence, 20-30 parts of a Fulu coo flower extract, 20-30 parts of a clivia flower extract and 20-30 parts of a winter jasmine extract.
Further, in a preferred embodiment, the raw materials include, in parts by weight: 15 parts of propylene glycol, 3 parts of carbomer, 6 parts of glycerol stearate, 7 parts of talcum powder, 2 parts of neutralizer, 1 part of sodium benzoate, 1 part of essence, 25 parts of a florfenicol extract, 25 parts of a clivia extract and 25 parts of a verruca japonica extract.
In a fourth aspect, the present invention provides a method of preparing a whitening, moisturizing skin care product as set forth in any one of the above, comprising: the components of the raw materials are mixed.
The preparation method provided by the invention is simple to operate, the whitening and moisturizing skin care product can be conveniently and rapidly prepared, and the prepared whitening and moisturizing skin care product has good whitening and moisturizing performances.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention more clear, the technical solutions of the embodiments of the present invention will be clearly and completely described below. The specific conditions are not noted in the examples and are carried out according to conventional conditions or conditions recommended by the manufacturer. The reagents or apparatus used were conventional products commercially available without the manufacturer's attention.
The features and capabilities of the present invention are described in further detail below in connection with the examples.
Example 1
The raw material components of the whitening and moisturizing skin care product provided by the embodiment are as follows:
comprises the following components in parts by weight: 15 parts of propylene glycol, 3 parts of carbomer, 6 parts of glycerol stearate, 7 parts of talcum powder, 2 parts of neutralizer, 1 part of sodium benzoate, 1 part of essence, 25 parts of a florfenicol extract, 25 parts of a clivia extract and 45 parts of a verruca japonica extract.
Wherein, the extract of the clivia miniata is prepared by the following method: soaking fresh clivia leaves in water at a feed liquid ratio of 1:40 (kg: L), performing ultrasonic extraction with power of 400w for 120min; and after the ultrasonic treatment is finished, heating and boiling for 10min, filtering with gauze, taking filtrate, adding active carbon into the filtrate for decolorization, wherein the decolorization temperature is 80 ℃, filtering until the solution is clear and free of active carbon, collecting filtrate, and sterilizing at 121 ℃ for 10min to obtain the clivia miniata extract.
The winter jasmine extract is prepared by the following steps: soaking fresh flos Rosae Rugosae in water at a ratio of 1:40 (kg: L), ultrasonic extracting at a power of 400w for 120min, boiling for 10min, filtering with gauze, decolorizing with active carbon at 80deg.C, filtering to obtain clear solution without active carbon, collecting filtrate, and sterilizing at 121deg.C under high pressure for 10min to obtain flos Rosae Rugosae extract.
The extract of the florfenicol is prepared by the following method: taking fresh Fulu petals, naturally airing, mixing with 70% ethanol, extracting with ultrasonic power of 300w for 60min at a feed-liquid ratio of 1:10 (kg: L); filtering, recovering ethanol, concentrating to density of 1.1 (room temperature), and dissolving the extract with water at mass/volume ratio of 1:2 (kg: L), and sterilizing at 121deg.C for 10min to obtain the extract.
The tyrosinase activity inhibitory effect of each extract and its combination is shown in experimental example 1.
The preparation method of the whitening and moisturizing skin care product provided by the embodiment comprises the following steps:
15 parts of propylene glycol, 3 parts of carbomer, 6 parts of glycerol stearate, 7 parts of talcum powder, 25 parts of Fulu koua extract and a proper amount of deionized water are stirred at room temperature (the rotating speed is 1000 r/min) for dispersion, and then stirred and emulsified at 70-80 ℃; then adding 25 parts of the clivia extract, 25 parts of the winter jasmine extract, 2 parts of the neutralizer, 1 part of sodium benzoate and 1 part of essence, maintaining the temperature at 70-80 ℃, continuously stirring at the rotating speed of 800 r/min, homogenizing and emulsifying, and naturally cooling to obtain the whitening, moisturizing and skin-care product.
Experimental example 1
Tyrosinase activity inhibition assay
The method comprises the following steps: tyrosinase activity detection kit (Beijing Soy Bao technology Co., ltd., brand BC 4050) was used in combination with visible spectrophotometry to detect tyrosinase inhibitory activity of each of the extracts and combinations thereof of example 1, and the extracts used in each of the experimental groups were as follows:
experiment group 1: extract of clivia;
experiment group 2: an extract of winter jasmine;
experiment group 3: an extract of a flower of the group consisting of a formosana;
experiment group 4: mixing and sampling the extract of clivia flower and the extract of winter jasmine in a volume ratio of 1:1;
experimental group 5: mixing the extract of the clivia flower and the extract of the Fulu coo flower according to the volume ratio of 1:1, and then adding a sample;
experiment group 6: mixing flos Helianthi extract and Fulu coo extract at volume ratio of 1:1, and adding sample;
experiment group 7: mixing the extract of the clivia flower, the extract of the winter jasmine flower and the extract of the florida according to the volume ratio of 1:1:1, and then adding the sample. In the detection process, the extract sample application amount of each experimental group is the same, and the results are shown in table 1:
TABLE 1
Experimental grouping | Sample application volume | Tyrosinase inhibition rate |
Experiment group 1 | 0.02mL | 36% |
Experiment group 2 | 0.02mL | 20% |
Experiment group 3 | 0.02mL | 45% |
Experiment group 4 | 0.02mL | 32% |
Experiment group 5 | 0.02mL | 50% |
Experiment group 6 | 0.02mL | 40% |
Experiment group 7 | 0.02mL | 61% |
As can be seen from table 1, when the three extracts of clivia extract + winter jasmine extract + formosan extract were used in combination, the tyrosinase inhibition rate was significantly higher than that of the individual extracts and the combination of the two.
In addition, the inventor finds that if the floras are extracted in the same extraction mode as the clivia flower during the research and development process, the obtained extract has no tyrosinase inhibition effect, and experimental data show that the tyrosinase inhibition rate is close to 0. The inventors have found that the tyrosinase inhibition rate of the extract of the flower of the Fulu-colestuary was increased sharply by changing the extraction mode, i.e., the extraction mode of example 1 (see experiment group 3 in Table 1), which means that the flower of Fulu-colestuary is suitable for the extraction with alcohol, not water, to prepare the extract having tyrosinase inhibition rate.
Experimental example 2
Skin whitening performance test
Referring to the method of example 1, a whitening and moisturizing skin care product was prepared by using the combination of the extracts of experimental example 1 and experimental group 3 as a control group 1;
referring to the method of example 1, but without using any extract, the same procedure as in example 1 was used for other raw materials to prepare a whitening and moisturizing skin care product as a blank.
20 skin healthy volunteers were selected and divided into 2 groups:
group A: the whitening and moisturizing skin care product of example 1 + blank control was used;
group B: the whitening and moisturizing skin care product of control group 1 was used with a blank control.
The method comprises the following steps: the region of 3cm multiplied by 3cm inside the left and right forearms of the volunteer is the tested part, one side is coated with the whitening and moisturizing skin care product to be tested, the other side is coated with the blank control sample, and the consumption of the sample coated each time is 0.1g. The preparation is used for 1 time in the morning and at night each day for 3 weeks. The melanin content in the skin was measured before use, at the end of week 3, at week 4 and at week 5, respectively, and was measured with a skin melanin tester manufactured by CK electronics, germany. The skin melanin rate of change was calculated as follows: melanin change rate (%) = skin melanin content measured after application/skin melanin content measured before application x 100%. The results are shown in Table 2 below, where the melanin change rates of the respective groups are shown as average values.
TABLE 2
Experimental grouping | Before application | Week 3 | Week 4 | Week 5 | Week 6 |
Group A test | 100% | 65% | 73% | 88% | 98% |
Group A air conditionerWhite rules | 100% | 98% | 100% | 100% | 100% |
Group B test | 100% | 72% | 89% | 96% | 100% |
Blank of group B | 100% | 99% | 100% | 100% | 100% |
As can be seen from table 2, after the whitening and moisturizing skin care product of example 1 is applied, the melanin content is significantly reduced (p < 0.05), and compared with the whitening and moisturizing skin care product of control 1, the whitening and moisturizing skin care product of example 1 can inhibit melanin generation (p < 0.05) more significantly, and it is particularly notable that after the application is stopped, the recovery of the tested melanin is also slower, the whitening and moisturizing skin care product of example 1 is applied, the tested melanin is recovered to the level before the application at week 6, and the whitening and moisturizing skin care product of control 1 is recovered to the level before the application at week 5; this demonstrates that the whitening and moisturizing skin care product of example 1 of the present invention can maintain the whitening effect for a long period of time, which is unexpected to those skilled in the art.
Experimental example 3
Moisture retention performance test
20 skin healthy volunteers were selected and divided into 2 groups:
group A: the whitening and moisturizing skin care product of example 1 + blank control was used;
group B: the whitening and moisturizing skin care product of control group 1 was used with a blank control.
A square experimental area with the size of 3CM multiplied by 3CM is marked on the left and right forearm of a volunteer, the left arm is used as a test area of a skin care product to be tested (the whitening and moisturizing skin care product of example 1 or the whitening and moisturizing skin care product of a control group 1), the corresponding symmetrical area of the right arm is used as a blank control area (the skin care product of the blank control group is smeared), then the moisture content of each test part is tested and detected by a Corneometer CM825, and the moisture content increase rate is calculated: increase rate = (test area value-blank area value)/blank area value x 100%, each group expressed as average value was detected at 1h, 2h, 4h after application, respectively. The results are shown in Table 3.
TABLE 3 Table 3
Experimental grouping | 1h | 2h | 4h |
Group A | 66% | 61% | 53% |
Group B | 58% | 40% | 26% |
As can be seen from table 3, the rate of increase in moisture content was higher for the skin care product of example 1 than for control group 1, and the rate of decrease in moisture content was slower for the area where the skin care product of example 1 was used over time, which fully demonstrated that the skin care product of example 1 was higher in moisturizing performance and longer in moisturizing time.
The above description is only of the preferred embodiments of the present invention and is not intended to limit the present invention, but various modifications and variations can be made to the present invention by those skilled in the art. Any modification, equivalent replacement, improvement, etc. made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (6)
1. A whitening and moisturizing composition containing natural plant extracts, which is characterized by comprising the following extracts: an extract of clivia flower, an extract of winter jasmine flower and an extract of florfenicol flower; the mass ratio of the clivia extract to the winter jasmine extract to the florida extract is 1:1:1;
the clivia extract and the winter jasmine extract are both water extracts, and the florist extract is an alcohol extract;
the clivia extract or the winter jasmine extract is prepared by the following method:
soaking clivia leaves or winter jasmine leaves in water, performing first ultrasonic extraction, heating and boiling, filtering, taking filtrate, and decolorizing to obtain the clivia flower extract or winter jasmine extract; wherein the mass volume ratio of the clivia leaves or the winter jasmine leaves to the water is 1:30-50; the power of the first ultrasonic extraction is 100-600w, and the extraction time is 60-120min; heating and boiling for 10-15min;
the extract of the florfenicol is prepared by the following method:
mixing the dried Fulu-colestuary petals with ethanol, performing second ultrasonic extraction, filtering and concentration to obtain an extract, and dissolving the extract with water to obtain the Fulu-colestuary flower extract; the concentration of the ethanol is 70-80%, and the mass-volume ratio of the ethanol to the ethanol is 1:10-15; the power of the second ultrasonic extraction is 200-300w, and the extraction time is 30-60min; concentrating to a density of 1.1-1.2; the mass volume ratio of the extract to the water is 1:1-2.
2. Use of the whitening and moisturizing composition of claim 1 in the preparation of a whitening and moisturizing skin care product.
3. A whitening and moisturizing skin care product, characterized in that the raw materials comprise the whitening and moisturizing composition of claim 1.
4. The whitening and moisturizing skin care product according to claim 3, wherein the raw materials further comprise: propylene glycol, carbomer, glycerol stearate, talcum powder, neutralizer, sodium benzoate and essence.
5. The whitening and moisturizing skin care product according to claim 4, wherein the raw materials comprise, in parts by weight: 15 parts of propylene glycol, 3 parts of carbomer, 6 parts of glycerol stearate, 7 parts of talcum powder, 2 parts of neutralizer, 1 part of sodium benzoate, 1 part of essence, 25 parts of a florfenicol extract, 25 parts of a clivia extract and 25 parts of a verruca japonica extract.
6. A method for preparing the whitening and moisturizing skin care product according to any one of claims 3 to 5, which comprises: the components of the raw materials are mixed.
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