CN112006950A - Rose eye firming cream and preparation method thereof - Google Patents
Rose eye firming cream and preparation method thereof Download PDFInfo
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- CN112006950A CN112006950A CN201910472580.7A CN201910472580A CN112006950A CN 112006950 A CN112006950 A CN 112006950A CN 201910472580 A CN201910472580 A CN 201910472580A CN 112006950 A CN112006950 A CN 112006950A
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- rose
- petals
- water
- eye cream
- cell sap
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The invention discloses rose tightening eye cream and a preparation method thereof. The preparation method comprises the following steps: firstly, preparing rose cellular fluid; and (II) mixing and homogenizing the components. Compared with the traditional eye cream, the eye cream has simpler components, and has no other chemicals except glycerin, propylene glycol fatty acid ester and sodium hyaluronate which maintain the basic characteristics of the eye cream.
Description
Technical Field
The invention relates to rose tightening eye cream and a preparation method thereof, and belongs to the field of processing of cosmetics combined with biotechnology.
Background
Roses are petals of flowers of roses (rosarugosa thunb) of the rosaceous family, are warm in nature, sweet in taste and slightly bitter in taste, and are mainly produced in provinces such as Shandong, Gansu, Anhui, Zhejiang, Hebei and inner Mongolia. Besides the ornamental value, roses also have multiple purposes. Modern medicine shows that the rose contains more than 300 chemical components, wherein the chemical components contain substances which are beneficial to beauty, such as quercetin, fatty oil containing essence, organic acid and the like; contains polyphenols, flavonoids and other chemical components, and has effects in reducing and eliminating free radicals, resisting oxidation, resisting thrombi, resisting cancer, resisting inflammation, resisting bacteria, regulating immunity, reducing blood lipid and preventing heart disease; the flower also contains 18 kinds of amino acids and microelements required by human body, and has effects of relieving stuffiness, resolving stagnation, dispersing stomach qi, strengthening liver, strengthening lung, removing toxic substance, removing phytotoxicity caused by antibiotic substance, balancing endocrine, relieving nerve fatigue, hangover, climacteric disorder, constipation, removing speckle, regulating female physiology, promoting blood circulation, and caring skin.
The rose flower cell sap is a byproduct in the production process of dried rose buds, has the natural flower fragrance of rose flowers, has wide application, can improve the skin texture, promotes blood circulation and metabolism, has pleasant fragrance due to the fact that the stock solution contains a large amount of rose essential oil components, can be directly used as a moisturizing skin care product, and has the effects of whitening and removing freckles.
With the improvement of living standard and the acceleration of living rhythm of people, the eyes of people are aged and injured in different degrees when facing computers, mobile phones, staying up overnight and the like for a long time, so that the skin around the eyes is dry and astringent, dehydrated and black eye circles are bred to finally form eye marks, and for people who love beauty, the deterioration of the skin around the eyes directly influences the color development and appearance of the whole people, and the theory that the old eyes are old first is adopted. To alleviate skin aging around the eyes, many eye creams are applied.
Disclosure of Invention
The technical problem to be solved by the invention is as follows: a rose eye cream for tightening eyes and a preparation method thereof are provided.
In order to solve the technical problems, the invention adopts the technical scheme that:
the rose firming eye cream comprises glycerin, propylene glycol fatty acid ester, sodium hyaluronate and rose cellular fluid. Wherein the mass parts of the components are as follows: 5-10 parts of glycerol, 1-6 parts of propylene glycol fatty acid ester, 1-6 parts of sodium hyaluronate and 20-35 parts of rose cell sap.
The invention also provides a preparation method of the rose tightening eye cream, which comprises the following steps:
firstly, preparing rose cellular fluid:
(1) collecting and cleaning Damascus roses: collecting edible Damascus roses in flowering period of 5-6 months, removing perianth, withered rose petals and stamen, and rinsing the petals.
(2) Primary acidification of rose: adding 10-20 times of water into rose petal, adding 3-8 times of organic acid into water, and acidifying for 0.5-1 hr.
(3) Primary fermentation of rose petals: taking out the rose petals in the previous step, adding 1-3 times of water by weight, adding 0.03-0.06 part of each of yeast and bacillus subtilis strain, fermenting at 35-40 deg.C for 1-3 h.
(4) Enzymolysis of the rose: fishing out the rose petals in the previous step, adding 5-10 times of water by weight, and then adding beta-mannase, cellulase and lysozyme into the water, wherein the unit amount of the enzyme added per kilogram of the rose petals is as follows: 700-900U, 100-200U and 200-300U at 30-40 ℃ for enzymolysis for 0.5-2h, and then inactivating the enzyme; then filtering to obtain rose fermentation supernatant, and reserving the rose fermentation supernatant.
(5) Baking the filtered rose petals in an oven at 40-50 ℃, drying at three-stage temperature, maintaining at 30 ℃ for 2h, 38 ℃ for 3-5h and 35 ℃ for 3h, and collecting condensed steam to obtain condensed water.
(6) Mixing the supernatant obtained in the step 4 and the condensed water obtained in the step 5 with the condensed water, and filtering impurities to obtain primary rose cell sap.
(7) And (4) concentrating the rose cell sap obtained in the step (6) under reduced pressure, and removing 30-50% of water to obtain the rose cell sap.
Mixing the two components uniformly
Respectively micronizing glycerol, propylene glycol fatty acid ester and half weight of rose cell sap with ultrahigh pressure homogenizer at homogenizing pressure of 110-130MPa for 10-20min, and oil drop with particle size distribution of 30-80 nm.
Adding sodium hyaluronate and the rest rose cell sap, increasing the pressure of a homogenizer to 140MPa, homogenizing for 9-20min, and vacuum refrigerating at 10-200 ℃ for 10-18h to obtain the rose tightening eye cream.
The invention has the beneficial effects that:
the active ingredient of the tightening eye cream is a rose product, and an industrial direction is provided for expanding the rose industry.
The rose cell sap is natural cell sap extracted from roses, and the rose cell sap obtained by the early-stage biological extraction method and the conventional drying extraction method can fully extract active ingredients in the roses, including essential oil, polyphenols, flavonoids and the like.
Compared with the traditional eye cream, the eye cream has simpler components, and has no other chemicals except glycerin, propylene glycol fatty acid ester and sodium hyaluronate which maintain the basic characteristics of the eye cream.
Detailed Description
Example 1
The rose tightening eye cream provided by the embodiment comprises glycerin, propylene glycol fatty acid ester, sodium hyaluronate and rose cellular fluid. Wherein the mass parts of the components are as follows: 5-10 parts of glycerol, 1-6 parts of propylene glycol fatty acid ester, 1-6 parts of sodium hyaluronate and 20-35 parts of rose cell sap.
The invention also provides a preparation method of the rose tightening eye cream, which comprises the following steps:
firstly, preparing rose cellular fluid:
(1) collecting and cleaning Damascus roses: collecting edible Damascus roses in flowering period of 5-6 months, removing perianth, withered rose petals and stamen, and rinsing the petals.
(2) Primary acidification of rose: adding 20 parts by weight of water into rose petals, then adding 8 parts by weight of citric acid into the water, and acidifying for 1 h.
(3) Primary fermentation of rose petals: taking out the rose petals in the previous step, adding 3 times of water by weight, adding 0.06 part of each of saccharomycete and bacillus subtilis, fermenting and decomposing for 2 hours at 40 ℃ in a short time.
(4) Enzymolysis of the rose: fishing out the rose petals in the previous step, adding 10 times of water by weight, and then adding beta-mannase, cellulase and lysozyme into the water, wherein the unit amount of the enzyme added per kilogram of the rose petals is as follows: 900U, 200U and 300U at 40 ℃, and inactivating enzyme after enzymolysis for 2 h; then filtering to obtain rose fermentation supernatant, and reserving the rose fermentation supernatant.
(5) And (3) baking the filtered rose petals in a baking oven at 50 ℃, drying at a three-stage temperature, maintaining at 30 ℃ for 2 hours, 38 ℃ for 3-5 hours and 35 ℃ for 3 hours, and collecting condensed steam to obtain condensed water.
(6) Mixing the supernatant obtained in the step 4 and the condensed water obtained in the step 5 with the condensed water, and filtering impurities to obtain primary rose cell sap.
(7) And (4) concentrating the rose cell sap obtained in the step (6) under reduced pressure, and removing 30-50% of water to obtain the rose cell sap.
Mixing the two components uniformly
Respectively micronizing glycerol, propylene glycol fatty acid ester and half weight of rose cell sap with ultrahigh pressure homogenizer at homogenizing pressure of 110-130MPa for 10-20min, and oil drop with particle size distribution of 30-80 nm.
Adding sodium hyaluronate and the rest rose cell sap, increasing the pressure of a homogenizer to 140MPa, homogenizing for 9-20min, and vacuum refrigerating at 10-200 ℃ for 10-18h to obtain the rose tightening eye cream.
Example 2
The rose tightening eye cream provided by the embodiment comprises glycerin, propylene glycol fatty acid ester, sodium hyaluronate and rose cellular fluid. Wherein the mass parts of the components are as follows: 5-10 parts of glycerol, 1-6 parts of propylene glycol fatty acid ester, 1-6 parts of sodium hyaluronate and 20-35 parts of rose cell sap.
The invention also provides a preparation method of the rose tightening eye cream, which comprises the following steps:
firstly, preparing rose cellular fluid:
(1) collecting and cleaning Damascus roses: collecting edible Damascus roses in flowering period of 5-6 months, removing perianth, withered rose petals and stamen, and rinsing the petals.
(2) Primary acidification of rose: adding 10 times of water by weight into rose petals, then adding 3 times of malic acid by weight into the water, and acidifying for 0.5 h.
(3) Primary fermentation of rose petals: taking out the rose petals in the previous step, adding 1 time of water by weight, adding 0.03 part of each of saccharomycete and bacillus subtilis, fermenting at 35 ℃ for 1 hour.
(4) Enzymolysis of the rose: fishing out the rose petals in the previous step, adding 5 times of water by weight, and then adding beta-mannase, cellulase and lysozyme into the water, wherein the unit amount of the enzyme added per kilogram of the rose petals is as follows: 700U, 100U and 200U at 30-40 deg.C, and inactivating enzyme after enzymolysis for 0.5 hr; then filtering to obtain rose fermentation supernatant, and reserving the rose fermentation supernatant.
(5) And (3) baking the filtered rose petals in a baking oven at 40 ℃, drying at a three-stage temperature, maintaining at 30 ℃ for 2 hours, 38 ℃ for 3-5 hours and 35 ℃ for 3 hours, and collecting condensed steam to obtain condensed water.
(6) Mixing the supernatant obtained in the step 4 and the condensed water obtained in the step 5 with the condensed water, and filtering impurities to obtain primary rose cell sap.
(7) And (4) concentrating the rose cell sap obtained in the step (6) under reduced pressure, and removing 30-50% of water to obtain the rose cell sap.
Mixing the two components uniformly
Respectively micronizing glycerol, propylene glycol fatty acid ester and half weight of rose cell sap with ultrahigh pressure homogenizer at homogenizing pressure of 110-130MPa for 10-20min, and oil drop with particle size distribution of 30-80 nm.
Adding sodium hyaluronate and the rest rose cell sap, increasing the pressure of a homogenizer to 140MPa, homogenizing for 9-20min, and vacuum refrigerating at 10-200 ℃ for 10-18h to obtain the rose tightening eye cream.
Example 3 comparison of essential oil content in Rose cell sap
In the prior art, the rose is reported to be used for preparing the eye cream, and the invention has the innovation that the extraction process of the rose cell sap is optimized and improved, and the extraction rate of active ingredients in the rose is improved.
The preparation method of the rose cellular fluid of the embodiment 1 of the invention is compared with the dry distillation method disclosed in the Chinese patent CN101536968A, and the extraction rate of typical active ingredient essential oil in the cellular fluid obtained by the preparation method and the dry distillation method is tested.
After a great deal of experimental research of the inventor, the method is adopted to process more than 5 tons of fresh Damascus roses, and the oil yield of the method in the embodiment 1 is between 0.06 and 0.08 percent. The oil yield of the dry distillation method represented by the Chinese patent CN101536968A is between 0.02 and 0.03 percent.
Claims (3)
1. The rose firming eye cream is characterized by comprising glycerin, propylene glycol fatty acid ester, sodium hyaluronate and rose cellular fluid.
2. The rose tightening eye cream as recited in claim 1, wherein the rose tightening eye cream comprises the following components in parts by mass: 5-10 parts of glycerol, 1-6 parts of propylene glycol fatty acid ester, 1-6 parts of sodium hyaluronate and 20-35 parts of rose cell sap.
3. The preparation method of the rose tightening eye cream is characterized by comprising the following steps:
firstly, preparing rose cellular fluid:
(1) collecting and cleaning Damascus roses: collecting edible Damascus roses in flowering period of 5-6 months, removing perianth, withered rose petals and stamen, and rinsing the petals;
(2) primary acidification of rose: adding 10-20 times of water by weight into rose petals, then adding 3-8 times of organic acid by weight into the water, and acidifying for 0.5-1 h;
(3) primary fermentation of rose petals: taking out the rose petals in the previous step, adding 1-3 times of water by weight, adding 0.03-0.06 part of each of yeast and bacillus subtilis strain, fermenting at 35-40 deg.C for 1-3 h;
(4) enzymolysis of the rose: fishing out the rose petals in the previous step, adding 5-10 times of water by weight, and then adding beta-mannase, cellulase and lysozyme into the water, wherein the unit amount of the enzyme added per kilogram of the rose petals is as follows: 700-900U, 100-200U and 200-300U at 30-40 ℃ for enzymolysis for 0.5-2h, and then inactivating the enzyme; then filtering to obtain rose fermentation supernatant, and reserving the rose fermentation supernatant;
(5) baking the filtered rose petals in an oven at 40-50 deg.C, drying at three-stage temperature, maintaining at 30 deg.C for 2 hr, 38 deg.C for 3-5 hr, and 35 deg.C for 3 hr, collecting condensed steam to obtain condensed water,
(6) mixing the supernatant obtained in the step 4 and the condensed water obtained in the step 5, and filtering impurities to obtain primary rose cell sap;
(7) concentrating the rose cell sap obtained in the step 6 under reduced pressure, and removing 30-50% of water to obtain the rose cell sap;
mixing the two components uniformly
Respectively micronizing glycerol, propylene glycol fatty acid ester and half weight of rose cell sap by using an ultrahigh pressure homogenizer, wherein the homogenizing pressure is 110-130MPa, the homogenizing time is 10-20min, and the particle size distribution of oil drops is 30-80 nm;
adding sodium hyaluronate and the rest rose cell sap, increasing the pressure of a homogenizer to 140MPa, homogenizing for 9-20min, and vacuum refrigerating at 10-200 ℃ for 10-18h to obtain the rose tightening eye cream.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910472580.7A CN112006950A (en) | 2019-05-31 | 2019-05-31 | Rose eye firming cream and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910472580.7A CN112006950A (en) | 2019-05-31 | 2019-05-31 | Rose eye firming cream and preparation method thereof |
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| CN112006950A true CN112006950A (en) | 2020-12-01 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201910472580.7A Pending CN112006950A (en) | 2019-05-31 | 2019-05-31 | Rose eye firming cream and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101536968A (en) * | 2009-04-28 | 2009-09-23 | 济南天源玫瑰制品开发有限公司 | Cellular fluid of fresh flowers of roses and preparation method thereof |
| CN105287283A (en) * | 2015-10-28 | 2016-02-03 | 青岛滨海玫瑰科技发展有限公司 | Fresh rose flower cell sap skin rejuvenation lotion and preparation method thereof |
| CN107904062A (en) * | 2018-01-17 | 2018-04-13 | 山东云中农业开发有限公司 | A kind of preparation method of rose claret |
| CN107904116A (en) * | 2018-01-17 | 2018-04-13 | 山东云中农业开发有限公司 | The preparation method of rose Maotai-flavor liquor |
-
2019
- 2019-05-31 CN CN201910472580.7A patent/CN112006950A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101536968A (en) * | 2009-04-28 | 2009-09-23 | 济南天源玫瑰制品开发有限公司 | Cellular fluid of fresh flowers of roses and preparation method thereof |
| CN105287283A (en) * | 2015-10-28 | 2016-02-03 | 青岛滨海玫瑰科技发展有限公司 | Fresh rose flower cell sap skin rejuvenation lotion and preparation method thereof |
| CN107904062A (en) * | 2018-01-17 | 2018-04-13 | 山东云中农业开发有限公司 | A kind of preparation method of rose claret |
| CN107904116A (en) * | 2018-01-17 | 2018-04-13 | 山东云中农业开发有限公司 | The preparation method of rose Maotai-flavor liquor |
Non-Patent Citations (1)
| Title |
|---|
| 恒基农业开发河北有限公司: "尚养花湾玫瑰沁养紧致眼霜", 《国产非特殊用途化妆品备案信息平台》 * |
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Application publication date: 20201201 |