CN111956565B - Wrinkle-removing whitening and deoiling mask and preparation method thereof - Google Patents
Wrinkle-removing whitening and deoiling mask and preparation method thereof Download PDFInfo
- Publication number
- CN111956565B CN111956565B CN202011044134.5A CN202011044134A CN111956565B CN 111956565 B CN111956565 B CN 111956565B CN 202011044134 A CN202011044134 A CN 202011044134A CN 111956565 B CN111956565 B CN 111956565B
- Authority
- CN
- China
- Prior art keywords
- mask
- base cloth
- dogwood
- mask base
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
- A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
- A61K8/65—Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/81—Preparation or application process involves irradiation
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Dermatology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to a wrinkle-removing whitening and deoiling mask and a preparation method thereof, belonging to the technical field of beauty product preparation. The wrinkle-removing whitening and degreasing mask has the beauty effects of enriching blood, activating blood, promoting qi, nourishing blood and promoting granulation, promotes qi and blood circulation of skin, dissipates pathogenic toxin, achieves the beauty purposes of moisturizing skin, removing wrinkles and whitening, and defending invasion of exogenous pathogenic factors, wherein collagen polypeptide can improve the fat content of skin, so that the skin is slimmer, moist, soft and elastic, and simultaneously has normal breathing and perspiration, various skin problems are relieved, procyanidine, kojic acid and arbutin are high-efficiency free radical scavengers, excellent antioxidation effect can be achieved, whitening effect is increased, grease components secreted in facial pores can be effectively enriched, and excellent degreasing effect is achieved; finally, the facial mask base cloth with excellent adsorptivity is used for adsorbing and immobilizing functional liquid, so that the content of active ingredients in the facial mask is increased, and the beauty effect of the facial mask is improved.
Description
Technical Field
The invention relates to a wrinkle-removing whitening and deoiling mask and a preparation method thereof, belonging to the technical field of beauty product preparation.
Background
The facial mask is one type of skin care product. The principle of the facial mask is to temporarily isolate external air and pollution by using short time covered on the face, improve skin temperature, expand pores of the skin, promote sweat gland secretion and metabolism, increase oxygen content of the skin, facilitate the skin to remove products of metabolism of epidermal cells and accumulated grease substances, and the moisture in the facial mask permeates into the cuticle of the epidermis to soften the skin and make the skin naturally bright and elastic.
The facial mask has effects of cleaning, building body and protecting face. However, the adsorption capacity of the cloth in the mask to each medicine component is poor, so that the content of the medicine components in the mask for protecting the skin is low, and the skin beautifying effect of the mask is limited.
In view of the above-mentioned drawbacks, the present inventors have actively studied and innovated to create a wrinkle-removing, whitening and oil-removing mask and a preparation method thereof, so that the mask has a more industrial value.
Disclosure of Invention
In order to solve the technical problems, the invention aims to provide a wrinkle-removing whitening and oil-removing facial mask and a preparation method thereof.
The embodiment of the invention relates to a wrinkle-removing whitening and deoiling mask, which comprises mask base cloth and functional liquid;
the mask base cloth is prepared by performing spunlaced weaving on sodium alginate viscose fiber and bamboo fiber, and then performing high-temperature high-pressure modification;
the functional liquid comprises the following components in parts by weight:
15-20 parts of dogwood extract;
15-20 parts of collagen polypeptide;
5-8 parts of procyanidine;
8-10 parts of kojic acid;
15-20 parts of arbutin;
60 to 70 parts of sodium chloride solution with the mass fraction of 0.9 percent.
The preparation method of the wrinkle-removing whitening and deoiling mask provided by the embodiment of the invention comprises the following specific preparation steps:
(1) Preparing sodium alginate viscose fiber:
regulating the pH of an aqueous solution of sodium alginate, adding epichlorohydrin, heating, reacting, cooling to obtain a pre-reactant, adding the pre-reactant into viscose, reacting to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose fibers;
(2) Preparing a mask base cloth crude product:
carrying out water jet reinforcement on sodium alginate viscose fiber and bamboo fiber, and drying to obtain a mask base cloth crude product;
(3) Preparing a mask base cloth:
mixing the crude product of the mask base cloth with the citric acid solution, and steaming at high temperature and high pressure to obtain the mask base cloth for later use;
(4) Preparing dry dogwood powder:
taking fresh dogwood fruits, cleaning, freezing, directly transferring into hot water for boiling, taking out, crushing, and drying to obtain dogwood dry powder;
(5) Preparing a dogwood extract:
mixing Corni fructus dry powder and ethanol solution, ultrasonic extracting, filtering, and concentrating the filtrate by rotary evaporation to obtain Corni fructus extract;
(6) Preparation of functional liquid:
weighing Corni fructus extract, collagen polypeptide, procyanidin, kojic acid, arbutin and sodium chloride solution, and stirring and mixing to obtain functional liquid;
(7) Preparation of a wrinkle-removing whitening and deoiling mask:
and soaking the mask base cloth by using the obtained functional liquid, and taking out, sterilizing and disinfecting after the soaking is finished to obtain the wrinkle-removing whitening and deoiling mask.
Further, the specific preparation steps are as follows:
(1) Preparing sodium alginate viscose fiber:
filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, regulating the pH to 8 by using a sodium hydroxide solution, adding epichlorohydrin with the mass fraction of 3% of sodium alginate into the beaker, heating, stirring for reaction, cooling to obtain a pre-reactant, adding the pre-reactant into the viscose according to the mass ratio of sodium alginate to the viscose of 1:25, stirring for reaction for 1-2 h to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose fiber;
(2) Preparing a mask base cloth crude product:
respectively opening and carding the sodium alginate viscose fiber and the bamboo fiber, and then cross-lapping, wherein the paving density is 50g/m 2 Carrying out water jet reinforcement on the laid fiber net, and drying to obtain a mask base cloth crude product;
(3) Preparing a mask base cloth:
mixing the obtained crude product of the mask base cloth with 5% of citric acid solution by mass fraction, and placing into a high-pressure reaction kettle, and steaming at high temperature and high pressure to obtain the mask base cloth for later use;
(4) Preparing dry dogwood powder:
taking mature fresh dogwood fruits, cleaning, freezing, directly transferring into hot water, boiling, taking out, crushing, sieving with a 40-mesh sieve, and drying at 50-60 ℃ for 7-8 hours to obtain dogwood dry powder;
(5) Preparing a dogwood extract:
mixing the obtained dry powder of dogwood and ethanol solution with the mass fraction of 75%, loading into an ultrasonic extractor, performing ultrasonic extraction, filtering the extract, and concentrating the filtrate by rotary evaporation to 10% of the original volume to obtain dogwood extract;
(6) Preparation of functional liquid:
weighing 15-20 parts of dogwood extract, 15-20 parts of collagen polypeptide, 5-8 parts of procyanidine, 8-10 parts of kojic acid, 15-20 parts of arbutin and 60-70 parts of sodium chloride solution with mass fraction of 0.9% according to parts by weight, and stirring and mixing to obtain a functional liquid;
(7) Preparation of a wrinkle-removing whitening and deoiling mask:
and (3) soaking the mask base cloth with the obtained functional liquid, taking out the mask base cloth soaked with the functional liquid after the soaking is finished, and placing the mask base cloth in an ultraviolet disinfection cabinet for sterilization and disinfection to obtain the wrinkle-removing whitening and deoiling mask.
Further, in the step (1), the heating temperature is 70-80 ℃, and the stirring reaction time is 2-3 hours.
Further, in the step (2), the mass ratio of the sodium alginate viscose fiber to the bamboo fiber is 1:3.
Further, in the step (3), the mass ratio of the crude product of the mask base cloth to the citric acid solution with the mass fraction of 5% is 1:10, the pressure of high-temperature high-pressure cooking is 1.5-1.6 Mpa, the temperature of high-temperature high-pressure cooking is 200-300 ℃, and the time of high-temperature high-pressure cooking is 8-10 h.
Further, the temperature of the freezing treatment in the step (4) is-2 ℃, the time of the freezing treatment is 20-25 h, the temperature of the hot water is 70-80 ℃, and the time of boiling in the hot water is 3-5 min.
Further, in the step (5), the mass ratio of the dry dogwood powder to the ethanol solution with the mass fraction of 75% is 1:20, the ultrasonic extraction temperature is 40-50 ℃, the ultrasonic extraction frequency is 45-60 kHz, and the ultrasonic extraction time is 30-40 min.
Further, the time for soaking the mask base cloth in the functional liquid in the step (7) is 24-26 hours.
By adopting the scheme, the invention has at least the following advantages:
the wrinkle-removing whitening and degreasing mask has the beauty effects of enriching blood, activating blood, promoting qi, nourishing blood and promoting granulation, promotes qi and blood circulation of skin, dissipates pathogenic toxin, achieves the beauty purposes of moisturizing skin, removing wrinkles and whitening, and defending invasion of exogenous pathogenic factors, wherein collagen polypeptide can improve the fat content of skin, so that the skin is slimmer, moist, soft and elastic, and simultaneously has normal breathing and perspiration, various skin problems are relieved, procyanidine, kojic acid and arbutin are high-efficiency free radical scavengers, excellent antioxidation effect can be achieved, whitening effect is increased, grease components secreted in facial pores can be effectively enriched, and excellent degreasing effect is achieved; finally, the mask base cloth with excellent adsorptivity is used for adsorbing and immobilizing functional liquid, so that the content of active ingredients in the mask is increased, and the beautifying effect of the mask is improved.
The foregoing description is only an overview of the present invention, and is intended to provide a more thorough understanding of the present invention, and is to be accorded the full scope of the present invention.
Detailed Description
The following describes the embodiments of the present invention in further detail with reference to examples. The following examples are illustrative of the invention and are not intended to limit the scope of the invention.
(1) Filling sodium alginate aqueous solution with mass fraction of 3% into a beaker, regulating pH to 8 with sodium hydroxide solution, adding epichlorohydrin with mass fraction of 3% of sodium alginate into the beaker, heating to 70-80 ℃, stirring for reaction for 2-3 h, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to mass ratio of sodium alginate to viscose of 1:25, stirring for reaction for 1-2 h to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose fiber; firstly, preparing alginate fiber with excellent skin affinity through wet spinning, and improving the skin affinity of the mask;
(2) Opening and carding the sodium alginate viscose fiber and the bamboo fiber respectively according to the mass ratio of 1:3, and then cross-lapping, wherein the pavement density is 50g/m 2 Carrying out water jet reinforcement on the laid fiber net, and drying to obtain a mask base cloth crude product; weaving a composite mask base cloth crude product by taking alginate and bamboo fibers as raw materials through water needling;
(3) The obtained crude product of the mask base cloth and citric acid solution with the mass fraction of 5% are mixed according to the mass ratio of 1:10, after mixing, placing the mixture into a high-pressure reaction kettle, increasing the pressure in the reaction kettle to 1.5-1.6 Mpa, increasing the temperature to 200-300 ℃, and steaming at high temperature and high pressure for 8-10 h, thus obtaining the mask base cloth for later use; mixing a crude product of the composite mask base cloth with organic acid, and then carrying out high-temperature high-pressure treatment, wherein the organic acid is used as a catalyst, so that part of cellulose in bamboo fibers is hydrolyzed, and the hydrolysis leads to furfural production, the produced furfural is further polycondensated under the conditions of high temperature and high pressure to form a furfural polymer, so that the mask base cloth is partially resinated, the produced furfural resin polymer has viscosity, the mask base cloth can absorb mask functional liquid components more easily, the content of active ingredients in the mask is increased, the beautifying effect of the mask is improved, and the formed furfural resin polymer is hydrophobic and oleophilic and is matched with the porous structure of the water-jet base cloth, so that grease components secreted in facial pores can be effectively enriched, and the facial mask has excellent deoiling effect;
(4) Taking mature fresh dogwood fruits, cleaning the fresh dogwood fruits, freezing the fresh dogwood fruits at the temperature of minus 2 ℃ for 20 to 25 hours, directly transferring the fresh dogwood fruits into hot water at the temperature of 70 to 80 ℃ for boiling for 3 to 5 minutes, taking out the fresh dogwood fruits, crushing the fresh dogwood fruits, sieving the crushed dogwood fruits by a 40-mesh sieve, and drying the crushed dogwood fruits at the temperature of 50 to 60 ℃ for 7 to 8 hours to obtain dry dogwood powder; the double treatment of freezing and hot boiling leads the tissue structure of the dogwood to be destroyed, is beneficial to the dissolution of the internal effective components and facilitates the subsequent extraction;
(5) Mixing the obtained dry powder of dogwood and an ethanol solution with the mass fraction of 75% according to the mass ratio of 1:20, then loading the mixture into an ultrasonic extractor, carrying out ultrasonic extraction at the frequency of 45-60 kHz for 30-40 min at the temperature of 40-50 ℃, filtering the extract, and carrying out rotary evaporation concentration on the filtrate until the volume of the filtrate is 10% of that of the original product to obtain the dogwood extract; the ethanol solution is used as an inorganic solvent, the ursolic acid in the dogwood is extracted through ultrasonic assistance, the ursolic acid can promote the activation and renewal of epidermal cells, reduce the coagulation force among keratinocytes, enable aged cells to fall off smoothly, avoid abnormal cutin accumulation, increase the moisturizing capability of skin, prevent hair follicle openings from being blocked, facilitate smooth discharge of sebum, promote the degreasing of a mask, simultaneously promote the smoothness of hair follicles, facilitate active ingredients in functional liquid of the mask to permeate into the skin, and enhance the beautifying effect;
(6) Weighing 15-20 parts of dogwood extract, 15-20 parts of collagen polypeptide, 5-8 parts of procyanidine, 8-10 parts of kojic acid, 15-20 parts of arbutin and 60-70 parts of sodium chloride solution with mass fraction of 0.9% according to parts by weight, and stirring and mixing to obtain a functional liquid; the cornel extract is utilized in the functional liquid to remove cutin, on one hand, the degreasing effect is enhanced, on the other hand, the whitening effect is improved, the collagen polypeptide can improve the fat content of skin, so that the skin is smoother, moist, soft and elastic, and meanwhile, the skin breathes and sweats are normal, various skin problems are relieved, the effects of whitening and removing wrinkles are achieved, in addition, procyanidine, kojic acid and arbutin have excellent whitening effects, physiological saline with the concentration of 0.9% is used, and the skin is more skin-friendly, so that the skin absorption is facilitated, and the beautifying effect is further improved;
(7) Soaking the mask base cloth for 24-26 h by using the obtained functional liquid, taking out the mask base cloth soaked with the functional liquid after soaking, and sterilizing and disinfecting in an ultraviolet sterilizing cabinet to obtain the wrinkle-removing whitening and deoiling mask. Finally, the facial mask base cloth with excellent adsorptivity is used for adsorbing and immobilizing functional liquid, so that the content of active ingredients in the facial mask is increased, and the beauty effect of the facial mask is improved.
Example 1
Filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, regulating the pH to 8 by using a sodium hydroxide solution, adding epichlorohydrin with the mass fraction of 3% of sodium alginate into the beaker, heating to 70 ℃, stirring and reacting for 2 hours, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to the mass ratio of sodium alginate to viscose of 1:25, stirring and reacting for 1 hour to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose fiber; opening and carding the sodium alginate viscose fiber and the bamboo fiber respectively according to the mass ratio of 1:3, and then cross-lapping, wherein the pavement density is 50g/m 2 Carrying out water jet reinforcement on the laid fiber net, and drying to obtain a mask base cloth crude product; the obtained crude product of the mask base cloth and citric acid solution with the mass fraction of 5% are mixed according to the mass ratio of 1:10, mixing, placing into a high-pressure reaction kettle, increasing the pressure in the reaction kettle to 1.5Mpa, increasing the temperature to 200 ℃, and steaming at high temperature and high pressure for 8 hours, thus obtaining the mask base cloth for later use; taking mature fresh dogwood fruits, cleaning, freezing at-2 ℃ for 20 hours, directly transferring into 70 ℃ hot water, boiling for 3 minutes, taking out, crushing, sieving with a 40-mesh sieve, and drying at 50 ℃ for 7 hours to obtain dogwood dry powder; mixing the obtained dry powder of dogwood and ethanol solution with the mass fraction of 75% according to the mass ratio of 1:20, then loading into an ultrasonic extractor, carrying out ultrasonic extraction at the frequency of 45kHz for 30min at the temperature of 40 ℃, filtering the extract, and carrying out rotary evaporation concentration on the filtrate to 10% of the original volume to obtain the dogwood extract; weighing 15 parts of dogwood extract, 15 parts of collagen polypeptide, 5 parts of procyanidine, 8 parts of kojic acid, 15 parts of arbutin and 60 parts of sodium chloride solution with the mass fraction of 0.9% according to parts by weight, and stirring and mixing to obtain a functional liquid; and soaking the mask base cloth for 24 hours by using the obtained functional liquid, taking out the mask base cloth soaked with the functional liquid after soaking, and placing the mask base cloth in an ultraviolet disinfection cabinet for sterilization and disinfection to obtain the wrinkle-removing whitening and deoiling mask.
Example 2
Filling 3% sodium alginate aqueous solution into a beaker, regulating the pH to 8 with sodium hydroxide solution, adding 3% epichlorohydrin of sodium alginate into the beaker, heating to 72 ℃,stirring and reacting for 2 hours, cooling to obtain a pre-reactant, adding the pre-reactant into the viscose according to the mass ratio of sodium alginate to the viscose of 1:25, stirring and reacting for 1 hour to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose fiber; opening and carding the sodium alginate viscose fiber and the bamboo fiber respectively according to the mass ratio of 1:3, and then cross-lapping, wherein the pavement density is 50g/m 2 Carrying out water jet reinforcement on the laid fiber net, and drying to obtain a mask base cloth crude product; the obtained crude product of the mask base cloth and citric acid solution with the mass fraction of 5% are mixed according to the mass ratio of 1:10, mixing, placing into a high-pressure reaction kettle, increasing the pressure in the reaction kettle to 1.5Mpa, increasing the temperature to 220 ℃, and steaming at high temperature and high pressure for 8 hours, thus obtaining the mask base cloth for later use; taking mature fresh dogwood fruits, cleaning, freezing at-2 ℃ for 21 hours, directly transferring into 71 ℃ hot water, boiling for 3 minutes, taking out, crushing, sieving with a 40-mesh sieve, and drying at 51 ℃ for 7 hours to obtain dogwood dry powder; mixing the obtained dry powder of dogwood and ethanol solution with the mass fraction of 75% according to the mass ratio of 1:20, then loading into an ultrasonic extractor, carrying out ultrasonic extraction at the frequency of 45kHz for 31min at the temperature of 41 ℃, filtering the extract, and carrying out rotary evaporation concentration on the filtrate to 10% of the original volume to obtain the dogwood extract; weighing 16 parts of dogwood extract, 16 parts of collagen polypeptide, 5 parts of procyanidine, 8 parts of kojic acid, 16 parts of arbutin and 62 parts of sodium chloride solution with the mass fraction of 0.9% according to parts by weight, and stirring and mixing to obtain a functional liquid; and soaking the mask base cloth for 24 hours by using the obtained functional liquid, taking out the mask base cloth soaked with the functional liquid after soaking, and placing the mask base cloth in an ultraviolet disinfection cabinet for sterilization and disinfection to obtain the wrinkle-removing whitening and deoiling mask.
Example 3
Filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, regulating the pH to 8 by using a sodium hydroxide solution, adding epichlorohydrin with the mass fraction of 3% of sodium alginate into the beaker, heating to 75 ℃, stirring and reacting for 2 hours, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to the mass ratio of sodium alginate to viscose of 1:25, stirring and reacting for 1 hour to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose fiber; according to mass ratioOpening and carding the sodium alginate viscose fiber and the bamboo fiber respectively at a ratio of 1:3, and then cross-lapping, wherein the pavement density is 50g/m 2 Carrying out water jet reinforcement on the laid fiber net, and drying to obtain a mask base cloth crude product; the obtained crude product of the mask base cloth and citric acid solution with the mass fraction of 5% are mixed according to the mass ratio of 1:10, mixing, placing into a high-pressure reaction kettle, increasing the pressure in the reaction kettle to 1.5Mpa, increasing the temperature to 250 ℃, and steaming at high temperature and high pressure for 8 hours, thus obtaining the mask base cloth for later use; taking mature fresh dogwood fruits, cleaning, freezing at-2 ℃ for 23 hours, directly transferring into hot water at 75 ℃ for boiling for 3 minutes, taking out, crushing, sieving with a 40-mesh sieve, and drying at 55 ℃ for 7 hours to obtain dogwood dry powder; mixing the obtained dry powder of dogwood and ethanol solution with the mass fraction of 75% according to the mass ratio of 1:20, then loading into an ultrasonic extractor, carrying out ultrasonic extraction at the frequency of 50kHz for 35min at 45 ℃, filtering the extract, and carrying out rotary evaporation concentration on the filtrate to 10% of the original volume to obtain the dogwood extract; weighing 18 parts of dogwood extract, 18 parts of collagen polypeptide, 7 parts of procyanidine, 9 parts of kojic acid, 18 parts of arbutin and 65 parts of sodium chloride solution with the mass fraction of 0.9% according to parts by weight, and stirring and mixing to obtain a functional liquid; and soaking the mask base cloth for 25 hours by using the obtained functional liquid, taking out the mask base cloth soaked with the functional liquid after soaking, and placing the mask base cloth in an ultraviolet disinfection cabinet for sterilization and disinfection to obtain the wrinkle-removing whitening and deoiling mask.
Example 4
Filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, regulating the pH to 8 by using a sodium hydroxide solution, adding epichlorohydrin with the mass fraction of 3% of sodium alginate into the beaker, heating to 78 ℃, stirring for reaction for 3 hours, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to the mass ratio of sodium alginate to viscose being 1:25, stirring for reaction for 2 hours to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose fiber; opening and carding the sodium alginate viscose fiber and the bamboo fiber respectively according to the mass ratio of 1:3, and then cross-lapping, wherein the pavement density is 50g/m 2 Carrying out water jet reinforcement on the laid fiber net, and drying to obtain a mask base cloth crude product; will be put onThe obtained mask base cloth crude product and 5% citric acid solution are mixed according to the mass ratio of 1:10, mixing, placing into a high-pressure reaction kettle, increasing the pressure in the reaction kettle to 1.6Mpa, increasing the temperature to 280 ℃, and steaming at high temperature and high pressure for 9 hours to obtain a mask base fabric for later use; taking mature fresh dogwood fruits, cleaning, freezing at-2 ℃ for 24 hours, directly transferring into 78 ℃ hot water, boiling for 5 minutes, taking out, crushing, sieving with a 40-mesh sieve, and drying at 58 ℃ for 8 hours to obtain dogwood dry powder; mixing the obtained dry powder of dogwood and ethanol solution with the mass fraction of 75% according to the mass ratio of 1:20, then loading into an ultrasonic extractor, carrying out ultrasonic extraction at 48 ℃ and 48kHz frequency for 38min, filtering the extract, and carrying out rotary evaporation concentration on the filtrate to 10% of the original volume to obtain dogwood extract; weighing 18 parts of dogwood extract, 19 parts of collagen polypeptide, 7 parts of procyanidine, 9 parts of kojic acid, 19 parts of arbutin and 68 parts of sodium chloride solution with mass fraction of 0.9% according to parts by weight, and stirring and mixing to obtain a functional liquid; and soaking the mask base cloth for 25 hours by using the obtained functional liquid, taking out the mask base cloth soaked with the functional liquid after soaking, and placing the mask base cloth in an ultraviolet disinfection cabinet for sterilization and disinfection to obtain the wrinkle-removing whitening and deoiling mask.
Example 5
Filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, regulating the pH to 8 by using a sodium hydroxide solution, adding epichlorohydrin with the mass fraction of 3% of sodium alginate into the beaker, heating to 80 ℃, stirring for reaction for 3 hours, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to the mass ratio of sodium alginate to viscose being 1:25, stirring for reaction for 2 hours to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose fiber; opening and carding the sodium alginate viscose fiber and the bamboo fiber respectively according to the mass ratio of 1:3, and then cross-lapping, wherein the pavement density is 50g/m 2 Carrying out water jet reinforcement on the laid fiber net, and drying to obtain a mask base cloth crude product; the obtained crude product of the mask base cloth and citric acid solution with the mass fraction of 5% are mixed according to the mass ratio of 1:10, then placing the mixture into a high-pressure reaction kettle, increasing the pressure in the reaction kettle to 1.6Mpa, increasing the temperature to 300 ℃, steaming at high temperature and high pressure for 10 hours, after steaming is finished,obtaining the mask base cloth for standby; taking mature fresh dogwood fruits, cleaning, freezing at-2 ℃ for 25 hours, directly transferring into 80 ℃ hot water, boiling for 5 minutes, taking out, crushing, sieving with a 40-mesh sieve, and drying at 60 ℃ for 8 hours to obtain dogwood dry powder; mixing the obtained dry powder of dogwood and ethanol solution with the mass fraction of 75% according to the mass ratio of 1:20, then loading into an ultrasonic extractor, carrying out ultrasonic extraction at the frequency of 60kHz for 40min at 50 ℃, filtering the extract, and carrying out rotary evaporation concentration on the filtrate to 10% of the original volume to obtain the dogwood extract; weighing 20 parts of dogwood extract, 20 parts of collagen polypeptide, 8 parts of procyanidine, 10 parts of kojic acid, 20 parts of arbutin and 70 parts of sodium chloride solution with the mass fraction of 0.9% according to parts by weight, and stirring and mixing to obtain a functional liquid; and (3) soaking the mask base cloth for 26 hours by using the obtained functional liquid, taking out the mask base cloth soaked with the functional liquid after the soaking is finished, and placing the mask base cloth in an ultraviolet disinfection cabinet for sterilization and disinfection to obtain the wrinkle-removing whitening and deoiling mask.
Comparative example 1: the preparation method is basically the same as that of the example 1, except that the crude product of the mask base cloth is directly used for replacing the mask base cloth, and the mask is also prepared;
comparative example 2: the preparation method is basically the same as that of the example 1, except that the common non-woven fabric is directly used for replacing the mask base fabric, and the mask is also prepared;
comparative example 3: the preparation method is basically the same as that of the example 1, except that the dogwood extract of the invention is not added, and the mask is also prepared;
performance tests were performed on the wrinkle-removing, whitening and degreasing masks in examples 1 to 5, and the test results are shown in table 1:
the detection method comprises the following steps:
the detection method for the crease-resistant whitening and degreasing performance comprises the following steps:
160 testers were selected, aged 28-50 years, randomly divided into 8 groups of 20 individuals each, and statistically treated groups had no significant difference in skin condition. The skin states of a tester before and after the test are tested by using a face image analyzer VISIA-CR and a multifunctional skin tester CK-MPA10, the test is repeated for 3 times each time, and an average value is taken to obtain data of the skin elasticity improvement rate, the wrinkle reduction rate, the moisture improvement rate, the pigment index reduction rate and the facial fat reduction rate; the mask produced in trial example 1 of group 1, the mask produced in trial example 2 of group 2, the mask produced in trial example 3 of group 3, the mask produced in trial example 4 of group 4, the mask produced in trial example 5 of group 5, the mask produced in trial comparative example 1 of group 6, the mask produced in trial comparative example 2 of group 7, the mask produced in comparative example 3 of group 8; the trial method comprises the following steps: after the face is cleaned by clean water, the face is smeared once every 2 days, 5 g is smeared at 10 points each time for 28 days, the average value of 20 tester data in each group is taken as the trial result data of each group, and the result is shown in table 1.
TABLE 1 Performance test results
As can be seen from the detection data in the above table, in comparative example 1, the crude mask base cloth is directly used to replace the mask base cloth, so that the skin elasticity improvement rate, the wrinkle reduction rate, the moisture improvement rate, the pigment index reduction rate and the facial grease reduction rate are all significantly reduced, therefore, according to the invention, after the crude composite mask base cloth is mixed with the organic acid, the high-temperature and high-pressure treatment is performed, the organic acid is used as a catalyst, so that part of cellulose in the bamboo fiber is hydrolyzed, the hydrolysis results in furfural, the generated furfural is further condensed under the high-temperature and high-pressure condition to form a furfural polymer, so that part of the mask base cloth is resinated, the generated furfural resin polymer has viscosity, the mask base cloth is easier to adsorb functional liquid components of the mask, the content of active ingredients in the mask is increased, the beautifying effect of the mask is improved, and the formed furfural resin polymer is hydrophobic and oleophilic, and the porous structure of the water-jet base cloth is matched, so that grease components secreted in the face pores can be effectively enriched, and the degreasing effect is excellent;
in comparative example 2, the mask base cloth is directly replaced by the common non-woven fabric, so that the skin elasticity improvement rate, the wrinkle reduction rate, the moisture improvement rate, the pigment index reduction rate and the facial grease reduction rate are all remarkably reduced, and are lower than those in comparative example 1, and therefore, the performance of the composite mask base cloth woven by using alginate and bamboo fibers as raw materials through water needling is more excellent than that of the non-woven fabric, and the performance of the composite mask base cloth is remarkably enhanced after high-temperature and high-pressure steaming;
comparative example 3, since the cornel extract of the present invention was not added, the skin elasticity improvement rate, wrinkle reduction rate, moisture improvement rate, pigment index reduction rate and facial fat reduction rate were all significantly reduced, and thus it can be seen that the present invention uses an ethanol solution as an inorganic solvent, extracts ursolic acid components in cornel with the assistance of ultrasound, and ursolic acid can promote the activation and renewal of epidermal facial cells, reduce the coagulation force between keratinocytes, and enable aged cells to fall off smoothly, avoid abnormal cutin accumulation, increase the moisturizing ability of skin, and prevent hair follicle openings from being blocked, facilitate smooth discharge of sebum, promote degreasing of facial mask, and simultaneously the smoothness of hair follicle is favorable for penetration of active ingredients in facial mask functional liquid into skin, enhancing beauty effect, and has a wide application prospect.
The above description is only of the preferred embodiments of the present invention and is not intended to limit the present invention, and it should be noted that it is possible for those skilled in the art to make several improvements and modifications without departing from the technical principle of the present invention, and these improvements and modifications should also be regarded as the protection scope of the present invention.
Claims (5)
1. A wrinkle-removing whitening and deoiling mask is characterized in that: comprises a facial mask base cloth and functional liquid;
the mask base cloth is prepared by performing spunlaced weaving on sodium alginate viscose fiber and bamboo fiber, and then performing high-temperature high-pressure modification;
the functional liquid comprises the following components in parts by weight:
15-20 parts of dogwood extract;
15-20 parts of collagen polypeptide;
5-8 parts of procyanidine;
8-10 parts of kojic acid;
15-20 parts of arbutin;
60 to 70 parts of sodium chloride solution with mass fraction of 0.9%;
the mass ratio of the sodium alginate viscose fiber to the bamboo fiber is 1:3;
the high-temperature high-pressure modification specifically comprises the following steps of: 10, mixing the coarse mask base cloth product woven by the water jet weaving and a citric acid solution with the mass fraction of 5%, and steaming at high temperature and high pressure for 8-10 h under the conditions that the pressure is 1.5-1.6 MPa and the temperature is 200-300 ℃;
the preparation method of the dogwood extract comprises the steps of taking fresh dogwood fruits, cleaning, freezing, directly transferring into hot water, boiling, taking out, crushing, drying to obtain dogwood dry powder, wherein the freezing temperature is-2 ℃, the freezing time is 20-25 h, the hot water temperature is 70-80 ℃, and the boiling time in hot water is 3-5 min; mixing the dry dogwood powder with the mass ratio of 1:20 and ethanol solution with the mass fraction of 75%, performing ultrasonic extraction for 30-40 min at the temperature of 40-50 ℃ and the frequency of 45-60 kHz, filtering, and performing rotary evaporation concentration on the filtrate to obtain the dogwood extract.
2. A method for preparing the wrinkle-removing, whitening and deoiling mask as claimed in claim 1, which is characterized in that: the preparation method comprises the following specific preparation steps:
(1) Preparing sodium alginate viscose fiber:
regulating the pH of an aqueous solution of sodium alginate, adding epichlorohydrin, heating, reacting, cooling to obtain a pre-reactant, adding the pre-reactant into viscose, reacting to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose fibers;
(2) Preparing a mask base cloth crude product:
carrying out water jet reinforcement on sodium alginate viscose fiber and bamboo fiber in a mass ratio of 1:3, and drying to obtain a mask base cloth crude product;
(3) Preparing a mask base cloth:
the mass ratio is 1:10, mixing the coarse product of the mask base cloth woven by the water jet weaving method with a citric acid solution with the mass fraction of 5%, and steaming at high temperature and high pressure for 8-10 hours under the conditions of the pressure of 1.5-1.6 MPa and the temperature of 200-300 ℃ to obtain the mask base cloth for later use;
(4) Preparing dry dogwood powder:
taking fresh dogwood fruits, cleaning, freezing, directly transferring into hot water, boiling, taking out, crushing, and drying to obtain dogwood dry powder, wherein the temperature of freezing is-2 ℃, the time of freezing is 20-25 h, the temperature of hot water is 70-80 ℃, and the boiling time in hot water is 3-5 min;
(5) Preparing a dogwood extract:
mixing dogwood dry powder with the mass ratio of 1:20 and ethanol solution with the mass fraction of 75%, performing ultrasonic extraction for 30-40 min at the temperature of 40-50 ℃ and the frequency of 45-60 kHz, filtering, and performing rotary evaporation concentration on the filtrate to obtain dogwood extract;
(6) Preparation of functional liquid:
weighing Corni fructus extract, collagen polypeptide, procyanidin, kojic acid, arbutin and sodium chloride solution, and stirring and mixing to obtain functional liquid;
(7) Preparation of a wrinkle-removing whitening and deoiling mask:
and soaking the mask base cloth by using the obtained functional liquid, and taking out, sterilizing and disinfecting after the soaking is finished to obtain the wrinkle-removing whitening and deoiling mask.
3. The method for preparing the wrinkle-removing, whitening and deoiling mask according to claim 2, wherein the method comprises the following steps: the preparation method comprises the following specific preparation steps:
(1) Preparing sodium alginate viscose fiber:
filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, regulating the pH to 8 by using a sodium hydroxide solution, adding epichlorohydrin with the mass fraction of 3% of sodium alginate into the beaker, heating, stirring for reaction, cooling to obtain a pre-reactant, adding the pre-reactant into the viscose according to the mass ratio of sodium alginate to the viscose of 1:25, stirring for reaction for 1-2 h to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose fiber;
(2) Preparing a mask base cloth crude product:
mixing the sodium alginate viscose fiber and bamboo fiberOpening and carding respectively, and then cross-lapping, wherein the laying density is 50g/m 2 Carrying out water jet reinforcement on the laid fiber net, and drying to obtain a mask base cloth crude product;
(3) Preparing a mask base cloth:
the mass ratio is 1:10, mixing the coarse product of the mask base cloth woven by the water jet weaving method with a citric acid solution with the mass fraction of 5%, and steaming at high temperature and high pressure for 8-10 hours under the conditions of the pressure of 1.5-1.6 MPa and the temperature of 200-300 ℃ to obtain the mask base cloth for later use;
(4) Preparing dry dogwood powder:
taking fresh dogwood fruits, cleaning, freezing, directly transferring into hot water, boiling, taking out, crushing, sieving with a 40-mesh sieve, drying at 50-60 ℃ for 7-8 hours to obtain dogwood dry powder, wherein the freezing temperature is-2 ℃, the freezing time is 20-25 hours, the hot water temperature is 70-80 ℃, and the boiling time in hot water is 3-5 minutes;
(5) Preparing a dogwood extract:
mixing dry dogwood powder with the mass ratio of 1:20 and ethanol solution with the mass fraction of 75%, performing ultrasonic extraction for 30-40 min at the temperature of 40-50 ℃ and the frequency of 45-60 kHz, filtering, and performing rotary evaporation concentration on the filtrate to 10% of the original volume to obtain dogwood extract;
(6) Preparation of functional liquid:
weighing 15-20 parts of dogwood extract, 15-20 parts of collagen polypeptide, 5-8 parts of procyanidine, 8-10 parts of kojic acid, 15-20 parts of arbutin and 60-70 parts of sodium chloride solution with mass fraction of 0.9% according to parts by weight, and stirring and mixing to obtain a functional liquid;
(7) Preparation of a wrinkle-removing whitening and deoiling mask:
and (3) soaking the mask base cloth with the obtained functional liquid, taking out the mask base cloth soaked with the functional liquid after the soaking is finished, and placing the mask base cloth in an ultraviolet disinfection cabinet for sterilization and disinfection to obtain the wrinkle-removing whitening and deoiling mask.
4. The method for preparing the wrinkle-removing, whitening and deoiling mask according to claim 3, wherein the method comprises the following steps: the heating temperature in the step (1) is 70-80 ℃, and the stirring reaction time is 2-3 h.
5. The method for preparing the wrinkle-removing, whitening and deoiling mask according to claim 3, wherein the method comprises the following steps: the time for soaking the mask base cloth in the functional liquid in the step (7) is 24-26 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011044134.5A CN111956565B (en) | 2020-09-29 | 2020-09-29 | Wrinkle-removing whitening and deoiling mask and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202011044134.5A CN111956565B (en) | 2020-09-29 | 2020-09-29 | Wrinkle-removing whitening and deoiling mask and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN111956565A CN111956565A (en) | 2020-11-20 |
| CN111956565B true CN111956565B (en) | 2023-10-03 |
Family
ID=73387578
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202011044134.5A Active CN111956565B (en) | 2020-09-29 | 2020-09-29 | Wrinkle-removing whitening and deoiling mask and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN111956565B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114588086A (en) * | 2022-03-17 | 2022-06-07 | 广州无添加主义化妆品有限公司 | High-temperature-resistant milky-white mask body without demulsification |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104337738A (en) * | 2014-11-14 | 2015-02-11 | 刘芳 | Composition of dogwood extracts for skin wrinkle resisting and preparation method thereof |
| CN108166157A (en) * | 2017-12-25 | 2018-06-15 | 合肥洁诺无纺布制品有限公司 | Antibacterial spunlace non-woven cloth beauty mask base fabric of a kind of moisture absorption and preparation method thereof |
| CN111560708A (en) * | 2020-04-08 | 2020-08-21 | 青岛大学 | Water-absorbent gelling spunlace fabric containing alginate fibers and preparation method and application thereof |
| CN111658574A (en) * | 2020-06-12 | 2020-09-15 | 青岛大学 | Dry sheet type facial mask containing active essence and preparation method thereof |
-
2020
- 2020-09-29 CN CN202011044134.5A patent/CN111956565B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104337738A (en) * | 2014-11-14 | 2015-02-11 | 刘芳 | Composition of dogwood extracts for skin wrinkle resisting and preparation method thereof |
| CN108166157A (en) * | 2017-12-25 | 2018-06-15 | 合肥洁诺无纺布制品有限公司 | Antibacterial spunlace non-woven cloth beauty mask base fabric of a kind of moisture absorption and preparation method thereof |
| CN111560708A (en) * | 2020-04-08 | 2020-08-21 | 青岛大学 | Water-absorbent gelling spunlace fabric containing alginate fibers and preparation method and application thereof |
| CN111658574A (en) * | 2020-06-12 | 2020-09-15 | 青岛大学 | Dry sheet type facial mask containing active essence and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN111956565A (en) | 2020-11-20 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106963692B (en) | A cosmetic composition containing Fucus vesiculosus extract | |
| CN104825351B (en) | A kind of Lignum Aquilariae Resinatum whitening cleansing facial milk containing and preparation method thereof | |
| CN104971031A (en) | Skin regenerating repair and anti-aging mask for electromagnetic radiation and fog-haze pollution | |
| CN107536798A (en) | A kind of female sex organ care compositions | |
| CN111956565B (en) | Wrinkle-removing whitening and deoiling mask and preparation method thereof | |
| CN107802543A (en) | A kind of shining skin Biofibre facial mask of Rosa roxburghii element and preparation method thereof | |
| CN108743431A (en) | A kind of small-molecular peptides facial mask of anti-ageing beauty treatment and preparation method thereof | |
| CN109394612A (en) | Facial mask and preparation method thereof is repaired in a kind of moisturizing | |
| CN110302064B (en) | Whitening and moisturizing essence and whitening and moisturizing mask prepared from same | |
| CN108175741A (en) | A kind of anti-aging beauty-care frost and preparation method thereof | |
| CN112190529B (en) | Sheep casing collagen powder and application thereof in preparation of anti-aging skin care product | |
| CN112501784B (en) | Preparation method of antioxidant skin-friendly composite fiber spunlace nonwoven mask cloth | |
| CN107890455A (en) | A kind of preparation method of the reparation anti-wrinkle facial mask liquid containing snail mucus and sodium hyaluronate | |
| CN104887602A (en) | Jasmine hair and face cleaning liquid | |
| CN112618430A (en) | Camellia procyanidine mask and preparation method thereof | |
| CN107375154A (en) | A kind of nti-freckle white composition and preparation method thereof only | |
| CN110859758A (en) | Whitening anti-aging repair type medical cold compress patch and preparation method thereof | |
| CN110339108A (en) | A kind of moisturizing efficiently adjusts the facial mask liquid and preparation method thereof of sebum secretion amount | |
| CN108403558A (en) | A kind of dendrobium candidum mask product | |
| KR102110323B1 (en) | Cosmetic composition for reducing inflammation in skin and enhancing skin moisture, and a mask pack using the same | |
| CN115089532A (en) | Anti-aging cosmetic and preparation method thereof | |
| CN112716863A (en) | Graphene rose essence facial mask and preparation method thereof | |
| CN111759768A (en) | Whitening and cutin removing toner and preparation method thereof | |
| KR20010090063A (en) | Mud omitted | |
| CN110123716A (en) | A kind of preparation method of the compound acne-expelling face pack liquid of pericarp and its method for processing facial mask |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| TA01 | Transfer of patent application right | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20230907 Address after: 7th Floor, Building 1, No. 517 Shuangfeng Road, Fotang Town, Yiwu City, Jinhua City, Zhejiang Province, 321000 (self declared) Applicant after: Zhejiang Ousijie Biotechnology Co.,Ltd. Address before: 210046 no.18-f1992, Yinchun Road, science and technology R & D base, Maigaoqiao Pioneer Park, Qixia District, Nanjing City, Jiangsu Province Applicant before: Nanjing Feitian Yimiao Technology Service Co.,Ltd. |
|
| GR01 | Patent grant | ||
| GR01 | Patent grant |