CN111956565A - Wrinkle-removing, skin-whitening and oil-removing mask and preparation method thereof - Google Patents
Wrinkle-removing, skin-whitening and oil-removing mask and preparation method thereof Download PDFInfo
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- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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Abstract
The invention relates to a wrinkle-removing, whitening and oil-removing mask and a preparation method thereof, belonging to the technical field of preparation of beauty products. The wrinkle-removing, whitening and deoiling mask disclosed by the invention has the beautifying effects of enriching blood, activating blood, promoting qi circulation, nourishing blood and promoting tissue regeneration, can promote qi and blood circulation of skin, dispel pathogenic toxins, and achieve the beautifying purposes of moistening skin, removing wrinkles, whitening and defending exogenous pathogenic factors, wherein the collagen polypeptide can improve the skin fat content, so that the skin is smoother, moistened, soft and elastic, meanwhile, the skin can breathe and sweat normally, and various skin problems are alleviated; finally, the facial mask base cloth with excellent adsorbability is used for adsorbing the solid-carrying functional liquid, so that the content of effective components in the facial mask is increased, and the beautifying effect of the facial mask is improved.
Description
Technical Field
The invention relates to a wrinkle-removing, whitening and oil-removing mask and a preparation method thereof, belonging to the technical field of preparation of beauty products.
Background
Facial masks, one category of skin care products. The most important purpose is to make up the cleaning work that makeup removal and face washing are still insufficient, and other maintenance functions such as water replenishing and moisture preserving, whitening, anti-aging, grease balancing and the like are realized by matching with other essential components on the basis.
The facial mask has effects of cleaning, building body and protecting face. However, the adsorption capacity of the cloth in the mask to each medicinal component is poor, so that the content of the medicinal components playing a role in protecting the skin in the mask is low, and the skin beautifying effect of the mask is limited.
In view of the above defects, the designer actively makes research and innovation to create a wrinkle-removing, whitening and oil-removing facial mask and a preparation method thereof, so that the facial mask has industrial utilization value.
Disclosure of Invention
In order to solve the technical problems, the invention aims to provide a wrinkle-removing, skin-whitening and oil-removing mask and a preparation method thereof.
The wrinkle-removing, whitening and oil-removing mask comprises mask base cloth and functional liquid;
the mask base fabric is prepared by carrying out spunlace weaving on sodium alginate viscose fibers and bamboo fibers and then carrying out high-temperature and high-pressure modification;
the functional liquid comprises the following components in parts by weight:
15-20 parts of dogwood extract;
15-20 parts of collagen polypeptide;
5-8 parts of procyanidine;
8-10 parts of kojic acid;
15-20 parts of arbutin;
60-70 parts of 0.9 mass percent sodium chloride solution.
The preparation method of the wrinkle-removing, whitening and oil-removing mask provided by the embodiment of the invention comprises the following specific preparation steps:
(1) preparing sodium alginate viscose fiber:
adjusting the pH value of a sodium alginate aqueous solution, adding epoxy chloropropane, heating, reacting, cooling to obtain a pre-reactant, adding the pre-reactant into viscose, reacting to obtain a mixture, and performing wet spinning on the mixture to obtain sodium alginate viscose;
(2) preparing a crude product of the mask base cloth:
carrying out spunlace reinforcement on sodium alginate viscose fibers and bamboo fibers, and drying to obtain a crude product of the mask base fabric;
(3) preparing a mask base cloth:
mixing the crude product of the mask base cloth with citric acid solution, and steaming at high temperature and high pressure to obtain mask base cloth for later use;
(4) preparing dogwood dry powder:
taking fresh dogwood fruits, washing, freezing, directly boiling in hot water, taking out, crushing, and drying to obtain dry dogwood powder;
(5) preparing a dogwood extract:
mixing dry powder of Corni fructus with ethanol solution, ultrasonic extracting, filtering, and concentrating the filtrate by rotary evaporation to obtain Corni fructus extract;
(6) preparing functional liquid:
weighing Corni fructus extract, collagen polypeptide, procyanidine, kojic acid, arbutin and sodium chloride solution, stirring and mixing to obtain functional liquid;
(7) preparing a wrinkle-removing, whitening and oil-removing mask:
soaking the facial mask base cloth in the obtained functional liquid, taking out after soaking, and sterilizing to obtain the facial mask with effects of removing wrinkles, whitening skin and removing oil.
Further, the preparation method comprises the following specific steps:
(1) preparing sodium alginate viscose fiber:
filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, adjusting the pH to 8 by using a sodium hydroxide solution, adding epoxy chloropropane with the mass fraction of 3% of the sodium alginate into the beaker, heating, stirring, reacting, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to the mass ratio of the sodium alginate to the viscose of 1:25, stirring and reacting for 1-2 h to obtain a mixture, and spinning the mixture by a wet method to obtain the sodium alginate viscose;
(2) preparing a crude product of the mask base cloth:
opening and carding the sodium alginate viscose fiber and the bamboo fiber respectively, and then cross-lapping with a lapping density of 50g/m2Carrying out spunlace reinforcement on the laid fiber net, and drying to obtain a crude product of the mask base cloth;
(3) preparing a mask base cloth:
mixing the obtained crude product of the mask base cloth with citric acid solution with the mass fraction of 5%, putting into a high-pressure reaction kettle, steaming at high temperature and high pressure, and obtaining the mask base cloth after the steaming is finished;
(4) preparing dogwood dry powder:
taking ripe fresh dogwood fruits, washing the dogwood fruits, freezing the dogwood fruits, directly transferring the dogwood fruits into hot water for boiling, taking out the dogwood fruits, crushing the dogwood fruits, sieving the dogwood fruits by a 40-mesh sieve, and drying the dogwood fruits for 7-8 hours at 50-60 ℃ to obtain dogwood dry powder;
(5) preparing a dogwood extract:
mixing the obtained dogwood dry powder with 75% of ethanol solution by mass, putting into an ultrasonic extractor, performing ultrasonic extraction, filtering the extract, and performing rotary evaporation and concentration on the filtrate to 10% of the original volume to obtain the dogwood extract;
(6) preparing functional liquid:
weighing 15-20 parts of dogwood extract, 15-20 parts of collagen polypeptide, 5-8 parts of procyanidine, 8-10 parts of kojic acid, 15-20 parts of arbutin and 60-70 parts of sodium chloride solution with the mass fraction of 0.9% in parts by weight, and stirring and mixing to obtain a functional liquid;
(7) preparing a wrinkle-removing, whitening and oil-removing mask:
soaking the facial mask base cloth in the obtained functional liquid, taking out the facial mask base cloth soaked with the functional liquid after soaking, and sterilizing in an ultraviolet disinfection cabinet to obtain the facial mask with effects of removing wrinkles, whitening and removing oil.
Further, the heating temperature in the step (1) is 70-80 ℃, and the stirring reaction time is 2-3 hours.
Further, the mass ratio of the sodium alginate viscose fibers to the bamboo fibers in the step (2) is 1: 3.
Further, in the step (3), the mass ratio of the crude facial film substrate to the citric acid solution with the mass fraction of 5% is 1: 10, the pressure of the high-temperature high-pressure cooking is 1.5-1.6 Mpa, the temperature of the high-temperature high-pressure cooking is 200-300 ℃, and the time of the high-temperature high-pressure cooking is 8-10 hours.
Further, the temperature of the freezing treatment in the step (4) is-2 ℃, the time of the freezing treatment is 20-25 hours, the temperature of hot water is 70-80 ℃, and the time of the boiling in the hot water is 3-5 min.
Further, in the step (5), the mass ratio of the dried powder of the cornus officinalis to the 75% ethanol solution is 1:20, the temperature of ultrasonic extraction is 40-50 ℃, the frequency of ultrasonic extraction is 45-60 kHz, and the time of ultrasonic extraction is 30-40 min.
Further, the time for soaking the mask base cloth by the functional liquid in the step (7) is 24-26 hours.
By adopting the scheme, the invention at least has the following advantages:
the wrinkle-removing, whitening and deoiling mask disclosed by the invention has the beautifying effects of enriching blood, activating blood, promoting qi circulation, nourishing blood and promoting tissue regeneration, can promote qi and blood circulation of skin, dispel pathogenic toxins, and achieve the beautifying purposes of moistening skin, removing wrinkles, whitening and defending exogenous pathogenic factors, wherein the collagen polypeptide can improve the skin fat content, so that the skin is smoother, moistened, soft and elastic, meanwhile, the skin can breathe and sweat normally, and various skin problems are alleviated; finally, the facial mask base cloth with excellent adsorbability is used for adsorbing the immobilized functional liquid, the content of active ingredients in the facial mask is increased, and therefore the beautifying effect of the facial mask is improved.
The foregoing is a summary of the present invention, and in order to provide a clear understanding of the technical means of the present invention and to be implemented in accordance with the present specification, the following is a detailed description of the preferred embodiments of the present invention.
Detailed Description
The following examples are given to further illustrate the embodiments of the present invention. The following examples are intended to illustrate the invention but are not intended to limit the scope of the invention.
(1) Filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, adjusting the pH to 8 by using a sodium hydroxide solution, adding epoxy chloropropane with the mass fraction of 3% of the sodium alginate into the beaker, heating to 70-80 ℃, stirring for reaction for 2-3 h, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to the mass ratio of the sodium alginate to the viscose of 1:25, stirring for reaction for 1-2 h to obtain a mixture, and performing wet spinning on the mixture to obtain sodium alginate viscose; firstly, alginate fibers with excellent skin affinity are prepared by wet spinning, so that the skin affinity of the mask is improved;
(2) respectively opening and carding the sodium alginate viscose fibers and the bamboo fibers according to the mass ratio of 1:3, and then cross-lapping with the lapping density of 50g/m2Carrying out spunlace reinforcement on the laid fiber net, and drying to obtain a crude product of the mask base cloth; taking alginate and bamboo fiber as raw materials, and weaving a crude product of the composite mask base cloth by spunlace;
(3) and mixing the obtained crude product of the mask base cloth and a citric acid solution with the mass fraction of 5% according to the mass ratio of 1: 10, mixing, putting into a high-pressure reaction kettle, raising the pressure in the reaction kettle to 1.5-1.6 Mpa, raising the temperature to 200-300 ℃, cooking at high temperature and high pressure for 8-10 hours, and obtaining mask base cloth for later use after cooking; mixing the crude product of the composite mask base cloth and organic acid, then carrying out high-temperature high-pressure treatment, and taking the organic acid as a catalyst, so that part of cellulose in the bamboo fibers is hydrolyzed, furfural is generated due to hydrolysis, the generated furfural can be further condensed under the conditions of high temperature and high pressure to form a furfural polymer, so that the mask base cloth is partially resinified, and the generated furfural resin polymer has viscosity, so that the mask base cloth can easily adsorb mask functional liquid components, the content of effective components in the mask is increased, and the beautifying effect of the mask is improved;
(4) taking ripe fresh dogwood fruits, washing the dogwood fruits, freezing the dogwood fruits at the temperature of minus 2 ℃ for 20-25 hours, directly transferring the dogwood fruits into hot water at the temperature of 70-80 ℃, boiling the dogwood fruits for 3-5 minutes, taking out the dogwood fruits, crushing the dogwood fruits, sieving the dogwood fruits by a 40-mesh sieve, and drying the dogwood fruits for 7-8 hours at the temperature of 50-60 ℃ to obtain dogwood dry powder; the structure of the dogwood is damaged through double treatment of freezing and hot boiling, so that the dissolution of internal active ingredients is facilitated, and the subsequent extraction is convenient;
(5) mixing the obtained dogwood dry powder with 75% of ethanol solution according to the mass ratio of 1:20, putting the mixture into an ultrasonic extraction instrument, carrying out ultrasonic extraction at the temperature of 40-50 ℃ and the frequency of 45-60 kHz for 30-40 min, filtering the extract, and carrying out rotary evaporation and concentration on the filtrate to 10% of the original volume to obtain the dogwood extract; the ethanol solution is used as an inorganic solvent, and the ursolic acid in the dogwood is extracted by ultrasonic assistance, so that the ursolic acid can promote the activation and the renewal of epidermal cells, reduce the condensation force among corneocytes, enable aged cells to smoothly fall off, avoid abnormal cutin accumulation, increase the moisture retention capacity of the skin, prevent hair follicle openings from being blocked, facilitate the smooth discharge of sebum, promote the oil removal of the mask, facilitate the effective components in the mask functional liquid to permeate into the skin due to the smoothness of the hair follicles, and enhance the beautifying effect;
(6) weighing 15-20 parts of dogwood extract, 15-20 parts of collagen polypeptide, 5-8 parts of procyanidine, 8-10 parts of kojic acid, 15-20 parts of arbutin and 60-70 parts of sodium chloride solution with the mass fraction of 0.9% in parts by weight, and stirring and mixing to obtain a functional liquid; the cornus officinalis extract is used in the functional liquid to remove cutin, so that the deoiling effect is enhanced, the whitening effect is improved, the collagen polypeptide can improve the skin fat content, the skin is more tender, moist, soft and elastic, the skin breathing and perspiration are normal, various skin problems are reduced, the whitening and wrinkle removing effects are achieved, in addition, proanthocyanidins, kojic acid and arbutin have excellent whitening effects, and the physiological saline with the concentration of 0.9% is used, so that the cornus officinalis extract is more skin-friendly, is beneficial to skin absorption, and further the beautifying effect is improved;
(7) and soaking the mask base cloth in the obtained functional liquid for 24-26 hours, taking out the mask base cloth soaked with the functional liquid after soaking is finished, and placing the mask base cloth in an ultraviolet disinfection cabinet for sterilization and disinfection to obtain the wrinkle-removing, whitening and oil-removing mask. Finally, the facial mask base cloth with excellent adsorbability is used for adsorbing the solid-carrying functional liquid, so that the content of effective components in the facial mask is increased, and the beautifying effect of the facial mask is improved.
Example 1
Filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, adjusting the pH to 8 by using a sodium hydroxide solution, adding epoxy chloropropane with the mass fraction of 3% of the sodium alginate into the beaker, heating to 70 ℃, stirring for reaction for 2 hours, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to the mass ratio of the sodium alginate to the viscose of 1:25, stirring for reaction for 1 hour to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose; respectively opening and carding the sodium alginate viscose fibers and the bamboo fiber fibers according to the mass ratio of 1:3, and then cross-lapping with the lapping density of 50g/m2Carrying out spunlace reinforcement on the laid fiber net, and drying to obtain a crude product of the mask base cloth; and mixing the obtained crude product of the mask base cloth and a citric acid solution with the mass fraction of 5% according to the mass ratio of 1: 10 mixing, putting into a high-pressure reaction kettle, raising the pressure in the reaction kettle to 1.5Mpa, raising the temperature to 200 ℃, cooking at high temperature and high pressure for 8 hours, and obtaining the mask base cloth for later use after cooking; taking ripe fresh dogwood fruits, washing, freezing at-2 ℃ for 20h, directly transferring into hot water at 70 ℃ for boiling for 3min, taking out, crushing, sieving with a 40-mesh sieve, and drying at 50 ℃ for 7h to obtain dogwood dry powder; mixing the obtained Corni fructus dry powder with 75% ethanol solution at a mass ratio of 1:20, placing into an ultrasonic extraction apparatus, and ultrasonically extracting at 40 deg.C and 45kHzTaking for 30min, filtering the extract, and concentrating the filtrate by rotary evaporation to 10% of the original volume to obtain Corni fructus extract; weighing 15 parts of dogwood extract, 15 parts of collagen polypeptide, 5 parts of procyanidine, 8 parts of kojic acid, 15 parts of arbutin and 60 parts of sodium chloride solution with the mass fraction of 0.9%, and stirring and mixing to obtain a functional liquid; soaking the facial mask base cloth with the obtained functional liquid for 24h, taking out the facial mask base cloth soaked with the functional liquid after soaking, and placing in an ultraviolet disinfection cabinet for sterilization and disinfection to obtain the facial mask with effects of removing wrinkles, whitening and removing oil.
Example 2
Filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, adjusting the pH to 8 by using a sodium hydroxide solution, adding epoxy chloropropane with the mass fraction of 3% of the sodium alginate into the beaker, heating to 72 ℃, stirring for reaction for 2 hours, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to the mass ratio of the sodium alginate to the viscose of 1:25, stirring for reaction for 1 hour to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose; respectively opening and carding the sodium alginate viscose fibers and the bamboo fiber fibers according to the mass ratio of 1:3, and then cross-lapping with the lapping density of 50g/m2Carrying out spunlace reinforcement on the laid fiber net, and drying to obtain a crude product of the mask base cloth; and mixing the obtained crude product of the mask base cloth and a citric acid solution with the mass fraction of 5% according to the mass ratio of 1: 10 mixing, putting into a high-pressure reaction kettle, raising the pressure in the reaction kettle to 1.5Mpa, raising the temperature to 220 ℃, cooking at high temperature and high pressure for 8 hours, and obtaining mask base cloth for later use after cooking; taking ripe fresh dogwood fruits, washing the dogwood fruits, freezing the dogwood fruits at the temperature of minus 2 ℃ for 21 hours, directly transferring the dogwood fruits into hot water at the temperature of 71 ℃ for boiling for 3 minutes, taking out the dogwood fruits, crushing the dogwood fruits, sieving the dogwood fruits by a 40-mesh sieve, and drying the dogwood fruits at the temperature of 51 ℃ for 7 hours to obtain dogwood dry powder; mixing the obtained dry powder of dogwood and 75% of ethanol solution according to the mass ratio of 1:20, putting the mixture into an ultrasonic extraction instrument, carrying out ultrasonic extraction at 41 ℃ and the frequency of 45kHz for 31min, filtering the extract, and carrying out rotary evaporation and concentration on the filtrate to 10% of the original volume to obtain the dogwood extract; weighing 16 parts of dogwood extract, 16 parts of collagen polypeptide, 5 parts of procyanidine, 8 parts of kojic acid and 16 parts of bearberryStirring and mixing glycoside and 62 parts of 0.9 mass percent sodium chloride solution to obtain functional liquid; soaking the facial mask base cloth with the obtained functional liquid for 24h, taking out the facial mask base cloth soaked with the functional liquid after soaking, and placing in an ultraviolet disinfection cabinet for sterilization and disinfection to obtain the facial mask with effects of removing wrinkles, whitening and removing oil.
Example 3
Filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, adjusting the pH to 8 by using a sodium hydroxide solution, adding epoxy chloropropane with the mass fraction of 3% of the sodium alginate into the beaker, heating to 75 ℃, stirring for reaction for 2 hours, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to the mass ratio of the sodium alginate to the viscose of 1:25, stirring for reaction for 1 hour to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose; respectively opening and carding the sodium alginate viscose fibers and the bamboo fiber fibers according to the mass ratio of 1:3, and then cross-lapping with the lapping density of 50g/m2Carrying out spunlace reinforcement on the laid fiber net, and drying to obtain a crude product of the mask base cloth; and mixing the obtained crude product of the mask base cloth and a citric acid solution with the mass fraction of 5% according to the mass ratio of 1: 10 mixing, putting into a high-pressure reaction kettle, raising the pressure in the reaction kettle to 1.5Mpa, raising the temperature to 250 ℃, cooking at high temperature and high pressure for 8 hours, and obtaining mask base cloth for later use after cooking; taking ripe fresh dogwood fruits, washing the dogwood fruits, freezing the dogwood fruits at the temperature of minus 2 ℃ for 23 hours, directly transferring the dogwood fruits into hot water at the temperature of 75 ℃ for boiling for 3 minutes, taking out the dogwood fruits, crushing the dogwood fruits, sieving the dogwood fruits by a 40-mesh sieve, and drying the dogwood fruits at the temperature of 55 ℃ for 7 hours to obtain dogwood dry powder; mixing the obtained dry powder of dogwood and 75% of ethanol solution according to the mass ratio of 1:20, putting the mixture into an ultrasonic extraction instrument, carrying out ultrasonic extraction at the temperature of 45 ℃ and the frequency of 50kHz for 35min, filtering the extract, and carrying out rotary evaporation and concentration on the filtrate to 10% of the original volume to obtain the dogwood extract; weighing 18 parts of dogwood extract, 18 parts of collagen polypeptide, 7 parts of procyanidine, 9 parts of kojic acid, 18 parts of arbutin and 65 parts of sodium chloride solution with the mass fraction of 0.9%, stirring and mixing to obtain functional liquid; soaking facial mask base cloth with the obtained functional liquid for 25h, taking out the facial mask base cloth soaked with the functional liquid after soaking, and placing in ultraviolet disinfection cabinetSterilizing and disinfecting to obtain the wrinkle-removing, whitening and oil-removing facial mask.
Example 4
Filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, adjusting the pH to 8 by using a sodium hydroxide solution, adding epoxy chloropropane with the mass fraction of 3% of the sodium alginate into the beaker, heating to 78 ℃, stirring for reaction for 3 hours, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to the mass ratio of the sodium alginate to the viscose of 1:25, stirring for reaction for 2 hours to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose; respectively opening and carding the sodium alginate viscose fibers and the bamboo fiber fibers according to the mass ratio of 1:3, and then cross-lapping with the lapping density of 50g/m2Carrying out spunlace reinforcement on the laid fiber net, and drying to obtain a crude product of the mask base cloth; and mixing the obtained crude product of the mask base cloth and a citric acid solution with the mass fraction of 5% according to the mass ratio of 1: 10 mixing, putting into a high-pressure reaction kettle, raising the pressure in the reaction kettle to 1.6Mpa, raising the temperature to 280 ℃, cooking at high temperature and high pressure for 9 hours, and obtaining the mask base cloth for later use after cooking; taking ripe fresh dogwood fruits, washing the dogwood fruits, freezing the dogwood fruits at the temperature of minus 2 ℃ for 24 hours, directly transferring the dogwood fruits into hot water at the temperature of 78 ℃ for boiling for 5 minutes, taking out the dogwood fruits, crushing the dogwood fruits, sieving the dogwood fruits by a 40-mesh sieve, and drying the dogwood fruits for 8 hours at the temperature of 58 ℃ to obtain dogwood dry powder; mixing the obtained dry powder of dogwood and 75% of ethanol solution according to the mass ratio of 1:20, putting the mixture into an ultrasonic extraction instrument, carrying out ultrasonic extraction at 48 ℃ and 48kHz for 38min, filtering the extract, and carrying out rotary evaporation and concentration on the filtrate to 10% of the original volume to obtain the dogwood extract; weighing 18 parts of dogwood extract, 19 parts of collagen polypeptide, 7 parts of procyanidine, 9 parts of kojic acid, 19 parts of arbutin and 68 parts of sodium chloride solution with the mass fraction of 0.9% in parts by weight, and stirring and mixing to obtain functional liquid; soaking the facial mask base cloth with the obtained functional liquid for 25h, taking out the facial mask base cloth soaked with the functional liquid after soaking, and placing in an ultraviolet disinfection cabinet for sterilization and disinfection to obtain the facial mask with effects of removing wrinkles, whitening and removing oil.
Example 5
Putting 3% sodium alginate water solution into a beaker, adjusting pH to 8 with sodium hydroxide solution, adding sodium alginate water solutionAdding epoxy chloropropane accounting for 3% of the mass of sodium alginate into a beaker, heating to 80 ℃, stirring for reaction for 3 hours, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to the mass ratio of the sodium alginate to the viscose of 1:25, stirring for reaction for 2 hours to obtain a mixture, and spinning the mixture by a wet method to obtain sodium alginate viscose; respectively opening and carding the sodium alginate viscose fibers and the bamboo fiber fibers according to the mass ratio of 1:3, and then cross-lapping with the lapping density of 50g/m2Carrying out spunlace reinforcement on the laid fiber net, and drying to obtain a crude product of the mask base cloth; and mixing the obtained crude product of the mask base cloth and a citric acid solution with the mass fraction of 5% according to the mass ratio of 1: 10, mixing, putting into a high-pressure reaction kettle, raising the pressure in the reaction kettle to 1.6Mpa, raising the temperature to 300 ℃, cooking at high temperature and high pressure for 10 hours, and obtaining mask base cloth for later use after cooking; taking ripe fresh dogwood fruits, washing, freezing at-2 ℃ for 25h, directly transferring into hot water at 80 ℃ for boiling for 5min, taking out, crushing, sieving with a 40-mesh sieve, and drying at 60 ℃ for 8h to obtain dogwood dry powder; mixing the obtained dry powder of dogwood and 75% of ethanol solution according to the mass ratio of 1:20, putting the mixture into an ultrasonic extraction instrument, carrying out ultrasonic extraction at the temperature of 50 ℃ and the frequency of 60kHz for 40min, filtering the extract, and carrying out rotary evaporation and concentration on the filtrate to 10% of the original volume to obtain the dogwood extract; weighing 20 parts of dogwood extract, 20 parts of collagen polypeptide, 8 parts of procyanidine, 10 parts of kojic acid, 20 parts of arbutin and 70 parts of sodium chloride solution with the mass fraction of 0.9%, stirring and mixing to obtain functional liquid; soaking the facial mask base cloth with the obtained functional liquid for 26h, taking out the facial mask base cloth soaked with the functional liquid after soaking, and placing in an ultraviolet disinfection cabinet for sterilization and disinfection to obtain the facial mask with effects of removing wrinkles, whitening and removing oil.
Comparative example 1: the preparation method is basically the same as that of example 1, except that the mask base cloth is directly replaced by the crude product of the mask base cloth, and the mask is prepared in the same way;
comparative example 2: the preparation method was substantially the same as that of example 1, except that a mask was prepared in the same manner by directly replacing the mask base cloth with a general nonwoven fabric;
comparative example 3: the preparation method was substantially the same as that of example 1, except that a mask was also prepared without adding the extract of dogwood of the present invention;
the performance of the wrinkle-removing, whitening and oil-removing facial masks in examples 1-5 is tested, and the test results are shown in table 1:
the detection method comprises the following steps:
the method for detecting the crease-resistance, whitening and deoiling performance comprises the following steps:
160 subjects aged 28-50 were selected and randomly divided into 8 groups of 20 subjects each, and the groups were statistically treated to have no significant difference in skin condition. Testing the skin state of the testee before and after the test by using a facial image analyzer VISIA-CR and a multifunctional skin tester CK-MPA10, repeating the test for 3 times each time, and averaging to obtain data of skin elasticity improvement rate, wrinkle reduction rate, moisture increase rate, pigment index reduction rate and facial oil reduction rate; group 1 used the mask produced in example 1, group 2 used the mask produced in example 2, group 3 used the mask produced in example 3, group 4 used the mask produced in example 4, group 5 used the mask produced in example 5, group 6 used the mask produced in comparative example 1, group 7 used the mask produced in comparative example 2, and group 8 used the mask produced in comparative example 3; the trial method comprises the following steps: after face cleaning with clean water, the face is smeared on the whole face once every 2 days, 5 g of the face is smeared at 10 o' clock in each night for 28 days, and the average value of the data of 20 testers in each group is taken as the trial result data of each group, and the result is shown in table 1.
TABLE 1 Performance test results
As can be seen from the detection data in the above table, in comparative example 1, because the mask base cloth is directly replaced by the crude product of the mask base cloth, the skin elasticity improvement rate, the wrinkle reduction rate, the moisture improvement rate, the pigment index reduction rate and the facial oil reduction rate are all significantly reduced, therefore, the invention mixes the crude product of the composite mask base cloth with organic acid and then carries out high-temperature high-pressure treatment, takes the organic acid as a catalyst, so that part of cellulose in bamboo fiber is hydrolyzed, and furfural is generated due to hydrolysis, the generated furfural is further condensed under the conditions of high temperature and high pressure to form furfural polymer, so that the mask base cloth is partially resinified, and the generated furfural resin polymer has viscosity, so that the mask base cloth can easily adsorb the components of the mask functional liquid, the content of the effective components in the mask is increased, so that the beauty effect of the mask is improved, and secondly, the formed furfural resin polymer is hydrophobic and oleophilic, the oil removal agent is matched with the porous structure of the spunlace base cloth, so that oil components secreted in facial pores can be effectively enriched, and the oil removal effect is excellent;
in comparative example 2, since the common non-woven fabric is directly used to replace the mask base fabric, the skin elasticity improvement rate, wrinkle reduction rate, moisture improvement rate, pigment index reduction rate and facial oil reduction rate are all significantly reduced, and are lower than those in comparative example 1, so that the performance of the composite mask base fabric woven by taking alginate and bamboo fiber as raw materials is more excellent than that of the non-woven fabric, and the performance is significantly enhanced after high-temperature and high-pressure steaming;
in contrast example 3, the dogwood extract of the present invention is not added, so that the skin elasticity improvement rate, wrinkle reduction rate, moisture improvement rate, pigment index reduction rate, and facial oil reduction rate are all significantly reduced, and thus, the present invention uses an ethanol solution as an inorganic solvent, and extracts an ursolic acid component in dogwood by ultrasound assistance, and the ursolic acid can promote activation and renewal of epidermal cells, reduce the coagulation force among corneocytes, and enable aged cells to smoothly fall off, thereby preventing abnormal corneous accumulation, increasing the skin moisturizing ability, preventing the opening of hair follicles from being blocked, facilitating smooth sebum discharge, promoting oil removal of the mask, facilitating the effective components in the mask functional liquid to permeate into the skin, enhancing the cosmetic effect, and having a broad application prospect.
The above description is only a preferred embodiment of the present invention and is not intended to limit the present invention, it should be noted that, for those skilled in the art, many modifications and variations can be made without departing from the technical principle of the present invention, and these modifications and variations should also be regarded as the protection scope of the present invention.
Claims (9)
1. The wrinkle-removing, whitening and oil-removing mask is characterized in that: comprises a facial mask base cloth and functional liquid;
the mask base fabric is prepared by carrying out spunlace weaving on sodium alginate viscose fibers and bamboo fibers and then carrying out high-temperature and high-pressure modification;
the functional liquid comprises the following components in parts by weight:
15-20 parts of dogwood extract;
15-20 parts of collagen polypeptide;
5-8 parts of procyanidine;
8-10 parts of kojic acid;
15-20 parts of arbutin;
60-70 parts of 0.9 mass percent sodium chloride solution.
2. A preparation method of the wrinkle-removing, whitening and oil-removing mask is characterized by comprising the following steps: the preparation method comprises the following specific steps:
(1) preparing sodium alginate viscose fiber:
adjusting the pH value of a sodium alginate aqueous solution, adding epoxy chloropropane, heating, reacting, cooling to obtain a pre-reactant, adding the pre-reactant into viscose, reacting to obtain a mixture, and performing wet spinning on the mixture to obtain sodium alginate viscose;
(2) preparing a crude product of the mask base cloth:
carrying out spunlace reinforcement on sodium alginate viscose fibers and bamboo fibers, and drying to obtain a crude product of the mask base fabric;
(3) preparing a mask base cloth:
mixing the crude product of the mask base cloth with citric acid solution, and steaming at high temperature and high pressure to obtain mask base cloth for later use;
(4) preparing dogwood dry powder:
taking fresh dogwood fruits, washing, freezing, directly boiling in hot water, taking out, crushing, and drying to obtain dry dogwood powder;
(5) preparing a dogwood extract:
mixing dry powder of Corni fructus with ethanol solution, ultrasonic extracting, filtering, and concentrating the filtrate by rotary evaporation to obtain Corni fructus extract;
(6) preparing functional liquid:
weighing Corni fructus extract, collagen polypeptide, procyanidine, kojic acid, arbutin and sodium chloride solution, stirring and mixing to obtain functional liquid;
(7) preparing a wrinkle-removing, whitening and oil-removing mask:
soaking the facial mask base cloth in the obtained functional liquid, taking out after soaking, and sterilizing to obtain the facial mask with effects of removing wrinkles, whitening skin and removing oil.
3. The preparation method of the wrinkle-removing, whitening and oil-removing mask as claimed in claim 2, wherein: the preparation method comprises the following specific steps:
(1) preparing sodium alginate viscose fiber:
filling a sodium alginate aqueous solution with the mass fraction of 3% into a beaker, adjusting the pH to 8 by using a sodium hydroxide solution, adding epoxy chloropropane with the mass fraction of 3% of the sodium alginate into the beaker, heating, stirring, reacting, cooling to obtain a pre-reactant, adding the pre-reactant into viscose according to the mass ratio of the sodium alginate to the viscose of 1:25, stirring and reacting for 1-2 h to obtain a mixture, and spinning the mixture by a wet method to obtain the sodium alginate viscose;
(2) preparing a crude product of the mask base cloth:
opening and carding the sodium alginate viscose fiber and the bamboo fiber respectively, and then cross-lapping with a lapping density of 50g/m2Carrying out spunlace reinforcement on the laid fiber net, and drying to obtain a crude product of the mask base cloth;
(3) preparing a mask base cloth:
mixing the obtained crude product of the mask base cloth with citric acid solution with the mass fraction of 5%, putting into a high-pressure reaction kettle, steaming at high temperature and high pressure, and obtaining the mask base cloth after the steaming is finished;
(4) preparing dogwood dry powder:
taking ripe fresh dogwood fruits, washing the dogwood fruits, freezing the dogwood fruits, directly transferring the dogwood fruits into hot water for boiling, taking out the dogwood fruits, crushing the dogwood fruits, sieving the dogwood fruits by a 40-mesh sieve, and drying the dogwood fruits for 7-8 hours at 50-60 ℃ to obtain dogwood dry powder;
(5) preparing a dogwood extract:
mixing the obtained dogwood dry powder with 75% of ethanol solution by mass, putting into an ultrasonic extractor, performing ultrasonic extraction, filtering the extract, and performing rotary evaporation and concentration on the filtrate to 10% of the original volume to obtain the dogwood extract;
(6) preparing functional liquid:
weighing 15-20 parts of dogwood extract, 15-20 parts of collagen polypeptide, 5-8 parts of procyanidine, 8-10 parts of kojic acid, 15-20 parts of arbutin and 60-70 parts of sodium chloride solution with the mass fraction of 0.9% in parts by weight, and stirring and mixing to obtain a functional liquid;
(7) preparing a wrinkle-removing, whitening and oil-removing mask:
soaking the facial mask base cloth in the obtained functional liquid, taking out the facial mask base cloth soaked with the functional liquid after soaking, and sterilizing in an ultraviolet disinfection cabinet to obtain the facial mask with effects of removing wrinkles, whitening and removing oil.
4. The preparation method of the wrinkle-removing, whitening and oil-removing mask as claimed in claim 3, wherein the preparation method comprises the following steps: the heating temperature in the step (1) is 70-80 ℃, and the stirring reaction time is 2-3 h.
5. The preparation method of the wrinkle-removing, whitening and oil-removing mask as claimed in claim 3, wherein the preparation method comprises the following steps: the mass ratio of the sodium alginate viscose fibers to the bamboo fibers in the step (2) is 1: 3.
6. The preparation method of the wrinkle-removing, whitening and oil-removing mask as claimed in claim 3, wherein the preparation method comprises the following steps: in the step (3), the mass ratio of the crude product of the facial film substrate to the citric acid solution with the mass fraction of 5% is 1: 10, the pressure of the high-temperature high-pressure cooking is 1.5-1.6 Mpa, the temperature of the high-temperature high-pressure cooking is 200-300 ℃, and the time of the high-temperature high-pressure cooking is 8-10 hours.
7. The preparation method of the wrinkle-removing, whitening and oil-removing mask as claimed in claim 3, wherein the preparation method comprises the following steps: the temperature of the freezing treatment in the step (4) is-2 ℃, the time of the freezing treatment is 20-25 hours, the temperature of hot water is 70-80 ℃, and the time of the boiling in the hot water is 3-5 min.
8. The preparation method of the wrinkle-removing, whitening and oil-removing mask as claimed in claim 3, wherein the preparation method comprises the following steps: in the step (5), the mass ratio of the dried powder of the cornus officinalis to the 75% ethanol solution is 1:20, the ultrasonic extraction temperature is 40-50 ℃, the ultrasonic extraction frequency is 45-60 kHz, and the ultrasonic extraction time is 30-40 min.
9. The preparation method of the wrinkle-removing, whitening and oil-removing mask as claimed in claim 3, wherein the preparation method comprises the following steps: and (5) soaking the facial mask base cloth in the functional liquid in the step (7) for 24-26 hours.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN114588086A (en) * | 2022-03-17 | 2022-06-07 | 广州无添加主义化妆品有限公司 | High-temperature-resistant milky-white mask body without demulsification |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104337738A (en) * | 2014-11-14 | 2015-02-11 | 刘芳 | Composition of dogwood extracts for skin wrinkle resisting and preparation method thereof |
| CN108166157A (en) * | 2017-12-25 | 2018-06-15 | 合肥洁诺无纺布制品有限公司 | Antibacterial spunlace non-woven cloth beauty mask base fabric of a kind of moisture absorption and preparation method thereof |
| CN111560708A (en) * | 2020-04-08 | 2020-08-21 | 青岛大学 | Water-absorbent gelling spunlace fabric containing alginate fibers and preparation method and application thereof |
| CN111658574A (en) * | 2020-06-12 | 2020-09-15 | 青岛大学 | Dry sheet type facial mask containing active essence and preparation method thereof |
-
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104337738A (en) * | 2014-11-14 | 2015-02-11 | 刘芳 | Composition of dogwood extracts for skin wrinkle resisting and preparation method thereof |
| CN108166157A (en) * | 2017-12-25 | 2018-06-15 | 合肥洁诺无纺布制品有限公司 | Antibacterial spunlace non-woven cloth beauty mask base fabric of a kind of moisture absorption and preparation method thereof |
| CN111560708A (en) * | 2020-04-08 | 2020-08-21 | 青岛大学 | Water-absorbent gelling spunlace fabric containing alginate fibers and preparation method and application thereof |
| CN111658574A (en) * | 2020-06-12 | 2020-09-15 | 青岛大学 | Dry sheet type facial mask containing active essence and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114588086A (en) * | 2022-03-17 | 2022-06-07 | 广州无添加主义化妆品有限公司 | High-temperature-resistant milky-white mask body without demulsification |
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