CN111847990A - High-performance waterproof antifouling real stone paint - Google Patents
High-performance waterproof antifouling real stone paint Download PDFInfo
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- CN111847990A CN111847990A CN202010690905.1A CN202010690905A CN111847990A CN 111847990 A CN111847990 A CN 111847990A CN 202010690905 A CN202010690905 A CN 202010690905A CN 111847990 A CN111847990 A CN 111847990A
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- stone paint
- antifouling
- real stone
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/30—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Other silicon-containing organic compounds; Boron-organic compounds
- C04B26/32—Compounds having one or more carbon-to-metal or carbon-to-silicon linkages ; Other silicon-containing organic compounds; Boron-organic compounds containing silicon
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B14/00—Use of inorganic materials as fillers, e.g. pigments, for mortars, concrete or artificial stone; Treatment of inorganic materials specially adapted to enhance their filling properties in mortars, concrete or artificial stone
- C04B14/02—Granular materials, e.g. microballoons
- C04B14/04—Silica-rich materials; Silicates
- C04B14/06—Quartz; Sand
- C04B14/068—Specific natural sands, e.g. sea -, beach -, dune - or desert sand
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00008—Obtaining or using nanotechnology related materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00034—Physico-chemical characteristics of the mixtures
- C04B2111/00146—Sprayable or pumpable mixtures
- C04B2111/00155—Sprayable, i.e. concrete-like, materials able to be shaped by spraying instead of by casting, e.g. gunite
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/27—Water resistance, i.e. waterproof or water-repellent materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/50—Mortars, concrete or artificial stone characterised by specific physical values for the mechanical strength
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Civil Engineering (AREA)
- Paints Or Removers (AREA)
Abstract
The invention relates to the technical field of coatings, in particular to a high-performance waterproof antifouling real stone paint. The traditional real stone paint adopts a cellulose thickener, and a large number of hydroxyl functional groups on the surface of the thickener greatly reduce the water-resistant antifouling property and the water-resistant property of the real stone paint. In order to solve the problem, the invention provides a high-performance waterproof antifouling really stone paint, wherein the added film-forming assistant is a compound of diethylene glycol monobutyl ether and diethanol butyl ether acetate, and the mass ratio of the diethylene glycol monobutyl ether to the diethanol butyl ether acetate is 1: 1-2; the added multifunctional auxiliary agent is a mixture of 2-butylaminoethanol and 2-N-dibutylaminoethanol, and the mass ratio of the 2-butylaminoethanol to the 2-N-dibutylaminoethanol is 1: 1.5. Compared with the traditional real stone paint, the high-performance waterproof antifouling real stone paint prepared by the method has better antifouling and waterproof performances.
Description
Technical Field
The invention relates to the technical field of coatings, in particular to a high-performance waterproof antifouling real stone paint.
Background
In order to achieve the effect of natural stone materials in the existing buildings, natural stone materials are commonly used, but the natural stone materials are limited by natural ores, are not uniform in color and pattern after decoration, cannot be renovated, and are difficult to mine and process and expensive; the unit volume weight is large, the load on the wall body is large, the wall body is not suitable for the decoration of light buildings, in addition, the construction difficulty is large, particularly, corner parts need special processing treatment, joint sealing glue needs to be added into gaps among the stones, and the whole waxing needs to be carried out after the construction is finished.
The spraying effect of the real stone paint is solemn and elegant, rich texture of natural stone can be fully displayed, and the natural broken stone is adopted to display the characteristics that the color is never faded, the long-term beautiful texture of the wall body is kept, and the like. The stone-like paint has wide application, and the decorative effect is comparable to that of stone, and is more suitable for moulding various artistic models than that of stone, and can be used as exterior wall, relief, beam column and other special-shaped wall surface decorations, and is suitable for making exterior wall paintings, and has granite, marble and granite color effects, and can obtain the effect of being fake and unreal. The traditional stone paint adopts a cellulose thickener, and a large amount of hydroxyl functional groups on the surface of the thickener greatly reduce the water and stain resistance and the water resistance of the stone paint (Guoqingquan, Riyongjin, Chengju. the stain resistance and the influence factor [ J ]. green building, 2003, 19(5): 15-18.), so that the surface of the stone paint is easy to be polluted and easy to fall off from an outer wall cavity in a humid environment.
Disclosure of Invention
Aiming at the problems in the prior art, the technical problems to be solved by the invention are as follows: the traditional real stone paint adopts a cellulose thickener, and a large number of hydroxyl functional groups on the surface of the thickener greatly reduce the water-resistant antifouling property and the water-resistant property of the real stone paint.
The technical scheme adopted by the invention for solving the technical problems is as follows: the invention provides a high-performance waterproof antifouling real stone paint which comprises the following components in parts by weight:
30-40 parts of silicone-acrylic emulsion
80-120 parts of natural colored sand
3-5 parts of rock slice
0.5-1 part of film-forming assistant
0.1 to 0.2 portion of thickening agent
0.05 to 0.1 portion of surfactant
0.1 to 0.2 portion of multifunctional additive
2-3 parts of antifouling agent
0.2 to 0.3 portion of defoaming agent
0.2 to 0.3 portion of water repellent
10-15 parts of water.
Specifically, the particle size of the natural colored sand is 20-100 meshes.
Specifically, the film-forming assistant is a mixture of diethylene glycol monobutyl ether and diethanol butyl ether acetate, and the mass ratio of the diethylene glycol monobutyl ether to the diethanol butyl ether acetate is 1: 1-2.
In particular, the thickener is a non-ionic thickener.
Specifically, the nonionic thickener is PEG-150 distearate, PEG-80 glyceryl tallowate or PEG-8 polypropylene glycol-3 diisostearate.
Specifically, the surfactant is sodium lauryl sulfonate.
Specifically, the multifunctional auxiliary agent is a mixture of 2-butylaminoethanol and 2-N-dibutylaminoethanol, and the mass ratio of the 2-butylaminoethanol to the 2-N-dibutylaminoethanol is 1: 1.5.
Specifically, the antifouling agent is a compound of nano zinc oxide, ethanol and sodium lauryl sulfonate, and the mass ratio of the nano zinc oxide to the ethanol to the sodium lauryl sulfonate is 10:5: 2.
The invention has the beneficial effects that:
(1) the stone-like paint prepared by the invention has bright appearance and color, strong water resistance and antifouling capability and is suitable for various base planes;
(2) the invention adopts the color sand with different grain diameters as the filling material, and the reasonable proportion ensures that the simulation effect of the real stone paint reaches the most ideal state, thereby having the effect of falseness and falseness.
Detailed Description
The present invention will now be described in further detail with reference to examples.
The natural colored sand adopted in the following examples and comparative examples consists of colored sand with the granularity of 80-100 meshes, 40-80 meshes and 20-40 meshes, and the mass ratio of the natural colored sand with each grain size is 1:1: 1; the grain diameter of the rock slices is 80-100 meshes; the silicone-acrylate emulsion is SD-5281; the water repellent is US SHP-50; the defoaming agent is a German bike BYK-024 aqueous defoaming agent; the film-forming auxiliary agent is a mixture of diethylene glycol monobutyl ether and diethanol butyl ether acetate, and the mass ratio of the diethylene glycol monobutyl ether to the diethanol butyl ether acetate is 1: 1-2; the multifunctional auxiliary agent is a mixture of 2-butylaminoethanol and 2-N-dibutylaminoethanol, and the mass ratio of the 2-butylaminoethanol to the 2-N-dibutylaminoethanol is 1: 1.5; the antifouling agent is a compound of nano zinc oxide, ethanol and sodium lauryl sulfonate, the mass ratio of the nano zinc oxide to the ethanol to the sodium lauryl sulfonate is 10:5:2, and the particle size of the nano zinc oxide is 80-100 nm.
Example 1
The high-performance waterproof antifouling real stone paint comprises the following components in parts by weight:
30 portions of silicone-acrylic emulsion
80 portions of natural colored sand
3 portions of rock slice
0.5 part of film-forming assistant
0.1 part of thickening agent
0.05 part of surfactant
0.1 part of multifunctional auxiliary agent
Antifouling agent 2 parts
0.2 portion of defoaming agent
0.2 portion of water repellent
10 parts of water;
in the film-forming auxiliary agent, the mass ratio of diethylene glycol monobutyl ether to diethanol butyl ether acetate is 1: 1;
the raw materials are mixed, stirred for 20 minutes at room temperature at the rotating speed of 600 revolutions per minute, and uniformly mixed to obtain the stone-like paint coating.
The mortar board is sprayed with the stone-like paint coating, the spraying pressure is 0.8Pa/cm < 2 >, the caliber of a spray gun is 8mm, the distance between the muzzle and the wall surface is 60cm, the spraying is carried out twice, the spraying thickness is 1mm each time, and the total thickness of a paint film is 2 mm.
Maintaining at 23 deg.c and 65% humidity for 14 days, and testing the stain resistance, temperature change resistance and tensile bond strength and the tensile bond strength after soaking in water in JG/T24-2000.
And (3) testing results:
stain resistance: grade 1 after 18 times of cycle tests;
Temperature change resistance: the coating begins to be pulverized, cracked, peeled and swelled for 30 times, and compared with the standard plate, the color begins to change;
the standard state of the bonding strength is 1.5MPa, and the standard state is 1MPa after soaking.
Example 2
The high-performance waterproof antifouling real stone paint comprises the following components in parts by weight:
35 portions of silicone-acrylic emulsion
100 portions of natural colored sand
4 portions of rock slice
Film-forming assistant 1 part
0.2 portion of thickening agent
0.1 part of surfactant
0.2 part of multifunctional auxiliary agent
Antifouling agent 3 parts
0.3 portion of defoaming agent
0.3 portion of water repellent
13 parts of water;
in the film-forming auxiliary agent, the mass ratio of diethylene glycol monobutyl ether to diethanol butyl ether acetate is 1: 2;
the raw materials are mixed, stirred for 20 minutes at room temperature at the rotating speed of 600 revolutions per minute, and uniformly mixed to obtain the stone-like paint coating.
The mortar board is sprayed with the stone-like paint coating, the spraying pressure is 0.8Pa/cm < 2 >, the caliber of a spray gun is 8mm, the distance between the muzzle and the wall surface is 60cm, the spraying is carried out twice, the spraying thickness is 1mm each time, and the total thickness of a paint film is 2 mm.
Maintaining at 23 deg.c and 65% humidity for 14 days, and testing the stain resistance, temperature change resistance and tensile bond strength and the tensile bond strength after soaking in water in JG/T24-2000.
And (3) testing results:
stain resistance: grade 1 after 16 cycles;
temperature change resistance: the coating begins to chalk, crack, peel off and bulge for 28 times, and compared with a standard plate, the color begins to change;
the standard state of the bonding strength is 1.2MPa, and the standard state is 0.8MPa after soaking.
Example 3
The high-performance waterproof antifouling real stone paint comprises the following components in parts by weight:
40 parts of silicone-acrylic emulsion
120 portions of natural colored sand
5 portions of rock slice
Film-forming assistant 1 part
0.2 portion of thickening agent
0.1 part of surfactant
0.2 part of multifunctional auxiliary agent
Antifouling agent 3 parts
0.3 portion of defoaming agent
0.3 portion of water repellent
15 parts of water;
in the film-forming auxiliary agent, the mass ratio of the diethylene glycol monobutyl ether to the diethyl ether acetate is 1: 1.5;
the raw materials are mixed, stirred for 20 minutes at room temperature at the rotating speed of 600 revolutions per minute, and uniformly mixed to obtain the stone-like paint coating.
The mortar board is sprayed with the stone-like paint coating with the spraying pressure of 0.8Pa/cm2The caliber of the spray gun is 8mm, the distance between the muzzle and the wall surface is 60cm, the spraying is carried out twice, the spraying thickness is 1mm each time, and the total thickness of a paint film is 2 mm.
Maintaining at 23 deg.c and 65% humidity for 14 days, and testing the stain resistance, temperature change resistance and tensile bond strength and the tensile bond strength after soaking in water in JG/T24-2000.
And (3) testing results:
stain resistance: grade 1 after 16 cycles;
temperature change resistance: the coating begins to chalk, crack, peel off and bulge for 25 times, and compared with a standard plate, the color begins to change;
the standard state of the bonding strength is 1.2MPa, and the standard state is 0.8MPa after soaking.
Comparative example 1 differs from example 1 in that: in the film-forming auxiliary agent, the mass ratio of diethylene glycol monobutyl ether to diethanol butyl ether acetate is 2: 1;
the test of stain resistance, temperature change resistance and tensile bond strength and the test of the tensile bond strength of the test piece after being soaked in water are carried out according to JG/T24-2000 synthetic resin emulsion sand wall building coating, and the test results are as follows:
stain resistance: grade 1 after 13 cycle tests;
temperature change resistance: the coating begins to chalk, crack, peel off and bulge for 20 times, and compared with a standard plate, the color begins to change;
the standard state of the bonding strength is 1.0MPa, and the standard state of the bonding strength is 0.6MPa after soaking.
Comparative example 2 differs from example 1 in that: in the multifunctional auxiliary agent, the mass ratio of 2-butylaminoethanol to 2-N-dibutylaminoethanol is 1: 1;
the test of stain resistance, temperature change resistance and tensile bond strength and the test of the tensile bond strength of the test piece after being soaked in water are carried out according to JG/T24-2000 synthetic resin emulsion sand wall building coating, and the test results are as follows:
Stain resistance: grade 1 after 15 times of cycle test;
temperature change resistance: the coating begins to chalk, crack, peel off and bulge for 22 times, and compared with a standard plate, the color begins to change;
the standard state of the bonding strength is 1.2MPa, and the standard state is 0.7MPa after soaking in water.
Comparative example 3 differs from example 1 in that: the antifouling agent is a compound of nano zinc oxide, ethanol and sodium lauryl sulfonate, and the mass ratio of the nano zinc oxide to the ethanol to the sodium lauryl sulfonate is 5:5: 2.
The test of stain resistance, temperature change resistance and tensile bond strength and the test of the tensile bond strength of the test piece after being soaked in water are carried out according to JG/T24-2000 synthetic resin emulsion sand wall building coating, and the test results are as follows:
stain resistance: grade 2 after 16 cycles;
temperature change resistance: the coating begins to chalk, crack, peel off and bulge for 23 times, and compared with the standard plate, the color begins to change;
the standard state of the bonding strength is 1.1MPa, and the standard state of the bonding strength is 0.6MPa after soaking.
Comparative example 4 differs from example 1 in that: in the film-forming auxiliary agent, the mass ratio of diethylene glycol monobutyl ether to diethanol butyl ether acetate is 1: 3;
the test of stain resistance, temperature change resistance and tensile bond strength and the test of the tensile bond strength of the test piece after being soaked in water are carried out according to JG/T24-2000 synthetic resin emulsion sand wall building coating, and the test results are as follows:
Stain resistance: grade 1 after 11 times of cycle test;
temperature change resistance: the coating begins to chalk, crack, peel off, bulge 18 times, and compared with the standard plate, the color begins to change;
the standard state of the bonding strength is 0.8MPa, and the standard state of the bonding strength is 0.5MPa after soaking.
Comparative example 5 differs from example 1 in that: the antifouling agent is a compound of nano zinc oxide, ethanol and sodium lauryl sulfonate, and the mass ratio of the nano zinc oxide to the ethanol to the sodium lauryl sulfonate is 15:5: 2.
The test of stain resistance, temperature change resistance and tensile bond strength and the test of the tensile bond strength of the test piece after being soaked in water are carried out according to JG/T24-2000 synthetic resin emulsion sand wall building coating, and the test results are as follows:
stain resistance: grade 2 after 12 times of cycle test;
temperature change resistance: the coating begins to chalk, crack, peel off and bulge for 22 times, and compared with a standard plate, the color begins to change;
the standard state of the bonding strength is 1.0MPa, and the standard state of the bonding strength is 0.7MPa after soaking.
In light of the foregoing description of the preferred embodiment of the present invention, many modifications and variations will be apparent to those skilled in the art without departing from the spirit and scope of the invention. The technical scope of the present invention is not limited to the content of the specification, and must be determined according to the scope of the claims.
Claims (8)
1. The high-performance waterproof antifouling real stone paint is characterized by comprising the following components in parts by weight:
30-40 parts of silicone-acrylic emulsion
80-120 parts of natural colored sand
3-5 parts of rock slice
0.5-1 part of film-forming assistant
0.1 to 0.2 portion of thickening agent
0.05 to 0.1 portion of surfactant
0.1 to 0.2 portion of multifunctional additive
2-3 parts of antifouling agent
0.2 to 0.3 portion of defoaming agent
0.2 to 0.3 portion of water repellent
10-15 parts of water.
2. The high-performance water-resistant antifouling real stone paint as claimed in claim 1, wherein: the particle size of the natural colored sand is 20-100 meshes.
3. The high-performance water-resistant antifouling real stone paint as claimed in claim 1, wherein: the film-forming auxiliary agent is a compound of diethylene glycol monobutyl ether and diethanol butyl ether acetate, and the mass ratio of the diethylene glycol monobutyl ether to the diethanol butyl ether acetate is 1: 1-2.
4. The high-performance water-resistant antifouling real stone paint as claimed in claim 1, wherein: the thickener is a nonionic thickener.
5. The high-performance water-resistant antifouling real stone paint as claimed in claim 4, wherein: the nonionic thickening agent is PEG-150 distearate, PEG-80 glyceryl tallowate or PEG-8 polypropylene glycol-3 diisostearate.
6. The high-performance water-resistant antifouling real stone paint as claimed in claim 1, wherein: the surfactant is sodium lauryl sulfonate.
7. The high-performance water-resistant antifouling real stone paint as claimed in claim 1, wherein: the multifunctional auxiliary agent is a mixture of 2-butylaminoethanol and 2-N-dibutylaminoethanol, and the mass ratio of the 2-butylaminoethanol to the 2-N-dibutylaminoethanol is 1: 1.5.
8. The high-performance water-resistant antifouling real stone paint as claimed in claim 1, wherein: the antifouling agent is a compound of nano zinc oxide, ethanol and sodium lauryl sulfonate, and the mass ratio of the nano zinc oxide to the ethanol to the sodium lauryl sulfonate is 10:5: 2.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010690905.1A CN111847990A (en) | 2020-07-17 | 2020-07-17 | High-performance waterproof antifouling real stone paint |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010690905.1A CN111847990A (en) | 2020-07-17 | 2020-07-17 | High-performance waterproof antifouling real stone paint |
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| CN111847990A true CN111847990A (en) | 2020-10-30 |
Family
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0566936A1 (en) * | 1992-04-09 | 1993-10-27 | Dow Corning Toray Silicone Company, Limited | Aquatic antifouling mortar composition |
| CN107177268A (en) * | 2017-06-07 | 2017-09-19 | 深圳市天得环境科技有限公司 | Oil-stain-preventing water paint |
| CN107540277A (en) * | 2017-08-17 | 2018-01-05 | 储旭 | The true mineral varnish coating of environmental protection |
| CN108300047A (en) * | 2018-01-29 | 2018-07-20 | 河北晨阳工贸集团有限公司 | A kind of indoor anti-pollution water-water coating and preparation method thereof |
| KR102081265B1 (en) * | 2019-07-05 | 2020-02-25 | 이태희 | Environmental―friendly waterproof paint compositions |
-
2020
- 2020-07-17 CN CN202010690905.1A patent/CN111847990A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0566936A1 (en) * | 1992-04-09 | 1993-10-27 | Dow Corning Toray Silicone Company, Limited | Aquatic antifouling mortar composition |
| CN107177268A (en) * | 2017-06-07 | 2017-09-19 | 深圳市天得环境科技有限公司 | Oil-stain-preventing water paint |
| CN107540277A (en) * | 2017-08-17 | 2018-01-05 | 储旭 | The true mineral varnish coating of environmental protection |
| CN108300047A (en) * | 2018-01-29 | 2018-07-20 | 河北晨阳工贸集团有限公司 | A kind of indoor anti-pollution water-water coating and preparation method thereof |
| KR102081265B1 (en) * | 2019-07-05 | 2020-02-25 | 이태희 | Environmental―friendly waterproof paint compositions |
Non-Patent Citations (3)
| Title |
|---|
| 吕少仿: "《精细化工新编》", 28 February 2003, 湖北科学技术出版社 * |
| 穆锐: "《涂料实用生产技术与配方》", 30 June 2002, 江西科学技术出版社 * |
| 郭清泉等: "漆膜的耐沾污性及影响因素", 《化学建材》 * |
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