CN111803416A - Anti-aging cream containing ampelopsis grossedentata and preparation method thereof - Google Patents
Anti-aging cream containing ampelopsis grossedentata and preparation method thereof Download PDFInfo
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- CN111803416A CN111803416A CN202010693288.0A CN202010693288A CN111803416A CN 111803416 A CN111803416 A CN 111803416A CN 202010693288 A CN202010693288 A CN 202010693288A CN 111803416 A CN111803416 A CN 111803416A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/066—Multiple emulsions, e.g. water-in-oil-in-water
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses anti-aging cream containing ampelopsis grossedentata and a preparation method thereof, and the anti-aging cream comprises the following raw materials: 0.01-3.0% of ampelopsis grossedentata leaf extract, 3-12% of lipophilic emulsifier, 3.5-14% of hydrophilic emulsifier, 10-15% of humectant, 8-12% of emollient, 1-3% of thickener, 0.05-0.3% of auxiliary material and the balance of water, adopting a W/O/W multiple emulsification system to dissolve the ampelopsis grossedentata leaf extract in an aqueous phase, emulsifying the aqueous phase through the lipophilic emulsifier to form a water-in-oil W/O emulsion system, emulsifying the W/O emulsion in most of the aqueous phase in the formula to form the W/O/W system, wrapping the ampelopsis grossedentata leaf extract in the W/O emulsion in the formula, isolating external oxygen, PH and metal ions, greatly reducing the risk of the ampelopsis grossedentata leaf extract to be oxidized, protecting the color of a product to be stable, the ampelopsis grossedentata, the humectant and the emollient in the product can keep activity and stability, have an anti-aging effect, have the effects of moistening and preserving skin, and prolong the use and storage time of the product.
Description
[ technical field ] A method for producing a semiconductor device
The invention belongs to the technical field of cosmetics, and particularly relates to anti-aging cream containing Ampelopsis grossedentata and a preparation method thereof.
[ background of the invention ]
Ampelopsis grossedentata is a wild woody vine plant of Ampelopsis of Vitaceae, the total flavone content in tender stems and leaves can reach 43.4-44.0%, and the content of the most main flavonoid, namely dihydromyricetin, in the tender stems and leaves can reach 37.4-38.5% to the maximum. Dihydromyricetin has multiple peculiar effects of strongly eliminating free radicals, resisting oxidation, resisting thrombus, resisting tumor, diminishing inflammation and the like. The ampelopsis grossedentata stem and leaf extract has strong inhibiting effect on common bacillus subtilis and staphylococcus aureus and has antiseptic and synergistic effects. The ampelopsis grossedentata stem and leaf extract has strong antioxidation, can remove free radicals, has better antioxidation capability than common vitamin C, nicotinamide, tranexamic acid and the like, can whiten and brighten skin, resist wrinkles, reduce loss of collagen and fibrin and has good anti-aging effect in cosmetics.
However, the existing cream containing ampelopsis grossedentata generally uses an O/W system, the extract of the ampelopsis grossedentata leaves is dissolved in the water phase of an external phase, and the extract of the ampelopsis grossedentata contains a large amount of flavone, so that the color of the extract is easy to change when the extract is applied to cosmetics, and the flavone in the formula is easy to turn yellow or even yellowish brown under the alkaline condition or the condition of containing ions Al3+, Fe3+ and Cu2+, thereby influencing the efficacy and appearance stability of the cosmetics.
[ summary of the invention ]
The invention provides anti-aging cream containing Ampelopsis grossedentata, aiming at solving the technical problem that the efficacy of the existing Ampelopsis grossedentata cream is poor due to the fact that the existing Ampelopsis grossedentata cream is easy to turn yellow.
The invention also aims to provide a preparation method of the anti-aging cream containing ampelopsis grossedentata.
An anti-aging cream containing Ampelopsis grossedentata comprises the following raw materials in percentage by weight: 0.01-3.0% of ampelopsis grossedentata leaf extract, 3-12% of lipophilic emulsifier, 3.5-14% of hydrophilic emulsifier, 10-15% of humectant, 8-12% of emollient, 1-3% of thickener, 0.05-0.3% of auxiliary material and the balance of water, wherein the total mass of the components is 100%.
The application adopts a W/O/W multiple emulsification system, the ampelopsis grossedentata leaf extract is dissolved in a water phase, the water phase containing the ampelopsis grossedentata leaf extract is emulsified through a lipophilic emulsifier to form a water-in-oil W/O emulsion system, most of the water phase in the formula is emulsified with W/O emulsion to form the W/O/W system, the ampelopsis grossedentata leaf extract is wrapped in the W/O emulsion of the formula to isolate external oxygen, PH and metal ions, the risk of oxidation of the ampelopsis grossedentata leaf extract is greatly reduced, the color stability of a product is protected, the color change of the ampelopsis grossedentata is reduced, the ampelopsis grossedentata, a humectant and an emollient in the product can keep activity and stability, the effects of moistening and moisturizing are achieved, the free radicals of the skin are removed, the effects of oxidation resistance and aging resistance are achieved, increase the use and storage time of the product.
Preferably, the anti-aging cream containing the ampelopsis grossedentata is of a W/O/W structure, wherein the extract of the ampelopsis grossedentata leaves and a part of water form an internal water phase, the lipophilic emulsifier, the hydrophilic emulsifier and the emollient form an oil phase, and the humectant, the thickener and the rest of water form an external water phase. The two-membrane three-phase structure is formed by water-in-oil in water, the Ampelopsis grossedentata is coated on the inner side by the inner water phase, the inner water phase is coated by the oil phase, the oil phase is coated by the outer water phase, an inner-layer interfacial film is formed at the interface of the inner oil/water by the lipophilicity of the lipophilic emulsifier, and an outer-layer interfacial film is formed at the interface of the outer oil/water by the hydrophilicity of the hydrophilic emulsifier, so that the strength and the stability of the structure are improved.
Preferably, the lipophilic emulsifier is one or a combination of more than two of sucrose polystearate, cetyl palmitate, glycerol stearate, PEG-100 stearate and hydrogenated lecithin. Preferably, the glyceryl stearate and the PEG-100 stearate are compounded for use, and the sucrose polystearate and the cetyl palmitate are compounded, so that a synergistic effect can be generated, and the stability and the productivity are improved.
Preferably, the hydrophilic emulsifier is one or a combination of sorbitan isostearate and hydrogenated polyisobutene. Preferably, the emulsifier is used in a compound way, and is a nonionic emulsifier with HLB being more than 15, so that the stability of a multiple emulsification system is improved.
Preferably, the ampelopsis grossedentata leaf extract comprises ampelopsis grossedentata total flavonoids with the purity of 60-98% and dihydromyricetin with the purity of 60-98%. Can increase antioxidant effect and inhibit MDA production.
Preferably, the emollient is one or more of jojoba oil, shea butter, octyl methicone, bisabolol, dimethicone, cetyl alcohol, octyl methicone, meadowfoam seed oil, orange peel oil, and grapefruit peel oil.
Preferably, the humectant is any one or combination of a polyol humectant and a polysaccharide humectant; the polyalcohol humectant is one or any combination of glycerol, diglycerol, butanediol, propylene glycol, dipropylene glycol, sorbitol, panthenol, allantoin, polyethylene glycol-400, and PPG-10 methyl glucose ether; the polysaccharide humectant is one or any combination of hyaluronic acid, sodium hyaluronate, pullulan, trehalose and lima bean seed extract. Moisturizers are the most basic components in skin care products, and act on the skin by simulating the natural moisturizing system of human skin to delay water loss, provide temporary protection for the skin, reduce damage, promote repair, and the like.
Preferably, the auxiliary material comprises an excipient and a bacteriostatic agent, the excipient is essence or essential oil, and the bacteriostatic agent is one or any combination of 1, 2-hexanediol, caprylyl glycol, ethylhexyl glycerol and glyceryl caprylate. The bacteriostatic agent is a preservative replacing system, has clear mechanism and no toxic or side effect.
Preferably, the thickening agent comprises one or any combination of carbomer, xanthan gum and modified acrylic acid copolymer. The xanthan gum contains a large amount of hydrophilic groups, is a good surface active substance, and has the effects of resisting oxidation, preventing skin aging and the like.
The preparation method of the anti-aging cream containing ampelopsis grossedentata is characterized by comprising the following steps:
(1) weighing the ampelopsis grossedentata leaves and part of water according to the formula ratio, and uniformly mixing to form an internal water phase;
(2) weighing lipophilic emulsifier according to the formula ratio, and uniformly mixing to form a first oil phase;
(3) slowly adding the internal water phase in the step (1) into the first oil phase in the step (2) to form a water-in-oil W/O emulsion;
(4) weighing hydrophilic emulsifier and emollient according to the formula ratio, heating to 80-85 deg.C, stirring and dissolving to form a second oil phase;
(5) weighing the rest water, the humectant and the thickener according to the formula ratio, heating to 80-85 ℃, stirring and dissolving to obtain an external water phase;
(6) pumping the second oil phase in the step (4) into the external water phase in the step (5), homogenizing and stirring for 5-15min, adding the water-in-oil W/O emulsion in the step (3) when the temperature reaches 50-55 ℃, homogenizing and stirring uniformly, slowly homogenizing and stirring until the paste is fine and uniform, adding auxiliary materials when the temperature reaches 45-50 ℃, cooling to 40 ℃, adjusting the pH to 5.5-6.5, and discharging.
Compared with the prior art, the invention has the following advantages:
the application discloses anti-aging cream containing ampelopsis grossedentata, which comprises the following raw materials: 0.01-3.0% of Ampelopsis grossedentata leaf extract, 3-12% of lipophilic emulsifier, 3.5-14% of hydrophilic emulsifier, 10-15% of humectant, 8-12% of emollient, 1-3% of thickener, 0.05-0.3% of auxiliary material and the balance of water, the application adopts a W/O/W multiple emulsification system, the Ampelopsis grossedentata leaf extract is dissolved in an aqueous phase, the aqueous phase containing the Ampelopsis grossedentata leaf extract is emulsified by the lipophilic emulsifier to form a water-in-oil W/O emulsion system, most of the aqueous phase in the formula is emulsified by the W/O emulsion to form the W/O/W system, the Ampelopsis grossedentata leaf extract is wrapped in the W/O emulsion of the formula to isolate external oxygen, PH and metal ions, thereby greatly reducing the risk of oxidation of the Ampelopsis grossedentata leaf extract, the color of the product is protected to be stable, the color change of the ampelopsis grossedentata is reduced, the ampelopsis grossedentata, the humectant and the emollient in the product can keep activity and stability, the effects of moistening and moisturizing, scavenging free radicals of skin, resisting oxidation and aging are achieved, the effects of moistening and moisturizing the skin are achieved, and the using and storing time of the product is prolonged.
According to the preparation method of the anti-aging cream containing ampelopsis grossedentata, a one-step emulsification method is adopted to prepare a multiple emulsification system W/O/W, so that the discoloration of the ampelopsis grossedentata can be reduced, the stability of the product can be improved, and the cream is suitable for large-scale continuous production.
[ detailed description ] embodiments
The following is a detailed description of the present invention:
the specific technical scheme of the invention is described by combining specific embodiments 1-4:
example 1:
an anti-aging cream containing Ampelopsis grossedentata comprises the following steps:
(1) weighing Ampelopsis grossedentata leaves according to the formula ratio, extracting with 3% of water, and mixing uniformly to form an internal water phase;
(2) weighing lipophilic emulsifier according to the formula ratio in the table 1, and uniformly mixing to form a first oil phase;
(3) slowly adding the internal water phase in the step (1) into the first oil phase in the step (2) to form a water-in-oil W/O emulsion;
(4) weighing hydrophilic emulsifier and emollient according to the formula ratio, heating to 80-85 deg.C, stirring and dissolving to form a second oil phase;
(5) weighing the rest water, the humectant, carbomer and xanthan gum according to the formula ratio, heating to 80-85 ℃, and stirring to dissolve to obtain an external water phase;
(6) pumping the second oil phase in the step (4) into the external water phase in the step (5), homogenizing and stirring for 5min, setting the temperature to 80 ℃, adding a modified acrylic copolymer (mixture), homogenizing, stirring and thickening, adding triethanolamine for neutralization when the temperature reaches 50 ℃, adding the water-in-oil W/O emulsion in the step (3) after homogenizing and stirring uniformly, slowly homogenizing and stirring until the paste is fine and uniform, adding auxiliary materials when the temperature reaches 50 ℃, cooling to 40 ℃ after stirring uniformly, adjusting the pH to 5.5, and blanking.
Example 2:
(1) weighing Ampelopsis grossedentata leaves according to the formula ratio, extracting with 3% of water, and mixing uniformly to form an internal water phase;
(2) weighing lipophilic emulsifier according to the formula ratio in the table 1, and uniformly mixing to form a first oil phase;
(3) slowly adding the internal water phase in the step (1) into the first oil phase in the step (2) to form a water-in-oil W/O emulsion;
(4) weighing hydrophilic emulsifier and emollient according to the formula ratio, heating to 85 ℃, stirring and dissolving to form a second oil phase;
(5) weighing the rest water, the humectant, carbomer and xanthan gum according to the formula ratio, heating to 80-85 ℃, and stirring to dissolve to obtain an external water phase;
(6) pumping the second oil phase in the step (4) into the external water phase in the step (5), homogenizing and stirring for 10min, setting the temperature to 85 ℃, adding a modified acrylic copolymer (mixture), homogenizing, stirring and thickening, adding triethanolamine for neutralization when the temperature reaches 50 ℃, adding the water-in-oil W/O emulsion in the step (3) after homogenizing and stirring uniformly, slowly homogenizing and stirring until the paste is fine and uniform, adding auxiliary materials when the temperature reaches 50 ℃, cooling to 40 ℃ after stirring uniformly, adjusting the pH to 6.0, and blanking.
Example 3:
(1) weighing Ampelopsis grossedentata leaves according to the formula ratio, extracting with 3% of water, and mixing uniformly to form an internal water phase;
(2) weighing lipophilic emulsifier according to the formula ratio in the table 1, and uniformly mixing to form a first oil phase;
(3) slowly adding the internal water phase in the step (1) into the first oil phase in the step (2) to form a water-in-oil W/O emulsion;
(4) weighing hydrophilic emulsifier and emollient according to the formula ratio, heating to 80 ℃, stirring and dissolving to form a second oil phase;
(5) weighing the rest water, the humectant, carbomer and xanthan gum according to the formula ratio, heating to 80-85 ℃, and stirring to dissolve to obtain an external water phase;
(6) pumping the second oil phase in the step (4) into the external water phase in the step (5), homogenizing and stirring for 5min, setting the temperature to 80 ℃, adding a modified acrylic copolymer (mixture), homogenizing, stirring and thickening, adding triethanolamine for neutralization when the temperature reaches 55 ℃, adding the water-in-oil W/O emulsion in the step (3) after homogenizing and stirring uniformly, slowly homogenizing and stirring until the paste is fine and uniform, adding auxiliary materials when the temperature reaches 50 ℃, cooling to 40 ℃ after stirring uniformly, adjusting the pH to 6.5, and discharging.
Example 4:
(1) weighing Ampelopsis grossedentata leaves according to the formula ratio, extracting with 3% of water, and mixing uniformly to form an internal water phase;
(2) weighing lipophilic emulsifier according to the formula ratio in the table 1, and uniformly mixing to form a first oil phase;
(3) slowly adding the internal water phase in the step (1) into the first oil phase in the step (2) to form a water-in-oil W/O emulsion;
(4) weighing hydrophilic emulsifier and emollient according to the formula ratio, heating to 80-85 deg.C, stirring and dissolving to form a second oil phase;
(5) weighing the rest water, the humectant, carbomer and xanthan gum according to the formula ratio, heating to 80-85 ℃, and stirring to dissolve to obtain an external water phase;
(6) pumping the second oil phase in the step (4) into the external water phase in the step (5), homogenizing and stirring for 15min, setting the temperature to 80 ℃, adding a modified acrylic copolymer (mixture), homogenizing, stirring and thickening, adding triethanolamine for neutralization when the temperature reaches 50 ℃, adding the water-in-oil W/O emulsion in the step (3) after homogenizing and stirring uniformly, slowly homogenizing and stirring until the paste is fine and uniform, adding auxiliary materials when the temperature reaches 50 ℃, cooling to 40 ℃ after stirring uniformly, adjusting the pH to 5.5, and discharging.
Table 1: the anti-aging cream for Ampelopsis grossedentata of embodiments 1-4 comprises the following components in parts by weight:
the performance test of the anti-aging cream containing Ampelopsis grossedentata prepared in the example 1 to the comparative example 1 (the common O/W cream prepared by using the 0.1% Ampelopsis grossedentata leaf extract) and the test items comprise:
1. stability test
100g of each of the creams of examples 1 to 4 and comparative example 1 was placed in a sealed glass bottle and subjected to a three-month-old high-temperature aging test under test conditions of 40 ℃ to observe changes in appearance at the end of the test.
And (3) testing results: the creams of examples 1-4 were normal in color, unchanged, while the appearance of comparative example 1 turned yellow.
Secondly, efficacy testing:
the test method comprises the following steps:
a panel one (100) used a common wrinkle-removing product on the market, 2 times a day, in the morning and evening, for 1 month continuously;
group two (100 persons) used the product of example 1 of the present invention 2 times a day in the morning and evening for 1 month;
a third group (100 persons) used the product of example 2 of the present invention 2 times a day in the morning and at the evening for 1 month;
a panel of four (100 persons) using the product of example 3 of the invention 2 times a day in the morning and evening for 1 month;
group five (100 persons) used the product of example 4 of the present invention 2 times a day in the morning and evening for 1 month;
six (100) subgroups used the product of the invention example 2 to stand for 3 months at normal temperature, and then used for 1 month continuously in the morning and at night each day;
seven (100 persons) of subgroup were kept in the morning and evening 2 times a day for 1 month after 3 months using the Ampelopsis dentata leaf extract ordinary O/W cream of this comparative example 1.
Table 2: and (3) efficacy test results:
grouping | Wrinkle reduction | Deep wrinkle disappearance | Without improvement | High efficiency |
Group one | 62 | 5 | 33 | 67% |
Group two | 76 | 24 | 0 | 100% |
Group III | 69 | 31 | 0 | 100% |
Group four | 81 | 19 | 0 | 100% |
Group five | 72 | 28 | 0 | 100% |
Six group | 79 | 21 | 0 | 100% |
Seven small group | 35 | 1 | 64 | 36% |
And (4) analyzing results: the products of examples 1-4 of the present application are effective in removing wrinkles and maintain their color and use efficacy after being left for a period of time. The application adopts a W/O/W multiple emulsification system, the ampelopsis grossedentata leaf extract is dissolved in a water phase, the water phase containing the ampelopsis grossedentata leaf extract is emulsified through a lipophilic emulsifier to form a water-in-oil W/O emulsion system, most of the water phase in the formula is emulsified with W/O emulsion to form the W/O/W system, the ampelopsis grossedentata leaf extract is wrapped in the W/O emulsion of the formula to isolate external oxygen, PH and metal ions, the risk of oxidation of the ampelopsis grossedentata leaf extract is greatly reduced, the color stability of a product is protected, the color change of the ampelopsis grossedentata is reduced, the ampelopsis grossedentata, a humectant and an emollient in the product can keep activity and stability, the effects of moistening and moisturizing are achieved, the free radicals of the skin are removed, the effects of oxidation resistance and aging resistance are achieved, increase the use and storage time of the product.
Claims (10)
1. An anti-aging cream containing Ampelopsis grossedentata is characterized by comprising the following raw materials in percentage by weight: 0.01-3.0% of ampelopsis grossedentata leaf extract, 3-12% of lipophilic emulsifier, 3.5-14% of hydrophilic emulsifier, 10-15% of humectant, 8-12% of emollient, 1-3% of thickener, 0.05-0.3% of auxiliary material and the balance of water, wherein the total mass of the components is 100%.
2. The anti-aging cream containing Ampelopsis grossedentata as claimed in claim 1, wherein the anti-aging cream containing Ampelopsis grossedentata is of W/O/W structure, wherein the internal water phase is composed of the extract of Ampelopsis grossedentata leaves and a part of water, the oil phase is composed of lipophilic emulsifier, hydrophilic emulsifier and emollient, and the external water phase is composed of humectant, thickener and the rest water.
3. The anti-aging cream containing ampelopsis grossedentata according to claim 1, wherein the lipophilic emulsifier is one or a combination of two or more of sucrose polystearate, cetyl palmitate, glyceryl stearate, PEG-100 stearate, and hydrogenated lecithin.
4. The anti-aging cream containing Ampelopsis grossedentata according to claim 1, wherein the hydrophilic emulsifier is one or a combination of sorbitan isostearate and hydrogenated polyisobutene.
5. The cream as claimed in claim 1, wherein the extract of Ampelopsis grossedentata comprises 60-98% of total flavonoids of Ampelopsis grossedentata and 60-98% of dihydromyricetin.
6. The anti-aging cream containing Ampelopsis grossedentata according to claim 1, wherein said emollient is one or a combination of two or more of jojoba oil, shea butter, octyl methicone, bisabolol, dimethicone, cetyl alcohol, octyl methicone, meadowfoam seed oil, orange peel oil, grapefruit peel oil.
7. The anti-aging cream containing ampelopsis grossedentata according to claim 1, wherein the moisturizer is any one or a combination of a polyol moisturizer and a polysaccharide moisturizer;
the polyalcohol humectant is one or any combination of glycerol, diglycerol, butanediol, propylene glycol, dipropylene glycol, sorbitol, panthenol, allantoin, polyethylene glycol-400, and PPG-10 methyl glucose ether;
the polysaccharide humectant is one or any combination of hyaluronic acid, sodium hyaluronate, pullulan, trehalose and lima bean seed extract.
8. The cream of claim 1, wherein the auxiliary materials comprise an aromatizer and a bacteriostatic agent, the aromatizer is essence or essential oil, and the bacteriostatic agent is one or any combination of 1, 2-hexanediol, caprylyl glycol, ethylhexyl glycerin and caprylate glycerin.
9. The anti-aging cream containing Ampelopsis grossedentata according to claim 1, wherein the thickener comprises one or any combination of carbomer, xanthan gum, modified acrylic acid copolymer.
10. A method of preparing anti-aging cream containing ampelopsis grossedentata according to any of claims 1 to 9, characterized by comprising the steps of:
(1) weighing the ampelopsis grossedentata leaves and part of water according to the formula ratio, and uniformly mixing to form an internal water phase;
(2) weighing lipophilic emulsifier according to the formula ratio, and uniformly mixing to form a first oil phase;
(3) slowly adding the internal water phase in the step (1) into the first oil phase in the step (2) to form a water-in-oil W/O emulsion;
(4) weighing hydrophilic emulsifier and emollient according to the formula ratio, heating to 80-85 deg.C, stirring and dissolving to form a second oil phase;
(5) weighing the rest water, the humectant and the thickener according to the formula ratio, heating to 80-85 ℃, stirring and dissolving to obtain an external water phase;
(6) pumping the second oil phase in the step (4) into the external water phase in the step (5), homogenizing and stirring for 5-15min, adding the water-in-oil W/O emulsion in the step (3) when the temperature reaches 50-55 ℃, homogenizing and stirring uniformly, slowly homogenizing and stirring until the paste is fine and uniform, adding auxiliary materials when the temperature reaches 45-50 ℃, cooling to 40 ℃, adjusting the pH to 5.5-6.5, and discharging.
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CN115531275A (en) * | 2022-11-04 | 2022-12-30 | 广州品硬生物科技有限公司 | Soothing and repairing essence and preparation method thereof |
CN116808115A (en) * | 2023-05-31 | 2023-09-29 | 姚美华 | Application of ampelopsis grossedentata extract in preparation of antibacterial and/or repairing products |
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