KR101756812B1 - Cosmetic composition for skin moisturing effect comprising fermentation extract and oxygen water - Google Patents
Cosmetic composition for skin moisturing effect comprising fermentation extract and oxygen water Download PDFInfo
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- KR101756812B1 KR101756812B1 KR1020150104289A KR20150104289A KR101756812B1 KR 101756812 B1 KR101756812 B1 KR 101756812B1 KR 1020150104289 A KR1020150104289 A KR 1020150104289A KR 20150104289 A KR20150104289 A KR 20150104289A KR 101756812 B1 KR101756812 B1 KR 101756812B1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/22—Peroxides; Oxygen; Ozone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
Abstract
The present invention relates to a cosmetic composition for skin moisturizing including a fermented extract and oxygenated water. More specifically, the present invention relates to a cosmetic composition for skin moisturizing including a fermented extract and oxygenated water, A cosmetic composition for moisturizing the skin is provided.
The cosmetic composition for skin moisturizing of the present invention effectively absorbs cosmetic ingredients to the skin to provide excellent moisturizing effect and provides antioxidative effect and the like, thereby being able to form a glossy, healthy and smooth skin, Can be usefully used as a component.
Description
The present invention relates to a cosmetic composition for skin moisturizing, and more particularly to a cosmetic composition for moisturizing skin containing a fermented extract.
The skin is divided into three layers of epidermis, dermis and subcutaneous fat tissue in order from the outside, and functions to protect the human body from physical and chemical stimulation from external environment. In particular, the skin carries about 65 to 70% of the human body's moisture, that is, various physiologically active substances necessary for the human body, and helps the skin to maintain a soft and moist state, It plays an important role. In addition, the epidermis is divided into stratum corneum, granular layer, superficial layer, and basal layer from the outside. Cells of the stratum corneum act like bricks, and intercellular lipids between keratinocytes act like mortar to form skin barrier [J. Invest. Dermatol. 80 (Suppl.), 44-49. 1983]. The stratum corneum of the epidermis contains about 10 to 20% of water and is located at the outermost part of the human body, thereby suppressing evaporation of water to the outside of the body, and blocking the excessive penetration of substances from the outside. These stratum corneum surfaces are wrapped with a thin natural protective film made of sebum from the sebaceous glands and perspiration from the sweat glands, which can prevent water evaporation. To explain further, you can think of a sponge (stratum corneum) that fills up with water wrapped in a plastic wrap (a natural protective film) that does not pass water. The cells that make up this stratum corneum have a high concentration of Natural Moisturizing Factor (NMF), which is a water-soluble component, which helps the skin to maintain flexibility and maintain proper moisture. For example, The material is not only water-soluble, but also effectively combines with moisture to inhibit drying of moisture from the skin [J. Invest. Dermatol. 54, 24-31, 1970]. However, there is a tendency that the skin temperature is controlled by the change of the environment or the life pattern, the artificial temperature control of the cooling / heating, the skin stress due to various stresses and environmental pollution generated in the social life, The moisture of the stratum corneum is decreased, the skin becomes dry, the surface becomes rough, and the skin appears to be dull and dull. Therefore, the need for a skin moisturizer is increasing.
In general, cosmetics are used to protect the skin from external factors and to create a colorful look with added color tone, which is usually a chemical that uses the interaction of chemical components. When the main ingredient of the cosmetic material is a chemical ingredient as described above, a long-term skin effect may cause side effects depending on the person, which may cause damage to the skin. Also, It causes skin fatigue phenomenon easily, even if keratin is generated or elasticity is lowered.
Generally, the interval of the skin cells is 70 to 80 nm in size, and the cosmetic ingredient should be smaller in order to permeate into the skin cell gap. However, since most of the molecular weight of cosmetics is larger than this, cosmetics are not able to pass through the dermis and are turned around. Liposomes, nanoparticles, and the like.
One of the ways to do this is to consider the process of fermentation. Fermentation is the process by which microorganisms degrade organic matter using their own enzymes. Fermentation is the process by which each component is degraded by the action of microorganisms and another new component is synthesized, which increases nutritional value and creates new nutrients. The fermentation process has the advantage of increasing the bioavailability as well as enhancing the absorption rate of the body by decomposing organic matter into a low molecular structure. Accordingly, the fermentation ingredient can be absorbed to the dermis layer because the microparticles and the yeast react with each other during the fermentation of the raw material and the molecular particles are decomposed to 80 nm or less.
Another reason to pay attention to the fermentation raw material is to produce a new substance through the process of new water decomposition through fermentation. Comparing the nutrients of representative fermented food, Chungkookjang, with the nutrients of the raw soybean, it can be confirmed that essential amino acids, vitamins B1 / B2, niacin, and pantothenic acid were produced after fermentation process. Most fermented raw materials are known to have increased protein, amino acid, vitamins, and organic acids through microbial metabolism. Actual microorganisms are living, and they produce vitamin B groups such as folic acid, riboflavin, niacin, thiamine, and biotin, and the nutrients that depend on which materials are fermented are different.
In addition, some raw materials taken from nature may contain toxic substances that can irritate and cause skin troubles. In the fermentation process, the toxic substance is changed or removed as a safety substance and the stability becomes relatively high. Through the actual fermentation process, toxic substances such as heavy metals and pesticides in the material are removed and heavy metals in the skin are also released. In addition, yeast natural fermentation produces substances that prevent other harmful microorganisms from growing, reducing the chance of adverse effects on skin.
There are many limitations when the skin tries to absorb the active ingredient contained in the natural product. Because the natural active ingredients are larger than the molecular size that can be absorbed by human skin, it is necessary to cut them finely when they are used as cosmetic raw materials. The ingredients that have undergone fermentation by using microorganisms can be absorbed into the skin without loss of efficacy and effectiveness, can act on the skin, maintain the unique moisturizing effect of the natural ingredients, and anticipate synergistic effects such as antioxidative, antibacterial and anti-inflammatory effects have.
On the other hand, olive trees, a symbol of longevity, are not to be abandoned. Fruit is used as an olive oil, and this oil is rich in unsaturated fats that are beneficial to vascular health. Leaves in the mouth The dove in the mouth means peace, and the olive pipe made of olive leaves and branches is symbolized by glory on the winner of the Olympic marathon. These olive leaves were also used as medicine from ancient Egypt. There are traces of olive leaf water used as a preservative when making the royal family mummified, and there is also evidence of treating the disease with sacred water given to high fever patients. The main role of sterilization power is Oleuropein, which is absorbed into the blood by separating the polyphenol component into the oleic acid and the aglycone by the acid and enzyme on the body. Absorbed Euleriolic Acid and Aglycone cause blood, bacteria, viruses, fungi, and bacteria to penetrate into various parts of the body while destroying the proteins that encircle the strains to prevent them from further activating. Supply is interrupted and sterilized. These olefinic fins are distributed in the bark, leaves, roots, and fruits of olive trees, but they are presumed to be distributed most in olive leaves. The content of olive - eurfin in the leaf extract is 50 times that of olive oil.
Oleuropein, an antioxidant, acts to relieve aging by eliminating free radicals. The antioxidant power of the olive leaf extract is known to be 4 times that of vitamin C, which is an antioxidant vitamin, and twice that of green tea or grape seed extract (see the results of ORAC research by Dr. Philip Sheras, team of the Australian Complementary Medicine Center) It is known that it can prevent skin aging such as increase of elasticity and decrease in elasticity, and also inhibits inflammation such as redness, thereby helping to prevent skin damage (refer to a joint research result of Ehime University, Japan powder medicine). The results of the research on the wound healing effect and antioxidant power of the olive leaf and the regeneration effect of the main ingredient oleuropein are as follows. [Note 1] Olive leaf extract and its main component oleuropein prevent chronic ultraviolet B radiation- induced skin damage and carcinogenesis in hairless mice. 2. Wound repair potential of Olea europaea L. leaf extracts revealed by in vivo experimental models and comparative evaluation of extracts' antioxidant activity.
Peppermint is especially effective in sterilization and insecticidal action of mint, and it is effective for removing bad breath and used for toothpaste. Leaves are used as a padded poultice for skin irritation, bruises, and itching. Peppermint contains tannins, flavonoids and phenolic acids, which not only promote antimicrobial application (antiviral, antibacterial) in our body, promote digestion, enhance liver function, relax blood vessels and improve blood circulation It plays a role in lowering the blood cholesterol level. Also, vitamins A, C, niacin, and magnesium. It contains nutrients such as iron, iodine, potassium, copper, and sulfur.
It was called peppermint because the fragrance resembled the poignant nature of pepper. Origin is Europe, but also in Europe, the United States / Japan / China also grows. Menthol, which is the main ingredient of essential oils, is effective in relieving skin and mucous membranes, and is effective in antibacterial and pain relief. It is used as an edible, medicinal and aromatic agent in ancient Egypt, an important ingredient of perfume in ancient Greece, Was used as an additive. Peppermint is particularly effective for medicinal purposes in Europe. Comparing the content of menthol, it does not reach the mint, but the other ingredients that produce a unique flavor and sweetness make it more effective than mint. And such ingredients stimulate the stomach wall to release the gas in the intestines and promote digestion, and refreshing fragrance makes the mouth fresh, so it fits well after the meal. It also has a tonic and antiparasitic effect and is effective in toothpaste because it is effective in removing bad breath. If the leaves are used as a poultice, it will be effective for skin irritation, bruise, itching, and it will last for a long time if left in the bathroom.
Red clover is a leguminous plant originating in Europe and is also called rabbit water. It has been cultivated for a long time as an animal that is cultivated for animal feed. Red clover is called purple clover because it is pink with flower. Red clover, a shamrock familiar in Korea, is a herb used as an herb from ancient times. It is widely applied to blood purification, natural hormones, menopausal women's disease, neural stabilization, strengthening of the immune system, and flowers have anti-inflammatory and diuretic effects. Drinking flowers with herbal tea improves eczema and cough. It is also used for arthritis.
Red clover has a function to cleanse the blood and it contains natural antibiotic ingredient and it is good for skin diseases such as acne, eczema and psoriasis, and it is also used by many people with skin diseases. Red clover is important not only for livestock but also for making tea with clover petals and for salads to enhance the taste and flavor of the food. The clover contains fine minerals called molybdenum. It has been known to have a good effect on removing waste products. Recently, it has been known that clover contains many isoflavones, which are known to be good for women. .
Also, oxygen water means water containing more oxygen than ordinary water. Ordinary water contains 6 to 8 mg of oxygen per liter. Oxygen water, on the other hand, contains 4 to 10 times more oxygen than ordinary water, and it is known to help not only the metabolism of animals / plants but also the immunity against diseases. Recently, we are approaching consumers in various forms in accordance with the current trend of well-being life, and many effects are being revealed through various studies.
Oxygen efficacy includes atopy skin treatment, enhancement of blood circulation, blood pressure control, anti-bacterial and anti-virus, tissue regeneration, detoxification, increased energy supply to cells, physical / Increased efficiency, metabolism, relieve stress, lower fatigue, skin beauty effect, high diet through lactic acid decomposition, prevention and treatment of allergy such as rhinitis and atopy.
However, a mixture of olive leaf fermentation extract, peppermint leaf fermentation extract and red clover fermentation extract, and fermented extract and oxygenated water has not been reported to be useful for skin moisturizing.
In the following, conventional techniques for skin moisturizing cosmetic compositions using natural products are described.
The invention of Patent Application No. 2002-0023735 discloses a cosmetic composition for moisturizing which contains jasmine extract, arnica extract and jarow extract, more specifically, jatamin extract, arnica extract and jarow extract in an amount of 0.01 to 60% by weight based on the total weight of the cosmetic composition And a cosmetic composition for moisturizing the skin.
In addition, the invention of Patent Application No. 2007-0103701 relates to a cosmetic composition for moisturizing comprising an extract of Prunella Vulgaris extract and Aloe Barbadensis leaf as an active ingredient, and more particularly to a cosmetic composition for moisturizing, The present invention relates to a moisturizing cosmetic composition containing as an active ingredient, an extract of honey grass leaf containing oleanolic acid and urosolic acid and an aloe vera extract which is a plant for supplying moisture to skin.
In addition, the invention of Patent Application No. 2013-0038017 relates to a skin aging-inhibiting effect, a whitening effect, a moisturizing cosmetic composition and a manufacturing method thereof of a fermented liquid of a crude oil extract, more specifically, One extract of water or a solvent such as water is added to the dry weight of the powdered corn syrup at a temperature of 25 to 30 DEG C for 12 to 24 hours. The extract is filtered with a filter cloth and sterilized with a 0.2-μm filter. The skin aging inhibitory effect and the whitening effect of the fermented milk extract of fermented milk extract containing the fermented extract of fermented sour milk obtained by adding 5% to 10% of a culture medium of Kazachstania unispora and culturing at 20 to 25 ° C for 4 to 7 days And a method for manufacturing a moisturizing cosmetic composition.
In addition, the invention of Patent Application No. 2011-0116726 relates to a method for manufacturing a moisturizing cosmetic composition using the extract of Dust extract and a moisturizing cosmetic composition prepared therefrom, A step of inoculating lactic acid bacteria to the dried doduk and then fermenting; Aging the fermented broth after the fermentation to obtain a fermented broccoli; drying the obtained fermented broccoli; Adding the dried fermented broth to a solvent to prepare an extract; And adding the extract to an emulsion base for a cosmetic preparation to prepare a cosmetic composition, and a moisturizing cosmetic composition prepared therefrom.
Also, the invention of Patent Application No. 2010-0067781 relates to a fermentation method of mulberry or its extract, a fermented extract thereof and a cosmetic composition containing the same, and more particularly to a method of fermenting mulberry or its extract naturally fermenting, It is possible to remove the smell of harmful bacteria such as spoilage bacteria, Escherichia coli, and anaerobic bacteria by removing the odor from the harmful harmful substance by extracting it with the salt of fermented by adding the salt of the extract, and to improve the whitening, anti-aging, anti wrinkle, A fermented extract thereof, and a cosmetic composition containing the fermented extract.
In addition, the invention of Patent Application No. 2008-0125089 relates to a cosmetic composition for moisturizing the skin, and more particularly to a cosmetic composition for skin moisturizing, which comprises a fermented extract of fermented sour milk obtained by culturing yeast or lactic acid bacteria with and without acid The present invention relates to a cosmetic composition which is free from the problem of inducing disease and has excellent skin moisturizing effect.
In addition, the invention of Patent Application No. 2012-0049648 includes (i) Fermented Persicae Semen Extract, (ii) Fermented Pumpkin Seed Extract, (iii) Artemisia princeps Pamp Extract, and And mixtures thereof as an active ingredient. The present invention also relates to a cosmetic composition for moisturizing the skin.
An object of the present invention is to provide a cosmetic composition for skin moisturizing which minimizes the problems of the prior art, has excellent skin moisturizing effect, has an antioxidative effect, and can form healthy and smooth skin.
In order to achieve the above object, the present invention provides a cosmetic composition for skin moisturizing comprising an extract of fermentation including olive leaf fermentation extract, peppermint leaf fermentation extract and red clover fermentation extract and oxygenated water as an active ingredient.
The cosmetic composition for skin moisturizing of the present invention effectively absorbs cosmetic ingredients to the skin to provide excellent moisturizing effect and provides antioxidative effect and the like, thereby being able to form a glossy, healthy and smooth skin, Can be usefully used as a component.
Hereinafter, the present invention will be described in detail.
The present invention provides a cosmetic composition for skin moisturizing comprising an extract of fermentation comprising an olive leaf fermentation extract, a peppermint leaf fermentation extract and a red clover fermentation extract and oxygenated water as an active ingredient.
As one component of the skin moisturizing cosmetic composition of the present invention, an olive leaf fermentation extract, a peppermint leaf fermentation extract and a red clover fermentation extract are included.
The olive leaf fermentation extract can be obtained by the following method.
First, olive leaf dry powder is suspended in purified water, and lactic acid bacteria are contacted with this suspension and cultured to obtain a culture. The lactic acid bacteria may be Lactobacillus spp . , And the culture is carried out at a culture temperature of 20 to 25 캜 for 1 to 3 days, preferably at a culture temperature of 25 캜 for about 3 days. The thus obtained culture was centrifuged to obtain a supernatant, which was filtered to obtain an olive leaf fermentation extract.
In addition, the peppermint leaf fermentation extract and the red clover fermentation extract can be obtained by the same method as the above-mentioned preparation method of the olive leaf fermentation extract. Herein, olive leaves, peppermint leaves, and red clover are all available in the art and can be obtained by various routes.
In addition, the olive leaf fermentation extract, peppermint leaf fermentation extract and red clover fermentation extract of the present invention can be obtained in the form of a fermentation extract as described above, as well as three dry powdery raw materials are suspended in purified water together, Followed by fermentation extraction. More specifically, olive leaf dry powder, peppermint leaf dry powder and red clover dry powder are suspended in purified water at once, and the suspension is contacted with lactic acid bacteria and cultured to obtain a culture.
In addition, the other component of the cosmetic composition for skin moisturizing of the present invention includes oxygenated water.
In the present invention, oxygen water generally used in the art can be used. For example, unlike the oxygen dissolution technique using a pressurized or forced oxygen dissolving technique, the oxygen dissolution technique converts water molecules into nano particles, So that oxygen is spontaneously dissolved between the molecules [see Patent No. 10-0948813]. Further, the oxygen water may contain dissolved oxygen of 20 to 200 ppm. By supplying water containing such a high concentration of oxygen directly on the skin, it can return the hypoxic state of the skin cells to the original state and activate the cells, thereby improving the moisturizing power.
The cosmetic composition for skin moisturizing of the present invention can be obtained by adding oxygenated water to an olive leaf fermentation extract, a peppermint leaf fermentation extract and a red clover fermentation extract as described above.
In this case, the cosmetic composition for skin moisturizing may contain the respective fermentation extract and oxygen water in the same weight ratio, and more specifically, it may contain 1 to 10% by weight of the olive leaf fermentation extract, 1 to 10% of the peppermint leaf fermentation extract 1 to 10% by weight of red clover fermentation extract, and 1 to 10% by weight of oxygenated water. If the amount is less than the above range, the moisturizing effect and antioxidation effect on the skin may be deteriorated. If it exceeds the above range, the effect of additional addition may not be exhibited.
The cosmetic composition for skin moisturizing according to the present invention effectively absorbs cosmetic ingredients to the skin to provide excellent moisturizing effect and provides antioxidative effect and the like, which can form a glossy, healthy and smooth skin. And can be usefully used as an active ingredient.
Examples of products to which the present composition can be added include cosmetics such as various creams, lotions and skins, and cleansing, cleansing agents, soaps, treatments, and essences. More specifically, The composition has a formulation selected from the group consisting of suspensions, emulsions, pastes, gels, creams, lotions, powders, soaps, surfactant-containing cleansing, oils, powder foundations, emulsion foundations, wax foundations and sprays.
The cosmetic composition of the present invention comprises a composition selected from the group consisting of water-soluble vitamins, oil-soluble vitamins, high molecular weight peptides, polymeric polysaccharides, sphingolipids and seaweed extracts.
The water-soluble vitamin is not particularly limited as long as it can be compounded in cosmetics. Preferably, vitamin B, vitamin B2, vitamin B6, pyridoxine, pyridoxine hydrochloride, vitamin B12, pantothenic acid, nicotinic acid, nicotinic acid amide, folic acid, vitamin C, (Sodium thiamine hydrochloride, sodium ascorbic acid salt, etc.) or derivatives thereof (sodium ascorbic acid-2-phosphate salt, ascorbic acid-2-phosphate magnesium salt, etc.) can also be added to water-soluble vitamins . The water-soluble vitamin can be obtained by a conventional method such as a microorganism conversion method, a purification method from a culture of a microorganism, an enzymatic method, or a chemical synthesis method.
Usable vitamins include vitamins such as vitamin A, carotene, vitamin D2, vitamin D3, vitamin E (d1-alpha tocopherol, d-alpha tocopherol, d-alpha tocopherol) Alpha-tocopherol vitamin E, DL-pantothenyl alcohol, D-pantothenyl alcohol, pantothenyl ethyl laurate, and the derivatives thereof (palmitic acid ascorbin, stearic acid ascorbic acid, dipalmitic acid ascorbin, dl-alpha tocopherol acetate, Ether, etc.) are also included in the usable vitamins used in the present invention. Usability Vitamins can be obtained by a conventional method such as a microorganism conversion method, a purification method from a culture of a microorganism, an enzyme or a chemical synthesis method.
The polymeric peptide may be any compound as long as it can be compounded in cosmetics, and examples thereof include collagen, hydrolyzed collagen, gelatin, elastin, hydrolyzed elastin, and keratin. The polymeric peptide can be obtained by a conventional method such as purification from a culture broth of a microorganism, an enzymatic method, or a chemical synthesis method, or it can be purified from natural products such as ducks such as pigs and cows and silk fiber of silkworms.
The polymeric polysaccharide may be any compound as long as it can be incorporated in cosmetics, and examples thereof include hydroxyethyl cellulose, xanthan gum, sodium hyaluronate, chondroitin sulfate or a salt thereof (sodium salt, etc.). For example, chondroitin sulfate or a salt thereof can be usually purified from mammals or fish.
Sphingo lipids may be any as long as they can be incorporated into cosmetics, and preferable examples thereof include ceramides, phytosphingosine and sphingoglycolipids. Sphingoid lipids can be purified from ordinary mammals, fish, shellfish, yeast or plants by conventional methods or can be obtained by chemical synthesis.
Seaweed extract may be any compound that can be incorporated into cosmetics. Preferably, the seaweed extract may be a grape extract, a red mildew extract, or a green algae extract, or may be a color guanine, arginic acid, sodium alginate, Potassium sulfate and the like are also included in the seaweed extract used in the present invention. Seaweed extract can be obtained from seaweed by a conventional method.
The cosmetic of the present invention may be blended with other essential ingredients, if necessary, in combination with the essential ingredients. Examples of the compounding ingredients that may be added include organic solvents such as a preservative component, a moisturizer, an emollient, a surfactant, an organic and inorganic pigment, an organic powder, an ultraviolet absorbent, a preservative, a bactericide, an antioxidant, a plant extract, a pH adjuster, A blood circulation accelerator, a cold agent, an antiperspirant agent, and purified water. Examples of the oil retaining component include ester-based oil retaining, hydrocarbon-based oil retaining, silicone-based oil retaining, fluoric oil retaining, animal retention and plant retention. Examples of ester-based fats include glyceryl tri-2-ethylhexanoate, cetyl 2-ethylhexanoate, isopropyl myristate, butyl myristate, isopropyl palmitate, ethyl stearate, octyl palmitate, isostearyl isostearate, Butyl isopropyl myristate, isopropyl myristate, isopropyl myristate, isopropyl myristate, isopropyl myristate, isopropyl myristate, butyl, ethyl linoleate, isopropyl linoleate, ethyl oleate, isosilyl myristate, isostearic acid isostearyl, isostearyl palmitate, octyldodecyl myristate, Trimethylol propane, triisostearic acid trimethylol propane, tetra 2-ethylhexanoic acid pentaerythritol tetra (2-ethylhexanoate) , Decyl caprylate, decyl laurate, hexyl laurate, decyl myristate, myristyl myristate, myristine acid stearate, stearyl stearate, decyl oleate, ricinoleic acid Isopropyl palmitate, isostearyl stearate, isostearyl stearate, isodecyl oleate, octyldodecyl oleate, octyldodecyl linoleate, isopropyl stearate, isopropyl stearate, isopropyl stearate, Ethylhexanoate, stearyl 2-ethylhexanoate, stearyl 2-ethylhexanoate, hexyl isostearate, ethylene glycol dioctanoate, ethylene glycol dioleate, propylene glycol dicaprate, di (capryl, capric acid) propylene glycol, Propylene glycol dicaprylate, propylene glycol dicaprylate, neopentyl glycol dicaprate, neopentyl glycol dioctanoate, glyceryl tricarboxylate, glyceryl triunsaturated acid, glyceryl triisopalmitate, glyceryl triisostearate, octyl dodecanoate Silane, octanoic acid, octanoic acid, octanoic acid, octanoic acid octanoate, octanoic acid octanoate, octanoic acid octanoate, octanoic acid octanoate, octanoic acid octanoate, octanoic acid octanoate, Octyldecyl lactate, octyldecyl lactate, polyglycerin isostearic acid ester, triisocetyl citrate, triisocylic citrate, triisooctyl citrate, lauryl lactate, myristyl lactate, octyldecyl lactate, citric acid tri Ethylhexyl stearate, diethyl stearate, ethyl stearate, ethyl stearate, ethyl stearate, ethyl stearate, ethyl stearate, ethyl stearate, But are not limited to, dioctyl sebacate, cholesteryl stearate, cholesteryl isostearate, cholesteryl hydroxystearate, cholesteryl oleate, dihydrocholestearyl oleate, pitostearyl isostearate, Stearoyl hydroxystearic acid isostearyl, 12-stearoyl hydroxystearic acid stearyl, Stearoyl hydroxystearic acid, and esters such as 12-stearoyl hydroxystearic acid and saxate.
Examples of the hydrocarbon hydrocarbon-based fats include hydrocarbon fats and oils such as squalene, liquid paraffin, alpha-olefin oligomer, isoparaffin, ceresin, paraffin, floating isoparaffin, polybutene, microcrystalline wax and vaseline.
Examples of silicone based oils include polymethyl silicone, methylphenyl silicone, methyl cyclopolysiloxane, octamethylpolysiloxane, decamethylpolysiloxane, dodecamethylcyclosiloxane, dimethylsiloxane-methylcetyloxysiloxane copolymer, dimethylsiloxane-methylstarchoxysiloxane copolymer, alkyl Modified silicone oils, and amino-modified silicone oils.
Examples of the fluorine-based oil include perfluoropolyether and the like. Examples of animal or vegetable oils include avocado oil, almond oil, olive oil, sesame oil, rice bran oil, new flower oil, soybean oil, corn oil, rape oil, apricot kernel oil, palm kernel oil, palm oil, castor oil, , Corn oil, palm oil, palm oil, cucumber nut oil, wheat germ oil, rice germ oil, shea butter, coltsfoot colostrum, marker daisy nut oil, mead home oil, egg oil, , Canned wax, carnauba wax, liquid lanolin, hardened castor oil, and the like.
Examples of the moisturizing agent include water-soluble low-molecular moisturizing agents, oil-soluble molecular moisturizing agents, water-soluble polymers, and oil-soluble polymers. Examples of the water-soluble low-molecular moisturizing agent include serine, glutamine, sorbitol, mannitol, sodium pyrrolidone-carboxylate, glycerin, propylene glycol, 1,3-butylene glycol, ethylene glycol, polyethylene glycol B Glycol (polymerization degree n = 2 or more), polyglycerin B (polymerization degree n = 2 or more), lactic acid, lactic acid salt and the like.
Examples of the lipid-soluble low-molecular moisturizing agent include cholesterol and cholesterol ester.
Examples of the water-soluble polymer include carboxyvinyl polymer, polyaspartic acid, tragacanth, xanthan gum, methylcellulose, hydroxymethylcellulose, hydroxyethylcellulose, hydroxypropylcellulose, carboxymethylcellulose, water-soluble chitin, chitosan, dextrin have. Examples of the oil-soluble polymer include polyvinylpyrrolidone / eicosene copolymer, polyvinylpyrrolidone / hexadecene copolymer, nitrocellulose, dextrin fatty acid ester, and polymer silicone.
Examples of the emollients include long chain acyl glutamic acid cholesteryl ester, hydroxystearic acid cholesteryl, 12-hydroxystearic acid, stearic acid, rosin acid, and lanolin fatty acid cholesteryl ester.
Examples of the surfactant include nonionic surfactants, anionic surfactants, cationic surfactants, and amphoteric surfactants. Examples of the nonionic surfactant include self emulsifying monostearic acid glycerin, propylene glycol fatty acid ester, glycerin fatty acid ester, polyglycerin fatty acid ester, sorbitan fatty acid ester, POE (polyoxyethylene) sorbitan fatty acid ester, POE sorbit fatty acid ester, POE-POP fatty acid ester, POE alkyl ether, POE fatty acid ester, POE hardened castor oil, POE castor oil, POE.POP (polyoxyethylene.polyoxypropylene) copolymer, POE.POP alkyl ether, polyether- Acid alkanolamides, alkylamine oxides, hydrogenated soybean phospholipids, and the like. Examples of the anionic surfactant include fatty acid soap, alpha-acylsulfonate, alkylsulfonate, alkylarylsulfonate, alkylnaphthalenesulfonate, alkylsulfate, POE alkyl ether sulfate, alkylamide sulfate, alkyl phosphate, POE alkyl ginseng salt, Alkylsulfosuccinates, sodium alkylsulfoacetates, acylated hydrolyzed collagen peptide salts, perfluoroalkyl phosphate esters, and the like can be given. have. Examples of the cationic surfactant include alkyl trimethyl ammonium chloride, stearyl trimethyl ammonium chloride, stearyl trimethyl ammonium bromide, cetostearyl trimethyl ammonium chloride, distearyl dimethyl ammonium chloride, stearyl dimethyl benzyl ammonium chloride, behenyl trimethyl ammonium chloride, Benzalkonium, diethylaminoethylamide stearate, dimethylaminopropylamide stearate, quaternary ammonium salts of lanolin derivatives, and the like. Examples of the amphoteric surfactant include carboxybetaine, amidebetaine, sulfobetaine, hydroxysulfobetaine, amidosulfobetaine, phosphobetaine, aminocarboxylate, imidazoline derivative, amideamine Amphoteric surfactants and the like. Examples of the organic and inorganic pigments include inorganic pigments such as silicic acid, silicic anhydride, magnesium silicate, talc, sericite, mica, kaolin, Bengala, clay, bentonite, titanium mica, titanium oxide, bismuth chloride, zirconium oxide, magnesium oxide, Inorganic pigments such as calcium sulfate, barium sulfate, magnesium sulfate, calcium carbonate, magnesium carbonate, iron oxide, chromium oxide, chromium oxide, chromium hydroxide, But are not limited to, polyamide, polyester, polypropylene, polystyrene, polyurethane, vinyl resin, urea resin, phenol resin, fluororesin, silicon resin, acrylic resin, melamine resin, epoxy resin, polycarbonate resin, Silk powder, cellulose, CI Pigment Yellow, CI Pigment Orange, and composite pigments of inorganic pigments and organic pigments thereof.
As the organic powder, metallic soap such as calcium stearate; Metal alkyl phosphates such as zinc sodium cetylate, zinc laurylate and calcium lauryl laurate; Acylamino acid polyvalent metal salts such as N-lauroyl-beta-alanine calcium, N-lauroyl-beta-alanine zinc and N-lauroylglycine calcium; Amidosulfonic acid multivalent metal salts such as N-lauroyl-taurine calcium and N-palmitoyl-taurine calcium; Such as N-epsilon-lauroyl-L-lysine, N-epsilon-palmitoylidene, N-alpha-paratyylnitine, N-alpha-lauroyl arginine, Acyl basic amino acids; N-acylpolypeptides such as N-lauroylglycylglycine; Alpha-amino fatty acids such as alpha-aminocaprylic acid, alpha-aminoaurauric acid, and the like; Polyethylene, polypropylene, nylon, polymethylmethacrylate, polystyrene, divinylbenzene-styrene copolymer, ethylene tetrafluoride, and the like. Examples of ultraviolet absorbers include paraaminobenzoic acid, ethyl parnamobenzoate, amyl paranobenzoate, octyl paranobenzoate, ethyleneglycol salicylate, phenyl salicylate, benzyl salicylate, benzyl salicylate, butylphenyl salicylate, homomenthyl salicylate, benzyl cinnamate , Octyl methoxycinnamate, dioctyl methoxycinnamate, mono-2-ethylhexane glyceryl dipyrromethoxycinnamate, isopropyl paratumoxycinnamate, diisopropyl-diisopropyl cinnamate ester mixture, Carninoic acid, ethyl urocanoate, hydroxymethoxybenzophenone, hydroxymethoxybenzophenone sulfonic acid and salts thereof, dihydroxymethoxybenzophenone, sodium dihydroxymethoxybenzophenone disulfonate, dihydroxybenzophenone , Tetrahydroxybenzophenone, 4- tert -butyl-4'-methoxydibenzoylmethane, 2,4,6-trianylino-p- (carbo-2'-ethylhexyl- 1,3,5-triazine , 2- (2-hydroxy-5-methylphenyl) benzotriazole, and the like. Examples of the bactericide include hinokitiol, trichloroacid, trichlorohydrodiphenyl ether, crohexidine gluconate, phenoxyethanol, resorcin, isopropylmethylphenol, azulene, salicylic acid, zinc filitione, benzalkonium chloride, No. 301, mononitro, eicosyl sodium, undecylenic acid, and the like. Examples of the antioxidant include butylhydroxy anisole, gallic acid propyl, and eicosorbic acid. Examples of the pH adjusting agent include citric acid, sodium citrate, malic acid, sodium malate, fumaric acid, sodium pyrophosphate, succinic acid, sodium succinate, sodium hydroxide, sodium monohydrogenphosphate and the like. Examples of the alcohol include higher alcohols such as cetyl alcohol. In addition, any of the above components may be blended within the range not to impair the objects and effects of the present invention, but is preferably 0.01 to 5% by weight, more preferably 0.01 to 5% Preferably 0.01 to 3% by weight.
The cosmetic of the present invention may take the form of a solution, an emulsion, a viscous mixture or the like. The ingredients contained in the cosmetic composition of the present invention may contain, as an active ingredient, the ingredients commonly used in cosmetic compositions in addition to the fermented extract and oxygenated water. Examples thereof include stabilizers, solubilizers, vitamins, And the like. The cosmetic composition of the present invention can be prepared in any formulations conventionally produced in the art, and examples thereof include emulsions, creams, lotions, packs, foundations, lotions, essences, and hair cosmetics. Specifically, the cosmetic composition of the present invention can be used as a skin lotion, a skin softener, a skin toner, an astringent, a lotion, a milk lotion, a moisturizing lotion, a nutrition lotion, a massage cream, a nutrition cream, a moisturizing cream, a hand cream, a foundation, , Packs, soaps, cleansing foams, cleansing lotions, cleansing creams, body lotions and body cleansers. When the formulation of the present invention is a paste, a cream or a gel, an animal fiber, a plant fiber, a wax, a paraffin, a starch, a tracer, a cellulose derivative, polyethylene glycol, silicon, bentonite, silica, talc or zinc oxide . When the formulation of the present invention is a powder or a spray, lactose, talc, silica, aluminum hydroxide, calcium silicate or polyamide powder may be used as a carrier component. In the case of a spray, in particular, chlorofluorohydrocarbons, Propane / butane or dimethyl ether. When the formulation of the present invention is a solution or an emulsion, a solvent, a solvent or an emulsifier is used as a carrier component, and examples thereof include water, ethanol, isopropanol, ethylcarbonate, ethyl acetate, benzyl alcohol, benzyl benzoate, 1,3-butyl glycol oil, glycerol aliphatic ester, polyethylene glycol or fatty acid esters of sorbitan. When the formulation of the present invention is a suspension, a carrier such as water, a liquid diluent such as ethanol or propylene glycol, a suspension such as ethoxylated isostearyl alcohol, polyoxyethylene sorbitol ester and polyoxyethylene sorbitan ester, Cellulose, aluminum metahydroxide, bentonite, agar or tracant, etc. may be used. When the formulation of the present invention is an interface-active agent-containing cleansing, it is preferable to use, as the carrier component, aliphatic alcohol sulfate, aliphatic alcohol ether sulfate, sulfosuccinic acid monoester, isethionate, imidazolinium derivative, methyltaurate, sarcosinate, Amide ether sulfate, alkylamidobetaine, aliphatic alcohol, fatty acid glyceride, fatty acid diethanolamide, vegetable oil, linolenic derivative or ethoxylated glycerol fatty acid ester.
Hereinafter, the present invention will be described in detail with reference to Examples, Experimental Examples and Formulation Examples.
However, the following Examples, Experimental Examples and Formulation Examples are merely illustrative of the present invention, and the contents of the present invention are not limited by Examples, Experimental Examples and Formulation Examples.
< Example 1> Cosmetics Preparation of composition
(1) Preparation of fermented extract
1% by weight of dried olive leaf powder, 1% by weight of dried peppermint leaf powder, or 1% by weight of dried red clover powder was added to the purified water as a culture medium for preparing the fermented extract of the present invention, Lt; / RTI > The sterilized medium was inoculated with lactobacillus lactic acid bacteria and cultured at a culture temperature of 25 캜 for about 3 days.
After the fermentation, the supernatant was separated by continuous centrifugation at 8,000 rpm. The lactic acid bacteria were removed from the supernatant by using a membrane filter equipped with a 0.2 mu m filter to obtain an olive leaf fermentation extract, a peppermint leaf fermentation extract or a retort clover fermentation extract.
(2) Cosmetics Preparation of composition
The olive leaf fermentation extract, the peppermint leaf fermentation extract or the retort clover fermentation extract prepared above and the oxygen water were mixed and stirred at the same weight ratio, respectively, to prepare a cosmetic composition.
< Experimental Example 1> NBT method Measurement of antioxidant effect
To confirm the antioxidative level of the cosmetic composition (hereinafter referred to as 'composition of Example 1') containing the olive leaf fermentation extract, peppermint leaf fermentation extract, fermented extract of Red Clover and oxygenated water obtained in Example 1, And antioxidant, retinol, and BHT, and antioxidant was measured by NBT method.
The active oxygen produced by xanthine and xanthine oxidase was measured by the NBT method and the effect of the test substance on the removal of active oxygen, that is, the effect of scavenging reactive oxygen was measured.
The NBT method is a method for producing active oxygen by xanthine and xanthine oxidase and measuring the blue color produced by the reaction of the produced active oxygen with Nitro Blue Tetrazolium (NBT) at a wavelength of 560 nm, The oxygen scavenging rate was measured and the measurement method was as follows.
2.4 ml of 0.05 M Na 2 CO 3 , 0.1 ml of a 3 mM xanthine solution, 0.1 ml of a 3 mM EDTA solution, 0.1 ml of a BSA solution and 0.1 ml of a 0.72 mM NBT solution were added to a bial, and a sample solution The composition of Example 1, retinol and BHT), respectively, and left at 25 캜 for 10 minutes. After incubation, 0.1 ml of a xanthine oxidase solution was added, and the mixture was rapidly stirred. The mixture was incubated at 25 ° C for 20 minutes, and 0.1 ml of a 6 mM CuCl 2 solution was added thereto to stop the reaction. The absorbance at 560 nm (St) Were measured. The blank test was performed using distilled water instead of the sample solution, and the absorbance (Bt) was measured in the same manner as described above. The blank of the sample solution was measured for absorbance (Bo) in the same manner as above using distilled water instead of xanthine oxidase solution.
The measurement results were calculated by the following equation (1).
[Equation 1]
(%) = [1- (S t -S o ) / (B t -B o )] X 100
Here, S t : the absorbance of the sample solution at 560 nm after the enzymatic reaction
B t : Absorbance at 560 nm after enzyme reaction of blank test solution
S o : absorbance at 560 nm before the reaction in the absence of enzyme in the sample solution
B o : Absorbance at 560 nm before the reaction in the absence of enzyme in the blank test solution
As can be seen from the results of the measurement of the antioxidative effect shown in Table 1 above, excellent antioxidative effects were observed in all of the samples tested at the treatment concentration of 0.1 wt% as an active oxygen scavenging ratio of 90% or more. It showed higher antioxidative effect than retinol and BHT, which are common antioxidants.
From the above results, it was deduced that the cosmetic composition containing the olive leaf fermentation extract, the peppermint leaf fermentation extract, the red clover fermentation extract and the oxygenated water composition as the active ingredient of the present invention is excellent in antioxidative effect.
< Experimental Example 2> Cosmetics The skin of the composition Moisturizing Measure
(1) Cosmetics Preparation of a skin moisturizing product containing the composition
The products containing the cosmetic composition of the present invention and conventional products were prepared as shown in Table 2 below.
More specifically,
① Olive leaf fermentation extract, peppermint leaf fermentation extract, red clover fermentation extract, oxygen water, and / or cetanol, honey wax, surfactant, and vegetable oil were dissolved by heating to 80 ° C.
② Add concentrated glycerin, preservative, and purified water to 100, and dissolve by heating to 80 ℃.
(3) The above (1) was added to (2) and emulsified by mixing and stirring with a stirrer.
(4) The carboxyvinyl polymer and triethanolamine were added while stirring the contents of the above (3), and the mixture was stirred using a stirrer.
(5) The above stirred contents were cooled to 40 ° C, and then the fragrance was added thereto. The mixture was cooled to 30 ° C and aged.
(2) Measurement of skin moisturizing effect
To compare the skin moisturizing effects of the cosmetic preparations according to Examples 2 and 3 and Comparative Example 1 prepared above, 20 women of 20 to 40 years old were subjected to the following tests: Formulation Example 1, Formulation Example 2, and Comparative Example The product of Example 1 was applied evenly, and after about 90 minutes, the moisture resistance before and after the application was evaluated by a moisture meter (CM 820) using a moisture meter (CM 820).
(△ Hydration)
As a result of measuring the skin moisturizing effect of the cosmetic composition, excellent moisturizing effect of the cosmetic composition containing olive leaf fermentation extract, peppermint leaf fermentation extract, red clover fermentation extract and oxygenated water of the present invention was confirmed.
In order to compare the usability of the products according to Examples 2 and 3 and Comparative Example 1 above, panel tests were conducted on 20 women aged 20 to 40, and the results are shown in Table 4 below.
The evaluation grade is as follows. In the evaluation method, 5 points were stabilized and the numerical value was the average value of 20 persons.
1. Very bad
2. It is bad.
3. It is normal.
4. Good.
5 Very good.
As a result of the investigation, it can be seen that the cosmetic composition of the present invention is significantly superior in spreadability, skin permeability, smoothness and glossiness than the conventional products.
An example of a cosmetic composition containing the composition of Example 1 of the present invention is described below through Formulation Examples 1 to 4.
≪ Formulation Example 1 >
As an example of a cosmetic product, a nutritional lotion containing the composition of Example 1 of the present invention was prepared by a conventional method according to the composition shown in Table 5 below.
≪ Formulation Example 2 >
As one example of cosmetics, nutritional creams containing the composition of Example 1 of the present invention were prepared in a conventional manner according to the composition shown in Table 6 below.
≪ Formulation Example 3 >
As an example of a cosmetic product, a pack containing the composition of Example 1 of the present invention was prepared in a conventional manner according to the composition shown in Table 7 below.
≪ Formulation Example 4 > Lotion
As an example of cosmetics, lotions containing the composition of Example 1 of the present invention were prepared in a conventional manner according to the composition shown in Table 8 below.
Claims (6)
The fermented extract obtained by suspending an olive leaf dried powder in purified water, inoculating Lactobacillus spp., And culturing at a culture temperature of 20 to 25 캜 for 1 to 3 days,
A fermented extract obtained by suspending a peppermint leaf dried powder in purified water, inoculating Lactobacillus spp. And culturing at a culture temperature of 20 to 25 캜 for 1 to 3 days,
Characterized in that the fermented extract of Red Clover is a fermented extract obtained by suspending Red Clover dried powder in purified water, inoculating Lactobacillus spp., And culturing at a culture temperature of 20 to 25 ° C for 1 to 3 days Wherein the cosmetic composition for skin moisturizes.
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KR102116022B1 (en) * | 2019-07-16 | 2020-05-27 | (주)코이즈 | Cosmetic composition with microspheres containing high concentration of oxygen and method for producing the same |
KR20220156119A (en) | 2021-05-17 | 2022-11-25 | 래스 주식회사 | Cosmetic composition comprising extract of white clover for enhancing skin barrier |
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CN107412077A (en) * | 2017-09-05 | 2017-12-01 | 安徽华健生物科技有限公司 | It is a kind of it is sun-proof repair skin olive growing leaves it is ultraviolet stress submerged fermentation extract preparation method |
KR102147801B1 (en) * | 2018-10-05 | 2020-08-26 | 아주대학교 산학협력단 | Pharmaceutical composition comprising fermented extract of peppermint for preventing or treating of respiratory diseases |
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KR102422924B1 (en) * | 2020-06-03 | 2022-07-21 | (주)나우코스 | Cosmetic composition comprising mixture of fermentation extracts of olea europaea leaf for alleviating skin inflammation or skin hyperpigmentation by yellow sand or fine dust |
KR102315510B1 (en) | 2021-03-22 | 2021-10-22 | 협동조합 바이오융합기술 | Antioxidant composite containing lactic acid bacteria and Manufacturing method thereof |
KR102325570B1 (en) * | 2021-07-28 | 2021-11-12 | 주식회사 라오가닉 | Cosmetic composition for moisturizing and skin barrier improvement containing nanoliposomes containing oxygen water and ceramide, and method for preparing the same |
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KR102116022B1 (en) * | 2019-07-16 | 2020-05-27 | (주)코이즈 | Cosmetic composition with microspheres containing high concentration of oxygen and method for producing the same |
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KR20220156119A (en) | 2021-05-17 | 2022-11-25 | 래스 주식회사 | Cosmetic composition comprising extract of white clover for enhancing skin barrier |
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