CN111803396A - Cosmetic composition based on retinaldehyde and glycylglycine oleamide and preparation method thereof - Google Patents
Cosmetic composition based on retinaldehyde and glycylglycine oleamide and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/671—Vitamin A; Derivatives thereof, e.g. ester of vitamin A acid, ester of retinol, retinol, retinal
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention discloses a cosmetic composition based on retinaldehyde and glycylglycine oleamide and a preparation method thereof. The cosmetic composition comprises: 6-15% of glycerol, 2-5% of butanediol, 0.1-0.5% of xanthan gum, 0.05-0.1% of disodium ethylene diamine tetraacetate, 0.1-0.5% of panthenol, 1-3% of methyl glucose sesquistearate, 1-3% of PEG-100 stearate, 3-6% of polydimethylsiloxane, 4-8% of squalane, 0.1-0.5% of retinal, 1-4% of glycylglycine oleamide, 2-3% of truffle extract, 1-2% of plant leaf extract, 0.1-0.2% of caprylyl glycol and the balance of water. The cosmetic composition has the advantages of long-lasting moisture retention and good absorption, and effective components such as retinene, glycylglycine oleamide, truffle extract and the like are absorbed by skin and act synergistically, so that fine lines and wrinkles can be effectively reduced, rough skin can be smoothed, and skin texture can be improved.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a cosmetic composition based on retinaldehyde and glycylglycine oleamide and a preparation method thereof.
Background
The skin is the largest organ of the human body, and healthy skin is smooth and elastic and ages with age. Women begin to wrinkle at age 25-30, gradually become mottled, and then the skin becomes loose, rough, dull, and wrinkles deepen more. Therefore, the research focus of cosmetics on removing wrinkles and delaying aging is one of the research focuses. The cosmetics sold in the market mainly preserve moisture and often cannot achieve a good wrinkle-removing effect.
Disclosure of Invention
The present invention aims to provide a cosmetic composition based on retinaldehyde and glycylglycine oleamide and a preparation method thereof, so as to solve the technical problems.
In order to solve the technical problems, the technical scheme of the invention is as follows:
in a first aspect, the present invention provides a cosmetic composition based on retinaldehyde and glycylglycine oleamide, comprising, in weight percent: 6-15% of glycerol, 2-5% of butanediol, 0.1-0.5% of xanthan gum, 0.05-0.1% of disodium ethylene diamine tetraacetate, 0.1-0.5% of panthenol, 1-3% of methyl glucose sesquistearate, 1-3% of PEG-100 stearate, 3-6% of polydimethylsiloxane, 4-8% of squalane, 0.1-0.5% of retinal, 1-4% of glycylglycine oleamide, 2-3% of truffle extract, 1-2% of plant leaf extract, 0.1-0.2% of caprylyl glycol and the balance of water.
Preferably, the truffle extract is selected from any one or more of a truffle nigrospora extract, a truffle purpurea extract and a truffle alba extract.
Further preferably, the truffle extract is a truffle nigrospora extract.
Preferably, the plant leaf extract is selected from any one or more of rosewood leaf extract, waxberry leaf extract and grape leaf extract.
More preferably, the plant leaf extract is composed of the dalbergia wood leaf extract and the grape leaf extract according to the weight ratio of 0.5-1: 1.
Preferably, the cosmetic composition for retinoids and glycylglycine oleamide comprises the following components in percentage by weight: 12% of glycerin, 3% of butanediol, 0.2% of xanthan gum, 0.1% of disodium ethylene diamine tetraacetate, 0.2% of panthenol, 2% of methylglucose sesquistearate, 2% of PEG-100 stearate, 5% of polydimethylsiloxane, 6.5% of squalane, 0.3% of retinal, 3% of glycylglycine oleamide, 2.4% of truffle extract, 1.5% of plant leaf extract, 0.2% of caprylyl glycol and the balance of water.
In a second aspect, the present invention provides a method for preparing a cosmetic composition based on retinal and glycylglycine oleamide according to the first aspect, comprising the steps of:
(1) adding methyl glucose sesquistearate, PEG-100 stearate, polydimethylsiloxane and squalane into a stirring pot, heating to 80-85 ℃, and uniformly stirring and mixing to obtain a component A;
(2) adding water, glycerol, butanediol, xanthan gum, disodium ethylene diamine tetraacetate and panthenol into a stirring pot, heating to 80-85 ℃, and uniformly stirring and mixing to obtain a component B;
(3) adding the component B into a vacuum emulsifying pot, adding the component A, homogenizing at 80-85 ℃ for 10-15 min, cooling to 40-50 ℃, adding retinal, glycylglycine oleamide, truffle extract, plant leaf extract and caprylyl glycol, homogenizing for 5-10 min, and stirring uniformly.
Compared with the prior art, the invention has the following effective effects:
the cosmetic composition provided by the invention has the advantages of lasting moisture retention and good absorption, and the effective components such as retinal, glycylglycine oleamide, truffle extract and plant leaf extract are absorbed by the skin and act synergistically to improve the microcirculation condition of the skin, regulate the metabolism of epidermis and stratum corneum, effectively reduce fine lines and wrinkles, smooth rough skin and improve skin texture.
Drawings
FIG. 1 is a bar graph of the rate of change of skin elasticity provided by the present invention.
Detailed Description
The following further describes embodiments of the present invention with reference to the drawings. It should be noted that the description of the embodiments is provided to help understanding of the present invention, but the present invention is not limited thereto. In addition, the technical features involved in the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
Example 1
The present example provides a method for preparing a cosmetic composition based on retinal and glycylglycine oleamide, comprising the steps of:
(1) preparing the following raw materials in percentage by weight: 12% of glycerin, 3% of butanediol, 0.2% of xanthan gum, 0.1% of disodium ethylene diamine tetraacetate, 0.2% of panthenol, 2% of methylglucose sesquistearate, 2% of PEG-100 stearate, 5% of polydimethylsiloxane, 6.5% of squalane, 0.3% of retinal, 3% of glycylglycine oleamide, 2.4% of tuber melanosporum nigrum extract, 1.5% of plant leaf extract, 0.2% of caprylyl glycol and the balance of water, wherein the plant leaf extract is composed of dalbergia wood leaf extract and grape leaf extract according to a weight ratio of 3: 4;
(2) adding methyl glucose sesquistearate, PEG-100 stearate, polydimethylsiloxane and squalane into a stirring pot, heating to 80 ℃, and stirring and mixing uniformly to obtain a component A;
(3) adding water, glycerol, butanediol, xanthan gum, disodium ethylene diamine tetraacetate and panthenol into a stirring pot, heating to 80 ℃, and uniformly stirring and mixing to obtain a component B;
(4) adding the component B into a vacuum emulsifying pot, adding the component A, homogenizing at 80 deg.C for 12min, cooling to 40 deg.C, adding retinaldehyde, glycylglycine oleamide, Tuber melanosporum extract, plant leaf extract, and octyl glycol, homogenizing for 8min, and stirring.
Example 2
The present example provides a method for preparing a cosmetic composition based on retinal and glycylglycine oleamide, comprising the steps of:
(1) preparing the following raw materials in percentage by weight: 6% of glycerin, 5% of butanediol, 0.5% of xanthan gum, 0.1% of disodium ethylene diamine tetraacetate, 0.5% of panthenol, 3% of methylglucose sesquistearate, 1% of PEG-100 stearate, 6% of polydimethylsiloxane, 8% of squalane, 0.5% of retinal, 1% of glycylglycine oleamide, 3% of tuber melanosporum extract, 1% of plant leaf extract, 0.2% of caprylyl glycol and the balance of water, wherein the plant leaf extract is composed of a dalbergia wood leaf extract and a grape leaf extract according to a weight ratio of 1: 2;
(2) adding methyl glucose sesquistearate, PEG-100 stearate, polydimethylsiloxane and squalane into a stirring pot, heating to 85 ℃, and stirring and mixing uniformly to obtain a component A;
(3) adding water, glycerol, butanediol, xanthan gum, disodium ethylene diamine tetraacetate and panthenol into a stirring pot, heating to 85 ℃, and uniformly stirring and mixing to obtain a component B;
(4) adding the component B into a vacuum emulsifying pot, adding the component A, homogenizing at 85 deg.C for 10min, cooling to 50 deg.C, adding retinaldehyde, glycylglycine oleamide, Tuber melanosporum extract, plant leaf extract, and octyl glycol, homogenizing for 5min, and stirring.
Example 3
The present example provides a method for preparing a cosmetic composition based on retinal and glycylglycine oleamide, comprising the steps of:
(1) preparing the following raw materials in percentage by weight: 15% of glycerin, 2% of butanediol, 0.1% of xanthan gum, 0.05% of disodium ethylene diamine tetraacetate, 0.1% of panthenol, 1% of methylglucose sesquistearate, 3% of PEG-100 stearate, 3% of polydimethylsiloxane, 4% of squalane, 0.1% of retinal, 4% of glycylglycine oleamide, 2% of tuber melanosporum extract, 2% of plant leaf extract, 0.1% of octyl glycol and the balance of water, wherein the plant leaf extract is composed of dalbergia wood leaf extract and grape leaf extract according to a weight ratio of 1: 1;
(2) adding methyl glucose sesquistearate, PEG-100 stearate, polydimethylsiloxane and squalane into a stirring pot, heating to 85 ℃, and stirring and mixing uniformly to obtain a component A;
(3) adding water, glycerol, butanediol, xanthan gum, disodium ethylene diamine tetraacetate and panthenol into a stirring pot, heating to 85 ℃, and uniformly stirring and mixing to obtain a component B;
(4) adding the component B into a vacuum emulsifying pot, adding the component A, homogenizing at 85 deg.C for 15min, cooling to 50 deg.C, adding retinaldehyde, glycylglycine oleamide, Tuber melanosporum extract, plant leaf extract, and octyl glycol, homogenizing for 10min, and stirring.
Example 4
Preparing the following raw materials in percentage by weight: 12% of glycerin, 3% of butanediol, 0.2% of xanthan gum, 0.1% of disodium ethylenediamine tetraacetate, 0.2% of panthenol, 2% of methylglucose sesquistearate, 2% of PEG-100 stearate, 5% of polydimethylsiloxane, 6.5% of squalane, 0.3% of retinal, 3% of glycylglycine oleamide, 2.4% of Tuber melanosporum extract, 1.5% of plant leaf extract, 0.2% of caprylyl glycol and the balance of water, wherein the plant leaf extract is composed of a Myrica rubra leaf extract and a grape leaf extract in a weight ratio of 3:4, and the finished product is prepared according to the preparation method of example 1.
Example 5
Preparing the following raw materials in percentage by weight: 12% of glycerin, 3% of butanediol, 0.2% of xanthan gum, 0.1% of disodium ethylenediamine tetraacetate, 0.2% of panthenol, 2% of methylglucose sesquistearate, 2% of PEG-100 stearate, 5% of polydimethylsiloxane, 6.5% of squalane, 0.3% of retinal, 3% of glycylglycine oleamide, 2.4% of tuber melanosporum nigrum extract, 1.5% of plant leaf extract, 0.2% of caprylyl glycol and the balance of water, wherein the plant leaf extract is composed of a dalbergia wood leaf extract and a mulberry leaf extract in a weight ratio of 3:4, and the finished product is prepared according to the preparation method of example 1.
Example 6
To further illustrate the beneficial effects of the present invention, a similar preparation method to that of example 1 was employed, and this example only differs from example 1 in that: the present example used a tuber mushroom extract.
Example 7
To further illustrate the beneficial effects of the present invention, a similar preparation method to that of example 1 was employed, and this example only differs from example 1 in that: the present example used a truffle extract.
Example 8
Preparing the following raw materials in percentage by weight: glycerol 6%, butanediol 5%, xanthan gum 0.5%, disodium ethylene diamine tetraacetate 0.1%, panthenol 0.5%, methylglucose sesquistearate 3%, PEG-100 stearate 1%, polydimethylsiloxane 6%, squalane 8%, retinal 1%, glycylglycine oleamide 1%, tuber melanosporum extract 3%, plant leaf extract 1%, octyl glycol 0.2%, and the balance of water, wherein the plant leaf extract is composed of a rosewood leaf extract and a grape leaf extract in a weight ratio of 1:2, and the finished product is prepared according to the preparation method of example 1.
Example 9
Preparing the following raw materials in percentage by weight: glycerol 6%, butanediol 5%, xanthan gum 0.5%, disodium ethylene diamine tetraacetate 0.1%, panthenol 0.5%, methylglucose sesquistearate 3%, PEG-100 stearate 1%, polydimethylsiloxane 6%, squalane 8%, retinal 0.5%, glycylglycine oleamide 0.1%, tuber melanosporum extract 3%, plant leaf extract 1%, caprylyl glycol 0.2%, and water in balance, wherein the plant leaf extract is composed of a rosewood leaf extract and a grape leaf extract in a weight ratio of 1:2, and the finished product is prepared according to the preparation method of example 1.
Example 10
Preparing the following raw materials in percentage by weight: glycerol 6%, butanediol 5%, xanthan gum 0.5%, disodium ethylene diamine tetraacetate 0.1%, panthenol 0.5%, methylglucose sesquistearate 3%, PEG-100 stearate 1%, polydimethylsiloxane 6%, squalane 8%, retinal 0.5%, glycylglycine oleamide 1%, plant leaf extract 1%, caprylyl glycol 0.2%, and water in balance, wherein the plant leaf extract is composed of a dalbergia wood leaf extract and a grape leaf extract in a weight ratio of 1:2, and the finished product is prepared according to the preparation method of example 1.
And (3) aging test of the product:
1. the products obtained in the above examples were subjected to a heat resistance test, a cold resistance test and a centrifugation test:
(1) heat resistance stability test (48 ℃, 40 days): no oil-water separation phenomenon exists, and the product is qualified;
(2) cold stability test (-15 ℃, 40 days): no oil-water separation phenomenon exists, and the product is qualified;
(3) centrifuge stability test (4000r/min, 30 min): and (4) passing.
2. 50 subjects with the age of 20-50 years are selected, randomly divided into 10 groups, products obtained in the examples 1-10 are tried respectively, 0.03g of the product obtained in the examples 1-10 is taken respectively, the product is attached to the back of the subject by a special adhesive tape, the skin reaction of the back of the subject is observed after the product is removed for 30min, 6 hours, 12 hours, 24 hours and 48 hours respectively, and the result is recorded according to the skin reaction grading standard in the cosmetic hygiene Specification (2007 edition).
The test results show that: each group of subjects have no adverse skin reaction, which indicates that the products obtained in examples 1-10 are safe to use.
3. Selecting 100 subjects with the age of 25-40 years, randomly dividing the subjects into 10 groups, using the products of the embodiments 1-10 for 10 subjects in each group, applying a proper amount of the products to the face in the morning and at night every day, slightly looping until the products are completely absorbed, respectively testing the skin elasticity index by using a skin tester before trial and after 7 days of continuous trial, calculating the average value of each group, and further calculating the skin elasticity change rate, wherein the calculation formula is as follows: the skin elasticity change rate (after-test skin elasticity index-before-test skin elasticity index)/before-test skin elasticity index × 100%, and the results are shown in fig. 1.
The above results show that: the product in the example 1 has the best wrinkle removing effect, compared with the products in the examples 8-10, the product in the example 1 has better wrinkle removing effect by compounding a proper amount of retinaldehyde, glycylglycine oleamide, truffle extract and plant leaf extract, and the components have synergistic effect.
The embodiments of the present invention have been described in detail with reference to the accompanying drawings, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, and the scope of protection is still within the scope of the invention.
Claims (7)
1. A cosmetic composition based on retinal and glycylglycine oleamide, characterized in that it comprises, in percentages by weight: 6-15% of glycerol, 2-5% of butanediol, 0.1-0.5% of xanthan gum, 0.05-0.1% of disodium ethylene diamine tetraacetate, 0.1-0.5% of panthenol, 1-3% of methyl glucose sesquistearate, 1-3% of PEG-100 stearate, 3-6% of polydimethylsiloxane, 4-8% of squalane, 0.1-0.5% of retinal, 1-4% of glycylglycine oleamide, 2-3% of truffle extract, 1-2% of plant leaf extract, 0.1-0.2% of caprylyl glycol and the balance of water.
2. The cosmetic composition based on retinal and glycylglycine oleamide according to claim 1, wherein the truffle extract is selected from any one or more of a truffle nigrospora extract, a truffle charantia extract and a truffle alba extract.
3. The cosmetic composition based on retinal and glycylglycine oleamide according to claim 2, characterized in that the truffle extract is truffle nigrospora extract.
4. The cosmetic composition according to claim 1, wherein the plant leaf extract is selected from any one or more of extracts of rosewood leaves, red bayberry leaves and grape leaves.
5. The cosmetic composition based on retinal and glycylglycine oleamide according to claim 4, wherein the plant leaf extract is composed of a dalbergia wood leaf extract and a grape leaf extract at a weight ratio of 0.5 to 1: 1.
6. The cosmetic composition based on retinal and glycylglycine oleamide according to claim 1, wherein the cosmetic composition based on retinal and glycylglycine oleamide comprises, in weight percent: 12% of glycerin, 3% of butanediol, 0.2% of xanthan gum, 0.1% of disodium ethylene diamine tetraacetate, 0.2% of panthenol, 2% of methylglucose sesquistearate, 2% of PEG-100 stearate, 5% of polydimethylsiloxane, 6.5% of squalane, 0.3% of retinal, 3% of glycylglycine oleamide, 2.4% of truffle extract, 1.5% of plant leaf extract, 0.2% of caprylyl glycol and the balance of water.
7. A process for preparing a cosmetic composition based on retinaldehyde and glycylglycine oleamide according to claim 1, comprising the steps of:
(1) adding methyl glucose sesquistearate, PEG-100 stearate, polydimethylsiloxane and squalane into a stirring pot, heating to 80-85 ℃, and uniformly stirring and mixing to obtain a component A;
(2) adding water, glycerol, butanediol, xanthan gum, disodium ethylene diamine tetraacetate and panthenol into a stirring pot, heating to 80-85 ℃, and uniformly stirring and mixing to obtain a component B;
(3) adding the component B into a vacuum emulsifying pot, adding the component A, homogenizing at 80-85 ℃ for 10-15 min, cooling to 40-50 ℃, adding retinal, glycylglycine oleamide, truffle extract, plant leaf extract and caprylyl glycol, homogenizing for 5-10 min, and stirring uniformly.
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