CN111617005A - High-foam fine soap-based mixed facial cleanser and preparation method thereof - Google Patents
High-foam fine soap-based mixed facial cleanser and preparation method thereof Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses a high-foam fine soap-based mixed facial cleanser and a preparation method thereof. The raw materials of the high-foaming fine soap-based mixed facial cleanser comprise lauric acid, myristic acid, palmitic acid, stearic acid, oleate mixture, methyl hydroxybenzoate, oleic acid mixture, glycerol, chelating agent, potassium hydroxide, glyceryl oleate, sodium isostearoyl lactylate, sodium methyl cocoyl taurate mixture, pigment, phenoxyethanol, essence, anise extract and yeast extract. The facial cleanser provided by the invention is mild and non-irritant, has good high and low temperature stability and good pearlescent appearance, is easy to spread, is very convenient to use, can form foam blocks, is rich and fine in foam, is easy to wash, and is clean, fresh and tight in skin after washing; the preparation process provided by the invention is simple and has high process reproducibility.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a high-foam fine soap-based mixed facial cleanser and a preparation method thereof.
Background
Soap-based facial cleansers are one of the very popular facial cleansing products in the daily line of chemistry in recent years. The soap-based facial cleanser has good pearlescent appearance, is easy to spread, is very convenient to use, quick to foam, rich in foam, high in cleaning force and very clean in skin after washing. However, the soap-based facial cleanser has strong degreasing capability on skin, so that the skin feel after washing is poor, and the skin is easy to dry and tense; moreover, soap-based cleansing creams are not stable at high and low temperatures, are liable to separate at high temperatures, and are liable to become hard and coarse at low temperatures. The foam fineness, the pearl appearance and the high and low temperature stability can not be considered at the same time.
Disclosure of Invention
The invention aims to provide a high-foam fine soap-based mixed facial cleanser and a preparation method thereof, and aims to solve the technical problems.
In order to achieve the purpose, the technical scheme of the invention is as follows:
in a first aspect, the high-foam fine soap-based mixed facial cleanser provided by the invention comprises the following raw materials in percentage by weight: 4.5-7% of potassium hydroxide, 10-30% of glycerol, 0.05-0.2% of chelating agent, 1-10% of lauric acid, 1-10% of myristic acid, 1-20% of palmitic acid, 1-10% of stearic acid, 1-10% of oleate mixture, 0.1-0.3% of methyl hydroxybenzoate, 0.1-2% of oil ester mixture, 1.1-11% of dispersion liquid of titanium dioxide, 0.1-1% of silicone oil, 431-10% of polyquaternium-ammonium salt, 0.1-1% of glyceryl oleate, 0.1-1% of sodium isostearoyl lactylate, 1-10% of mixture of sodium methyl cocoyl taurate, 0-1% of pigment, 0.1-1% of phenoxyethanol, 0.1-1% of essence, 0.1-1% of hypsizygus marmoreus extract, 0.1-1% of yeast.
Preferably, the chelating agent is disodium edetate.
Preferably, the titanium dioxide dispersion liquid is prepared by mixing, homogenizing and dispersing titanium dioxide and water according to the weight ratio of 1: 5-10.
Preferably, the oleate mixture is prepared by mixing stearic acid, cholesteryl hydroxystearate, hydrogenated castor oil and glycerol hydroxystearate according to the weight ratio of 1:1:1: 1.
Preferably, the grease mixture is formed by mixing polyglycerol-10 and isostearic acid ester according to the weight ratio of 2: 1.
Preferably, the pigment is at least one selected from the group consisting of yellow pigments and red pigments.
Preferably, the mixture of the sodium methyl cocoyl taurate is prepared by mixing sodium methyl cocoyl taurate, sodium chloride and water according to the weight ratio of 1:0.1: 2.
Preferably, the silicone oil is bis (C)13-15Alkoxy) PG-amino terminated polydimethylsiloxane.
In a second aspect, the present invention provides a method for preparing a high-foam fine soap-based mixed facial cleanser according to the first aspect, comprising the following steps:
(1) sequentially putting a mixture of lauric acid, myristic acid, palmitic acid, stearic acid, oleate, methyl hydroxybenzoate and oleic acid into an oil pan, stirring and heating, heating to 80-85 ℃, and preserving heat until the mixture is uniformly mixed to obtain a phase B;
(2) putting glycerol, a chelating agent and water with the formula amount of 80-90% into a water kettle, starting stirring, then adding potassium hydroxide, and stirring until the mixture is completely dissolved to be transparent to obtain a phase A;
(3) pumping the vacuum degree of the emulsifying pot to be not higher than-0.05 MP, respectively filtering the phase A and the phase B, slowly pumping the phase A and the phase B into the vacuum emulsifying pot at 65-75 ℃, adding the residual water according to the formula amount, uniformly stirring, homogenizing for 3-5 min till the phase A and the phase B are completely dispersed, and insulating and saponifying for 0.5-2 hours at 80-85 ℃;
(4) after the saponification is finished when the material body is in a uniform and particle-free state, filtering, adding the dispersion liquid of the titanium dioxide and the silicone oil which are dispersed and homogenized in advance, preserving heat and stirring at 80-85 ℃, and stirring for at least 10min until the material body is in a uniform and particle-free state;
(5) cooling to a temperature not higher than 70 ℃, adding polyquaternium-43, and stirring for 5-15 min to be uniform under heat preservation; then cooling to a temperature not higher than 60 ℃, sequentially adding a mixture of glyceryl oleate, sodium isostearoyl lactylate and sodium methyl cocoyl taurate, and stirring for 5-15 min at the constant temperature until the mixture is uniform;
(6) cooling to a temperature not higher than 45 ℃, adding the pigment, phenoxyethanol, essence, hypsizygus marmoreus extract and yeast extract, and stirring for 5-15 min to be uniform under heat preservation;
(7) and (3) after the temperature is reduced to 38 ℃, observing that the material body is in a uniform and fine pearly-lustre state, and filtering and discharging after the material body is qualified.
Compared with the prior art, the invention has the beneficial effects that:
the facial cleanser provided by the invention is mild and non-irritant, has good high and low temperature stability and good pearlescent appearance, is easy to spread, is very convenient to use, can form foam blocks, is rich and fine in foam, is easy to wash, and is clean, fresh and tight in skin after washing; the preparation process provided by the invention is simple and has high process reproducibility.
Detailed Description
The following further describes the embodiments of the present invention. It should be noted that the description of the embodiments is provided to help understanding of the present invention, but the present invention is not limited thereto. In addition, the technical features involved in the embodiments of the present invention described below may be combined with each other as long as they do not conflict with each other.
It should be noted that the oleate blends in the following examples and comparative examples were prepared by mixing stearic acid, cholesteryl hydroxystearate, hydrogenated castor oil, and glyceryl hydroxystearate in a weight ratio of 1:1:1: 1.
It should be noted that the grease mixtures in the following examples and comparative examples were prepared by mixing polyglycerin-10 and isostearic acid ester at a weight ratio of 2: 1.
It should be noted that the mixture of sodium methylcocoyl taurate in the following examples and comparative examples was prepared by mixing sodium methylcocoyl taurate, sodium chloride, and water in a weight ratio of 1:0.1: 2.
Example 1
The preparation method of the high-foam fine soap-based mixed facial cleanser provided by the embodiment comprises the following steps:
(1) weighing the following components in percentage by weightRaw materials in percentage: 5% of potassium hydroxide, 20% of glycerol, 0.1% of disodium ethylene diamine tetraacetate, 5% of lauric acid, 5% of myristic acid, 15% of palmitic acid, 5% of stearic acid, 4% of oleate mixture, 0.2% of methylparaben, 0.5% of oleyl ester mixture, 1.2% of titanium dioxide dispersion liquid and bis (C)13-15Alkoxy) PG-amino end polydimethylsiloxane 0.5%, polyquaternary ammonium salt-434%, glyceryl oleate 0.5%, sodium isostearoyl lactylate 0.8%, mixture of sodium methyl cocoyl taurate 8%, yellow pigment 0.1%, red pigment 0.1%, phenoxyethanol 0.2%, essence 0.3%, sea fennel extract 0.5%, yeast extract 0.5%, and balance of water, wherein the titanium dioxide dispersion liquid is prepared by mixing, homogenizing and dispersing titanium dioxide and water according to a weight ratio of 1: 10.
(2) Sequentially putting a mixture of lauric acid, myristic acid, palmitic acid, stearic acid, oleate, methyl hydroxybenzoate and oleic acid into an oil pan, stirring and heating, heating to 80 ℃, and preserving heat until the mixture is uniformly mixed to obtain a phase B;
(3) putting glycerol, disodium ethylene diamine tetraacetate and water with the formula amount of 90% into a water kettle, starting stirring, then adding potassium hydroxide, and stirring until the mixture is completely dissolved to be transparent to obtain a phase A;
(4) pumping the emulsifying pot to a vacuum degree of not higher than-0.05 MP, respectively filtering the phase A and the phase B, slowly pumping into the vacuum emulsifying pot at 65 ℃, adding the rest water, stirring, homogenizing for 5min to completely disperse, and performing heat preservation and saponification at 80 ℃ for 1 hour;
(5) after the saponification is finished when the material body is in a uniform and particle-free state, filtering, and adding the dispersion liquid of the titanium pigment and the bis (C) which are dispersed and homogenized in advance13-15Alkoxy) PG-ammonia end polydimethylsiloxane, stirring at the temperature of 80 ℃ for at least 10min until the material body is in a uniform and particle-free state;
(6) cooling to a temperature not higher than 70 ℃, adding polyquaternium-43, and stirring for 10min to be uniform under heat preservation; then cooling to a temperature not higher than 60 ℃, sequentially adding a mixture of glyceryl oleate, sodium isostearoyl lactylate and sodium methyl cocoyl taurate, and stirring for 10min at the constant temperature until the mixture is uniform;
(7) cooling to a temperature not higher than 45 deg.C, adding pigment, phenoxyethanol, essence, fructus Anisi Stellati extract, and yeast extract, stirring for 10min to obtain a uniform mixture;
(8) and (3) after the temperature is reduced to 38 ℃, observing that the material body is in a uniform and fine pearly-lustre state, and filtering and discharging after the material body is qualified.
Example 2
The preparation method of the high-foam fine soap-based mixed facial cleanser provided by the embodiment comprises the following steps:
(1) weighing the following raw materials in percentage by weight: 6% of potassium hydroxide, 18% of glycerol, 0.1% of disodium ethylene diamine tetraacetate, 5% of lauric acid, 3% of myristic acid, 10% of palmitic acid, 3% of stearic acid, 6% of oleate mixture, 0.2% of methylparaben, 0.6% of oleyl ester mixture, 5.5% of titanium dioxide dispersion liquid and bis (C)13-150.6% of alkoxy) PG-amino end polydimethylsiloxane, 438% of polyquaternary ammonium salt, 0.5% of glyceryl oleate, 0.5% of sodium isostearoyl lactylate, 6% of a mixture of sodium methyl cocoyl taurate, 0.3% of phenoxyethanol, 0.5% of essence, 0.5% of sea fennel extract, 0.5% of yeast extract and the balance of water, wherein the titanium dioxide dispersion liquid is prepared by mixing, homogenizing and dispersing titanium dioxide and water according to the weight ratio of 1: 10.
(2) Sequentially putting a mixture of lauric acid, myristic acid, palmitic acid, stearic acid, oleate, methyl hydroxybenzoate and oleic acid into an oil pan, stirring and heating, heating to 85 ℃, and preserving heat until the mixture is uniformly mixed to obtain a phase B;
(3) putting glycerol, disodium ethylene diamine tetraacetate and water with the formula amount of 80% into a water kettle, starting stirring, then adding potassium hydroxide, and stirring until the mixture is completely dissolved to be transparent to obtain a phase A;
(4) pumping the emulsifying pot to a vacuum degree of not higher than-0.05 MP, respectively filtering the phase A and the phase B, slowly pumping into the vacuum emulsifying pot at 75 ℃, adding the rest water, stirring, homogenizing for 3min till complete dispersion, and performing heat preservation and saponification at 85 ℃ for 1 hour;
(5) after the saponification is finished when the material body is in a uniform and particle-free state, filtering, and adding the dispersion liquid of the titanium pigment and the bis (C) which are dispersed and homogenized in advance13-15Alkoxy) PG-amino terminated polydimethyl siliconSiloxane, stirring at 85 ℃ for at least 10min until the material body is in a uniform and particle-free state;
(6) cooling to a temperature not higher than 70 ℃, adding polyquaternium-43, and stirring for 15min to be uniform under the condition of heat preservation; then cooling to a temperature not higher than 60 ℃, sequentially adding a mixture of glyceryl oleate, sodium isostearoyl lactylate and sodium methyl cocoyl taurate, and stirring for 10min at the constant temperature until the mixture is uniform;
(7) cooling to a temperature not higher than 45 deg.C, adding pigment, phenoxyethanol, essence, fructus Anisi Stellati extract, and yeast extract, stirring for 10min to obtain a uniform mixture;
(8) and (3) after the temperature is reduced to 38 ℃, observing that the material body is in a uniform and fine pearly-lustre state, and filtering and discharging after the material body is qualified.
Example 3
Weighing the following raw materials in percentage by weight: 5.5% of potassium hydroxide, 15% of glycerol, 0.1% of disodium ethylene diamine tetraacetate, 4% of lauric acid, 6% of myristic acid, 18% of palmitic acid, 4% of stearic acid, 8% of oleate mixture, 0.2% of methylparaben, 0.4% of oleyl ester mixture, 2.7% of titanium dioxide dispersion, and bis (C)13-150.4% of alkoxy) PG-amino end polydimethylsiloxane, 436% of polyquaternary ammonium salt, 0.5% of glyceryl oleate, 0.5% of sodium isostearoyl lactylate, 4% of a mixture of sodium methyl cocoyl taurate, 0.2% of phenoxyethanol, 0.2% of essence, 0.5% of sea fennel extract, 0.5% of yeast extract and the balance of water, wherein the titanium dioxide dispersion liquid is prepared by mixing, homogenizing and dispersing titanium dioxide and water according to the weight ratio of 1:5, and then preparing a finished product according to the steps (2) to (8) of the embodiment 2.
Example 4
Weighing the following raw materials in percentage by weight: 4.5% of potassium hydroxide, 30% of glycerol, 0.05% of disodium ethylene diamine tetraacetate, 10% of lauric acid, 1% of myristic acid, 20% of palmitic acid, 1% of stearic acid, 1% of oleate mixture, 0.1% of methylparaben, 0.1% of oleyl ester mixture, 11% of titanium dioxide dispersion liquid and bis (C)13-15Alkoxy) PG-amino end polydimethylsiloxane 0.1%, polyquaternium-431%, glyceryl oleate 0.1%, sodium isostearoyl lactylate 0.1%, sodium methyl cocoyl taurateThe titanium dioxide powder is prepared by mixing, homogenizing and dispersing titanium dioxide and water according to the weight ratio of 1:10, and then preparing a finished product according to the steps (2) to (8) of the embodiment 1.
Example 5
Weighing the following raw materials in percentage by weight: 7% of potassium hydroxide, 10% of glycerol, 0.2% of disodium ethylene diamine tetraacetate, 1% of lauric acid, 10% of myristic acid, 1% of palmitic acid, 10% of stearic acid, 10% of oleate mixture, 0.3% of methylparaben, 2% of oleyl ester mixture, 1.1% of titanium dioxide dispersion liquid, and bis (C)13-15Alkoxy) PG-amino end polydimethylsiloxane 1%, polyquaternary ammonium salt-4310%, glyceryl oleate 1%, sodium isostearoyl lactylate 1%, mixture of sodium methyl cocoyl taurate 10%, yellow pigment 0.2%, red pigment 0.3%, phenoxyethanol 0.5%, essence 1%, sea fennel extract 1%, yeast extract 1% and the balance of water, wherein the titanium dioxide dispersion liquid is prepared by mixing, homogenizing and dispersing titanium dioxide and water according to the weight ratio of 1:10, and then preparing a finished product according to the steps (2) to (8) of the example 1.
Through detection, the products obtained in the above examples 1-5 can all reach the following physicochemical indexes:
to further illustrate the beneficial effects of the present invention, the present invention also tests the high and low temperature stability of the products obtained in the above examples:
taking 3 parts of the products obtained in the embodiments 1-5 as samples to be detected, wherein the volume of each sample is 40mL, respectively filling the samples into transparent plastic bottles, respectively placing the transparent plastic bottles into thermostats at room temperature, 5 ℃ and 50 ℃, continuously observing for 3 months, then taking out the samples in the thermostats at 5 ℃ and 50 ℃ to return to the room temperature, and observing the appearance of the samples. The observation shows that: compared with the samples at room temperature, the products obtained in examples 1 to 5 have no changes in appearance such as delamination, thinning, hardening and the like when the temperature is 5 ℃, 50 ℃, 5 ℃ to room temperature, and 50 ℃ to room temperature.
To further illustrate the beneficial effects of the present invention, the present invention also tests the products obtained in the above examples as follows:
selecting 50 female subjects with the age of 18-53 years, randomly dividing into five groups, and respectively trying the products obtained in the above examples 1-5 by the following trial method: wetting hands and faces with water, putting 1-2 g of a sample on one wet hand, spreading the sample with the other hand, kneading and foaming the sample with two hands, slightly kneading and massaging the two hands on the faces for 2-3 min, washing the hands and the faces with running water, and naturally drying the hands and the faces. The test subjects score spreadability, foaming speed, foam rich fineness, skin feel after washing and cleaning difficulty according to the use feeling of the test subjects, the scoring standard adopts a 5-point system, 1 point is the worst, 5 points are the best, the evaluation result is the average point of all the test subjects, and the higher the average point is, the better the effect is. The test results are shown in the following table:
the embodiments of the present invention have been described in detail, but the present invention is not limited to the described embodiments. It will be apparent to those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, and the scope of protection is still within the scope of the invention.
Claims (9)
1. The high-foam fine soap-based mixed facial cleanser is characterized by comprising the following raw materials in percentage by weight: 4.5-7% of potassium hydroxide, 10-30% of glycerol, 0.05-0.2% of chelating agent, 1-10% of lauric acid, 1-10% of myristic acid, 1-20% of palmitic acid, 1-10% of stearic acid, 1-10% of oleate mixture, 0.1-0.3% of methyl hydroxybenzoate, 0.1-2% of oil ester mixture, 1.1-11% of dispersion liquid of titanium dioxide, 0.1-1% of silicone oil, 431-10% of polyquaternium-ammonium salt, 0.1-1% of glyceryl oleate, 0.1-1% of sodium isostearoyl lactylate, 1-10% of mixture of sodium methyl cocoyl taurate, 0-1% of pigment, 0.1-1% of phenoxyethanol, 0.1-1% of essence, 0.1-1% of hypsizygus marmoreus extract, 0.1-1% of yeast.
2. The high-foam, fine soap-based mixed facial cleanser of claim 1, wherein said chelating agent is disodium edetate.
3. The high-foam fine soap-based mixed facial cleanser according to claim 1, wherein the dispersion liquid of titanium dioxide is prepared by mixing, homogenizing and dispersing titanium dioxide and water according to a weight ratio of 1: 5-10.
4. The high-foam fine soap-based mixed facial cleanser of claim 1, wherein the oleate mixture is prepared by mixing stearic acid, cholesteryl hydroxystearate, hydrogenated castor oil and glyceryl hydroxystearate according to a weight ratio of 1:1:1: 1.
5. The high-foam fine soap-based mixed facial cleanser of claim 1, wherein the oil mixture is formed by mixing polyglycerol-10 and isostearic acid ester according to a weight ratio of 2: 1.
6. The high lathering mild soap based mixed facial cleanser according to claim 1, wherein said coloring matter is at least one selected from the group consisting of yellow coloring matter and red coloring matter.
7. The high-foam fine soap-based mixed facial cleanser according to claim 1, wherein the mixture of sodium methyl cocoyl taurate is prepared by mixing sodium methyl cocoyl taurate, sodium chloride and water according to a weight ratio of 1:0.1: 2.
8. The high foaming soap of claim 1The base mixed facial cleanser is characterized in that the silicone oil is bis (C)13-15Alkoxy) PG-amino terminated polydimethylsiloxane.
9. A method for preparing the high-foam fine soap-based mixed facial cleanser according to any one of claims 1 to 8, comprising the following steps:
(1) sequentially putting a mixture of lauric acid, myristic acid, palmitic acid, stearic acid, oleate, methyl hydroxybenzoate and oleic acid into an oil pan, stirring and heating, heating to 80-85 ℃, and preserving heat until the mixture is uniformly mixed to obtain a phase B;
(2) putting glycerol, a chelating agent and water with the formula amount of 80-90% into a water kettle, starting stirring, then adding potassium hydroxide, and stirring until the mixture is completely dissolved to be transparent to obtain a phase A;
(3) pumping the vacuum degree of the emulsifying pot to be not higher than-0.05 MP, respectively filtering the phase A and the phase B, slowly pumping the phase A and the phase B into the vacuum emulsifying pot at 65-75 ℃, adding the residual water according to the formula amount, uniformly stirring, homogenizing for 3-5 min till the phase A and the phase B are completely dispersed, and insulating and saponifying for 0.5-2 hours at 80-85 ℃;
(4) after the saponification is finished when the material body is in a uniform and particle-free state, filtering, adding the dispersion liquid of the titanium dioxide and the silicone oil which are dispersed and homogenized in advance, preserving heat and stirring at 80-85 ℃, and stirring for at least 10min until the material body is in a uniform and particle-free state;
(5) cooling to a temperature not higher than 70 ℃, adding polyquaternium-43, and stirring for 5-15 min to be uniform under heat preservation; then cooling to a temperature not higher than 60 ℃, sequentially adding a mixture of glyceryl oleate, sodium isostearoyl lactylate and sodium methyl cocoyl taurate, and stirring for 5-15 min at the constant temperature until the mixture is uniform;
(6) cooling to a temperature not higher than 45 ℃, adding the pigment, phenoxyethanol, essence, hypsizygus marmoreus extract and yeast extract, and stirring for 5-15 min to be uniform under heat preservation;
(7) and (3) after the temperature is reduced to 38 ℃, observing that the material body is in a uniform and fine pearly-lustre state, and filtering and discharging after the material body is qualified.
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| CN202010620663.9A CN111617005A (en) | 2020-06-30 | 2020-06-30 | High-foam fine soap-based mixed facial cleanser and preparation method thereof |
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| CN202010620663.9A CN111617005A (en) | 2020-06-30 | 2020-06-30 | High-foam fine soap-based mixed facial cleanser and preparation method thereof |
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Cited By (3)
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| CN112274446A (en) * | 2020-10-30 | 2021-01-29 | 广州市妆妍生物技术有限公司 | Ceramide refreshing amino acid facial cleanser and preparation method thereof |
| CN112370393A (en) * | 2020-12-10 | 2021-02-19 | 泉后(广州)生物科技研究院有限公司 | Hair washing mousse composition and preparation method and application thereof |
| CN113845984A (en) * | 2021-11-04 | 2021-12-28 | 天津郁美净集团有限公司 | Mild and stable soap-based cleansing cream and preparation process thereof |
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Application publication date: 20200904 |