CN111494265A - Tremella repairing and moisturizing mask - Google Patents
Tremella repairing and moisturizing mask Download PDFInfo
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- CN111494265A CN111494265A CN202010438931.5A CN202010438931A CN111494265A CN 111494265 A CN111494265 A CN 111494265A CN 202010438931 A CN202010438931 A CN 202010438931A CN 111494265 A CN111494265 A CN 111494265A
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- 241001506047 Tremella Species 0.000 title claims abstract description 36
- 230000003020 moisturizing effect Effects 0.000 title claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 177
- 238000003756 stirring Methods 0.000 claims abstract description 45
- 238000010438 heat treatment Methods 0.000 claims abstract description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 34
- 238000001816 cooling Methods 0.000 claims abstract description 25
- 229920001661 Chitosan Polymers 0.000 claims abstract description 18
- 238000002156 mixing Methods 0.000 claims abstract description 14
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 claims abstract description 13
- 230000000694 effects Effects 0.000 claims abstract description 12
- 239000000463 material Substances 0.000 claims description 54
- 238000012360 testing method Methods 0.000 claims description 34
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 24
- 229910052708 sodium Inorganic materials 0.000 claims description 19
- 239000011734 sodium Substances 0.000 claims description 19
- 239000008367 deionised water Substances 0.000 claims description 17
- 229910021641 deionized water Inorganic materials 0.000 claims description 17
- 229920001282 polysaccharide Polymers 0.000 claims description 17
- 239000005017 polysaccharide Substances 0.000 claims description 17
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical class CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 claims description 15
- GAWIXWVDTYZWAW-UHFFFAOYSA-N C[CH]O Chemical group C[CH]O GAWIXWVDTYZWAW-UHFFFAOYSA-N 0.000 claims description 15
- 241000252212 Danio rerio Species 0.000 claims description 15
- 229920002307 Dextran Polymers 0.000 claims description 15
- 235000020739 avocado extract Nutrition 0.000 claims description 15
- 238000000265 homogenisation Methods 0.000 claims description 15
- 150000004676 glycans Chemical class 0.000 claims description 14
- WCVRQHFDJLLWFE-UHFFFAOYSA-N pentane-1,2-diol Chemical compound CCCC(O)CO WCVRQHFDJLLWFE-UHFFFAOYSA-N 0.000 claims description 14
- 230000008439 repair process Effects 0.000 claims description 13
- 241000512259 Ascophyllum nodosum Species 0.000 claims description 12
- 229920002385 Sodium hyaluronate Polymers 0.000 claims description 12
- 235000019437 butane-1,3-diol Nutrition 0.000 claims description 12
- 229940010747 sodium hyaluronate Drugs 0.000 claims description 12
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 claims description 12
- SHWIJIJNPFXOFS-UHFFFAOYSA-N thiotaurine Chemical compound NCCS(O)(=O)=S SHWIJIJNPFXOFS-UHFFFAOYSA-N 0.000 claims description 12
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- 239000000230 xanthan gum Substances 0.000 claims description 12
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- 238000001514 detection method Methods 0.000 claims description 11
- 230000001954 sterilising effect Effects 0.000 claims description 10
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- FEBUJFMRSBAMES-UHFFFAOYSA-N 2-[(2-{[3,5-dihydroxy-2-(hydroxymethyl)-6-phosphanyloxan-4-yl]oxy}-3,5-dihydroxy-6-({[3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy}methyl)oxan-4-yl)oxy]-3,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl phosphinite Chemical compound OC1C(O)C(O)C(CO)OC1OCC1C(O)C(OC2C(C(OP)C(O)C(CO)O2)O)C(O)C(OC2C(C(CO)OC(P)C2O)O)O1 FEBUJFMRSBAMES-UHFFFAOYSA-N 0.000 claims description 9
- 229920002305 Schizophyllan Polymers 0.000 claims description 9
- 230000007059 acute toxicity Effects 0.000 claims description 5
- 231100000403 acute toxicity Toxicity 0.000 claims description 5
- 230000007665 chronic toxicity Effects 0.000 claims description 5
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- 210000002969 egg yolk Anatomy 0.000 claims description 5
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- 108010008359 protein kinase C lambda Proteins 0.000 claims description 5
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- 230000002335 preservative effect Effects 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- 239000002562 thickening agent Substances 0.000 claims description 2
- 230000000887 hydrating effect Effects 0.000 claims 8
- 229940058015 1,3-butylene glycol Drugs 0.000 claims 2
- 239000004909 Moisturizer Substances 0.000 claims 1
- 230000001815 facial effect Effects 0.000 claims 1
- 230000001333 moisturizer Effects 0.000 claims 1
- 238000004945 emulsification Methods 0.000 abstract description 4
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- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 9
- 230000006870 function Effects 0.000 description 7
- 239000003906 humectant Substances 0.000 description 7
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical compound NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 description 6
- KIUKXJAPPMFGSW-DNGZLQJQSA-N (2S,3S,4S,5R,6R)-6-[(2S,3R,4R,5S,6R)-3-Acetamido-2-[(2S,3S,4R,5R,6R)-6-[(2R,3R,4R,5S,6R)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylic acid Chemical compound CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 KIUKXJAPPMFGSW-DNGZLQJQSA-N 0.000 description 4
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 4
- 238000005345 coagulation Methods 0.000 description 4
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- 229920002674 hyaluronan Polymers 0.000 description 4
- 229960003160 hyaluronic acid Drugs 0.000 description 4
- -1 hydroxypropyl polysaccharide Chemical class 0.000 description 4
- 210000001161 mammalian embryo Anatomy 0.000 description 4
- 241001530056 Athelia rolfsii Species 0.000 description 3
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- 239000003795 chemical substances by application Substances 0.000 description 3
- 230000003750 conditioning effect Effects 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 206010012601 diabetes mellitus Diseases 0.000 description 3
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- 230000037303 wrinkles Effects 0.000 description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- KWIUHFFTVRNATP-UHFFFAOYSA-N Betaine Natural products C[N+](C)(C)CC([O-])=O KWIUHFFTVRNATP-UHFFFAOYSA-N 0.000 description 1
- KWIUHFFTVRNATP-UHFFFAOYSA-O N,N,N-trimethylglycinium Chemical compound C[N+](C)(C)CC(O)=O KWIUHFFTVRNATP-UHFFFAOYSA-O 0.000 description 1
- 239000004721 Polyphenylene oxide Substances 0.000 description 1
- 229920002125 Sokalan® Polymers 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 229960003237 betaine Drugs 0.000 description 1
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 description 1
- 229960001631 carbomer Drugs 0.000 description 1
- 230000008859 change Effects 0.000 description 1
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- 238000005260 corrosion Methods 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 125000003976 glyceryl group Chemical group [H]C([*])([H])C(O[H])([H])C(O[H])([H])[H] 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
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- 231100000419 toxicity Toxicity 0.000 description 1
- PQDJYEQOELDLCP-UHFFFAOYSA-N trimethylsilane Chemical compound C[SiH](C)C PQDJYEQOELDLCP-UHFFFAOYSA-N 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 230000002087 whitening effect Effects 0.000 description 1
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/55—Phosphorus compounds
- A61K8/553—Phospholipids, e.g. lecithin
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
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- Gerontology & Geriatric Medicine (AREA)
- Biophysics (AREA)
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- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention relates to the technical field of cosmetics, in particular to a tremella repairing and moisturizing mask which comprises the following steps: s1, preparing raw materials: preparing high-quality raw materials, and classifying the raw materials into A, B, C, D, E phases and F phases respectively; s2, heating raw materials: respectively putting the phase A raw material and the phase B raw material into a heating container for heating, and then putting the phase C raw material into the heating container for independently heating; s3, stirring raw materials: fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using a stirrer respectively until the phase raw materials are uniformly dispersed; s4, mixing and cooling: and (4) preparing a water bath kettle. The invention adopts a lipid emulsification system, and the liposome has two continuous structures of a hydrophilic part and a lipophilic part and has a large amount of bound water and hydrophobicity, thereby having good water locking function and the effect of inhibiting water evaporation, improving the permeability of stratum corneum, controlling the transdermal absorption speed, and adding a repairing component of carboxymethyl chitosan.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to a tremella repairing and moisturizing mask.
Background
The mask is a carrier of beauty care products, is a category of the beauty care products, and is the most important purpose of making up the insufficient cleaning work of makeup removal and face washing, and is matched with other essence components to realize other care functions such as moisturizing, whitening, anti-aging, grease balancing and the like.
Chinese patent No. CN201110429625.6 provides a nighttime repairing and moisturizing mask and a preparation method thereof, phase A: 0.01-0.06% of hyaluronic acid, 0.2-0.5% of carbomer, 261-5% of glyceryl polyether, 0.5-2% of bis-PEG-18 methyl dimethylsilane and 8-12% of butanediol; phase B: 3-5.5% of glycerin, 0.2-0.3% of betaine and 0.08-0.12%.
The nighttime repairing and moisturizing mask and the preparation method thereof in the CN201110429625.6 patent have the characteristics of necessary nutrition for rejuvenation at night, accelerating self-repair of skin and restoring skin smoothness, but the existing technical formula is a mask developed aiming at the problems of easy skin sensitivity, dry skin and poor repairing capability of diabetes patients, so that the development of a tremella repairing and moisturizing mask is urgently needed.
Disclosure of Invention
The invention aims to provide a tremella repairing and moisturizing mask to solve the problems that existing technical formulas in the background art are few in aim, and the mask is developed based on the problems that the skin of a diabetic patient is sensitive, the skin is dry and the repairing capability is poor.
The technical scheme of the invention is as follows: the tremella repairing and moisturizing mask comprises the following steps:
s1, preparing raw materials: preparing high-quality raw materials, and classifying the raw materials into A, B, C, D, E phases and F phases respectively;
s2, heating raw materials: respectively putting the phase A raw material and the phase B raw material into a heating container for heating, and then putting the phase C raw material into the heating container for independently heating;
s3, stirring raw materials: fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using a stirrer respectively until the phase raw materials are uniformly dispersed;
s4, mixing and cooling: preparing a water bath kettle, putting the phase A raw material into the water bath kettle, adding the phase B raw material into the phase A raw material, stirring for a period of time until the phase A raw material and the phase B raw material are uniformly mixed, and performing cooling treatment to obtain a phase A + phase B material;
s5, homogenizing and cooling: under the condition that the A + B phase materials are continuously stirred, slowly adding the C phase raw materials into the A + B phase materials to uniformly mix and disperse the three materials, homogenizing, and then cooling and stirring to obtain the A + B + C phase materials;
s6, blending and filling: when a certain temperature is reached, putting a D-phase raw material, an E-phase raw material and an F-phase raw material into an A + B + C-phase material, uniformly stirring and dispersing, putting into a sterilization kettle for sterilization until the temperature is room temperature to obtain an A + B + C + D + E + F-phase material, and filling the A + B + C + D + E + F-phase material to obtain a finished product;
s7, finished product detection: and randomly extracting part of finished products to test the safety and the repairing effect to obtain a test result.
Further, in S1, the high-quality raw materials are hydrogenated lecithin, avocado extract, 1, 3-butanediol, xanthan gum, sclerotium rolfsii gum, sodium hyaluronate, sodium carboxymethyl β -dextran sodium, hydroxyethyl chitosan, deionized water, kelp extract, thiotaurine, 1, 2-pentanediol, and tremella polysaccharide, respectively.
Furthermore, the phase A is composed of three of hydrogenated lecithin, avocado extract and 1, 3-butanediol, the phase B is composed of xanthan gum, sclerotium rolfsii gum, sodium hyaluronate and carboxymethyl β -dextran sodium, the phase C is composed of hydroxyethyl chitosan and deionized water, the phase D is composed of kelp extract, the phase E is composed of thiotaurine and deionized water, and the phase F is composed of 1, 2-pentanediol and tremella polysaccharide.
Further, the hydrogenated lecithin is prepared as an emulsifier, the proportion is 0.2%, the avocado extract is prepared as an emollient, the proportion is 0.15%, the 1, 3-butanediol and deionized water are prepared as solvents, the proportion is 3% and 78%, the xanthan gum is prepared as a thickening agent, the proportion is 0.2%, the sclerotium rolfsii gum and the sodium hyaluronate are prepared as humectants, the proportion is 4% and 0.05%, the carboxymethyl β -dextran sodium, hydroxyethyl chitosan, the kelp extract, thiotaurine and the tremella polysaccharide are prepared as skin conditioners, the proportions are respectively 2%, 0.2%, 2%, 0.2% and 5%, and the 1, 2-pentanediol is prepared as a preservative, and the proportion is 5%.
Further, in the step S2, the heating temperature of the phase A raw material and the phase B raw material is 75-85 ℃, and the heating temperature of the phase C raw material is 45-55 ℃.
In S3, the phase A material, the phase B material and the phase C material are sufficiently stirred by a stirrer at a rotation speed of 60-110 rpm for 10-20 minutes until the phase materials are uniformly dispersed.
Further, in the step S4, the phase A raw material and the phase B raw material are uniformly stirred for 15-25 minutes until the phase A raw material and the phase B raw material are uniformly mixed, and the temperature is reduced to 55-65 ℃ after the phase A raw material and the phase B raw material are stirred.
And in the S5, the C-phase raw material is added into the A + B-phase material, the three materials are uniformly mixed and dispersed, the homogenization treatment is carried out through a homogenizer, the homogenization speed is 8000 revolutions per minute, the homogenization is carried out for 15-20 minutes, the temperature is reduced to 40-50 ℃, in the S6, the stirring speed is 60-100 revolutions per minute, and the filling machine is used for filling until the temperature is 15-25 ℃.
Further, randomly drawing a part of finished products as samples, putting the zebra fish into a detection pool, contacting the samples with the zebra fish, testing the concentration to be 15-20 g/L, observing whether the zebra fish has the conditions of egg and embryo coagulation, failure in body segment development, lack of heartbeat and no separation of tails and egg yolks, testing acute toxicity and chronic toxicity, recording and taking pictures.
Further, in S7, the estrogen test and the component screening are performed on the sample, and the repairing function of the sample is recorded by photographing to obtain the test result.
Compared with the prior art, the tremella repairing and moisturizing mask provided by the invention has the following improvements and advantages:
the invention is a product developed aiming at the problems of easy skin sensitivity, dry skin and poor repair capability of a diabetic patient, and the product is prepared by adding nutritional ingredients such as moisture retention, patent repair and the like through a lipid type emulsification system and performing a lipid type emulsification step; the repairing component carboxymethyl chitosan is added; 1, 2-pentanediol with the effects of moisturizing, preventing corrosion and promoting infiltration is added into the product, so that the formula of the product is mild and non-irritant; the tremella polysaccharide which is used as medicine, food and skin care is added, so that the product is more effective and safer, the skin can be firmed, wrinkles can be eliminated, and the skin moistening effect is good.
Drawings
The invention is further explained below with reference to the figures and examples:
FIG. 1 is a schematic flow diagram of the present invention;
FIG. 2 is a schematic diagram of a test table of the safety and repair effect of zebrafish according to the present invention;
fig. 3 is a schematic diagram of a test picture of the safety and the repairing effect of the zebra fish of the present invention.
Detailed Description
The present invention will be described in detail below with reference to fig. 1 to 3, and the technical solutions in the embodiments of the present invention will be clearly and completely described, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides a tremella repairing and moisturizing mask through improvement,
example one
The tremella repairing and moisturizing mask comprises the following steps:
s1, preparing high-quality raw materials, classifying the raw materials into A, B, C, D, E phases and F phases respectively, classifying the high-quality raw materials into hydrogenated lecithin, avocado extract, 1, 3 butanediol, xanthan gum, scleroglucan, sodium hyaluronate, carboxymethyl β -sodium dextran, hydroxyethyl chitosan, deionized water, kelp extract, thiotaurine, 1, 2-pentanediol and tremella polysaccharide respectively, preparing the A phase from the hydrogenated lecithin, the avocado extract and 1, 3-butanediol respectively, preparing the B phase from the xanthan gum, the scleroglucan, sodium hyaluronate and carboxymethyl β -sodium dextran respectively, preparing the C phase from the hydroxyethyl chitosan and the deionized water respectively, preparing the D phase from the kelp extract, preparing the E phase from the thiotaurine and the deionized water respectively, preparing the F phase from the 1, 2-pentanediol and tremella polysaccharide respectively, preparing the hydrogenated lecithin as an emulsifier at a ratio of 0.2%, preparing the avocado extract as an emollient, preparing the 1.15%, preparing the 1, 3% and 1.78%, preparing the taurine and 0.05% as a conditioning agent, preparing the hydroxypropyl polysaccharide at a ratio of 0.05%, preparing the hydroxyethyl chitosan and 2% as a humectant, preparing the sodium dextran at a proportion of 0.05% and 5%, preparing the hyaluronic acid, preparing the humectant of the mucopolysaccharide and 0.5% and 2%, preparing the sodium thiogalactosylate and 2% respectively;
s2, heating raw materials: respectively putting the phase A raw material and the phase B raw material into a heating container for heating, and then putting the phase C raw material into the heating container for independently heating, wherein the heating temperature of the phase A raw material and the phase B raw material is 75 ℃, and the heating temperature of the phase C raw material is 45 ℃;
s3, stirring raw materials: fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using a stirrer respectively until the phase raw materials are uniformly dispersed, fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using the stirrer respectively at the rotating speed of 60 revolutions per minute for 10 minutes until the phase raw materials are uniformly dispersed;
s4, mixing and cooling: preparing a water bath kettle, putting a phase A raw material into the water bath kettle, adding a phase B raw material into the phase A raw material, stirring for a period of time until the phase A raw material and the phase B raw material are uniformly mixed, performing cooling treatment to obtain a phase A + phase B material, uniformly stirring the phase A raw material and the phase B raw material for 15 minutes until the phase A raw material and the phase B raw material are uniformly mixed, and cooling to 55 ℃ after stirring;
s5, homogenizing and cooling: under the condition that the A + B phase materials are continuously stirred, slowly adding the C phase raw materials into the A + B phase materials to uniformly mix and disperse the three materials, homogenizing, then cooling and stirring to obtain the A + B + C phase materials, adding the C phase raw materials into the A + B phase materials, uniformly mixing and dispersing the three materials, and carrying out homogenization treatment through a homogenizer, wherein the homogenization speed is 8000 revolutions per minute, the homogenization is carried out for 15 minutes, the temperature is reduced to 40 ℃, the stirring speed is 60 revolutions per minute in S6 until the temperature is 15 ℃, and filling is carried out by using a filling machine;
s6, blending and filling: when a certain temperature is reached, putting a D-phase raw material, an E-phase raw material and an F-phase raw material into an A + B + C-phase material, uniformly stirring and dispersing, putting into a sterilization kettle for sterilization until the temperature is room temperature to obtain an A + B + C + D + E + F-phase material, and filling the A + B + C + D + E + F-phase material to obtain a finished product;
s7, finished product detection: randomly extracting part of finished products to test the safety and the repair effect to obtain a test result, randomly extracting part of finished products to be used as samples, putting the zebra fish into a detection pool, enabling the samples to be in contact with the zebra fish, enabling the test concentration to be 15 g/L, observing whether the zebra fish has egg and embryo coagulation, fails to develop body segments, lacks heartbeat and has the condition that the tail part is not separated from egg yolk, testing acute toxicity and chronic toxicity, recording and photographing, testing estrogen and screening ingredients of the samples, and recording the repair function of the samples by photographing to obtain the test result.
Example two
The tremella repairing and moisturizing mask comprises the following steps:
s1, preparing high-quality raw materials, classifying the raw materials into A, B, C, D, E phases and F phases respectively, classifying the high-quality raw materials into hydrogenated lecithin, avocado extract, 1, 3 butanediol, xanthan gum, scleroglucan, sodium hyaluronate, carboxymethyl β -sodium dextran, hydroxyethyl chitosan, deionized water, kelp extract, thiotaurine, 1, 2-pentanediol and tremella polysaccharide respectively, preparing the A phase from the hydrogenated lecithin, the avocado extract and 1, 3-butanediol respectively, preparing the B phase from the xanthan gum, the scleroglucan, sodium hyaluronate and carboxymethyl β -sodium dextran respectively, preparing the C phase from the hydroxyethyl chitosan and the deionized water respectively, preparing the D phase from the kelp extract, preparing the E phase from the thiotaurine and the deionized water respectively, preparing the F phase from the 1, 2-pentanediol and tremella polysaccharide respectively, preparing the hydrogenated lecithin as an emulsifier at a ratio of 0.2%, preparing the avocado extract as an emollient, preparing the 1.15%, preparing the 1, 3% and 1.78%, preparing the taurine and 0.05% as a conditioning agent, preparing the hydroxypropyl polysaccharide at a ratio of 0.05%, preparing the hydroxyethyl chitosan and 2% as a humectant, preparing the sodium dextran at a proportion of 0.05% and 5%, preparing the hyaluronic acid, preparing the humectant of the mucopolysaccharide and 0.5% and 2%, preparing the sodium thiogalactosylate and 2% respectively;
s2, heating raw materials: respectively putting the phase A raw material and the phase B raw material into a heating container for heating, and then putting the phase C raw material into the heating container for independently heating, wherein the heating temperature of the phase A raw material and the phase B raw material is 80 ℃, and the heating temperature of the phase C raw material is 50 ℃;
s3, stirring raw materials: fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using a stirrer respectively until the phase raw materials are uniformly dispersed, fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using the stirrer respectively at the rotating speed of 80 revolutions per minute for 15 minutes until the phase raw materials are uniformly dispersed;
s4, mixing and cooling: preparing a water bath kettle, putting a phase A raw material into the water bath kettle, adding a phase B raw material into the phase A raw material, stirring for a period of time until the phase A raw material and the phase B raw material are uniformly mixed, performing cooling treatment to obtain a phase A + phase B material, uniformly stirring the phase A raw material and the phase B raw material for 20 minutes until the phase A raw material and the phase B raw material are uniformly mixed, and cooling to 55 ℃ after stirring;
s5, homogenizing and cooling: under the condition that the A + B phase materials are continuously stirred, slowly adding the C phase raw materials into the A + B phase materials to uniformly mix and disperse the three materials, homogenizing, then cooling and stirring to obtain the A + B + C phase materials, adding the C phase raw materials into the A + B phase materials, uniformly mixing and dispersing the three materials, and carrying out homogenization treatment through a homogenizer, wherein the homogenization speed is 8000 revolutions per minute, the homogenization is carried out for 18 minutes, the temperature is reduced to 40 ℃, the stirring speed is 80 revolutions per minute in S6, and the filling is carried out by using a filling machine until the temperature is 20 ℃;
s6, blending and filling: when a certain temperature is reached, putting a D-phase raw material, an E-phase raw material and an F-phase raw material into an A + B + C-phase material, uniformly stirring and dispersing, putting into a sterilization kettle for sterilization until the temperature is room temperature to obtain an A + B + C + D + E + F-phase material, and filling the A + B + C + D + E + F-phase material to obtain a finished product;
s7, finished product detection: randomly extracting part of finished products to test the safety and the repair effect to obtain a test result, randomly extracting part of finished products to be used as samples, putting the zebra fish into a detection pool, enabling the samples to be in contact with the zebra fish, enabling the test concentration to be 20 g/L, observing whether the zebra fish has egg and embryo coagulation, fails to develop body segments, lacks heartbeat and has the condition that the tail part is not separated from egg yolk, testing acute toxicity and chronic toxicity, recording and photographing, testing estrogen and screening ingredients of the samples, and recording the repair function of the samples by photographing to obtain the test result.
EXAMPLE III
The tremella repairing and moisturizing mask comprises the following steps:
s1, preparing high-quality raw materials, classifying the raw materials into A, B, C, D, E phases and F phases respectively, classifying the high-quality raw materials into hydrogenated lecithin, avocado extract, 1, 3 butanediol, xanthan gum, scleroglucan, sodium hyaluronate, carboxymethyl β -sodium dextran, hydroxyethyl chitosan, deionized water, kelp extract, thiotaurine, 1, 2-pentanediol and tremella polysaccharide respectively, preparing the A phase from the hydrogenated lecithin, the avocado extract and 1, 3-butanediol respectively, preparing the B phase from the xanthan gum, the scleroglucan, sodium hyaluronate and carboxymethyl β -sodium dextran respectively, preparing the C phase from the hydroxyethyl chitosan and the deionized water respectively, preparing the D phase from the kelp extract, preparing the E phase from the thiotaurine and the deionized water respectively, preparing the F phase from the 1, 2-pentanediol and tremella polysaccharide respectively, preparing the hydrogenated lecithin as an emulsifier at a ratio of 0.2%, preparing the avocado extract as an emollient, preparing the 1.15%, preparing the 1, 3% and 1.78%, preparing the taurine and 0.05% as a conditioning agent, preparing the hydroxypropyl polysaccharide at a ratio of 0.05%, preparing the hydroxyethyl chitosan and 2% as a humectant, preparing the sodium dextran at a proportion of 0.05% and 5%, preparing the hyaluronic acid, preparing the humectant of the mucopolysaccharide and 0.5% and 2%, preparing the sodium thiogalactosylate and 2% respectively;
s2, heating raw materials: respectively putting the phase A raw material and the phase B raw material into a heating container for heating, and then putting the phase C raw material into the heating container for independently heating, wherein the heating temperature of the phase A raw material and the phase B raw material is 85 ℃, and the heating temperature of the phase C raw material is 55 ℃;
s3, stirring raw materials: fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using a stirrer respectively until the phase raw materials are uniformly dispersed, fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using the stirrer respectively at the rotating speed of 110 revolutions per minute for 20 minutes until the phase raw materials are uniformly dispersed;
s4, mixing and cooling: preparing a water bath kettle, putting a phase A raw material into the water bath kettle, adding a phase B raw material into the phase A raw material, stirring for a period of time until the phase A raw material and the phase B raw material are uniformly mixed, performing cooling treatment to obtain a phase A + phase B material, uniformly stirring the phase A raw material and the phase B raw material for 25 minutes until the phase A raw material and the phase B raw material are uniformly mixed, and cooling to 65 ℃ after stirring;
s5, homogenizing and cooling: under the condition that the A + B phase materials are continuously stirred, slowly adding the C phase raw materials into the A + B phase materials to uniformly mix and disperse the three materials, homogenizing, then cooling and stirring to obtain the A + B + C phase materials, adding the C phase raw materials into the A + B phase materials, uniformly mixing and dispersing the three materials, and carrying out homogenization treatment through a homogenizer, wherein the homogenization speed is 8000 revolutions per minute, the homogenization is carried out for 20 minutes, the temperature is reduced to 50 ℃, the stirring speed is 80 revolutions per minute in S6, and the filling is carried out by using a filling machine until the temperature is 25 ℃;
s6, blending and filling: when a certain temperature is reached, putting a D-phase raw material, an E-phase raw material and an F-phase raw material into an A + B + C-phase material, uniformly stirring and dispersing, putting into a sterilization kettle for sterilization until the temperature is room temperature to obtain an A + B + C + D + E + F-phase material, and filling the A + B + C + D + E + F-phase material to obtain a finished product;
s7, finished product detection: randomly extracting part of finished products to test the safety and repair effect to obtain a test result, randomly extracting part of finished products to obtain a sample, putting the zebra fish into a detection pool, enabling the sample to be in contact with the zebra fish, enabling the test concentration to be 18 g/L, observing whether the zebra fish has egg and embryo coagulation, fails to develop body segments, lacks heartbeat and has the condition that the tail part is not separated from egg yolk, testing acute toxicity and chronic toxicity, recording and photographing, testing estrogen and screening components of the sample, recording the repair function of the sample by photographing to obtain the test result
The working principle is as follows: the second embodiment of the invention has better effect, the invention mainly adopts a lipid emulsification system, the liposome has two continuous structures of a hydrophilic part and a lipophilic part which have a large amount of combined water and hydrophobicity, thereby having good water locking function and the efficacy of inhibiting water evaporation, improving the permeability of horny layer, controlling the transdermal absorption speed, adding a moisturizing component of glycerol glucoside and a repairing component of carboxymethyl chitosan, adding 1, 2-pentanediol with moisturizing, antiseptic and permeation promoting effects into the product, leading the formula of the product to be milder and nonirritating, adding tremella polysaccharide with three purposes of medicine, food and skin care, leading the product to be more effective and safer, leading the skin to be firmed and eliminating wrinkles and having good skin moistening effect, leading zebra fish embryos to be capable of simulating complex in-vivo interaction and having high homology with human genome and biological systems, the change of the size and the shape of organs in the development process is an index which is simple and valuable for biological toxicity judgment, the test is convenient, part of finished products are randomly extracted to be used as samples, the zebra fish is placed into a detection pool, the samples are in contact with the zebra fish, the test concentration is more than 20 g/L, the repair efficacy is thirty-nine percent, and the repair function is strong.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.
Claims (10)
1. Tremella repair moisturizing facial mask, its characterized in that: the method comprises the following steps:
s1, preparing raw materials: preparing high-quality raw materials, and classifying the raw materials into A, B, C, D, E phases and F phases respectively;
s2, heating raw materials: respectively putting the phase A raw material and the phase B raw material into a heating container for heating, and then putting the phase C raw material into the heating container for independently heating;
s3, stirring raw materials: fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using a stirrer respectively until the phase raw materials are uniformly dispersed;
s4, mixing and cooling: preparing a water bath kettle, putting the phase A raw material into the water bath kettle, adding the phase B raw material into the phase A raw material, stirring for a period of time until the phase A raw material and the phase B raw material are uniformly mixed, and performing cooling treatment to obtain a phase A + phase B material;
s5, homogenizing and cooling: under the condition that the A + B phase materials are continuously stirred, slowly adding the C phase raw materials into the A + B phase materials to uniformly mix and disperse the three materials, homogenizing, and then cooling and stirring to obtain the A + B + C phase materials;
s6, blending and filling: when a certain temperature is reached, putting a D-phase raw material, an E-phase raw material and an F-phase raw material into an A + B + C-phase material, uniformly stirring and dispersing, putting into a sterilization kettle for sterilization until the temperature is room temperature to obtain an A + B + C + D + E + F-phase material, and filling the A + B + C + D + E + F-phase material to obtain a finished product;
s7, finished product detection: and randomly extracting part of finished products to test the safety and the repairing effect to obtain a test result.
2. The tremella repairing and hydrating mask as claimed in claim 1, wherein in S1, the high quality raw materials are hydrogenated lecithin, avocado extract, 1, 3 butylene glycol, xanthan gum, scleroglucan, sodium hyaluronate, sodium carboxymethyl β -dextran, hydroxyethyl chitosan, deionized water, kelp extract, thiotaurine, 1, 2-pentanediol and tremella polysaccharide, respectively.
3. The tremella repairing and hydrating mask as claimed in claim 1, wherein in S1, phase A is composed of hydrogenated lecithin, avocado extract and 1, 3 butylene glycol, phase B is composed of xanthan gum, scleroglucan, sodium hyaluronate and carboxymethyl β -sodium dextran, phase C is composed of hydroxyethyl chitosan and deionized water, phase D is composed of kelp extract, phase E is composed of thiotaurine and deionized water, and phase F is composed of 1, 2-pentanediol and tremella polysaccharide.
4. The tremella repairing and moisturizing mask as claimed in claim 2, wherein the hydrogenated lecithin is blended as an emulsifier in a ratio of 0.2%, the avocado extract is blended as an emollient in a ratio of 0.15%, 1, 3-butanediol and deionized water are blended as solvents in a ratio of 3% and 78%, xanthan gum is blended as a thickener in a ratio of 0.2%, scleroglucan and sodium hyaluronate are blended as moisturizers in a ratio of 4% and 0.05%, carboxymethyl β -sodium dextran, hydroxyethyl chitosan, kelp extract, thiotaurine and tremella polysaccharide are blended as skin conditioners in a ratio of 2%, 0.2%, 2%, 0.2% and 5%, and 1, 2-pentanediol is blended as a preservative in a ratio of 5%.
5. The tremella repairing hydrating mask as claimed in claim 1, wherein: in the S2, the heating temperature of the phase A raw material and the phase B raw material is 75-85 ℃, and the heating temperature of the phase C raw material is 45-55 ℃.
6. The tremella repairing hydrating mask as claimed in claim 1, wherein: in the S3, the phase A raw material, the phase B raw material and the phase C raw material are respectively and fully stirred by a stirrer, the rotating speed during stirring is 60-110 r/min, and the stirring is carried out for 10-20 min until the phase raw materials are uniformly dispersed.
7. The tremella repairing hydrating mask as claimed in claim 1, wherein: and in the S4, uniformly stirring the phase A raw material and the phase B raw material for 15-25 minutes until the phase A raw material and the phase B raw material are uniformly mixed, and cooling to 55-65 ℃ after stirring.
8. The tremella repairing hydrating mask as claimed in claim 1, wherein: and in the S5, the C-phase raw material is added into the A + B-phase material, the three materials are uniformly mixed and dispersed, the homogenization treatment is carried out through a homogenizer, the homogenization speed is 8000 revolutions per minute, the homogenization is carried out for 15-20 minutes, the temperature is reduced to 40-50 ℃, in the S6, the stirring speed is 60-100 revolutions per minute, and the filling machine is used for filling until the temperature is 15-25 ℃.
9. The tremella repairing hydrating mask as claimed in claim 1, wherein: and in the step S7, randomly drawing a part of finished products as samples, putting the zebra fish into a detection pool, enabling the samples to be in contact with the zebra fish, testing whether the zebra fish has the conditions that eggs and embryos are coagulated, the body nodes cannot be developed, the heartbeat is lacked and the tail part and the egg yolk are not separated, testing acute toxicity and chronic toxicity, and recording and taking pictures.
10. The tremella repairing hydrating mask as claimed in claim 1, wherein: in S7, estrogen test and component screening are carried out on the sample, and the repair function of the sample is recorded by photographing to obtain a test result.
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Application publication date: 20200807 |