CN111494265A - Tremella repairing and moisturizing mask - Google Patents

Tremella repairing and moisturizing mask Download PDF

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Publication number
CN111494265A
CN111494265A CN202010438931.5A CN202010438931A CN111494265A CN 111494265 A CN111494265 A CN 111494265A CN 202010438931 A CN202010438931 A CN 202010438931A CN 111494265 A CN111494265 A CN 111494265A
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phase
raw material
tremella
repairing
stirring
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尹卫群
蔡光欣
惠宏襄
黄丽翠
吴嫦颜
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Guangdong Chuangmei Anti Aging Research Co ltd
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Guangdong Chuangmei Anti Aging Research Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9706Algae
    • A61K8/9711Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/46Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
    • A61K8/466Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55Phosphorus compounds
    • A61K8/553Phospholipids, e.g. lecithin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/736Chitin; Chitosan; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/007Preparations for dry skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/70Biological properties of the composition as a whole
    • A61K2800/72Hypo-allergenic

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Abstract

The invention relates to the technical field of cosmetics, in particular to a tremella repairing and moisturizing mask which comprises the following steps: s1, preparing raw materials: preparing high-quality raw materials, and classifying the raw materials into A, B, C, D, E phases and F phases respectively; s2, heating raw materials: respectively putting the phase A raw material and the phase B raw material into a heating container for heating, and then putting the phase C raw material into the heating container for independently heating; s3, stirring raw materials: fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using a stirrer respectively until the phase raw materials are uniformly dispersed; s4, mixing and cooling: and (4) preparing a water bath kettle. The invention adopts a lipid emulsification system, and the liposome has two continuous structures of a hydrophilic part and a lipophilic part and has a large amount of bound water and hydrophobicity, thereby having good water locking function and the effect of inhibiting water evaporation, improving the permeability of stratum corneum, controlling the transdermal absorption speed, and adding a repairing component of carboxymethyl chitosan.

Description

Tremella repairing and moisturizing mask
Technical Field
The invention relates to the technical field of cosmetics, in particular to a tremella repairing and moisturizing mask.
Background
The mask is a carrier of beauty care products, is a category of the beauty care products, and is the most important purpose of making up the insufficient cleaning work of makeup removal and face washing, and is matched with other essence components to realize other care functions such as moisturizing, whitening, anti-aging, grease balancing and the like.
Chinese patent No. CN201110429625.6 provides a nighttime repairing and moisturizing mask and a preparation method thereof, phase A: 0.01-0.06% of hyaluronic acid, 0.2-0.5% of carbomer, 261-5% of glyceryl polyether, 0.5-2% of bis-PEG-18 methyl dimethylsilane and 8-12% of butanediol; phase B: 3-5.5% of glycerin, 0.2-0.3% of betaine and 0.08-0.12%.
The nighttime repairing and moisturizing mask and the preparation method thereof in the CN201110429625.6 patent have the characteristics of necessary nutrition for rejuvenation at night, accelerating self-repair of skin and restoring skin smoothness, but the existing technical formula is a mask developed aiming at the problems of easy skin sensitivity, dry skin and poor repairing capability of diabetes patients, so that the development of a tremella repairing and moisturizing mask is urgently needed.
Disclosure of Invention
The invention aims to provide a tremella repairing and moisturizing mask to solve the problems that existing technical formulas in the background art are few in aim, and the mask is developed based on the problems that the skin of a diabetic patient is sensitive, the skin is dry and the repairing capability is poor.
The technical scheme of the invention is as follows: the tremella repairing and moisturizing mask comprises the following steps:
s1, preparing raw materials: preparing high-quality raw materials, and classifying the raw materials into A, B, C, D, E phases and F phases respectively;
s2, heating raw materials: respectively putting the phase A raw material and the phase B raw material into a heating container for heating, and then putting the phase C raw material into the heating container for independently heating;
s3, stirring raw materials: fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using a stirrer respectively until the phase raw materials are uniformly dispersed;
s4, mixing and cooling: preparing a water bath kettle, putting the phase A raw material into the water bath kettle, adding the phase B raw material into the phase A raw material, stirring for a period of time until the phase A raw material and the phase B raw material are uniformly mixed, and performing cooling treatment to obtain a phase A + phase B material;
s5, homogenizing and cooling: under the condition that the A + B phase materials are continuously stirred, slowly adding the C phase raw materials into the A + B phase materials to uniformly mix and disperse the three materials, homogenizing, and then cooling and stirring to obtain the A + B + C phase materials;
s6, blending and filling: when a certain temperature is reached, putting a D-phase raw material, an E-phase raw material and an F-phase raw material into an A + B + C-phase material, uniformly stirring and dispersing, putting into a sterilization kettle for sterilization until the temperature is room temperature to obtain an A + B + C + D + E + F-phase material, and filling the A + B + C + D + E + F-phase material to obtain a finished product;
s7, finished product detection: and randomly extracting part of finished products to test the safety and the repairing effect to obtain a test result.
Further, in S1, the high-quality raw materials are hydrogenated lecithin, avocado extract, 1, 3-butanediol, xanthan gum, sclerotium rolfsii gum, sodium hyaluronate, sodium carboxymethyl β -dextran sodium, hydroxyethyl chitosan, deionized water, kelp extract, thiotaurine, 1, 2-pentanediol, and tremella polysaccharide, respectively.
Furthermore, the phase A is composed of three of hydrogenated lecithin, avocado extract and 1, 3-butanediol, the phase B is composed of xanthan gum, sclerotium rolfsii gum, sodium hyaluronate and carboxymethyl β -dextran sodium, the phase C is composed of hydroxyethyl chitosan and deionized water, the phase D is composed of kelp extract, the phase E is composed of thiotaurine and deionized water, and the phase F is composed of 1, 2-pentanediol and tremella polysaccharide.
Further, the hydrogenated lecithin is prepared as an emulsifier, the proportion is 0.2%, the avocado extract is prepared as an emollient, the proportion is 0.15%, the 1, 3-butanediol and deionized water are prepared as solvents, the proportion is 3% and 78%, the xanthan gum is prepared as a thickening agent, the proportion is 0.2%, the sclerotium rolfsii gum and the sodium hyaluronate are prepared as humectants, the proportion is 4% and 0.05%, the carboxymethyl β -dextran sodium, hydroxyethyl chitosan, the kelp extract, thiotaurine and the tremella polysaccharide are prepared as skin conditioners, the proportions are respectively 2%, 0.2%, 2%, 0.2% and 5%, and the 1, 2-pentanediol is prepared as a preservative, and the proportion is 5%.
Further, in the step S2, the heating temperature of the phase A raw material and the phase B raw material is 75-85 ℃, and the heating temperature of the phase C raw material is 45-55 ℃.
In S3, the phase A material, the phase B material and the phase C material are sufficiently stirred by a stirrer at a rotation speed of 60-110 rpm for 10-20 minutes until the phase materials are uniformly dispersed.
Further, in the step S4, the phase A raw material and the phase B raw material are uniformly stirred for 15-25 minutes until the phase A raw material and the phase B raw material are uniformly mixed, and the temperature is reduced to 55-65 ℃ after the phase A raw material and the phase B raw material are stirred.
And in the S5, the C-phase raw material is added into the A + B-phase material, the three materials are uniformly mixed and dispersed, the homogenization treatment is carried out through a homogenizer, the homogenization speed is 8000 revolutions per minute, the homogenization is carried out for 15-20 minutes, the temperature is reduced to 40-50 ℃, in the S6, the stirring speed is 60-100 revolutions per minute, and the filling machine is used for filling until the temperature is 15-25 ℃.
Further, randomly drawing a part of finished products as samples, putting the zebra fish into a detection pool, contacting the samples with the zebra fish, testing the concentration to be 15-20 g/L, observing whether the zebra fish has the conditions of egg and embryo coagulation, failure in body segment development, lack of heartbeat and no separation of tails and egg yolks, testing acute toxicity and chronic toxicity, recording and taking pictures.
Further, in S7, the estrogen test and the component screening are performed on the sample, and the repairing function of the sample is recorded by photographing to obtain the test result.
Compared with the prior art, the tremella repairing and moisturizing mask provided by the invention has the following improvements and advantages:
the invention is a product developed aiming at the problems of easy skin sensitivity, dry skin and poor repair capability of a diabetic patient, and the product is prepared by adding nutritional ingredients such as moisture retention, patent repair and the like through a lipid type emulsification system and performing a lipid type emulsification step; the repairing component carboxymethyl chitosan is added; 1, 2-pentanediol with the effects of moisturizing, preventing corrosion and promoting infiltration is added into the product, so that the formula of the product is mild and non-irritant; the tremella polysaccharide which is used as medicine, food and skin care is added, so that the product is more effective and safer, the skin can be firmed, wrinkles can be eliminated, and the skin moistening effect is good.
Drawings
The invention is further explained below with reference to the figures and examples:
FIG. 1 is a schematic flow diagram of the present invention;
FIG. 2 is a schematic diagram of a test table of the safety and repair effect of zebrafish according to the present invention;
fig. 3 is a schematic diagram of a test picture of the safety and the repairing effect of the zebra fish of the present invention.
Detailed Description
The present invention will be described in detail below with reference to fig. 1 to 3, and the technical solutions in the embodiments of the present invention will be clearly and completely described, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides a tremella repairing and moisturizing mask through improvement,
example one
The tremella repairing and moisturizing mask comprises the following steps:
s1, preparing high-quality raw materials, classifying the raw materials into A, B, C, D, E phases and F phases respectively, classifying the high-quality raw materials into hydrogenated lecithin, avocado extract, 1, 3 butanediol, xanthan gum, scleroglucan, sodium hyaluronate, carboxymethyl β -sodium dextran, hydroxyethyl chitosan, deionized water, kelp extract, thiotaurine, 1, 2-pentanediol and tremella polysaccharide respectively, preparing the A phase from the hydrogenated lecithin, the avocado extract and 1, 3-butanediol respectively, preparing the B phase from the xanthan gum, the scleroglucan, sodium hyaluronate and carboxymethyl β -sodium dextran respectively, preparing the C phase from the hydroxyethyl chitosan and the deionized water respectively, preparing the D phase from the kelp extract, preparing the E phase from the thiotaurine and the deionized water respectively, preparing the F phase from the 1, 2-pentanediol and tremella polysaccharide respectively, preparing the hydrogenated lecithin as an emulsifier at a ratio of 0.2%, preparing the avocado extract as an emollient, preparing the 1.15%, preparing the 1, 3% and 1.78%, preparing the taurine and 0.05% as a conditioning agent, preparing the hydroxypropyl polysaccharide at a ratio of 0.05%, preparing the hydroxyethyl chitosan and 2% as a humectant, preparing the sodium dextran at a proportion of 0.05% and 5%, preparing the hyaluronic acid, preparing the humectant of the mucopolysaccharide and 0.5% and 2%, preparing the sodium thiogalactosylate and 2% respectively;
s2, heating raw materials: respectively putting the phase A raw material and the phase B raw material into a heating container for heating, and then putting the phase C raw material into the heating container for independently heating, wherein the heating temperature of the phase A raw material and the phase B raw material is 75 ℃, and the heating temperature of the phase C raw material is 45 ℃;
s3, stirring raw materials: fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using a stirrer respectively until the phase raw materials are uniformly dispersed, fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using the stirrer respectively at the rotating speed of 60 revolutions per minute for 10 minutes until the phase raw materials are uniformly dispersed;
s4, mixing and cooling: preparing a water bath kettle, putting a phase A raw material into the water bath kettle, adding a phase B raw material into the phase A raw material, stirring for a period of time until the phase A raw material and the phase B raw material are uniformly mixed, performing cooling treatment to obtain a phase A + phase B material, uniformly stirring the phase A raw material and the phase B raw material for 15 minutes until the phase A raw material and the phase B raw material are uniformly mixed, and cooling to 55 ℃ after stirring;
s5, homogenizing and cooling: under the condition that the A + B phase materials are continuously stirred, slowly adding the C phase raw materials into the A + B phase materials to uniformly mix and disperse the three materials, homogenizing, then cooling and stirring to obtain the A + B + C phase materials, adding the C phase raw materials into the A + B phase materials, uniformly mixing and dispersing the three materials, and carrying out homogenization treatment through a homogenizer, wherein the homogenization speed is 8000 revolutions per minute, the homogenization is carried out for 15 minutes, the temperature is reduced to 40 ℃, the stirring speed is 60 revolutions per minute in S6 until the temperature is 15 ℃, and filling is carried out by using a filling machine;
s6, blending and filling: when a certain temperature is reached, putting a D-phase raw material, an E-phase raw material and an F-phase raw material into an A + B + C-phase material, uniformly stirring and dispersing, putting into a sterilization kettle for sterilization until the temperature is room temperature to obtain an A + B + C + D + E + F-phase material, and filling the A + B + C + D + E + F-phase material to obtain a finished product;
s7, finished product detection: randomly extracting part of finished products to test the safety and the repair effect to obtain a test result, randomly extracting part of finished products to be used as samples, putting the zebra fish into a detection pool, enabling the samples to be in contact with the zebra fish, enabling the test concentration to be 15 g/L, observing whether the zebra fish has egg and embryo coagulation, fails to develop body segments, lacks heartbeat and has the condition that the tail part is not separated from egg yolk, testing acute toxicity and chronic toxicity, recording and photographing, testing estrogen and screening ingredients of the samples, and recording the repair function of the samples by photographing to obtain the test result.
Example two
The tremella repairing and moisturizing mask comprises the following steps:
s1, preparing high-quality raw materials, classifying the raw materials into A, B, C, D, E phases and F phases respectively, classifying the high-quality raw materials into hydrogenated lecithin, avocado extract, 1, 3 butanediol, xanthan gum, scleroglucan, sodium hyaluronate, carboxymethyl β -sodium dextran, hydroxyethyl chitosan, deionized water, kelp extract, thiotaurine, 1, 2-pentanediol and tremella polysaccharide respectively, preparing the A phase from the hydrogenated lecithin, the avocado extract and 1, 3-butanediol respectively, preparing the B phase from the xanthan gum, the scleroglucan, sodium hyaluronate and carboxymethyl β -sodium dextran respectively, preparing the C phase from the hydroxyethyl chitosan and the deionized water respectively, preparing the D phase from the kelp extract, preparing the E phase from the thiotaurine and the deionized water respectively, preparing the F phase from the 1, 2-pentanediol and tremella polysaccharide respectively, preparing the hydrogenated lecithin as an emulsifier at a ratio of 0.2%, preparing the avocado extract as an emollient, preparing the 1.15%, preparing the 1, 3% and 1.78%, preparing the taurine and 0.05% as a conditioning agent, preparing the hydroxypropyl polysaccharide at a ratio of 0.05%, preparing the hydroxyethyl chitosan and 2% as a humectant, preparing the sodium dextran at a proportion of 0.05% and 5%, preparing the hyaluronic acid, preparing the humectant of the mucopolysaccharide and 0.5% and 2%, preparing the sodium thiogalactosylate and 2% respectively;
s2, heating raw materials: respectively putting the phase A raw material and the phase B raw material into a heating container for heating, and then putting the phase C raw material into the heating container for independently heating, wherein the heating temperature of the phase A raw material and the phase B raw material is 80 ℃, and the heating temperature of the phase C raw material is 50 ℃;
s3, stirring raw materials: fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using a stirrer respectively until the phase raw materials are uniformly dispersed, fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using the stirrer respectively at the rotating speed of 80 revolutions per minute for 15 minutes until the phase raw materials are uniformly dispersed;
s4, mixing and cooling: preparing a water bath kettle, putting a phase A raw material into the water bath kettle, adding a phase B raw material into the phase A raw material, stirring for a period of time until the phase A raw material and the phase B raw material are uniformly mixed, performing cooling treatment to obtain a phase A + phase B material, uniformly stirring the phase A raw material and the phase B raw material for 20 minutes until the phase A raw material and the phase B raw material are uniformly mixed, and cooling to 55 ℃ after stirring;
s5, homogenizing and cooling: under the condition that the A + B phase materials are continuously stirred, slowly adding the C phase raw materials into the A + B phase materials to uniformly mix and disperse the three materials, homogenizing, then cooling and stirring to obtain the A + B + C phase materials, adding the C phase raw materials into the A + B phase materials, uniformly mixing and dispersing the three materials, and carrying out homogenization treatment through a homogenizer, wherein the homogenization speed is 8000 revolutions per minute, the homogenization is carried out for 18 minutes, the temperature is reduced to 40 ℃, the stirring speed is 80 revolutions per minute in S6, and the filling is carried out by using a filling machine until the temperature is 20 ℃;
s6, blending and filling: when a certain temperature is reached, putting a D-phase raw material, an E-phase raw material and an F-phase raw material into an A + B + C-phase material, uniformly stirring and dispersing, putting into a sterilization kettle for sterilization until the temperature is room temperature to obtain an A + B + C + D + E + F-phase material, and filling the A + B + C + D + E + F-phase material to obtain a finished product;
s7, finished product detection: randomly extracting part of finished products to test the safety and the repair effect to obtain a test result, randomly extracting part of finished products to be used as samples, putting the zebra fish into a detection pool, enabling the samples to be in contact with the zebra fish, enabling the test concentration to be 20 g/L, observing whether the zebra fish has egg and embryo coagulation, fails to develop body segments, lacks heartbeat and has the condition that the tail part is not separated from egg yolk, testing acute toxicity and chronic toxicity, recording and photographing, testing estrogen and screening ingredients of the samples, and recording the repair function of the samples by photographing to obtain the test result.
EXAMPLE III
The tremella repairing and moisturizing mask comprises the following steps:
s1, preparing high-quality raw materials, classifying the raw materials into A, B, C, D, E phases and F phases respectively, classifying the high-quality raw materials into hydrogenated lecithin, avocado extract, 1, 3 butanediol, xanthan gum, scleroglucan, sodium hyaluronate, carboxymethyl β -sodium dextran, hydroxyethyl chitosan, deionized water, kelp extract, thiotaurine, 1, 2-pentanediol and tremella polysaccharide respectively, preparing the A phase from the hydrogenated lecithin, the avocado extract and 1, 3-butanediol respectively, preparing the B phase from the xanthan gum, the scleroglucan, sodium hyaluronate and carboxymethyl β -sodium dextran respectively, preparing the C phase from the hydroxyethyl chitosan and the deionized water respectively, preparing the D phase from the kelp extract, preparing the E phase from the thiotaurine and the deionized water respectively, preparing the F phase from the 1, 2-pentanediol and tremella polysaccharide respectively, preparing the hydrogenated lecithin as an emulsifier at a ratio of 0.2%, preparing the avocado extract as an emollient, preparing the 1.15%, preparing the 1, 3% and 1.78%, preparing the taurine and 0.05% as a conditioning agent, preparing the hydroxypropyl polysaccharide at a ratio of 0.05%, preparing the hydroxyethyl chitosan and 2% as a humectant, preparing the sodium dextran at a proportion of 0.05% and 5%, preparing the hyaluronic acid, preparing the humectant of the mucopolysaccharide and 0.5% and 2%, preparing the sodium thiogalactosylate and 2% respectively;
s2, heating raw materials: respectively putting the phase A raw material and the phase B raw material into a heating container for heating, and then putting the phase C raw material into the heating container for independently heating, wherein the heating temperature of the phase A raw material and the phase B raw material is 85 ℃, and the heating temperature of the phase C raw material is 55 ℃;
s3, stirring raw materials: fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using a stirrer respectively until the phase raw materials are uniformly dispersed, fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using the stirrer respectively at the rotating speed of 110 revolutions per minute for 20 minutes until the phase raw materials are uniformly dispersed;
s4, mixing and cooling: preparing a water bath kettle, putting a phase A raw material into the water bath kettle, adding a phase B raw material into the phase A raw material, stirring for a period of time until the phase A raw material and the phase B raw material are uniformly mixed, performing cooling treatment to obtain a phase A + phase B material, uniformly stirring the phase A raw material and the phase B raw material for 25 minutes until the phase A raw material and the phase B raw material are uniformly mixed, and cooling to 65 ℃ after stirring;
s5, homogenizing and cooling: under the condition that the A + B phase materials are continuously stirred, slowly adding the C phase raw materials into the A + B phase materials to uniformly mix and disperse the three materials, homogenizing, then cooling and stirring to obtain the A + B + C phase materials, adding the C phase raw materials into the A + B phase materials, uniformly mixing and dispersing the three materials, and carrying out homogenization treatment through a homogenizer, wherein the homogenization speed is 8000 revolutions per minute, the homogenization is carried out for 20 minutes, the temperature is reduced to 50 ℃, the stirring speed is 80 revolutions per minute in S6, and the filling is carried out by using a filling machine until the temperature is 25 ℃;
s6, blending and filling: when a certain temperature is reached, putting a D-phase raw material, an E-phase raw material and an F-phase raw material into an A + B + C-phase material, uniformly stirring and dispersing, putting into a sterilization kettle for sterilization until the temperature is room temperature to obtain an A + B + C + D + E + F-phase material, and filling the A + B + C + D + E + F-phase material to obtain a finished product;
s7, finished product detection: randomly extracting part of finished products to test the safety and repair effect to obtain a test result, randomly extracting part of finished products to obtain a sample, putting the zebra fish into a detection pool, enabling the sample to be in contact with the zebra fish, enabling the test concentration to be 18 g/L, observing whether the zebra fish has egg and embryo coagulation, fails to develop body segments, lacks heartbeat and has the condition that the tail part is not separated from egg yolk, testing acute toxicity and chronic toxicity, recording and photographing, testing estrogen and screening components of the sample, recording the repair function of the sample by photographing to obtain the test result
The working principle is as follows: the second embodiment of the invention has better effect, the invention mainly adopts a lipid emulsification system, the liposome has two continuous structures of a hydrophilic part and a lipophilic part which have a large amount of combined water and hydrophobicity, thereby having good water locking function and the efficacy of inhibiting water evaporation, improving the permeability of horny layer, controlling the transdermal absorption speed, adding a moisturizing component of glycerol glucoside and a repairing component of carboxymethyl chitosan, adding 1, 2-pentanediol with moisturizing, antiseptic and permeation promoting effects into the product, leading the formula of the product to be milder and nonirritating, adding tremella polysaccharide with three purposes of medicine, food and skin care, leading the product to be more effective and safer, leading the skin to be firmed and eliminating wrinkles and having good skin moistening effect, leading zebra fish embryos to be capable of simulating complex in-vivo interaction and having high homology with human genome and biological systems, the change of the size and the shape of organs in the development process is an index which is simple and valuable for biological toxicity judgment, the test is convenient, part of finished products are randomly extracted to be used as samples, the zebra fish is placed into a detection pool, the samples are in contact with the zebra fish, the test concentration is more than 20 g/L, the repair efficacy is thirty-nine percent, and the repair function is strong.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims (10)

1. Tremella repair moisturizing facial mask, its characterized in that: the method comprises the following steps:
s1, preparing raw materials: preparing high-quality raw materials, and classifying the raw materials into A, B, C, D, E phases and F phases respectively;
s2, heating raw materials: respectively putting the phase A raw material and the phase B raw material into a heating container for heating, and then putting the phase C raw material into the heating container for independently heating;
s3, stirring raw materials: fully stirring the phase A raw material, the phase B raw material and the phase C raw material by using a stirrer respectively until the phase raw materials are uniformly dispersed;
s4, mixing and cooling: preparing a water bath kettle, putting the phase A raw material into the water bath kettle, adding the phase B raw material into the phase A raw material, stirring for a period of time until the phase A raw material and the phase B raw material are uniformly mixed, and performing cooling treatment to obtain a phase A + phase B material;
s5, homogenizing and cooling: under the condition that the A + B phase materials are continuously stirred, slowly adding the C phase raw materials into the A + B phase materials to uniformly mix and disperse the three materials, homogenizing, and then cooling and stirring to obtain the A + B + C phase materials;
s6, blending and filling: when a certain temperature is reached, putting a D-phase raw material, an E-phase raw material and an F-phase raw material into an A + B + C-phase material, uniformly stirring and dispersing, putting into a sterilization kettle for sterilization until the temperature is room temperature to obtain an A + B + C + D + E + F-phase material, and filling the A + B + C + D + E + F-phase material to obtain a finished product;
s7, finished product detection: and randomly extracting part of finished products to test the safety and the repairing effect to obtain a test result.
2. The tremella repairing and hydrating mask as claimed in claim 1, wherein in S1, the high quality raw materials are hydrogenated lecithin, avocado extract, 1, 3 butylene glycol, xanthan gum, scleroglucan, sodium hyaluronate, sodium carboxymethyl β -dextran, hydroxyethyl chitosan, deionized water, kelp extract, thiotaurine, 1, 2-pentanediol and tremella polysaccharide, respectively.
3. The tremella repairing and hydrating mask as claimed in claim 1, wherein in S1, phase A is composed of hydrogenated lecithin, avocado extract and 1, 3 butylene glycol, phase B is composed of xanthan gum, scleroglucan, sodium hyaluronate and carboxymethyl β -sodium dextran, phase C is composed of hydroxyethyl chitosan and deionized water, phase D is composed of kelp extract, phase E is composed of thiotaurine and deionized water, and phase F is composed of 1, 2-pentanediol and tremella polysaccharide.
4. The tremella repairing and moisturizing mask as claimed in claim 2, wherein the hydrogenated lecithin is blended as an emulsifier in a ratio of 0.2%, the avocado extract is blended as an emollient in a ratio of 0.15%, 1, 3-butanediol and deionized water are blended as solvents in a ratio of 3% and 78%, xanthan gum is blended as a thickener in a ratio of 0.2%, scleroglucan and sodium hyaluronate are blended as moisturizers in a ratio of 4% and 0.05%, carboxymethyl β -sodium dextran, hydroxyethyl chitosan, kelp extract, thiotaurine and tremella polysaccharide are blended as skin conditioners in a ratio of 2%, 0.2%, 2%, 0.2% and 5%, and 1, 2-pentanediol is blended as a preservative in a ratio of 5%.
5. The tremella repairing hydrating mask as claimed in claim 1, wherein: in the S2, the heating temperature of the phase A raw material and the phase B raw material is 75-85 ℃, and the heating temperature of the phase C raw material is 45-55 ℃.
6. The tremella repairing hydrating mask as claimed in claim 1, wherein: in the S3, the phase A raw material, the phase B raw material and the phase C raw material are respectively and fully stirred by a stirrer, the rotating speed during stirring is 60-110 r/min, and the stirring is carried out for 10-20 min until the phase raw materials are uniformly dispersed.
7. The tremella repairing hydrating mask as claimed in claim 1, wherein: and in the S4, uniformly stirring the phase A raw material and the phase B raw material for 15-25 minutes until the phase A raw material and the phase B raw material are uniformly mixed, and cooling to 55-65 ℃ after stirring.
8. The tremella repairing hydrating mask as claimed in claim 1, wherein: and in the S5, the C-phase raw material is added into the A + B-phase material, the three materials are uniformly mixed and dispersed, the homogenization treatment is carried out through a homogenizer, the homogenization speed is 8000 revolutions per minute, the homogenization is carried out for 15-20 minutes, the temperature is reduced to 40-50 ℃, in the S6, the stirring speed is 60-100 revolutions per minute, and the filling machine is used for filling until the temperature is 15-25 ℃.
9. The tremella repairing hydrating mask as claimed in claim 1, wherein: and in the step S7, randomly drawing a part of finished products as samples, putting the zebra fish into a detection pool, enabling the samples to be in contact with the zebra fish, testing whether the zebra fish has the conditions that eggs and embryos are coagulated, the body nodes cannot be developed, the heartbeat is lacked and the tail part and the egg yolk are not separated, testing acute toxicity and chronic toxicity, and recording and taking pictures.
10. The tremella repairing hydrating mask as claimed in claim 1, wherein: in S7, estrogen test and component screening are carried out on the sample, and the repair function of the sample is recorded by photographing to obtain a test result.
CN202010438931.5A 2020-05-22 2020-05-22 Tremella repairing and moisturizing mask Pending CN111494265A (en)

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Application publication date: 20200807