CN111481467A - 赋予冷却效果的用于阻挡紫外线的化妆品组合物 - Google Patents
赋予冷却效果的用于阻挡紫外线的化妆品组合物 Download PDFInfo
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Abstract
本发明涉及一种气溶胶剂型的用于阻挡紫外线的化妆品组合物，其包括：气溶胶原液，其包括羟乙基纤维素(Hydroxyethyl‑cellulose)及紫外线阻挡剂；以及气溶胶喷射剂。
Description
相关申请的交叉引用
本申请要求于2019年01月25日提交的韩国专利申请No.10-2019-0009942的优先权和权益，其通过引用合并于此用于所有目的，如同在此完全阐述一样。
技术领域
涉及一种气溶胶剂型的用于阻挡紫外线的化妆品组合物，其包括气溶胶原液，其包括羟乙基纤维素(Hydroxyethyl-cellulose)及紫外线阻挡剂；以及气溶胶喷射剂。
背景技术
通常，大部分能够感觉到冷却效果的产品通过包括诸如乙醇的挥发性成分或薄荷醇(menthol)或其衍生物来赋予冷却效果。虽然这些方法有效地赋予冷却效果，但是诸如乙醇的挥发性成分趋于使剂型没有太大差异地划一化，且薄荷醇由于其对皮肤的刺激性，在用于阻挡紫外线的化妆品组合物中进一步受到限制。因此，需要一种能够在感觉到新的使用感的同时赋予冷却效果的新剂型。
含有喷射气体的气溶胶由于气体和喷射压在使用中受到限制。虽然能够使用气体来赋予少量冷却效果，但是除了在剂型本身中由于气体的方法外，没有其他可以感觉到冷却效果的剂型。因此，对能够赋予冷却效果的新的气溶胶剂型的产品的需求不断增加。
另外，虽然现时研究的含有滑石和丁烷的具有冷却效果的皮肤保湿用化妆品组合物，及气溶胶剂型的清洁用化妆品组合物等具有赋予皮肤冷却效果的功能，但是使用烷醇酰胺类表面活性剂使两层相结构不可能，并包括具有下降的保湿感的单价高的聚甲基丙烯酸甲酯粉末，且存在不能具有紫外线阻挡功能的缺点。
在这些背景下，本发明人已经完成了具有紫外线阻挡功能并可以以与现有的方法不同的方法赋予冷却效果和新的使用感的与气体形成一个凝胶(gel)状态的两层相或单一相液体结构的化妆品组合物。
先有技术文献
专利文献
(专利文献1)韩国注册专利第10-0602144号
(专利文献2)韩国注册专利第10-2014-0134359号
发明内容
一方面提供一种用于阻挡紫外线的化妆品组合物，其包括气溶胶原液，其包括羟乙基纤维素(Hydroxyethyl-cellulose)及紫外线阻挡剂；以及气溶胶喷射剂。
一方面提供一种用于阻挡紫外线的化妆品组合物，其包括气溶胶原液，其包括羟乙基纤维素(Hydroxyethyl-cellulose)及紫外线阻挡剂；以及气溶胶喷射剂。
所述气溶胶(aerosol)是指固体或液体的微粒子物理学地分散在气体中的胶体状态。所述气溶胶剂型的化妆品组合物可以是指将使喷射的气溶胶原液和喷射剂放入耐压密封容器中，且在喷射时由于喷射剂压力而均匀喷射化妆品的喷射剂。
只要是可以在化妆品组合物中使用的任何气溶胶喷射剂都可以不受限制地使用为所述气溶胶喷射剂。具体而言，所述气溶胶喷射剂可以选自氮、液化石油氣(LPG)、液化天然气(LNG)、二甲醚(DME)，及四氟丙烯-1234ZE(HFO-1234ZE)中的至少一种。
基于所述化妆品组合物的总重量，所述气溶胶喷射剂的含量可以为10重量％至70％重量％，具体地，可以为20重量％至70重量％，更具体地，可以为30重量％至70重量％，再更具体地，可以为40重量％至60重量％。
所述气溶胶原液是整个化妆品组合物中除气溶胶喷射剂之外的剩余材料，且可以是指通过被喷射来获得特定效果的有效物质。气溶胶原液可以处于液体、粉末或奶油状态，但是不特别限于此。
所述气溶胶原液可以包括增稠剂和紫外线阻挡剂。
所述增稠剂可以与增稠剂互换使用，并且可以包括所有增加化妆品组合物粘度的物质。所述增稠剂可以是无机增稠剂、有机增稠剂或其组合。具体而言，所述增稠剂可以选自膨润土、锂蒙脱石、聚乙烯吡咯烷酮、硅酸钠镁锂、聚丙烯酸钠、聚丙烯酸钠淀粉、玉米淀粉、硬脂酸钠黄原胶、丙烯酰二甲基牛磺酸铵/VP共聚物、丙烯酸(酯)类/C10-30烷醇丙烯酸酯交联聚合物、卡波姆、微晶纤维素、纤维素胶，以及羟乙基纤维素中的至少一种。
所述增稠剂可以是羟乙基纤维素(Hydroxyethyl-cellulose)。在一实施例中，确认了所述气溶胶剂型的用于阻挡紫外线的化妆品组合物通过包括羟乙基纤维素以能够赋予皮肤冷却效果和新的使用感。具体而言，确认了羟乙基纤维素在所述气溶胶剂型的化妆品组合物喷射时将喷射气体的捕获功能最大化，使即使没有现时使用的聚甲基丙烯酸甲酯也调节喷射时性状，来能够赋予皮肤冷却效果和新的使用感。另外，确认了所述组合物即使不含有现时用于赋予冷却效果的诸如醇类的挥发性成分或薄荷醇等，也可以表现出改善的冷却效果。
基于所述气溶胶原液的总重量，所述羟乙基纤维素的含量可以为0.1重量％至2.0重量％，具体地，可以为0.3重量％至1.8重量％，更具体地，可以为0.4重量％至1.6重量，再更具体地，可以为0.5重量％至1.2重量％。
所述紫外线阻挡剂不受限制，只要是常用于化妆品组合物中的具有紫外线阻挡目的的物质即可使用。所述紫外线阻挡剂可以是有机紫外线阻挡剂、无机紫外线阻挡剂，或其组合。所述有机紫外线阻挡剂可以选自胡莫柳酯、水杨酸乙基己酯、苯基苯并咪唑磺酸、奥克立林、甲氧基肉桂酸辛酯、丁基甲氧基二苯甲酰甲烷、双-乙基己氧苯酚甲氧苯基三嗪、乙基氨基羟基苯甲酰苯甲酸己酯、乙基己基三嗪酮、对甲氧基肉桂酸异戊酯、苯基二苯并咪唑四磺酸酯二钠，及4-甲基亚苄亚基樟脑中的至少一种。所述无机紫外线阻挡剂可以选自二氧化钛、氧化锌，及氧化锆中的至少一种。
所述化妆品组合物可以是由于两个以上的种非混合成分而不是单一相乳液(emulsion)而使成分组成层的层相化妆品组合物。所述层相化妆品组合物包括并分离水相层；以及与所述水相层分离的一个以上的油相层，优选地，所述层相化妆品组合物可以分离成两层或三层。此时，所述水相层和油相层可以根据化妆品组合物的组成来改变层的顺序。
所述油相层可以包括油、与油相层混合的成分，或所述有机紫外线阻挡剂，且所述油和与油相层混合的成分可以包括所有于化妆品组合物中包括的有用的成分。根据层相结构，所述油相层可以是酯类油，如二聚季戊四醇六C5-9酸酯类、C12-15醇乙基己酸酯、乳酸肉荳蔻酯、鲸蜡醇乙基己酸酯、新戊二醇二癸酸酯、辛酸十六烷基酯、豆蔻酸异丙酯、辛基十二醇肉豆蔻酸酯、月桂酸己酯、二-C12-13烷醇苹果酸酯、辛基十二醇硬脂酰氧基硬脂酸酯、二异硬脂醇苹果酸酯、季戊四醇四(乙基己酸)酯、双甘油三异硬脂酸酯等；植物油，如橄榄油、葡萄籽油、澳洲坚果油、荷荷芭油、蓖麻油、葵花籽油、薰衣草油等；硅油，如环戊硅氧烷、环己硅氧烷、环庚硅氧烷、环甲硅脂、环苯基聚甲基硅氧烷、环四聚二甲基硅氧烷、环三硅氧烷、聚二甲基硅氧烷、聚二甲基矽氧烷醇、苯基聚甲基硅氧烷、三氟丙基聚甲基硅氧烷、甲基聚三甲基硅氧烷、苯基三甲基聚矽氧烷，或其中两种或更多种的混合物。当使用与酯类油或植物油具有良好相容性的硅油时，所述硅油可以具有包括水相层的两层相结构，当使用聚二甲基硅氧烷、聚二甲基矽氧烷醇等时，可以设计成具有不同的比重来包括水相层以具有三层相结构。另外，作为除了所述油以外的在油相层混合的成分，可以包括雪松醇、生育酚，或视网醇等，且可以包括但不限于包括在化妆品组合物中的有用的成分。此时，可以在不妨碍根据本发明的层相化妆品组合物的多层形成的程度包括混合在所述油相层的成分。
基于所述化妆品组合物的总重量，所述油的含量可以为1.0重量至50重量％，具体地，可以为10重量％至50重量％，更具体地，可以为20重量％至50重量％，再更具体地，可以为30重量％至50重量％。在一实施例中，确认了所述化妆品组合物即使含有高浓度的油也稳定地保持剂型。
所述化妆品组合物可以是包括表面活性剂的单一相组合物。所述表面活性剂可以选自阴离子表面活性剂、阳离子表面活性剂、非离子表面活性剂、两性离子表面活性剂或其组合中的至少一种。基于所述气溶胶原液的总重量，所述表面活性剂的含量可以为0.1重量％至2.0重量％，具体地，可以为0.1重量％至0.8重量％，更具体地，可以为0.1重量％至0.7重量％，再更具体地，可以为0.1重量％至0.5重量％。
所述化妆品组合物可以包括着色剂。所述着色剂可以通过被涂布在皮肤或存在于皮肤上的毛发来产生所需的颜色，只要是不妨碍所述化妆品组合物的所需效果，所述着色剂可以不受限制地被包括在所述化妆品组合物中。所述着色剂可以选自白色着色剂、有色着色剂或其组合。基于所述化妆品组合物的总重量，所述着色剂的含量可以为1.0重量％至15重量％，具体地可以为1.0重量％至10重量％，更具体地可以为1.0重量％至8.0重量％，再更具体地可以为1.0重量％至6.0重量％。
所述化妆品组合物可以以保湿和溶剂目的包括多元醇或其衍生物。所述多元醇是在一个分子中具有多个羥基的醇，并且只要其在本领域中被称为保湿剂即可无限制地包括在内。具体而言，所述多元醇可以选自甘油、双甘油、1,2-己二醇、1,3-丁二醇、1,4-丁二醇、1,5-戊二醇、山梨糖醇、甘露醇、阿糖醇、木糖醇、丁二醇、丙二醇、乙二醇、四亚甲基二醇、二甘醇、二丙二醇、己烯乙二醇、戊二醇、季戊四醇、聚乙二醇、三羟甲基丙烷，及丙二醇中的至少一种。
所述化妆品组合物根据需要可以进一步添加诸如分散剂、体质颜料、着色剂、抗氧化剂、防腐剂、pH调节剂、保湿剂，和润滑剂等的成分。另外，所述用于阻挡紫外线的化妆品组合物还包括能够向皮肤提供补充必需营养素的物质，且可以优选地包括天然香，化妆品香，或植物提取物，但可以含有不限于此的助剂。
附图说明
图1是示出在喷射气溶胶剂型后的模样的示意图。
图2是示出在涂布组合物之前和之后的皮肤的热红外线照片的示意图。
图3是示出根据组合物的用途的皮肤表面温度变化的示意图。
具体实施方式
将通过以下实施例更详细地描述。然而，这些实施例仅用于说明事例，本发明的范围不限于这些实施例。
实施例1至4.气溶胶原液的制备
为了制备含有羟乙基纤维素和紫外线阻挡剂的气溶胶原液，制备了包括以下表1的成分且由以下表2所示的含量比组成的气溶胶原液即实施例1至4，及比较例1至2。
【表1】
具体而言，在烧杯中称量纯净水中的其他添加剂、多元醇和羟乙基纤维素，并使用乳化混合器在约75℃的温度下以3000rpm将混合物均匀混合。另外，在烧杯中称量紫外线阻挡剂并在约75℃的温度下将其融化后，将其在所述烧杯中混合，并以3000rpm均匀混合10分钟。此后，混合其他添加剂，然后冷却并除去气泡。
结果，气溶胶原液被制备成包括纯净水、多元醇、羟乙基纤维素，及油相，且所述油相包括油、混合在油相层中的成分或有机紫外线阻挡剂。另外，制备实施例4的气溶胶原液以进一步包括无机紫外线阻挡剂。
具体地，制备了包括以下表2的成分的实施例1至4，和比较例1至2的气溶胶原液。
【表2】
实施例5至10.制备气溶胶剂型的化妆品组合物
为了制备气溶胶剂型的用于阻挡紫外线的化妆品组合物，使用实施例1至4，和比较例1至2的气溶胶原液并制造二层相液体后，将其以适当的比例填充到耐压容器中来制备气溶胶化妆品组合物。
具体地，根据以下表3所示的气溶胶原液的含量、气溶胶喷射剂的种类和含量，制备了实施例5至10，和比较例3至6的化妆品组合物。
【表3】
试验例1.评估化妆品组合物的剂型形成、冷却效果，和使用感
对所述实施例5至10，和比较例3至6的化妆品组合物进行肉眼评估和使用感评估。
具体地，通过肉眼评估确认了气溶胶剂型的形成。通过公司内部效能评估根据涂布后随时间测量皮肤温度来评估冷却效果。使用感评估通过以九名年龄在25至35岁之间的评委作为对象对使用感以十分制为准评估了新颖性。
所述结果显示在以下表4中，且以肉眼观察所述制备的剂型在喷射后的模样的结果示于图1。
【表4】
如所述表4所示，气溶胶喷射剂含量小于10重量％的比较例3的组合物未形成气溶胶剂型，且气溶胶喷射剂含量大于70重量％的比较例4的组合物飞散得太严重并且使用感差。另外，不包括羟乙基纤维素的比较例5的组合物尽管含有适量的气溶胶喷射剂，但仍未形成气溶胶剂型。另外，包括过多的羟乙基纤维素的比较例6的组合物也未形成气溶胶剂型。
另外，确认了尽管实施例7的组合物包括与比较例5的组合物相同的含量比的气溶胶喷射剂，但是通过在气溶胶原液中包括羟乙基纤维素来形成气溶胶剂型，且显示出赋予冷却效果和使用感的新颖性的高效果。
换言之，确认了即使在气溶胶原液中包括油相，具体地高含量的油，通过包括羟乙基纤维素能够形成气溶胶剂型，且能够赋予冷却效果和改善的使用感。
另外，如图1所示，确认了所述实施例5至10的形成了气溶胶剂型的化妆品组合物在喷射时以泥浆状喷射。
试验例2.评估化妆品组合物的功能
对所述实施例5至10，和比较例3的气溶胶剂型的的化妆品组合物进行功能评估。具体而言，功能评估通过以九名年龄在25至35岁之间的评委作为对象对新的使用感以十分制为准来进行。
所述结果示于以下表5。
【表5】
如所述表5所示，虽然存在稍微的个人差异，大部分评估者评估了在利用实施例1至4的气溶胶原料制备的实施例5-至10的化妆品组合物中感觉到改善的使用感。特别地，高度评估了含有40重量％至60重量％的气溶胶喷射剂的实施例7至10的化妆品组合物的功能评估分数。相反，在即使利用了实施例2的气溶胶原料但含有5重量％的气溶胶喷射剂的实施例3的情况下，评估了未形成期望的气溶胶剂型且没有改善的使用感。
试验例3.根据涂布化妆品组合物确认皮肤表面温度降低的效果
通过在皮肤涂布所述实施例7的组合物来确认皮肤表面温度降低的效果。具体地，对5位评委作为对象于手臂上指定涂布区域和未涂布区域。分别拍摄了涂布所述组合物之前及涂布之后的热红外线照片并进行比较。在所述热红外线照中观察到紫色、红色，和黑色区域，并且意味着距离紫色越近，温度越低。
结果，如图2所示，虽然在涂布所述组合物之前在肉眼上没有观察到涂布区域和未涂布区域之间的差异，但是在涂布所述组合物之后在肉眼上也确认到涂布区域中出现了显着皮肤表面温度降低的效果。
另外，测量了在涂布所述组合物之前和之后的平均皮肤表面温度。涂布所述组合物之前的平均皮肤表面温度为26.3℃，且基于此确认了表面温度的下降率。
结果，如图3所示，在不涂布所述组合物时，皮肤表面温度的变化率微小，相反，由于周围环境，皮肤表面温度升高。相反，确认了在涂布所述组合物时，平均皮肤表面温度从26.3℃降低到24.0℃，且皮肤表面温度下降率为约8.7％。
根据上述结果，确认了与仅通过气溶胶剂型的气体产生的冷却效果相比，所述用于阻挡紫外线的化妆品组合物通过包括羟乙基纤维素能够赋予改善的冷却效果。
另外，在气溶胶喷射剂的情况下，少于10重量％不能形成期望的剂型，并且当超过70重量％时，喷射压太强引起冻伤的忧虑和内容物飞散，导致使用感差，因此，确认了当含有气溶胶喷射剂10重量％至70重量％时，可赋予改善的冷却效果和使用感。
气溶胶剂型的用于阻挡紫外线的化妆品组合物通过利用低沸点的喷射剂和羟乙基纤维素来在喷射时赋予冷却效果和新的使用感。
Claims (7)
1.一种用于阻挡紫外线的化妆品组合物，包括：
气溶胶原液，其包括羟乙基纤维素(Hydroxyethyl-cellulose)及紫外线阻挡剂；以及
气溶胶喷射剂。
2.根据权利要求1所述的用于阻挡紫外线的化妆品组合物，其中，
基于组合物总重量，所述组合物包括10重量％至70重量％的所述气溶胶喷射剂。
3.根据权利要求1所述的用于阻挡紫外线的化妆品组合物，其中，
基于原液总重量，所述气溶胶原液包括0.1重量％至1.8重量％的所述羟乙基纤维素。
4.根据权利要求1所述的用于阻挡紫外线的化妆品组合物，其中，
所述气溶胶喷射剂选自氮、液化石油氣(LPG)、液化天然气(LNG)、二甲醚(DME)及四氟丙烯-1234ZE(HFO-1234ZE)中的至少一种。
5.根据权利要求1所述的用于阻挡紫外线的化妆品组合物，其中，
所述紫外线阻挡剂选自胡莫柳酯、水杨酸乙基己酯、苯基苯并咪唑磺酸、奥克立林、甲氧基肉桂酸辛酯、丁基甲氧基二苯甲酰甲烷、双-乙基己氧苯酚甲氧苯基三嗪、乙基氨基羟基苯甲酰苯甲酸己酯、乙基己基三嗪酮、对甲氧基肉桂酸异戊酯、苯基二苯并咪唑四磺酸酯二钠及4-甲基亚苄亚基樟脑中的至少一种。
6.根据权利要求1所述的用于阻挡紫外线的化妆品组合物，其中，
所述组合物包括：水相层，其包括所述气溶胶原液及所述气溶胶喷射剂；以及与所述水相层分离的油相层；
其中，基于组合物总重量，所述油相层包括1.0重量％至50重量％的油。
7.根据权利要求1所述的用于阻挡紫外线的化妆品组合物，其中，
所述组合物在喷射时以泥浆状喷射。
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| KR102174526B1 (ko) | 2020-11-05 |
| KR20200092705A (ko) | 2020-08-04 |
| US20200237627A1 (en) | 2020-07-30 |
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