CN111334135A - Anti-cracking quick-drying type stone-like paint and preparation method thereof - Google Patents
Anti-cracking quick-drying type stone-like paint and preparation method thereof Download PDFInfo
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- CN111334135A CN111334135A CN201811547179.7A CN201811547179A CN111334135A CN 111334135 A CN111334135 A CN 111334135A CN 201811547179 A CN201811547179 A CN 201811547179A CN 111334135 A CN111334135 A CN 111334135A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D125/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
- C09D125/02—Homopolymers or copolymers of hydrocarbons
- C09D125/04—Homopolymers or copolymers of styrene
- C09D125/08—Copolymers of styrene
- C09D125/14—Copolymers of styrene with unsaturated esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention provides an anti-cracking quick-drying type real stone paint and a preparation method thereof, wherein the anti-cracking quick-drying type real stone paint is prepared from the following components in parts by weight: 180 parts of styrene-acrylic emulsion 140, 12-16 parts of ethylene glycol, 2-4 parts of stabilizer, 11-17 parts of cellulose, 1-3 parts of defoaming agent, 4-8 parts of dispersant, 2.4-3.6 parts of film-forming assistant, 18-26 parts of deionized water, 26-32 parts of nano silicon dioxide, 500 parts of natural colored sand 400, 7-11 parts of preservative and 1-5 parts of ammonia water. The anti-cracking quick-drying type really stone paint prepared by the invention has the advantages of good construction performance, short drying time, good water resistance and high application value.
Description
Technical Field
The invention relates to the technical field of real stone paint production, in particular to anti-cracking quick-drying real stone paint and a preparation method thereof.
Background
The house building decorated by the stone paint has natural, real and beautiful color, gives people elegant, harmonious and solemn aesthetic feeling, and is suitable for indoor and outdoor decoration of various buildings. The stone paint decoration is carried out on the surface building, and a vivid and natural effect can be built. The stone-like paint has good protective performance, can play roles of fire prevention, water prevention, acid and alkali resistance, pollution resistance, fastness and the like, can effectively prolong the service life of buildings, and has fewer types and poor performance in the market, so that the stone-like paint with better performance needs to be developed.
Disclosure of Invention
The technical problem to be solved is as follows: the invention aims to solve the defects in the prior art and provides an anti-cracking quick-drying type real stone paint and a preparation method thereof.
The technical scheme is as follows:
the invention provides an anti-cracking quick-drying type real stone paint which is prepared from the following components in parts by weight:
180 parts of styrene-acrylic emulsion 140, 12-16 parts of ethylene glycol, 2-4 parts of stabilizer, 11-17 parts of cellulose, 1-3 parts of defoaming agent, 4-8 parts of dispersant, 2.4-3.6 parts of film-forming assistant, 18-26 parts of deionized water, 26-32 parts of nano silicon dioxide, 500 parts of natural colored sand 400, 7-11 parts of preservative and 1-5 parts of ammonia water.
Preferably, the defoaming agent is formed by mixing sulfonated fatty acid, isopropanol and tributyl phosphate according to the weight ratio of 5:1: 2.
Preferably, the film-forming aid is formed by mixing propylene glycol phenyl ether and ethylene glycol butyl ether according to the weight ratio of 1: 2.
Preferably, the stabilizer is formed by mixing gum arabic, polyvinylpyrrolidone and cottonseed alcohol resin according to a weight ratio of 3:5: 1.
The invention also provides a preparation method of the anti-cracking quick-drying type real stone paint, which comprises the following steps:
step one, according to the weight portion, 18-26 portions of deionized water, 180 portions of styrene-acrylic emulsion 140 and 12-16 portions of ethylene glycol are put into a stirrer and stirred for 20-40min at the rotating speed of 100 and 200 r/min;
step two, continuously adding 11-17 parts of cellulose, 1-3 parts of defoaming agent, 4-8 parts of dispersing agent, 2.4-3.6 parts of film-forming additive, 2-4 parts of stabilizing agent, 26-32 parts of nano silicon dioxide and 1-5 parts of ammonia water, increasing the rotating speed to 300-400r/min, and stirring for 10-20 min;
and step three, adding 500 parts of natural color sand 400-.
Preferably, the rotation speed in the first step is 120-.
Preferably, the rotation speed in the second step is 340-.
Preferably, the rotation speed in the second step is 500-.
Has the advantages that: the anti-cracking quick-drying type really stone paint prepared by the invention has the advantages of good construction performance, short drying time, good water resistance and high application value. The anti-cracking quick-drying type stone-like paint prepared by the method has no difficulty in spraying and is convenient to construct, drying can be realized within 48-35h, the drying time of the stone-like paint is greatly shortened, the difficulty degree in the construction process is reduced, and the coating does not have the phenomena of bulging, cracking and peeling after being soaked in water for 96 h.
Detailed Description
Example 1
The preparation method of the anti-cracking quick-drying type real stone paint in the embodiment comprises the following steps:
step one, adding 26 parts by weight of deionized water, 140 parts by weight of styrene-acrylic emulsion and 16 parts by weight of ethylene glycol into a stirrer, and stirring for 40min at a speed of 100 r/min;
step two, continuously adding 11 parts of cellulose, 3 parts of defoaming agent, 4 parts of dispersing agent, 3.6 parts of film-forming additive, 2 parts of stabilizing agent, 32 parts of nano silicon dioxide and 1 part of ammonia water, increasing the rotating speed to 400r/min, and stirring for 10 min;
and step three, adding 500 parts of natural colored sand and 7 parts of preservative, and stirring at the rotating speed of 650r/min for 35min to obtain the anti-cracking quick-drying type real stone paint.
The defoaming agent is formed by mixing sulfonated fatty acid, isopropanol and tributyl phosphate according to the weight ratio of 5:1: 2.
The film-forming additive is formed by mixing propylene glycol phenyl ether and ethylene glycol butyl ether according to the weight ratio of 1: 2.
The stabilizer is prepared by mixing Arabic gum, polyvinylpyrrolidone and cottonseed alcohol resin according to the weight ratio of 3:5: 1.
Example 2
The preparation method of the anti-cracking quick-drying type real stone paint in the embodiment comprises the following steps:
step one, according to the parts by weight, 18 parts of deionized water, 180 parts of styrene-acrylic emulsion and 12 parts of ethylene glycol are put into a stirrer and stirred for 20min at a speed of 200 r/min;
secondly, continuing to add 17 parts of cellulose, 1 part of defoaming agent, 8 parts of dispersing agent, 2.4 parts of film-forming additive, 4 parts of stabilizing agent, 26 parts of nano silicon dioxide and 5 parts of ammonia water, increasing the rotating speed to 300r/min, and stirring for 20min;
and step three, adding 400 parts of natural colored sand and 11 parts of preservative, and stirring at the rotating speed of 450r/min for 45min to obtain the anti-crack quick-drying type real stone paint.
The defoaming agent is formed by mixing sulfonated fatty acid, isopropanol and tributyl phosphate according to the weight ratio of 5:1: 2.
The film-forming additive is formed by mixing propylene glycol phenyl ether and ethylene glycol butyl ether according to the weight ratio of 1: 2.
The stabilizer is prepared by mixing Arabic gum, polyvinylpyrrolidone and cottonseed alcohol resin according to the weight ratio of 3:5: 1.
Example 3
The preparation method of the anti-cracking quick-drying type real stone paint in the embodiment comprises the following steps:
step one, adding 24 parts by weight of deionized water, 150 parts by weight of styrene-acrylic emulsion and 15 parts by weight of ethylene glycol into a stirrer, and stirring for 35min at a speed of 120 r/min;
continuously adding 12 parts of cellulose, 2.5 parts of defoaming agent, 5 parts of dispersing agent, 3.4 parts of film-forming additive, 2.5 parts of stabilizing agent, 30 parts of nano silicon dioxide and 2 parts of ammonia water, increasing the rotating speed to 360r/min, and stirring for 12 min;
and step three, adding 460 parts of natural colored sand and 8 parts of preservative, and stirring at the rotating speed of 600r/min for 38min to obtain the anti-crack quick-drying type real stone paint.
The defoaming agent is formed by mixing sulfonated fatty acid, isopropanol and tributyl phosphate according to the weight ratio of 5:1: 2.
The film-forming additive is formed by mixing propylene glycol phenyl ether and ethylene glycol butyl ether according to the weight ratio of 1: 2.
The stabilizer is prepared by mixing Arabic gum, polyvinylpyrrolidone and cottonseed alcohol resin according to the weight ratio of 3:5: 1.
Example 4
The preparation method of the anti-cracking quick-drying type real stone paint in the embodiment comprises the following steps:
step one, 20 parts of deionized water, 170 parts of styrene-acrylic emulsion and 13 parts of ethylene glycol are added into a stirrer according to parts by weight, and stirred for 25min at a speed of 180 r/min;
step two, continuing to add 16 parts of cellulose, 1.5 parts of defoaming agent, 7 parts of dispersing agent, 2.6 parts of film-forming additive, 3.5 parts of stabilizing agent, 28 parts of nano silicon dioxide and 4 parts of ammonia water, increasing the rotating speed to 340r/min, and stirring for 18 min;
and step three, adding 420 parts of natural colored sand and 10 parts of preservative, and stirring at the rotating speed of 500r/min for 42min to obtain the anti-crack quick-drying type real stone paint.
The defoaming agent is formed by mixing sulfonated fatty acid, isopropanol and tributyl phosphate according to the weight ratio of 5:1: 2.
The film-forming additive is formed by mixing propylene glycol phenyl ether and ethylene glycol butyl ether according to the weight ratio of 1: 2.
The stabilizer is prepared by mixing Arabic gum, polyvinylpyrrolidone and cottonseed alcohol resin according to the weight ratio of 3:5:1
Example 5
The preparation method of the anti-cracking quick-drying type real stone paint in the embodiment comprises the following steps:
step one, adding 22 parts by weight of deionized water, 160 parts by weight of styrene-acrylic emulsion and 14 parts by weight of ethylene glycol into a stirrer, and stirring for 30min at a speed of 150 r/min;
step two, continuously adding 14 parts of cellulose, 2 parts of defoaming agent, 6 parts of dispersing agent, 3 parts of film-forming additive, 3 parts of stabilizing agent, 29 parts of nano silicon dioxide and 3 parts of ammonia water, increasing the rotating speed to 350r/min, and stirring for 16 min;
and step three, adding 440 parts of natural colored sand and 9 parts of preservative, and stirring at the rotating speed of 550r/min for 40min to obtain the anti-cracking quick-drying type real stone paint.
The defoaming agent is formed by mixing sulfonated fatty acid, isopropanol and tributyl phosphate according to the weight ratio of 5:1: 2.
The film-forming additive is formed by mixing propylene glycol phenyl ether and ethylene glycol butyl ether according to the weight ratio of 1: 2.
The stabilizer is prepared by mixing Arabic gum, polyvinylpyrrolidone and cottonseed alcohol resin according to the weight ratio of 3:5: 1.
Comparative example 1
This comparative example differs from example 1 in the film-forming aid. Specifically, the method comprises the following steps:
step one, adding 26 parts by weight of deionized water, 140 parts by weight of styrene-acrylic emulsion and 16 parts by weight of ethylene glycol into a stirrer, and stirring for 40min at a speed of 100 r/min;
step two, continuously adding 11 parts of cellulose, 3 parts of defoaming agent, 4 parts of dispersing agent, 3.6 parts of film-forming additive, 2 parts of stabilizing agent, 32 parts of nano silicon dioxide and 1 part of ammonia water, increasing the rotating speed to 400r/min, and stirring for 10 min;
and step three, adding 500 parts of natural colored sand and 7 parts of preservative, and stirring at the rotating speed of 650r/min for 35min to obtain the anti-cracking quick-drying type real stone paint.
The defoaming agent is formed by mixing sulfonated fatty acid, isopropanol and tributyl phosphate according to the weight ratio of 5:1: 2.
The film-forming additive is formed by mixing propylene glycol phenyl ether and ethylene glycol butyl ether according to the weight ratio of 1.2: 1.6.
The stabilizer is prepared by mixing Arabic gum, polyvinylpyrrolidone and cottonseed alcohol resin according to the weight ratio of 3:5: 1.
Comparative example 2
This comparative example differs from example 1 in the stabilizer. Specifically, the method comprises the following steps:
step one, adding 26 parts by weight of deionized water, 140 parts by weight of styrene-acrylic emulsion and 16 parts by weight of ethylene glycol into a stirrer, and stirring for 40min at a speed of 100 r/min;
step two, continuously adding 11 parts of cellulose, 3 parts of defoaming agent, 4 parts of dispersing agent, 3.6 parts of film-forming additive, 2 parts of stabilizing agent, 32 parts of nano silicon dioxide and 1 part of ammonia water, increasing the rotating speed to 400r/min, and stirring for 10 min;
and step three, adding 500 parts of natural colored sand and 7 parts of preservative, and stirring at the rotating speed of 650r/min for 35min to obtain the anti-cracking quick-drying type real stone paint.
The defoaming agent is formed by mixing sulfonated fatty acid, isopropanol and tributyl phosphate according to the weight ratio of 5:1: 2.
The film-forming additive is formed by mixing propylene glycol phenyl ether and ethylene glycol butyl ether according to the weight ratio of 1: 2.
The stabilizer is prepared by mixing Arabic gum, polyvinylpyrrolidone and cottonseed alcohol resin according to the weight ratio of 4:3: 1.
The crack-resistant quick-drying type real stone paint prepared in examples 1-5 and comparative examples 1-2 was subjected to a performance test:
| workability | Drying time (surface dry)/min | Water resistance (96 h) | |
| Example 1 | No difficulty in spraying and convenient construction | 48 | The coating does not bulge, crack or peel off |
| Example 2 | No difficulty in spraying and convenient construction | 45 | The coating does not bulge, crack or peel off |
| Example 3 | No difficulty in spraying and convenient construction | 40 | The coating does not bulge, crack or peel off |
| Example 4 | No difficulty in spraying and convenient construction | 39 | The coating does not bulge, crack or peel off |
| Example 5 | No difficulty in spraying and convenient construction | 35 | The coating does not bulge, crack or peel off |
| Comparative example 1 | No difficulty in spraying and convenient construction | 55 | The coating does not bulge, crack or peel off |
| Comparative example 2 | No difficulty in spraying and convenient construction | 48 | The coating has slight fine cracks |
According to the test results, the anti-cracking quick-drying type real stone paint prepared by the invention has the advantages of good construction performance, short drying time, good water resistance and high application value. The anti-cracking quick-drying type stone-like paint prepared by the method has no difficulty in spraying and is convenient to construct, drying can be realized within 48-35h, the drying time of the stone-like paint is greatly shortened, the difficulty degree in the construction process is reduced, and the coating does not have the phenomena of bulging, cracking and peeling after being soaked in water for 96 h.
Claims (8)
1. The anti-cracking quick-drying type real stone paint is characterized by being prepared from the following components in parts by weight:
180 parts of styrene-acrylic emulsion 140, 12-16 parts of ethylene glycol, 2-4 parts of stabilizer, 11-17 parts of cellulose, 1-3 parts of defoaming agent, 4-8 parts of dispersant, 2.4-3.6 parts of film-forming assistant, 18-26 parts of deionized water, 26-32 parts of nano silicon dioxide, 500 parts of natural colored sand 400, 7-11 parts of preservative and 1-5 parts of ammonia water.
2. The anti-cracking quick-drying type real stone paint as claimed in claim 1, wherein the defoaming agent is prepared by mixing sulfonated fatty acid, isopropanol and tributyl phosphate according to a weight ratio of 5:1: 2.
3. The anti-cracking quick-drying type real stone paint as claimed in claim 1, wherein the film forming aid is a mixture of propylene glycol phenyl ether and butyl cellosolve in a weight ratio of 1: 2.
4. The anti-cracking quick-drying type really stone paint as claimed in claim 1, wherein the stabilizer is a mixture of gum arabic, polyvinylpyrrolidone and cottonseed alcohol resin in a weight ratio of 3:5: 1.
5. The preparation method of the anti-cracking quick-drying type real stone paint is characterized by comprising the following steps of:
step one, according to the weight portion, 18-26 portions of deionized water, 180 portions of styrene-acrylic emulsion 140 and 12-16 portions of ethylene glycol are put into a stirrer and stirred for 20-40min at the rotating speed of 100 and 200 r/min;
step two, continuously adding 11-17 parts of cellulose, 1-3 parts of defoaming agent, 4-8 parts of dispersing agent, 2.4-3.6 parts of film-forming additive, 2-4 parts of stabilizing agent, 26-32 parts of nano silicon dioxide and 1-5 parts of ammonia water, increasing the rotating speed to 300-400r/min, and stirring for 10-20 min;
and step three, adding 500 parts of natural color sand 400-.
6. The method for preparing anti-cracking quick-drying type stone-like paint as claimed in claim 5, wherein the rotation speed in the first step is 120-.
7. The method for preparing anti-cracking quick-drying type stone-like paint as claimed in claim 5, wherein the rotation speed in step two is 340-.
8. The method for preparing anti-cracking quick-drying type stone-like paint as claimed in claim 5, wherein the rotation speed in step two is 500-.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811547179.7A CN111334135A (en) | 2018-12-18 | 2018-12-18 | Anti-cracking quick-drying type stone-like paint and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811547179.7A CN111334135A (en) | 2018-12-18 | 2018-12-18 | Anti-cracking quick-drying type stone-like paint and preparation method thereof |
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| CN111334135A true CN111334135A (en) | 2020-06-26 |
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| CN201811547179.7A Pending CN111334135A (en) | 2018-12-18 | 2018-12-18 | Anti-cracking quick-drying type stone-like paint and preparation method thereof |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103937355A (en) * | 2014-05-14 | 2014-07-23 | 重庆万彩世界涂料有限公司 | Base paint of waterborne stone-like coating and preparation method thereof |
| US20150191612A1 (en) * | 2012-07-27 | 2015-07-09 | Koninklijke Coöperative Cosun U.A. | Anti-cracking agent for water-borne acrylic paint and coating compositions |
| CN104789074A (en) * | 2015-05-06 | 2015-07-22 | 武汉德美涂料股份有限公司 | Novel natural stone paint and preparation method thereof |
| CN106189618A (en) * | 2016-07-20 | 2016-12-07 | 芜湖昊轩环保新材料有限公司 | Ground non-skid coating and preparation method thereof |
-
2018
- 2018-12-18 CN CN201811547179.7A patent/CN111334135A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20150191612A1 (en) * | 2012-07-27 | 2015-07-09 | Koninklijke Coöperative Cosun U.A. | Anti-cracking agent for water-borne acrylic paint and coating compositions |
| CN103937355A (en) * | 2014-05-14 | 2014-07-23 | 重庆万彩世界涂料有限公司 | Base paint of waterborne stone-like coating and preparation method thereof |
| CN104789074A (en) * | 2015-05-06 | 2015-07-22 | 武汉德美涂料股份有限公司 | Novel natural stone paint and preparation method thereof |
| CN106189618A (en) * | 2016-07-20 | 2016-12-07 | 芜湖昊轩环保新材料有限公司 | Ground non-skid coating and preparation method thereof |
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