CN111032616B - 将环状亚烷基脲转化为其相应亚烷基胺的多步法 - Google Patents

将环状亚烷基脲转化为其相应亚烷基胺的多步法 Download PDF

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Publication number
CN111032616B
CN111032616B CN201880050928.7A CN201880050928A CN111032616B CN 111032616 B CN111032616 B CN 111032616B CN 201880050928 A CN201880050928 A CN 201880050928A CN 111032616 B CN111032616 B CN 111032616B
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amine
removal step
alkylene
urea
temperature
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Chinese (zh)
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CN111032616A (zh
Inventor
A·J·B·坦恩凯特
M·J·T·拉吉马克斯
K·F·莱克
E·N·坎茨尔
S·约维奇
R·K·埃德温松
I·埃勒斯
H·范达
R·维尼曼
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Norion Chemicals International Ltd
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Norion Chemicals International Ltd
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/62—Preparation of compounds containing amino groups bound to a carbon skeleton by cleaving carbon-to-nitrogen, sulfur-to-nitrogen, or phosphorus-to-nitrogen bonds, e.g. hydrolysis of amides, N-dealkylation of amines or quaternary ammonium compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1456—Removing acid components
    • B01D53/1475—Removing carbon dioxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1493—Selection of liquid materials for use as absorbents
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/82—Purification; Separation; Stabilisation; Use of additives
    • C07C209/86—Separation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C211/00—Compounds containing amino groups bound to a carbon skeleton
    • C07C211/01—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms
    • C07C211/02—Compounds containing amino groups bound to a carbon skeleton having amino groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C07C211/14—Amines containing amino groups bound to at least two aminoalkyl groups, e.g. diethylenetriamines
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
    • B01D2252/20—Organic absorbents
    • B01D2252/202—Alcohols or their derivatives
    • B01D2252/2021—Methanol
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2252/00—Absorbents, i.e. solvents and liquid materials for gas absorption
    • B01D2252/20—Organic absorbents
    • B01D2252/204—Amines
    • B01D2252/20436—Cyclic amines
    • B01D2252/20447—Cyclic amines containing a piperazine-ring
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/50—Carbon oxides
    • B01D2257/504—Carbon dioxide
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/10—Process efficiency

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201880050928.7A 2017-08-11 2018-08-07 将环状亚烷基脲转化为其相应亚烷基胺的多步法 Active CN111032616B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP17185945 2017-08-11
EP17185945.7 2017-08-11
PCT/EP2018/071319 WO2019030190A1 (en) 2017-08-11 2018-08-07 MULTI-STEP PROCESS FOR CONVERTING CYCLIC ALKYLENE UREA TO THEIR CORRESPONDING ALKYLENE AMINES

Publications (2)

Publication Number Publication Date
CN111032616A CN111032616A (zh) 2020-04-17
CN111032616B true CN111032616B (zh) 2024-01-19

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CN201880050928.7A Active CN111032616B (zh) 2017-08-11 2018-08-07 将环状亚烷基脲转化为其相应亚烷基胺的多步法

Country Status (10)

Country Link
US (1) US11236039B2 (enExample)
EP (1) EP3665153A1 (enExample)
JP (2) JP2020530455A (enExample)
KR (1) KR20200036011A (enExample)
CN (1) CN111032616B (enExample)
BR (1) BR112020002389B1 (enExample)
CA (1) CA3071903A1 (enExample)
MX (1) MX2020001449A (enExample)
TW (1) TWI761570B (enExample)
WO (1) WO2019030190A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110072838B (zh) * 2016-12-15 2022-04-15 阿克苏诺贝尔化学品国际有限公司 制备亚乙基胺的方法
CN110072841B (zh) 2016-12-15 2022-04-19 阿克苏诺贝尔化学品国际有限公司 制备羟乙基亚乙基胺的方法
CN110959004B (zh) * 2017-07-10 2023-09-12 诺力昂化学品国际有限公司 制备亚乙基胺和亚乙基胺衍生物的方法
CN111032615B (zh) * 2017-08-11 2023-08-18 诺力昂化学品国际有限公司 将环状亚烷基脲转化为其相应亚烷基胺的两步法
EP3665152A1 (en) * 2017-08-11 2020-06-17 Nouryon Chemicals International B.V. Process for converting cyclic alkylene ureas into their corresponding alkylene amines
CN110997640B (zh) * 2017-08-11 2023-07-28 诺力昂化学品国际有限公司 将亚乙基胺化合物的环状单脲转化为亚乙基胺化合物的方法
JP7723608B2 (ja) * 2020-01-28 2025-08-14 東ソー株式会社 二酸化炭素分離用組成物、及び二酸化炭素の分離方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2812333A (en) * 1954-09-27 1957-11-05 Union Carbide Corp Process for the preparation of 1-(2-hydroxyethyl) imidazolidine-2
US4387249A (en) * 1981-12-18 1983-06-07 The Dow Chemical Company Process for the manufacture of diethylenetriamine
JP2007527895A (ja) * 2004-03-09 2007-10-04 デグサ ゲーエムベーハー 水での加水分解によりカルボジイミド基を有する化合物からアミンを製造する方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4503250A (en) * 1981-09-30 1985-03-05 Union Carbide Corporation Preparation of polyalkylene polyamines
SE513250C2 (sv) 1997-11-11 2000-08-07 Akzo Nobel Nv Amineringsförfarande för framställning av polyaminer
US9278905B2 (en) * 2012-03-02 2016-03-08 Kyushu University, National University Corporation Production method for compound comprising amino group and/or hydroxyl group
WO2017137529A1 (en) * 2016-02-12 2017-08-17 Akzo Nobel Chemicals International B.V. Process to convert cyclic alkylene ureas into their corresponding alkylene amines
CN110997640B (zh) * 2017-08-11 2023-07-28 诺力昂化学品国际有限公司 将亚乙基胺化合物的环状单脲转化为亚乙基胺化合物的方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2812333A (en) * 1954-09-27 1957-11-05 Union Carbide Corp Process for the preparation of 1-(2-hydroxyethyl) imidazolidine-2
US4387249A (en) * 1981-12-18 1983-06-07 The Dow Chemical Company Process for the manufacture of diethylenetriamine
JP2007527895A (ja) * 2004-03-09 2007-10-04 デグサ ゲーエムベーハー 水での加水分解によりカルボジイミド基を有する化合物からアミンを製造する方法

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TW201920065A (zh) 2019-06-01
TWI761570B (zh) 2022-04-21
JP2020530455A (ja) 2020-10-22
JP2023017864A (ja) 2023-02-07
MX2020001449A (es) 2020-03-20
KR20200036011A (ko) 2020-04-06
US20200165187A1 (en) 2020-05-28
WO2019030190A1 (en) 2019-02-14
RU2020109528A3 (enExample) 2021-09-14
RU2020109528A (ru) 2021-09-14
BR112020002389A2 (pt) 2020-09-01
US11236039B2 (en) 2022-02-01
EP3665153A1 (en) 2020-06-17
CA3071903A1 (en) 2019-02-14
BR112020002389B1 (pt) 2023-03-21
CN111032616A (zh) 2020-04-17

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