CN110914195B - 分子筛ssz-112、其合成及应用 - Google Patents

分子筛ssz-112、其合成及应用 Download PDF

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CN110914195B
CN110914195B CN201880047072.8A CN201880047072A CN110914195B CN 110914195 B CN110914195 B CN 110914195B CN 201880047072 A CN201880047072 A CN 201880047072A CN 110914195 B CN110914195 B CN 110914195B
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molecular sieve
source
aluminosilicate molecular
reaction mixture
ssz
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CN110914195A (zh
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谢丹
K·O·詹森
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Chevron USA Inc
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Chevron USA Inc
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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15X-ray diffraction
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00Catalysts comprising molecular sieves
    • B01J29/04Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00Catalysts, in general, characterised by their form or physical properties
    • B01J35/70Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08Heat treatment
    • B01J37/10Heat treatment in the presence of water, e.g. steam
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026After-treatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/30Scanning electron microscopy; Transmission electron microscopy
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/70Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/01Particle morphology depicted by an image
    • C01P2004/03Particle morphology depicted by an image obtained by SEM
    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/58Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins
    • C10G45/60Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used
    • C10G45/64Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used containing crystalline alumino-silicates, e.g. molecular sieves

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
CN201880047072.8A 2017-10-27 2018-10-04 分子筛ssz-112、其合成及应用 Active CN110914195B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201762577853P 2017-10-27 2017-10-27
US62/577,853 2017-10-27
PCT/IB2018/057710 WO2019082004A1 (en) 2017-10-27 2018-10-04 MOLECULAR SIEVES SSZ-112, SA SYNTHESIS AND ITS USE

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CN110914195A CN110914195A (zh) 2020-03-24
CN110914195B true CN110914195B (zh) 2023-04-25

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US (1) US10343927B2 (enExample)
EP (1) EP3700863B1 (enExample)
JP (1) JP7138697B2 (enExample)
KR (1) KR102610289B1 (enExample)
CN (1) CN110914195B (enExample)
ES (1) ES2901685T3 (enExample)
WO (1) WO2019082004A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP7648541B2 (ja) * 2019-05-15 2025-03-18 ビーエーエスエフ ソシエタス・ヨーロピア Cha-aftゼオライト連晶coe-10の製造方法及び不均一系触媒におけるその使用
US10822243B1 (en) * 2019-07-29 2020-11-03 Chevron U.S.A. Inc. Molecular sieve SSZ-118, its synthesis and use
WO2022199574A1 (en) * 2021-03-23 2022-09-29 Basf Corporation Synthesis of zeolitic materials having aft framework structure and scr catalysts comprising the same
JP2024511795A (ja) * 2021-03-23 2024-03-15 ビーエーエスエフ コーポレーション Aft骨格構造を有するゼオライト材料を含むscr触媒及びその合成
WO2024104392A1 (en) * 2022-11-16 2024-05-23 Basf Corporation Synthesis of zeolitic materials having aft framework structure and scr catalysts comprising the same
WO2025199095A1 (en) * 2024-03-19 2025-09-25 Basf Mobile Emissions Catalysts Llc Synthesis of eri rich zeolitic phase using trimethylcyclohexylammonium cation, its derivatives and mixtures
CN120132816B (zh) * 2025-05-16 2025-07-29 上海恒业微晶材料科技股份有限公司 一种低温液相分子筛脱氯剂及其制备方法

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20160068402A1 (en) * 2014-09-09 2016-03-10 Chevron U.S.A. Inc Method for preparing zeolite ssz-52
US20170056870A1 (en) * 2015-08-27 2017-03-02 Chevron U.S.A. Inc. Method for making molecular sieve ssz-91
US20170058209A1 (en) * 2015-08-27 2017-03-02 Chevron U.S.A. Inc. Processes using molecular sieve ssz-91
US20170291822A1 (en) * 2016-04-12 2017-10-12 Chevron U.S.A. Inc. Molecular sieve al-ssz-63 composition of matter and synthesis thereof
US20170291823A1 (en) * 2016-04-12 2017-10-12 Chevron U.S.A. Inc. Synthesis of molecular sieve ssz-98
US20170297918A1 (en) * 2016-04-14 2017-10-19 Chevron U.S.A. Inc. Synthesis of molecular sieve ssz-99

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4086186A (en) * 1976-11-04 1978-04-25 Mobil Oil Corporation Crystalline zeolite ZSM-34 and method of preparing the same
US4851204A (en) 1987-06-04 1989-07-25 Uop Crystalline aluminophosphate composition
US8202506B2 (en) * 2009-11-17 2012-06-19 Exxonmobil Research And Engineering Company High activity small crystal ZSM-12
CN107021508B (zh) 2011-09-06 2019-08-27 巴斯夫欧洲公司 使用n,n-二甲基有机模板合成沸石材料
US8512674B1 (en) * 2012-03-01 2013-08-20 Chevron U.S.A. Inc. Preparation of molecular sieve SSZ-23
US9192924B1 (en) * 2014-06-04 2015-11-24 Chevron U.S.A. Inc. Molecular sieve SSZ-99
CA2952437C (en) * 2014-06-18 2023-08-29 Basf Corporation Molecular sieve catalyst compositions, catalytic composites, systems, and methods
US9409786B2 (en) * 2014-07-03 2016-08-09 Chevron U.S.A. Inc. Molecular sieve SSZ-98
US9505626B2 (en) * 2014-09-09 2016-11-29 Chevron U.S.A. Inc. Molecular sieve SSZ-101
US9598289B2 (en) * 2014-10-24 2017-03-21 Chevron U.S.A. Inc. Molecular sieve SSZ-102
GB2542876B (en) * 2015-04-20 2019-10-23 Johnson Matthey Plc Structure Directing Agent
US9586829B2 (en) * 2015-05-21 2017-03-07 Chevron U.S.A. Inc. Molecular sieve SSZ-27
JP6988111B2 (ja) * 2017-03-17 2022-01-05 三菱ケミカル株式会社 酸素8員環ゼオライトの製造方法

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20160068402A1 (en) * 2014-09-09 2016-03-10 Chevron U.S.A. Inc Method for preparing zeolite ssz-52
US20170056870A1 (en) * 2015-08-27 2017-03-02 Chevron U.S.A. Inc. Method for making molecular sieve ssz-91
US20170058209A1 (en) * 2015-08-27 2017-03-02 Chevron U.S.A. Inc. Processes using molecular sieve ssz-91
US20170291822A1 (en) * 2016-04-12 2017-10-12 Chevron U.S.A. Inc. Molecular sieve al-ssz-63 composition of matter and synthesis thereof
US20170291823A1 (en) * 2016-04-12 2017-10-12 Chevron U.S.A. Inc. Synthesis of molecular sieve ssz-98
US20170297918A1 (en) * 2016-04-14 2017-10-19 Chevron U.S.A. Inc. Synthesis of molecular sieve ssz-99

Also Published As

Publication number Publication date
KR102610289B1 (ko) 2023-12-05
EP3700863A1 (en) 2020-09-02
KR20200077550A (ko) 2020-06-30
CN110914195A (zh) 2020-03-24
JP2021500286A (ja) 2021-01-07
JP7138697B2 (ja) 2022-09-16
US20190127231A1 (en) 2019-05-02
US10343927B2 (en) 2019-07-09
EP3700863B1 (en) 2021-09-29
ES2901685T3 (es) 2022-03-23
WO2019082004A1 (en) 2019-05-02

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