KR102610289B1 - 분자체 ssz-112, 이의 합성 및 용도 - Google Patents

분자체 ssz-112, 이의 합성 및 용도 Download PDF

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KR102610289B1
KR102610289B1 KR1020207014760A KR20207014760A KR102610289B1 KR 102610289 B1 KR102610289 B1 KR 102610289B1 KR 1020207014760 A KR1020207014760 A KR 1020207014760A KR 20207014760 A KR20207014760 A KR 20207014760A KR 102610289 B1 KR102610289 B1 KR 102610289B1
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cation
molecular sieve
methyl
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reaction mixture
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KR20200077550A (ko
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단 씨에
커트 오웬 젠슨
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셰브런 유.에스.에이.인크.
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    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/46—Other types characterised by their X-ray diffraction pattern and their defined composition
    • C01B39/48—Other types characterised by their X-ray diffraction pattern and their defined composition using at least one organic template directing agent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/15—X-ray diffraction
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/70—Catalysts, in general, characterised by their form or physical properties characterised by their crystalline properties, e.g. semi-crystalline
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
    • C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
    • C01B39/026—After-treatment
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2235/00—Indexing scheme associated with group B01J35/00, related to the analysis techniques used to determine the catalysts form or properties
    • B01J2235/30—Scanning electron microscopy; Transmission electron microscopy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/03—Particle morphology depicted by an image obtained by SEM
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G45/00—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds
    • C10G45/58—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins
    • C10G45/60—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used
    • C10G45/64—Refining of hydrocarbon oils using hydrogen or hydrogen-generating compounds to change the structural skeleton of some of the hydrocarbon content without cracking the other hydrocarbons present, e.g. lowering pour point; Selective hydrocracking of normal paraffins characterised by the catalyst used containing crystalline alumino-silicates, e.g. molecular sieves

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Catalysts (AREA)
KR1020207014760A 2017-10-27 2018-10-04 분자체 ssz-112, 이의 합성 및 용도 Active KR102610289B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201762577853P 2017-10-27 2017-10-27
US62/577,853 2017-10-27
PCT/IB2018/057710 WO2019082004A1 (en) 2017-10-27 2018-10-04 MOLECULAR SIEVES SSZ-112, SA SYNTHESIS AND ITS USE

Publications (2)

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KR20200077550A KR20200077550A (ko) 2020-06-30
KR102610289B1 true KR102610289B1 (ko) 2023-12-05

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Country Link
US (1) US10343927B2 (enExample)
EP (1) EP3700863B1 (enExample)
JP (1) JP7138697B2 (enExample)
KR (1) KR102610289B1 (enExample)
CN (1) CN110914195B (enExample)
ES (1) ES2901685T3 (enExample)
WO (1) WO2019082004A1 (enExample)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US12264076B2 (en) 2019-05-15 2025-04-01 Basf Mobile Emissions Catalysts Llc Process for the production of the CHA-AFT zeolite intergrowth COE-10 and use thereof in heterogeneous catalysis
KR102810138B1 (ko) * 2019-07-29 2025-05-21 셰브런 유.에스.에이.인크. 분자체 ssz-118, 이의 합성 및 용도
US20240174523A1 (en) * 2021-03-23 2024-05-30 Basf Corporation Synthesis of zeolitic material having aft framework structure and scr catalysts comprising the same
EP4313409A4 (en) * 2021-03-23 2025-01-29 BASF Corporation Scr catalyst comprising zeolitic material having aft framework structure and synthesis of the same
WO2024104392A1 (en) * 2022-11-16 2024-05-23 Basf Corporation Synthesis of zeolitic materials having aft framework structure and scr catalysts comprising the same
WO2025199095A1 (en) * 2024-03-19 2025-09-25 Basf Mobile Emissions Catalysts Llc Synthesis of eri rich zeolitic phase using trimethylcyclohexylammonium cation, its derivatives and mixtures
CN120132816B (zh) * 2025-05-16 2025-07-29 上海恒业微晶材料科技股份有限公司 一种低温液相分子筛脱氯剂及其制备方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013035054A1 (en) 2011-09-06 2013-03-14 Basf Se Synthesis of zeolitic materials using n,n-dimethyl organotemplates

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4086186A (en) * 1976-11-04 1978-04-25 Mobil Oil Corporation Crystalline zeolite ZSM-34 and method of preparing the same
US4851204A (en) * 1987-06-04 1989-07-25 Uop Crystalline aluminophosphate composition
US8202506B2 (en) 2009-11-17 2012-06-19 Exxonmobil Research And Engineering Company High activity small crystal ZSM-12
US8512674B1 (en) * 2012-03-01 2013-08-20 Chevron U.S.A. Inc. Preparation of molecular sieve SSZ-23
US9192924B1 (en) * 2014-06-04 2015-11-24 Chevron U.S.A. Inc. Molecular sieve SSZ-99
RU2727801C2 (ru) 2014-06-18 2020-07-24 Басф Корпорейшн Каталитические композиции молекулярного сита, каталитические композиты, системы и способы
US9409786B2 (en) * 2014-07-03 2016-08-09 Chevron U.S.A. Inc. Molecular sieve SSZ-98
US9796596B2 (en) * 2014-09-09 2017-10-24 Chevron U.S.A. Inc. Method for preparing zeolite SSZ-52
US9505626B2 (en) * 2014-09-09 2016-11-29 Chevron U.S.A. Inc. Molecular sieve SSZ-101
US9598289B2 (en) * 2014-10-24 2017-03-21 Chevron U.S.A. Inc. Molecular sieve SSZ-102
GB2542876B (en) 2015-04-20 2019-10-23 Johnson Matthey Plc Structure Directing Agent
US9586829B2 (en) * 2015-05-21 2017-03-07 Chevron U.S.A. Inc. Molecular sieve SSZ-27
US20170056870A1 (en) * 2015-08-27 2017-03-02 Chevron U.S.A. Inc. Method for making molecular sieve ssz-91
US9920260B2 (en) * 2015-08-27 2018-03-20 Chevron U.S.A. Inc. Processes using molecular sieve SSZ-91
WO2017180222A1 (en) 2016-04-12 2017-10-19 Chevron U.S.A. Inc. Synthesis of molecular sieve ssz-98
US9822012B2 (en) * 2016-04-12 2017-11-21 Chevron U.S.A. Inc. Molecular sieve Al-SSZ-63 composition of matter and synthesis thereof
US9908784B2 (en) * 2016-04-14 2018-03-06 Chevron U.S.A. Inc. Synthesis of molecular sieve SSZ-99
JP6988111B2 (ja) 2017-03-17 2022-01-05 三菱ケミカル株式会社 酸素８員環ゼオライトの製造方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2013035054A1 (en) 2011-09-06 2013-03-14 Basf Se Synthesis of zeolitic materials using n,n-dimethyl organotemplates

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
Chem. Rev. 2014, 114, 2, 1521-1543

Also Published As

Publication number Publication date
EP3700863B1 (en) 2021-09-29
CN110914195B (zh) 2023-04-25
KR20200077550A (ko) 2020-06-30
CN110914195A (zh) 2020-03-24
WO2019082004A1 (en) 2019-05-02
EP3700863A1 (en) 2020-09-02
US10343927B2 (en) 2019-07-09
JP2021500286A (ja) 2021-01-07
JP7138697B2 (ja) 2022-09-16
US20190127231A1 (en) 2019-05-02
ES2901685T3 (es) 2022-03-23

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