CN110711147A

CN110711147A - Facial mask with acne removing and acne mark repairing functions

Info

Publication number: CN110711147A
Application number: CN201911062732.2A
Authority: CN
Inventors: 后琦; 张目; 李继德; 朱润锋
Original assignee: Guangzhou Yue Cosmetics Co Ltd
Current assignee: Guangzhou Yue Cosmetics Co Ltd
Priority date: 2019-11-03
Filing date: 2019-11-03
Publication date: 2020-01-21
Anticipated expiration: 2039-11-03
Also published as: CN110711147B

Abstract

The invention discloses a facial mask with acne removing and acne mark repairing functions. The mask base cloth is made of gauze; the mask liquid mainly comprises the following components in percentage by weight: 0.6-1.5% of plantain extract, 0.5-1.5% of fermented grape extract and 0.5-1% of terminalia faba fruit extract. The components of the facial mask are scientifically proportioned, so that acne can be safely and effectively removed and acne marks can be repaired.

Description

Facial mask with acne removing and acne mark repairing functions

Technical Field

The invention relates to the field of cosmetics, in particular to a facial mask with acne removing and acne mark repairing functions.

Background

Acne, also known as comedo and whelk, is a chronic inflammatory dermatosis of hair follicle sebaceous glands, is frequently generated in parts rich in sebaceous glands, such as face, back and chest, and is one of the most common dermatosis, and according to the joint investigation results of the Chinese dermatosis society and the Chinese teenager union, the incidence rate of whelk in China is on the rising trend year by year, and more than 80 percent of young people suffer from whelk in different degrees.

The acne is caused by endocrine disturbance and relative increase of male hormone, so that sebaceous gland hyperplasia is stimulated, hair follicle cells are easy to block hair glands after excessive keratinization, and cells exfoliated from sebum cannot be normally excreted, so that the cells are deposited at hair follicle openings to form acne. These comedones are inflamed at the hair follicle site by various microorganisms, particularly Propionibacterium acnes, and appear as pimples, pustules, and the like.

According to investigation, acne has a great influence on the psychology and social interaction of teenager patients, and most patients show anxiety, lack of confidence, fear of communication with people, inferior quality and the like. Some teenagers also face the negative effects of acne marks, which are caused by pressing the acne during the acne period, causing skin inflammation, damage to skin tissues, and even possibly causing purulent infection and acne marks, and have great influence on the facial appearance.

According to the design report of the traditional cosmeceutical industry development pattern and investment planning prospect in 2016-2022 years published by intelligent beauty consultation, the method comprises the following steps: in 2015, the cosmetic needs of Chinese anti-acne medicines are as high as 61 hundred million, and about 400-600 million people increase each year. The acne removing product has considerable market prospect, and the facial mask is convenient to use and high in consumer acceptance. In view of the above situation, the facial mask with the acne removing and acne mark repairing functions has fresh skin feeling and good acne removing and acne mark repairing effects, improves acne muscles and brings beauty and confidence to people.

Disclosure of Invention

Based on the above, the invention aims to provide the facial mask with the functions of removing acnes and repairing acne marks.

A facial mask with effects of removing acne and repairing acne mark comprises mask base cloth and mask liquid.

In some embodiments, the material of the mask base cloth is gauze.

In some embodiments, the facial mask liquid mainly comprises the following components in percentage by weight: 0.6-1.5% of Plantago major (Plantago LANCEOLATA) extract, 0.5-1.5% of grape (VITIS VINIFERA) fermentation extract, and 0.5-1% of Terminalia faba (TERMINALIA FERDINANDIANA) fruit extract.

In some embodiments, the facial mask liquid further comprises the following components in percentage by weight: 0.3-0.5% of hydrolyzed olive (Olea EUROPAEA) leaf extract, 30.2-0.5% of ceramide, and 0.5-1% of trehalose.

In some embodiments, the facial mask liquid further comprises the following components in percentage by weight: 3.5 to 10 percent of polyol, 0.4 to 0.6 percent of preservative, 0.25 to 0.55 percent of rheology modifier and 0.01 to 0.025 percent of pH value regulator.

The polyalcohol can be one or more of glycerol, propylene glycol, 1, 2-hexanediol, 1, 3-propanediol, butanediol, pentanediol, sorbitol, polyethylene glycol-8, polyethylene glycol-32, dipropylene glycol, diglycerol, glyceryl polyether-26, polyglycerol-10 and polyglycerol-8.

In some embodiments, the polyol consists of glycerol, propylene glycol and 1, 2-hexanediol, and the mass ratio of the glycerol to the propylene glycol to the 1, 2-hexanediol is (1-3) to (2-6): (0.5-1).

The preservative can be one or more of methyl hydroxybenzoate, p-hydroxyacetophenone, iodopropynyl butylcarbamate, caprylyl glycol, phenoxyethanol, caprylyl hydroxamic acid, chlorphenesin and ethylhexylglycerin.

In some of these embodiments, the preservative is p-hydroxyacetophenone.

The rheology modifier can be one or more than one of xanthan gum, hydroxyethyl cellulose, carbomer, acrylic acid (ester) copolymer, sodium alginate, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, sodium magnesium lithium silicate, polyacrylate cross-linked polymer-6, sodium polyacrylate grafted starch, hydroxypropyl methyl cellulose, ammonium acryloyl dimethyl taurate/VP copolymer, acrylic acid (ester)/behenyl alcohol polyether-25 methacrylate copolymer, sodium polyacrylate, gellan gum, pectin, acrylic acid (ester)/vinyl isodecanoate cross-linked polymer, carrageenan, locust bean gum and SCLEROTIUM rolfsii hydrolysis (SCLEOTIUM ROLFSSII) gum.

In some embodiments, the rheology modifier is composed of polyacrylate cross-linked polymer-6, acrylic acid (ester)/vinyl isodecanoate cross-linked polymer and hydroxyethyl cellulose, and the mass ratio of the polyacrylate cross-linked polymer-6, the acrylic acid (ester)/vinyl isodecanoate cross-linked polymer and the hydroxyethyl cellulose is (0.2-0.4): 0.02-0.05): (0.03-0.1).

In some of these embodiments, the pH adjusting agent is aminomethyl propanol.

In some embodiments, the facial mask liquid further comprises the following components in percentage by weight: 0.01-0.03% of sodium hyaluronate, 0.2-0.6% of emulsified silicone oil, 0.1-0.3% of allantoin, 0.002-0.003% of proud and 0.001-0.002% of Roman chamomile essential oil.

The technical scheme provided by the embodiment of the invention has the following beneficial effects:

(1) the invention relates to a mask with acne removing and acne mark repairing functions, which utilizes PLANTAGO major (Plantago LANCEOLATA) extract containing active acteoside, has anti-inflammatory and antibacterial effects (Propionibacterium acnes), and reduces pustules and comedos. The fermentation extract of fructus Vitis Viniferae (VITIS VINIFERA) has antibacterial and antiinflammatory effects, contains lipid, polysaccharide, amino acids, and glucosamine, and has effects in improving skin immunity, promoting wound healing, and promoting skin repair. The extract of the fruits of the Terminalia catappa (TERMINALIA FERDINANDIANA) is rich in polyphenol and VC, can efficiently promote the synthesis of I-type procollagen, greatly promote the synthesis of hyaluronic acid, strengthen the structure of a dermis layer, enable the skin to be elastic, strong and smooth, improve the brightness and the glossiness of the skin and repair acne marks. Through scientific proportioning of plantain (Plantago LANCEOLATA) extract, grape (VITISVINIFERA) fermentation extract and Terminalia faba (TERMINALIA FERDINANDIANA) fruit extract, acne and acne mark can be safely and effectively removed and repaired;

(2) the facial mask with the functions of removing acnes and repairing the acne marks is added with the hydrolyzed olive (OLEA EUROPAEA) leaf extract, the ceramide 3, the trehalose and the sodium hyaluronate, and has the advantages of being beneficial to transmitting essence to the skin through the synergistic cooperation of the oil control, moisture preservation and repairing effective components, and the gauze membrane is distributed with the essence, so that the product effect is better exerted, and the acne removing and repairing effects of the facial mask with the functions of removing acnes and repairing the acne marks are further improved;

(3) the facial mask with the acne removing and acne mark repairing functions is stable in system, soft, smooth and refreshing in skin feel, mild and non-irritating, and due to the addition of the Roman chamomile essential oil, the pleasant fragrance of the product is provided, and the facial mask has the effects of sterilizing, diminishing inflammation, resisting histamine and relieving pressure.

Detailed Description

In order to make the objects, technical solutions and advantages of the present invention more apparent, embodiments of the present invention will be described in further detail below, but the embodiments of the present invention are not limited thereto, and process parameters or conditions not particularly noted may be performed with reference to conventional techniques.

The plantago major active ingredient of the plantago major of the invention is acteoside, which has the effects of resisting bacteria and inflammation and reducing pustules and acnes. The Plantago major (Plantago LANCEOLATA) extract is prepared by extracting with ethanol water solution for 1-3 times, mixing extractive solutions, and filtering. The Plantago major (Plantago LANCEOLATA) extract can also be commercially available material, and suitable material is SEBCLEAR^TMDB (from RAHN, Switzerland).

The grape (VITIS VINIFERA) fermentation extract is prepared by fermenting and extracting grapes serving as raw materials, contains lipid compounds, polysaccharides, amino acids and glucosamine, improves the immune function of skin, promotes wound healing and accelerates skin repair. The fermented extract of fructus Vitis Viniferae (VITIS VINIFERA) can be obtained by inoculating Rhodococcus to the culture medium of fructus Vitis Viniferae, fermenting, sterilizing, and filtering to obtain filtrate. The fermented extract of grape (VITIS VINIFERA) may also be a commercially available material, and a suitable material may be ProNature RED (from Hippocampus Biotech Co., Ltd.).

The Terminalia faba (TERMINALIA FERDINANDIANA) fruit extract is extracted from the plant kadu plum with the highest VC content in the world, is rich in polyphenol and VC, is a high-efficiency antioxidant, and can resist oxidative stress, improve skin luster, whiten and repair skin. The Terminalia catappa (TERMINALIA FERDINANDIANA) fruit extract can be extracted with ethanol water solution as solvent for 1-3 times, and the extractive solutions are combined and filtered. The extract of Terminalia Familii (TERMINALIAFERDINANDIANA) fruit can also be obtained from commercially available materials, and suitable material can be SUPEROX-C^TM(from Lucas Meyer Cosmetics, France).

The hydrolyzed olive (OLEA EUROPAEA) leaf extract is a product obtained by fermenting olive leaves serving as a raw material with tectorial zymophyte, and can inhibit sebum secretion, maintain normal sebum secretion balance and improve large pores. Suitable hydrolyzed olive (OLEA EUROPAEA) leaf extract may be a fermented olive leaf extract (from japan tablet house industries co., ltd.).

The ceramide 3 is a latest generation humectant developed in recent years, is a water-soluble lipid substance, has a structure similar to that of a substance forming the horny layer of the skin, can quickly permeate into the skin, is combined with water in the horny layer to form a net structure, and locks water. Ceramide 3 can maintain the barrier function of skin, improve the water holding capacity of skin, prevent inflammation and free radical injury caused by bacteria and viruses, and promote skin health.

The gauze membrane cloth provided by the invention is prepared by the following steps: ondon new materials (guangzhou) ltd. The medical cotton yarn in the middle layer and the Japanese imported superfine viscose in the upper and lower layers are compounded by adopting a special wet spunlace process without adding any glue substances, and fat substances contained in cotton are removed by degreasing, so that the membrane cloth can not absorb the material and the moisture on the skin. The gauze membrane cloth is made of pure natural materials, can be naturally degraded, does not irritate the skin, and the mesh shape of the middle layer is more beneficial to transmitting essence to the skin.

To better illustrate the objects, technical solutions and advantages of the present invention, the present invention is further elaborated by the following examples 1-4 and comparative examples 1-3, wherein the following raw materials are respectively taken in percentage by mass: water, glycerin, propylene glycol, polyacrylate crosspolymer-6, acrylic acid/vinyl isodecanoate crosspolymer, hydroxyethyl cellulose, sodium hyaluronate, allantoin, p-hydroxyacetophenone, 1,2 hexanediol, aminomethyl propanol, silicone emulsion, trehalose, ceramide 3, plantain (Plantago LANCEOLATA) extract, grape (VITIS VINIFERA) fermentation extract, Terminalia faba (TERMINALIA FERDINANDIANA) fruit extract, hydrolyzed olive leaf extract, Piaoning, Roman chamomile essential oil.

The Chinese name of the proud cosmetic is as follows: polyquaternium-73.

Table 1: EXAMPLES 1-4 ingredient proportioning Table

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TABLE 2 ingredient ratio tables for comparative examples 1-3

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The masks obtained in examples 1 to 4 and comparative examples 1 to 3 were subjected to a control test, and a product safety evaluation (human body patch test), a skin moisture loss value through skin (TEWL value) test, and an acne and acne mark repairing efficacy evaluation test were performed.

Experiment 1 product safety evaluation (human body skin patch test)

Firstly, testing a test article: examples 1 to 4 and comparative examples 1 to 3, and acne mark removing facial mask prepared in examples 1 to 4 and comparative examples 3

The test population requires: each person takes 7 samples in 30 persons, half of men and women and between 20 and 50 years of age, the skin of a subject is healthy, no allergic history of skin diseases exists, and the voluntary selection standard of the subject is met.

Secondly, a spot pasting method: selecting a standard spot tester (Beijing Yida), putting about 0.020-0.025g of a tested substance into a small chamber of the spot tester by a closed spot test method, applying the spot tester in the arm of a tested person for testing, removing the spot tester after 24 hours, observing skin reactions at 0.5 hour, 6 hours, 12 hours, 24 hours and 48 hours respectively, and recording the results according to the skin reaction grading standard of the skin closed spot test in the table 2. The results were recorded according to the skin reaction grading standard in the technical Specification for safety of cosmetics (2015 edition), and 30 subjects showed more than 5 cases of grade 1 adverse skin reactions, or more than 2 cases of grade 2 adverse skin reactions (more than 5 cases of grade 2 reactions in the Patch test for deodorant products), or any 1 case of grade 3 or more than 3 adverse skin reactions, and the subjects were judged to have adverse skin reactions on human body.

Table 3: skin reaction grading standard of skin closed patch test

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The response of the group of masks to human skin was evaluated according to the patch results, and then rated according to the degree scale of table 3, examples 1 to 4 and comparative examples 1 to 3 described in the present invention were subjected to patch tests, and skin reactions were observed at 0.5, 6, 12, 24, and 48 hours, wherein 0 cases showed adverse skin reactions, indicating that examples 1 to 4 and comparative examples 1 to 3 described in the present invention are safe.

Experiment 2 skin transdermal Water loss value (TEWL value) test

The test population requires: and selecting volunteers with acne and acne marks on the face, wherein each experimental group comprises 20 people, half of men and women and between 23 and 45 years old.

Secondly, a test method comprises the following steps: before a test, a subject cleans the face with warm water uniformly, spreads the membrane cloth inwards and applies the membrane cloth on the face lightly until the membrane cloth is completely attached, the membrane cloth is applied for 15 minutes, the membrane cloth is used for 3 times a week, the service cycle is 4 weeks, and the similar cosmetics are not used in the test cycle. The results of obtaining the percutaneous water loss (TEWL) using a skin water loss meter, TewameterTM300 (CK, Germany) are shown in Table 4. (the following data are all the results of 30min after using the product in an environment of constant temperature 22 ℃ and relative humidity 55%)

Through analyzing the skin percutaneous loss TEWL value, the smaller the TEWL value is, the better the skin barrier function is, and the more obvious the water locking effect is. Percent change (= after TEWL value used-before TEWL value used)/before TEWL value used 100%.

TABLE 4 TEWL variability record for skin dermal loss

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As can be seen from the data in table 4 above, the experimental data of the mask with the acne removing and acne mark repairing functions in example 3 of the present invention is the best, and the subjects in examples 1 to 4 all show that the mask with the acne removing and acne mark repairing functions has good water locking and moisturizing effects, and the effects after 4 weeks of use are obvious, which indicates that the mask with the acne removing and acne mark repairing functions has good moisturizing effects, and can strengthen the skin barrier and repair acne marks.

Experiment 3 acne removing and acne mark repairing efficacy evaluation test

The test population requires: the method comprises the steps of selecting volunteers with acne and obvious acne marks on the face, wherein the number of the volunteers is 140, and each experimental group comprises 20 volunteers, half of men and women and between 20 and 45 years old.

The test method comprises the following steps: the product is applied for 15 min 3 times per week, and the application period is 4 weeks, and the similar cosmetic is stopped during the test period. Subjects were evaluated clinically by the GAGS acne system scoring system before and 1 to 4 weeks of use and were analyzed by photo-taking before and after trial by a skin facial analyzer VISIA CR (Canfield, usa) and facial Image analysis software Image-Pro Plus (Media Cybernetics, Inc.) for the amount of acne mark removal or the degree of lightening visually observed.

The GAGS scoring method is a GlobalAcnene grading System (GAGS) of an acne comprehensive grading system proposed by Doshi et al in 1997, is a scoring method, and has the characteristics of accuracy, strong consistency, quickness, good overall evaluation effect and the like. The method specifically comprises the following steps: according to the density, distribution and approximate area of the pilosebaceous unit, the good hair part of the acne is divided into 6 areas: zone I, forehead, zone II: right cheek, zone iii: left cheek, region iv: nose, chin zone v, zone vi: chest and upper back. The factor values of the I, II and III zones are 2, the factor values of the IV and V zones are 1, and the factor value of the VI zone is 3. The skin damage score for each region is (the principle is that the most severe local skin damage determines the score for that region): the number of skin lesions was 0, 1 for white or black comedones, 2 for papulo-type acnes (red granules), 3 for pustular acnes (yellow pustules), and 4 for cystic acnes (large granules). The total score of each subarea is factor score multiplied by skin damage score, and the sum of the total scores of different subareas is the comprehensive score.

TABLE 5 GAGS acne System Scoring Standard

TABLE 6 GAGS score evaluation results

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Before P <0.05 VS usage, before P <0.01 VS usage

TABLE 7 evaluation criteria for acne mark repairing efficacy

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TABLE 8 repair acne mark test results

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It can be seen from tables 6 and 8 that the masks of examples 1-4 had a significantly reduced acne score after one week of use, a significantly reduced acne score after 2-4 weeks of use, and had statistical significance (P <0.01), more than 60% of the acne marks had disappeared after 2 weeks of use, more than 80% of the majority of volunteers had disappeared acne marks and the acne was at a mild grade after 4 weeks of use, with the effect of example 3 being more significant. Compared with comparative examples 1-3, examples 1-4 have more remarkable effects, which shows that the compound use of the PLANTAGO major (Plantago LANCEOLATA) extract, the grape (VITIS VINIFERA) fermentation extract and the Terminalia faba (TERMINALIA FERDINANDIANA) fruit extract has good synergistic effect on improving acne and repairing acne marks.

The above description is only a preferred embodiment of the present invention, and is not intended to limit the present invention in any way, so that any simple modification, equivalent change and modification made to the above embodiment according to the technical spirit of the present invention will still fall within the scope of the technical solution of the present invention without departing from the content of the technical solution of the present invention.

Claims

1. The mask with the functions of removing acnes and repairing acne marks is characterized by comprising mask base cloth and mask liquid; the mask liquid mainly comprises the following components in percentage by weight: 0.6-1.5% of Plantago major (Plantago LANCEOLATA) extract, 0.5-1.5% of grape (VITIS VINIFERA) fermentation extract, and 0.5-1% of Terminalia faba (TERMINALIAFERDINANDIANA) fruit extract.

2. The mask with the effects of removing acne and repairing acne marks according to claim 1, wherein the mask base cloth is made of gauze.

3. The mask liquid with the effects of removing acnes and repairing acne marks according to claim 1, which is characterized by further comprising the following components in percentage by weight: 0.3-0.5% of hydrolyzed olive (Olea EUROPAEA) leaf extract, 30.2-0.5% of ceramide, and 0.5-1% of trehalose.

4. The mask liquid with the effects of removing acnes and repairing acne marks according to claim 1, which is characterized by further comprising the following components in percentage by weight: 3.5 to 10 percent of polyol, 0.4 to 0.6 percent of preservative, 0.25 to 0.55 percent of rheology modifier and 0.01 to 0.025 percent of pH value regulator.

5. The mask with effects of removing acne and repairing acne marks according to claim 4, wherein the polyhydric alcohol is one or a mixture of more than one of glycerin, propylene glycol, 1, 2-hexanediol, 1, 3-propanediol, butanediol, pentanediol, sorbitol, polyethylene glycol-8, polyethylene glycol-32, dipropylene glycol, diglycerin, glyceryl polyether-26, polyglycerol-10, and polyglycerol-8.

6. The mask with effects of removing acne and repairing acne marks according to claim 5, wherein the polyhydric alcohol is composed of glycerin, propylene glycol and 1, 2-hexanediol, and the mass ratio of glycerin to propylene glycol to 1, 2-hexanediol is (1-3) to (2-6): (0.5-1).

7. The mask with effects of removing acne and repairing acne marks according to claim 3, wherein the preservative is one or more of methylparaben, p-hydroxyacetophenone, iodopropynyl butylcarbamate, caprylyl glycol, phenoxyethanol, caprylyl hydroxamic acid, chlorphenesin and ethylhexylglycerin.

8. The mask with effects of removing acne and repairing acne marks according to claim 1, wherein the preservative is p-hydroxyacetophenone.

9. The mask with effects of removing acne and repairing acne marks according to claim 1, wherein the rheology modifier is composed of polyacrylate cross-linked polymer-6, acrylic acid (ester)/vinyl isodecanoate cross-linked polymer and hydroxyethyl cellulose, and the mass ratio of the polyacrylate cross-linked polymer-6, the acrylic acid (ester)/vinyl isodecanoate cross-linked polymer and the hydroxyethyl cellulose is (0.2-0.4): 0.02-0.05): (0.03-0.1).

10. The mask liquid with the effects of removing acnes and repairing acne marks according to claim 1, which is characterized by further comprising the following components in percentage by weight: 0.01-0.03% of sodium hyaluronate, 0.2-0.6% of emulsified silicone oil, 0.1-0.3% of allantoin, 0.002-0.003% of proud and 0.001-0.002% of Roman chamomile essential oil.