CN110693808A - Toothpaste and preparation method thereof - Google Patents
Toothpaste and preparation method thereof Download PDFInfo
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- CN110693808A CN110693808A CN201911141906.4A CN201911141906A CN110693808A CN 110693808 A CN110693808 A CN 110693808A CN 201911141906 A CN201911141906 A CN 201911141906A CN 110693808 A CN110693808 A CN 110693808A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
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- Tropical Medicine & Parasitology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Cosmetics (AREA)
Abstract
The invention provides toothpaste, which comprises the following components in percentage by mass: 1-3 parts of wisteria extracting solution, 10-20 parts of edible essence, 10-20 parts of lactobacillus, 10-15 parts of hydrated silica, 30-60 parts of surfactant, 10-30 parts of cellulose gum, 10-20 parts of traditional Chinese medicine extract, 0.1-0.3 part of trichlorogalactose, 2-3 parts of sodium benzoate, 220 parts of sorbitol 200, 10-12 parts of polyethylene glycol-40010, 5-7 parts of carboxymethyl cellulose, 35-45 parts of silicon dioxide H type, 30-40 parts of silicon dioxide MIV type, 40-50 parts of silicon dioxide MIG type, 10-15 parts of sodium dodecyl sulfate and 300 parts of deionized water 100. The traditional Chinese medicine extract is a mixed extract of the south African leaves, the liquorice and the bletilla striata in a weight ratio of 5:3: 2.
Description
Technical Field
The invention belongs to the technical field of daily necessities, relates to toothpaste and further relates to a preparation method of the toothpaste.
Background
The toothpaste is a kind of oral hygiene product containing many ingredients, and is a paste-like substance formed by mixing abrasive, humectant, thickener, foaming agent, aromatic and water and other additives. People are used for cleaning teeth, keeping oral hygiene and keeping fresh breath. With the development of economy, the living standard of people is continuously improved, people not only can meet the requirement of toothpaste only with cleaning efficacy, but also the toothpaste is developed from a common cleaning type to an efficacy health care type. Aiming at frequent oral problems such as dental caries, dental plaque, dental calculus, halitosis and the like, a series of functional toothpastes aiming at related problems appear in the market, however, in order to achieve the required effect, the traditional toothpaste for preventing dental caries, whitening and refreshing breath usually adds chemical agents such as hydrogen peroxide into toothpaste products, and certain safety risks exist after long-term use. The product without adding chemical agents has the effects of preventing caries, whitening and refreshing breath and can not meet the requirements of people.
Disclosure of Invention
The invention aims to provide toothpaste, which solves the problem that in the prior art, more chemical agents exist in toothpaste.
The invention also aims to provide a preparation method of the toothpaste, which solves the problem that the toothpaste prepared by the prior art contains more chemical agents.
The technical scheme adopted by the invention is that,
the toothpaste comprises the following components in percentage by mass: 1-3 parts of wisteria extracting solution, 10-20 parts of edible essence, 10-20 parts of lactobacillus, 10-15 parts of friction agent, 30-60 parts of surfactant, 10-30 parts of cellulose gum, 10-20 parts of traditional Chinese medicine extract, 0.1-0.3 part of trichlorogalactose, 2-3 parts of sodium benzoate, 220 parts of sorbitol 200, 10-12 parts of polyethylene glycol-400, 5-7 parts of carboxymethyl cellulose, 35-45 parts of silicon dioxide H type, 30-40 parts of silicon dioxide MIV type, 40-50 parts of silicon dioxide MIG type, 10-15 parts of sodium dodecyl sulfate and 300 parts of deionized water 100.
The traditional Chinese medicine extract is a mixed extract of the south African leaves, the liquorice and the bletilla striata in a weight ratio of 5:3: 2.
The abrasive is hydrated silica.
A preparation method of toothpaste comprises the following steps:
step 1, weighing 1-3 parts of wisteria extracting solution, 10-20 parts of edible essence, 10-20 parts of lactobacillus, 10-15 parts of rubbing agent, 30-60 parts of surfactant, 10-30 parts of cellulose gum, 10-20 parts of traditional Chinese medicine extract prepared from south Africa leaves, liquorice and bletilla striata, 0.1-0.3 part of trichlorogalactose, 2-3 parts of sodium benzoate, 220 parts of sorbitol 200-.
Step 2, mixing the wisteria sinensis extract weighed in the step 1, lactobacillus, traditional Chinese medicine extract and deionized water, and putting into a metering gel-forming pot;
step 3, mixing the trichlorogalactose and the sodium dodecyl sulfate weighed in the step 1, heating to 70 ℃, filtering, and adding into the hair gel pot in the step 2;
step 4, putting the surfactant weighed in the step 1 into the gel forming pot in the step 3, soaking for 10-20 minutes, starting a stirring paddle of the gel forming pot, and controlling the stirring speed to be 20-40 r/min;
step 5, sequentially putting the sodium benzoate, the sorbitol and the polyethylene glycol-400 weighed in the step 1 into the foaming pot in the step 4 to obtain a premixing pot;
step 6, sequentially putting the cellulose gum and the carboxymethyl cellulose weighed in the step 1 into the premixing pot in the step 5, starting rapid stirring for 10-15min to dissolve and disperse the cellulose gum and the carboxymethyl cellulose uniformly until no agglomeration exists, then putting the cellulose gum and the carboxymethyl cellulose into a glue sending pot, continuously stirring and circulating for 10-20min, then sending the glue to a storage tank, and standing and storing for 5-8 h;
step 7, starting the paste making pot, starting the scraper plate for stirring, putting in the friction agent when controlling the vacuum degree of the paste making pot to be 0.03Mpa, and keeping rapid stirring for 5-10 min; when the vacuum degree is increased to 0.08Mpa, adding edible essence, starting rapid stirring for 20-30min after adding edible essence, adding the silica H type, the silica MIV type and the silica MIG type weighed in the step 1 when the vacuum degree reaches above 0.096Mpa, continuing stirring for 5-15min, stopping rapid stirring, and stirring at the speed of 20-40r/min for 10-20 min.
In the step 6 and the step 7, the speed of rapid stirring is 80-100 r/min.
The invention has the beneficial effects that: 1) the invention adopts the glucanase enzyme to cut the decomposition of alpha-1, 6 glucoside chain of glucan in dental plaque, so that cariogenic microorganisms can not attach to the surface of teeth, the glucan formed on the surface of the teeth is decomposed, and the formation of bacterial plaque is inhibited. In addition, the oral liquid can also dissolve cell walls of harmful bacteria or influence the metabolism of the bacteria, so that the harmful bacteria in the oral cavity die, and the effects of reducing the bacteria, strongly removing dental plaque, preventing decayed teeth and whitening teeth can be achieved. The toothpaste disclosed by the invention is safe in components, small in toxic and side effects, stable in toothpaste body and suitable for long-term use. The preparation process is simple, the components are sequentially and strictly added, so that the raw materials are uniformly mixed, the components supplement each other in the process of cleaning the oral cavity, and the effects of effectively removing bacteria, preventing decayed teeth and whitening teeth and refreshing breath can be achieved.
Detailed Description
The present invention will be described in detail with reference to the following embodiments.
The invention provides toothpaste, which comprises the following components in percentage by mass: 1-3 parts of wisteria extracting solution, 10-20 parts of edible essence, 10-20 parts of lactobacillus, 10-15 parts of hydrated silica, 30-60 parts of surfactant, 10-30 parts of cellulose gum, 10-20 parts of traditional Chinese medicine extract, 0.1-0.3 part of trichlorogalactose, 2-3 parts of sodium benzoate, 220 parts of sorbitol 200, 10-12 parts of polyethylene glycol-40010, 5-7 parts of carboxymethyl cellulose, 35-45 parts of silicon dioxide H type, 30-40 parts of silicon dioxide MIV type, 40-50 parts of silicon dioxide MIG type, 10-15 parts of sodium dodecyl sulfate and 300 parts of deionized water 100. The traditional Chinese medicine extract is a mixed extract of the south African leaves, the liquorice and the bletilla striata in a weight ratio of 5:3: 2.
The invention also provides a preparation method of the toothpaste, which comprises the following steps:
step 1, weighing 1-3 parts of wisteria extracting solution, 10-20 parts of edible essence, 10-20 parts of lactobacillus, 10-15 parts of rubbing agent, 30-60 parts of surfactant, 10-30 parts of cellulose gum, 10-20 parts of traditional Chinese medicine extract prepared from south Africa leaves, liquorice and bletilla striata, 0.1-0.3 part of trichlorogalactose, 2-3 parts of sodium benzoate, 220 parts of sorbitol 200-.
Step 2, mixing the wisteria sinensis extract weighed in the step 1, lactobacillus, traditional Chinese medicine extract and deionized water, and putting into a metering gel-forming pot;
step 3, mixing the trichlorogalactose and the sodium dodecyl sulfate weighed in the step 1, heating to 70 ℃, filtering, and adding into the hair gel pot in the step 2;
step 4, putting the surfactant weighed in the step 1 into the gel forming pot in the step 3, soaking for 10-20 minutes, starting a stirring paddle of the gel forming pot, and controlling the stirring speed to be 20-40 r/min;
step 5, sequentially putting the sodium benzoate, the sorbitol and the polyethylene glycol-400 weighed in the step 1 into the foaming pot in the step 4 to obtain a premixing pot;
step 6, sequentially putting the cellulose gum and the carboxymethyl cellulose weighed in the step 1 into the premixing pot in the step 5, starting the premixing pot at a stirring speed of 80-100r/min for 10-15min to dissolve and disperse the cellulose gum and the carboxymethyl cellulose uniformly until no agglomeration exists, then putting the premixed cellulose gum and the carboxymethyl cellulose into a glue sending pot, continuously stirring and circulating for 10-20min, then sending the glue to a storage tank, and standing and storing for 5-8 h;
step 7, starting the paste making pot, starting the scraper plate for stirring, putting the friction agent when controlling the vacuum degree of the paste making pot to be 0.03Mpa, and keeping the stirring speed of 80-100r/min for 5-10 min; when the vacuum degree is increased to 0.08Mpa, adding edible essence, starting stirring at 80-100r/min for 20-30min after adding edible essence, adding the silica H type, silica MIV type and silica MIG type weighed in the step 1 when the vacuum degree reaches above 0.096Mpa, continuing stirring for 5-15min, stopping rapid stirring, and stirring at 20-40r/min for 10-20 min.
Example 1
Step 1, weighing 1 part of wisteria extracting solution, 10 parts of edible essence, 10 parts of lactobacillus, 10 parts of friction agent, 30 parts of surfactant, 10 parts of cellulose gum, 10 parts of traditional Chinese medicine extract prepared from south Africa leaves, liquorice and bletilla striata, 0.1 part of trichlorogalactose, 2 parts of sodium benzoate, 200 parts of sorbitol, 10 parts of polyethylene glycol-40010 parts of carboxymethyl cellulose, 5 parts of silicon dioxide H type 35 parts, 30 parts of silicon dioxide MIV type, 40 parts of silicon dioxide MIG type, 10 parts of sodium dodecyl sulfate, 6 parts of essence and 100 parts of deionized water according to mass fraction.
Step 2, mixing the wisteria sinensis extract weighed in the step 1, lactobacillus, traditional Chinese medicine extract and deionized water, and putting into a metering gel-forming pot;
step 3, mixing the trichlorogalactose and the sodium dodecyl sulfate weighed in the step 1, heating to 70 ℃, filtering, and adding into the hair gel pot in the step 2;
step 4, putting the surfactant weighed in the step 1 into the gel-forming pot in the step 3, soaking for 10 minutes, starting a stirring paddle of the gel-forming pot, and controlling the stirring speed to be 20 r/min;
step 5, sequentially putting the sodium benzoate, the sorbitol and the polyethylene glycol-400 weighed in the step 1 into the foaming pot in the step 4 to obtain a premixing pot;
step 6, sequentially putting the cellulose gum and the carboxymethyl cellulose weighed in the step 1 into the premixing pot in the step 5, starting the premixing pot at a stirring speed of 80r/min for 10min to dissolve and disperse the cellulose gum and the carboxymethyl cellulose uniformly until no agglomeration exists, then putting the premixing pot into a glue sending pot, continuously stirring and circulating for 10min, then sending the glue to a storage tank, and standing and storing for 5 h;
step 7, starting the paste making pot, starting the scraper plate for stirring, putting the friction agent when controlling the vacuum degree of the paste making pot to be 0.03Mpa, and keeping the stirring speed at 8r/min for 10 min; and (3) when the vacuum degree is increased to 0.08Mpa, adding edible essence, starting stirring at the speed of 80r/min for 30min after adding the edible essence, adding the H type silicon dioxide, MIV type silicon dioxide and MIG type silicon dioxide weighed in the step (1) when the vacuum degree reaches above 0.096Mpa, continuing stirring for 5min, stopping rapid stirring, and stirring at the speed of 20r/min for 20 min.
Example 2
Step 1, weighing 3 parts of wisteria extracting solution, 20 parts of edible essence, 20 parts of lactobacillus, 15 parts of friction agent, 60 parts of surfactant, 30 parts of cellulose gum, 20 parts of traditional Chinese medicine extract prepared from south African leaves, liquorice and bletilla striata, 0.3 part of trichlorogalactose, 3 parts of sodium benzoate, 220 parts of sorbitol, 12 parts of polyethylene glycol-40012 parts of carboxymethyl cellulose, 7 parts of silicon dioxide H type, 40 parts of silicon dioxide MIV type, 50 parts of silicon dioxide MIG type, 15 parts of sodium dodecyl sulfate, 8 parts of essence and 300 parts of deionized water according to mass fraction.
Step 2, mixing the wisteria sinensis extract weighed in the step 1, lactobacillus, traditional Chinese medicine extract and deionized water, and putting into a metering gel-forming pot;
step 3, mixing the trichlorogalactose and the sodium dodecyl sulfate weighed in the step 1, heating to 70 ℃, filtering, and adding into the hair gel pot in the step 2;
step 4, putting the surfactant weighed in the step 1 into the gel-forming pot in the step 3, soaking for 20 minutes, starting a stirring paddle of the gel-forming pot, and controlling the stirring speed to be 40 r/min;
step 5, sequentially putting the sodium benzoate, the sorbitol and the polyethylene glycol-400 weighed in the step 1 into the foaming pot in the step 4 to obtain a premixing pot;
step 6, sequentially putting the cellulose gum and the carboxymethyl cellulose weighed in the step 1 into the premixing pot in the step 5, starting the premixing pot at a stirring speed of 100r/min for 10min to dissolve and disperse the cellulose gum and the carboxymethyl cellulose uniformly until no agglomeration exists, then putting the premixing pot into a glue sending pot, continuously stirring and circulating for 20min, then sending the glue to a storage tank, and standing and storing for 8 h;
step 7, starting the paste making pot, starting the scraper plate for stirring, putting the friction agent when controlling the vacuum degree of the paste making pot to be 0.03Mpa, and keeping the stirring speed of 100r/min for 5 min; when the vacuum degree is increased to 0.08Mpa, adding edible essence, starting stirring at 100r/min for 20min, when the vacuum degree reaches above 0.096Mpa, adding silica H, MIV, and MIG, stirring for 15min, stopping rapid stirring, and stirring at 40r/min for 10 min.
Example 3
Step 1, weighing 2 parts of wisteria extracting solution, 15 parts of edible essence, 15 parts of lactobacillus, 13 parts of friction agent, 45 parts of surfactant, 20 parts of cellulose gum, 15 parts of traditional Chinese medicine extract prepared from south African leaves, liquorice and bletilla striata, 0.2 part of trichlorogalactose, 2.5 parts of sodium benzoate, 210 parts of sorbitol, 11 parts of polyethylene glycol-40011 parts, 6 parts of carboxymethyl cellulose, 40 parts of silicon dioxide H type, 35 parts of silicon dioxide MIV type, 45 parts of silicon dioxide MIG type, 12 parts of sodium dodecyl sulfate, 7 parts of essence and 200 parts of deionized water according to mass fraction.
Step 2, mixing the wisteria sinensis extract weighed in the step 1, lactobacillus, traditional Chinese medicine extract and deionized water, and putting into a metering gel-forming pot;
step 3, mixing the trichlorogalactose and the sodium dodecyl sulfate weighed in the step 1, heating to 70 ℃, filtering, and adding into the hair gel pot in the step 2;
step 4, putting the surfactant weighed in the step 1 into the gel-forming pot in the step 3, soaking for 15 minutes, starting a stirring paddle of the gel-forming pot, and controlling the stirring speed to be 30 r/min;
step 5, sequentially putting the sodium benzoate, the sorbitol and the polyethylene glycol-400 weighed in the step 1 into the foaming pot in the step 4 to obtain a premixing pot;
step 6, sequentially putting the cellulose gum and the carboxymethyl cellulose weighed in the step 1 into the premixing pot in the step 5, starting the premixing pot at a stirring speed of 90r/min for 12min to dissolve and disperse the cellulose gum and the carboxymethyl cellulose uniformly until no agglomeration exists, then putting the premixing pot into a glue sending pot, continuously stirring and circulating for 15min, then sending the glue to a storage tank, and standing and storing for 6.5 h;
step 7, starting the paste making pot, starting the scraper plate for stirring, putting the friction agent when controlling the vacuum degree of the paste making pot to be 0.03Mpa, and keeping the stirring speed of 90r/min for 7.5 min; when the vacuum degree is increased to 0.08Mpa, adding edible essence, starting stirring at 90r/min for 25min, when the vacuum degree reaches above 0.096Mpa, adding silica H, MIV, and MIG, stirring for 10min, stopping rapid stirring, and stirring at 30r/min for 15 min.
Claims (5)
1. The toothpaste is characterized by comprising the following components in percentage by mass: 1-3 parts of wisteria extracting solution, 10-20 parts of edible essence, 10-20 parts of lactobacillus, 10-15 parts of friction agent, 30-60 parts of surfactant, 10-30 parts of cellulose gum, 10-20 parts of traditional Chinese medicine extract, 0.1-0.3 part of trichlorogalactose, 2-3 parts of sodium benzoate, 220 parts of sorbitol 200, 10-12 parts of polyethylene glycol-400, 5-7 parts of carboxymethyl cellulose, 35-45 parts of silicon dioxide H type, 30-40 parts of silicon dioxide MIV type, 40-50 parts of silicon dioxide MIG type, 10-15 parts of sodium dodecyl sulfate and 300 parts of deionized water 100.
2. The toothpaste of claim 1, wherein the herbal extract is a mixed extract of leaf of south Africa, licorice and bletilla striata in a weight ratio of 5:3: 2.
3. The toothpaste of claim 2, wherein said abrasive is hydrated silica.
4. The preparation method of the toothpaste is characterized by comprising the following steps:
step 1, weighing 1-3 parts of wisteria extracting solution, 10-20 parts of edible essence, 10-20 parts of lactobacillus, 10-15 parts of rubbing agent, 30-60 parts of surfactant, 10-30 parts of cellulose gum, 10-20 parts of traditional Chinese medicine extract prepared from south Africa leaves, liquorice and bletilla striata, 0.1-0.3 part of trichlorogalactose, 2-3 parts of sodium benzoate, 220 parts of sorbitol 200-.
Step 2, mixing the wisteria sinensis extract weighed in the step 1, lactobacillus, traditional Chinese medicine extract and deionized water, and putting into a metering gel-forming pot;
step 3, mixing the trichlorogalactose and the sodium dodecyl sulfate weighed in the step 1, heating to 70 ℃, filtering, and adding into the hair gel pot in the step 2;
step 4, putting the surfactant weighed in the step 1 into the gel forming pot in the step 3, soaking for 10-20 minutes, starting a stirring paddle of the gel forming pot, and controlling the stirring speed to be 20-40 r/min;
step 5, sequentially putting the sodium benzoate, the sorbitol and the polyethylene glycol-400 weighed in the step 1 into the foaming pot in the step 4 to obtain a premixing pot;
step 6, sequentially putting the cellulose gum and the carboxymethyl cellulose weighed in the step 1 into the premixing pot in the step 5, starting rapid stirring for 10-15min to dissolve and disperse the cellulose gum and the carboxymethyl cellulose uniformly until no agglomeration exists, then putting the cellulose gum and the carboxymethyl cellulose into a glue sending pot, continuously stirring and circulating for 10-20min, then sending the glue to a storage tank, and standing and storing for 5-8 h;
6) starting the paste making pot, starting the scraper plate for stirring, controlling the vacuum degree of the paste making pot to be 0.03Mpa, adding the friction agent, and keeping rapid stirring for 5-10 min; when the vacuum degree is increased to 0.08Mpa, adding edible essence, starting rapid stirring for 20-30min after adding the edible essence, when the vacuum degree reaches above 0.096Mpa, adding 35-45 parts of silicon dioxide H type, 30-40 parts of silicon dioxide MIV type and 40-50 parts of silicon dioxide MIG type, continuing stirring for 5-15min, stopping rapid stirring, and stirring at the speed of 20-40r/min for 10-20 min.
5. The method of claim 4, wherein the rapid agitation is at a speed of 80-100r/min in steps 6 and 7.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201911141906.4A CN110693808A (en) | 2019-11-20 | 2019-11-20 | Toothpaste and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201911141906.4A CN110693808A (en) | 2019-11-20 | 2019-11-20 | Toothpaste and preparation method thereof |
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| CN110693808A true CN110693808A (en) | 2020-01-17 |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004250374A (en) * | 2003-02-20 | 2004-09-09 | Nippon Zettoc Co Ltd | Composition for oral cavity |
| CN102600045A (en) * | 2012-04-24 | 2012-07-25 | 苏州维蒂卡科技有限公司 | Toothpaste composition |
| CN110123722A (en) * | 2019-06-17 | 2019-08-16 | 中山市多美化工有限公司 | A kind of ferment bamboo charcoal toothpaste and preparation method thereof |
| CN110327276A (en) * | 2019-08-12 | 2019-10-15 | 三椒口腔健康股份有限公司 | A kind of Chinese medicinal toothpaste and preparation method thereof |
-
2019
- 2019-11-20 CN CN201911141906.4A patent/CN110693808A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004250374A (en) * | 2003-02-20 | 2004-09-09 | Nippon Zettoc Co Ltd | Composition for oral cavity |
| CN102600045A (en) * | 2012-04-24 | 2012-07-25 | 苏州维蒂卡科技有限公司 | Toothpaste composition |
| CN110123722A (en) * | 2019-06-17 | 2019-08-16 | 中山市多美化工有限公司 | A kind of ferment bamboo charcoal toothpaste and preparation method thereof |
| CN110327276A (en) * | 2019-08-12 | 2019-10-15 | 三椒口腔健康股份有限公司 | A kind of Chinese medicinal toothpaste and preparation method thereof |
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