CN110664724A - Skin care product raw material containing roe extract for moisturizing, removing wrinkles and removing red blood streak and preparation method thereof - Google Patents
Skin care product raw material containing roe extract for moisturizing, removing wrinkles and removing red blood streak and preparation method thereof Download PDFInfo
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- CN110664724A CN110664724A CN201911146239.9A CN201911146239A CN110664724A CN 110664724 A CN110664724 A CN 110664724A CN 201911146239 A CN201911146239 A CN 201911146239A CN 110664724 A CN110664724 A CN 110664724A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention discloses a skin care product raw material containing roe extract for moisturizing, removing wrinkles and removing red blood streaks and a preparation method thereof, wherein the skin care product raw material comprises a phase A, a phase B and a phase C; wherein the phase A comprises: betaine: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture; the phase B comprises: fish egg extract: 0.5-3 parts; the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate. The raw materials of the skin care product can be applied to essence, water aqua, cream and emulsion in personal care products.
Description
Technical Field
The invention relates to the technical field of skin care products, and in particular relates to a skin care product raw material containing a fish egg extract for moisturizing, removing wrinkles and removing red blood streaks and a preparation method thereof.
Background
At present, the skin care products on the market have various types and different efficacies, including whitening, moisturizing, freckle removing, aging resisting and the like. However, many products are added with a few chemical substances which are harmful to human bodies, and although the substances have skin care effects of short-term whitening, anti-aging and the like on human skin, if the substances are used for a long time, the skin is seriously damaged, and acne, color spots, lipid secretion disorder and the like appear; the imitation skin care products contain a plurality of plant extracts, however, in the personal care products, the skin care products using the plant extracts as active substances are more than hundreds of skin care products, the effects brought by the personal care products are more perfect in the field of plant extraction sources according to the development of extraction modes or biotechnology, and further the types of fish egg extracts are still few, and the skin barrier moisturizing function is low due to the increasing tension of living pressure of people and the climate change.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides a skin care product raw material containing a fish egg extract for moisturizing, removing wrinkles and removing red blood streaks and a preparation method thereof.
The purpose of the invention can be achieved by adopting the following technical scheme:
compared with the prior art, the invention has the following advantages and effects:
1) the roe is rich in microelements, mineral salts, proteins, amino acids and recombinant basic fatty acids required by skin, but is difficult to be effectively applied to skin care products, and the activity of active substances beneficial to the skin in the roe is well retained by the supercritical CO2 fluid extraction technology.
2) The skin care product raw material containing the fish egg extract for moisturizing, removing wrinkles and removing red blood streaks provided by the invention effectively improves the skin barrier moisturizing function, improves the moisturizing effect by 31%, reduces the red blood streaks by 21%, and reduces wrinkles by about 32% in 8 weeks.
3) The raw materials of the skin care product can be applied to essence, water aqua, cream and emulsion in personal care products.
Drawings
FIG. 1 is a comparison graph of the water supplement moisturizing enhancement by 31% according to an embodiment of the invention;
FIG. 2 is a graph showing a 21% reduction in redness removal in an embodiment of the invention;
FIG. 3 is a graph of a 32% reduction in wrinkles for 8 weeks in accordance with an embodiment of the present invention;
FIG. 4 is a flow chart of a method for preparing skin care product materials in accordance with an embodiment of the present invention.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are some, but not all, embodiments of the present invention. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example one
The embodiment discloses a preparation method of a skin care product raw material containing a fish egg extract, wherein the skin care product raw material containing the fish egg extract comprises a phase A, a phase B and a phase C;
wherein the phase A comprises: betaine: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture;
the phase B comprises: fish egg extract: 0.5-3 parts;
the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate.
The fish egg extract contains small molecular peptides which are easily absorbed by the skin and have good effects on skin elasticity and wrinkles; however, the small molecule peptide is easy to lose activity under the influence of temperature and solvent, and the invention can well extract the small molecule peptide and other active ingredients beneficial to the skin by using the supercritical CO2 fluid extraction technology and retain the activity of the ingredients.
The preparation method of the skin care product raw material containing the fish egg extract comprises the following steps:
s1, preparing a fish egg extract: taking fresh roe, and pulverizing; feeding the raw material powder into a supercritical extraction kettle for supercritical CO2 extraction; feeding the extraction mixture into a supercritical separation kettle for separation;
in the present embodiment, the supercritical CO2 fluid extraction is adopted to well retain the active substances, whereas in the prior art, the separation product is usually added into distilled water for distillation, and the steam is condensed and recovered to obtain the roe extract, and the distillation operation of the prior art can cause a lot of active substances to be lost.
S2, screening raw materials: preparing basic ingredients according to the component ratio of the formula: wherein the phase A comprises: betaine: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture; the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate; the phase B comprises: fish egg extract: 0.5-3 parts;
s3, stirring for the first time: the phase a selected in the step S2 includes: betaine: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: fully mixing 90 parts of the mixture, heating the mixture to 80 ℃, then pouring the mixture into a homogenizer for homogenizing for 3min, and then cooling the mixture to 35 ℃ to obtain a phase A mixture;
s4, stirring for the second time: extracting the roe selected in the step S2: 0.5 part of the mixture is added into the phase A mixture obtained in the step S3 and fully and uniformly mixed to obtain an AB phase mixture;
s5, stirring for the third time: mixing the 1.2 hexanediol selected in the step S2: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone and 0.5 part of glyceryl caprylate are put into the AB phase mixture obtained in the step S4 and are fully and uniformly mixed, and then the finished product is obtained.
Wherein, in the step S1, the roe is physically crushed to be raw material powder with the grain diameter less than or equal to 40 meshes, when supercritical CO2 is used for extraction, the flow rate of CO2 is 20-25 kg/h, the extraction pressure is 20-25 MPa, the extraction temperature is 35 ℃, the extraction time is 1-3 hours, the separation pressure during supercritical separation is 8-12 MPa, the temperature is 40 ℃, the separation time is 1 hour, and the product of supercritical separation is added into water for distillation according to the proportion of 1 (40-60) g/L of the material-liquid ratio.
The temperature reduction in step S3 is natural cooling.
Wherein, the model of the homogenizer in the step S3 is RX-200 l.
Example two
The embodiment discloses a preparation method of a skin care product raw material containing a fish egg extract, wherein the skin care product raw material containing the fish egg extract comprises a phase A, a phase B and a phase C;
wherein phase a comprises: betaine: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 portions of
The phase B comprises: fish egg extract: 0.5-3 parts;
the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate.
The preparation method of the skin care product raw material containing the fish egg extract comprises the following steps:
s1, preparing a fish egg extract: taking fresh roe, and pulverizing; feeding the raw material powder into a supercritical extraction kettle for supercritical CO2 extraction; feeding the extraction mixture into a supercritical separation kettle for separation; adding the separated product into distilled water for distillation, and condensing and recovering steam to obtain roe extract;
s2, screening raw materials: preparing basic ingredients according to the component ratio of the formula: wherein the phase A comprises: betaine: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture; the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate; the phase B comprises: fish egg extract: 0.5-3 parts;
s3, stirring for the first time: the phase a selected in the step S2 includes: betaine: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: fully mixing 90 parts of the mixture, heating the mixture to 80 ℃, then pouring the mixture into a homogenizer for homogenizing for 3min, and then cooling the mixture to 35 ℃ to obtain a phase A mixture;
s4, stirring for the second time: extracting the roe selected in the step S2: 1.5 parts of the A phase mixture obtained in the step S3 is added to be fully and uniformly mixed to obtain an AB phase mixture;
s5, stirring for the third time: mixing the 1.2 hexanediol selected in the step S2: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone and 0.5 part of glyceryl caprylate are put into the AB phase mixture obtained in the step S4 and are fully and uniformly mixed, and then the finished product is obtained.
Wherein, in the step S1, the roe is physically crushed to be raw material powder with the grain diameter less than or equal to 40 meshes, when supercritical CO2 is used for extraction, the flow rate of CO2 is 20-25 kg/h, the extraction pressure is 20-25 MPa, the extraction temperature is 35 ℃, the extraction time is 1-3 hours, the separation pressure during supercritical separation is 8-12 MPa, the temperature is 40 ℃, the separation time is 1 hour, and the product of supercritical separation is added into water for distillation according to the proportion of 1 (40-60) g/L of the material-liquid ratio.
The temperature reduction in step S3 is natural cooling.
Wherein, the model of the homogenizer in the step S3 is RX-200 l.
EXAMPLE III
The embodiment discloses a preparation method of a skin care product raw material containing a fish egg extract, wherein the skin care product raw material containing the fish egg extract comprises a phase A, a phase B and a phase C;
wherein phase a comprises: betaine: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture;
the phase B comprises: 0.5-3 parts of fish egg extract;
the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate.
The preparation method of the skin care product raw material containing the fish egg extract comprises the following steps:
s1, preparing a fish egg extract: taking fresh roe, and pulverizing; feeding the raw material powder into a supercritical extraction kettle for supercritical CO2 extraction; feeding the extraction mixture into a supercritical separation kettle for separation; adding the separated product into distilled water for distillation, and condensing and recovering steam to obtain roe extract;
s2, screening raw materials: preparing basic ingredients according to the component ratio of the formula: wherein the phase A comprises: betaine: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture; wherein the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate; wherein the phase B comprises: fish egg extract: 0.5-3 parts;
s3, stirring for the first time: the phase a selected in the step S2 includes: betaine: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: fully mixing 90 parts of the mixture, heating the mixture to 80 ℃, then pouring the mixture into a homogenizer for homogenizing for 3min, and then cooling the mixture to 35 ℃ to obtain a phase A mixture;
s4, stirring for the second time: extracting the roe selected in the step S2: adding 3 parts of the mixture into the phase A mixture obtained in the step S3, and fully and uniformly mixing to obtain an AB phase mixture;
s5, stirring for the third time: mixing the 1.2 hexanediol selected in the step S2: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone and 0.5 part of glyceryl caprylate are put into the AB phase mixture obtained in the step S4 and are fully and uniformly mixed, and then the finished product is obtained.
Wherein, in the step S1, the roe is physically crushed to be raw material powder with the grain diameter less than or equal to 40 meshes, when supercritical CO2 is used for extraction, the flow rate of CO2 is 20-25 kg/h, the extraction pressure is 20-25 MPa, the extraction temperature is 35 ℃, the extraction time is 1-3 hours, the separation pressure during supercritical separation is 8-12 MPa, the temperature is 40 ℃, the separation time is 1 hour, and the product of supercritical separation is added into water for distillation according to the proportion of 1 (40-60) g/L of the material-liquid ratio.
Wherein, the temperature reduction in the step S3 is natural cooling;
wherein, the model of the homogenizer in the step S3 is RX-200 l.
The effect of extracellular test can be found by two tests and visual test added in the product, and the research on the invention is proved to effectively improve the skin barrier moisturizing function, the moisturizing is improved by 31 percent, the red blood silk is reduced by 21 percent, and the wrinkles are reduced by about 32 percent in 8 weeks.
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.
Claims (5)
1. A skin care product raw material containing roe extract for moisturizing, removing wrinkles and removing red blood streaks is characterized in that the skin care product raw material comprises a phase A, a phase B and a phase C;
wherein phase A comprises: betaine: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture;
the phase B comprises: fish egg extract: 0.5-3 parts;
the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate.
2. A preparation method of a skin care product raw material containing roe extract for moisturizing, removing wrinkles and removing red blood streaks is characterized by comprising the following steps:
s1, preparing a fish egg extract: taking fresh salmon roe, and pulverizing; feeding the raw material powder into a supercritical extraction kettle for supercritical CO2 extraction; feeding the extraction mixture into a supercritical separation kettle for separation; adding the separated product into distilled water for distillation, and condensing and recovering steam to obtain roe extract;
s2, screening raw materials: preparing basic ingredients according to the component ratio of the composition formula, wherein the phase A comprises: betaine: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: 90 parts of a mixture; the phase C comprises: 1.2 hexanediol: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone; 0.5 part of glycerol caprylate; the phase B comprises: fish egg extract: 0.5-3 parts;
s3, stirring for the first time: selecting betaine in the step S2: 0.05 part; carbomer: 0.2 part; butanediol: 0.05 part; water: 0.05 part; acryloyl dimethyl ammonium taurate/behenyl polyether-25: 0.12 part; methacrylate crosslinked polymer: 0.12 part; polyacrylate crosslinked polymer-6: 0.15 part; sodium hyaluronate: 0.05 part; water: fully mixing 90 parts of the mixture, heating the mixture to 80 ℃, then pouring the mixture into a homogenizer for homogenizing for 3min, and then cooling the mixture to 35 ℃ to obtain a phase A mixture;
s4, stirring for the second time: extracting the roe selected in the step S2: 0.5-3 parts of the mixture is added into the phase A mixture obtained in the step S3 and fully and uniformly mixed to obtain an AB phase mixture;
s5, stirring for the third time: mixing the 1.2 hexanediol selected in the step S2: 0.5 part; 0.5 part of caprylyl hydroximic acid; 0.5 part of p-hydroxyacetophenone and 0.5 part of glyceryl caprylate are put into the AB phase mixture obtained in the step S4 and are fully and uniformly mixed, and then the finished product is obtained.
3. The preparation method of the raw material of the skin care product containing the roe extract for moisturizing, wrinkle-removing and red blood streak removal according to claim 2, wherein in the step S1, the roe of salmon is physically crushed to obtain raw material powder with the particle size of less than or equal to 40 meshes, when the raw material powder is extracted by supercritical CO2, the flow rate of CO2 is 20-25 kg/h, the extraction pressure is 20-25 MPa, the extraction temperature is 35 ℃, the extraction time is 1-3 hours, the separation pressure during supercritical separation is 8-12 MPa, the temperature is 40 ℃, the separation time is 1 hour, and the product of supercritical separation is added into water for distillation according to the ratio of 1 (40-60) g/L.
4. The method for preparing the skin care product raw material containing the fish egg extract for moisturizing, removing wrinkles and removing red blood streaks according to claim 2, wherein the cooling in the step S3 is natural cooling.
5. The method for preparing the skin care product raw material containing the fish egg extract for moisturizing, removing wrinkles and removing red blood streaks, according to claim 2, is characterized in that the model of a homogenizer in the step S3 is RX-200 l.
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| IT202100009245A1 (en) * | 2021-04-13 | 2022-10-13 | Salamone Vincenzo | PROCESS OF OILING OF FISH ROES AND PRODUCTS THUS OBTAINED. |
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