CN103222937A - Skin external use composition comprising linseed extract - Google Patents
Skin external use composition comprising linseed extract Download PDFInfo
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- CN103222937A CN103222937A CN2012101206002A CN201210120600A CN103222937A CN 103222937 A CN103222937 A CN 103222937A CN 2012101206002 A CN2012101206002 A CN 2012101206002A CN 201210120600 A CN201210120600 A CN 201210120600A CN 103222937 A CN103222937 A CN 103222937A
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- caulis
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- folium lini
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/55—Linaceae (Flax family), e.g. Linum
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/30—Extraction of the material
- A61K2236/31—Extraction of the material involving untreated material, e.g. fruit juice or sap obtained from fresh plants
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Life Sciences & Earth Sciences (AREA)
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- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
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- Biotechnology (AREA)
- Dermatology (AREA)
- Birds (AREA)
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- Alternative & Traditional Medicine (AREA)
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- Medicinal Chemistry (AREA)
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- Cosmetics (AREA)
Abstract
The invention relates to a skin external use composition using linseed extract as effective constituents and specifically relates to a skin external use composition which uses sprout linseed extract as effective constituents and which has skin pore shrinkage and acne skin improvement effects.
Description
Technical field
The present invention relates to contain the Dermatologic preparation composition of core of Caulis et Folium Lini extract as effective ingredient, specifically, relate to and contain germination core of Caulis et Folium Lini extract, thereby have that skin pore shrinks and acne skin improves the Dermatologic preparation composition of effect as effective ingredient.
Background technology
The horn cell of the outermost layer-epidermis of skin continues to carry out cell differentiation, and the cell of differentiation was the cycle with 28 days, came off according to spinous layer, granular layer, cuticular order successively.Can not carry out smoothly as these cell cycles, horny layer will be piled up, and will stop up pore, and excretory sebum is hardened in pore, produces inflammation or acne.If produce the problem of these pores repeatedly, will influence pore corium on every side, cause quickening pore and enlarge.In addition, if the sebum secretion of sebaceous gland is excessive, too much sebum also can produce the pore problem, causes that pore enlarges and acne.
These pores seem to follow the string in case expansion once, will make whole skin seem coarse, so the pore contraction is one that needs most in skin problem in the problem of solution.
Caulis et Folium Lini (Linum usitatissimum L.) is linaceous annual herb, and height is 30-100 centimetre, and leaf is to stagger and wide fan-shaped.Caulis et Folium Lini is livid purple color or white, and fruit is that capsule is spherical, and seed is average flat avette, is yellowish-brown.Semen Lini also is called core of Caulis et Folium Lini, is mainly used in the preparation Semen Lini oil, and Semen Lini oil is used for printing China ink, oil painting lacquer.
In the patent of the compositions of the skin antioxidant effect of relevant core of Caulis et Folium Lini in the past, used with oil component as hair.But, not common core of Caulis et Folium Lini, shrink and acne is improved effect and do not reported at the pore of core of Caulis et Folium Lini extract that germinates and subcritical core of Caulis et Folium Lini extract.
Patent documentation: Korean registered patent gazette 10-0909206 number
Summary of the invention
The present inventor finds that the sub critical extraction thing of extract of the core of Caulis et Folium Lini of germination or core of Caulis et Folium Lini contains sometimes as effective ingredient, can reduce the sebum amount, and the pore refining size is improved acne skin, finishes the present invention thus.
Therefore, the purpose of this invention is to provide and contain the core of Caulis et Folium Lini extract as the pore of effective ingredient shrinks and the acne improvement is remarkably productive Dermatologic preparation composition.
The present invention relates to sebum minimizing, pore that the core of Caulis et Folium Lini extract contains as effective ingredient are shunk and acne improvement Dermatologic preparation composition.
In addition, the present invention relates to Dermatologic preparation composition that germination core of Caulis et Folium Lini extract is contained as effective ingredient.
And, the present invention relates to the Dermatologic preparation composition that the core of Caulis et Folium Lini sub critical extraction thing with the state that do not germinate contains as effective ingredient.
Further specify the present invention below.
The core of Caulis et Folium Lini of using among the present invention contains omega-3 fatty acid, protein, mineral, vitamin etc., particularly contains two molecule n-phenyl propyl
Natural goods-lignan (lignan) at the β position of n-propyl side chains be combined into.The lignan composition that contains in the core of Caulis et Folium Lini extract helps to reduce sebum amount, pore refining, improves acne skin.
The core of Caulis et Folium Lini that the core of Caulis et Folium Lini of using among the present invention preferably germinates.During the core of Caulis et Folium Lini that use to germinate, significantly improve lignan content, improve the content of effective essential, so can obtain the good result that reduces sebum amount, pore refining, improve acne skin biosis.
The germination of above-mentioned core of Caulis et Folium Lini can be used the conventional method in this field.For example,, preferably in 25 ℃ water, behind the adding core of Caulis et Folium Lini, kept 5-8 hour at 21-27 ℃, preferred 7 hours, then core of Caulis et Folium Lini is immersed in the water, at 25-30 ℃, preferably under 27 ℃ temperature conditions, implement illumination condition and dark condition repeatedly, germinate.At this moment, illumination condition was implemented 17-19 hour, and dark condition was implemented 5-7 hour; Preferably, illumination condition was implemented 18 hours, and dark condition was implemented 6 hours, cultivated to continue 5-7 days, preferably cultivated germination in 6 days.
The extraction of above-mentioned core of Caulis et Folium Lini extract can utilize the conventional extracting method in this field to make, and preferably adopts solvent extraction method, super critical extraction or sub critical extraction method, more preferably the sub critical extraction method.The sub critical extraction method is, under the temperature and pressure condition below the critical point of the liquids and gases coexistence of solvent, it as extracting the extraction method that solvent uses, made water as above-mentioned solvent among the present invention.In addition, in the super critical extraction,,, need organic solvent as secondary solvent in order to extract polar substances owing to use carbon dioxide.Therefore, compare with super critical extraction, the sub critical extraction method has the advantage that does not need these additional auxiliary organic solvents, and, making water as extracting solvent, reaction also can be hydrolyzed.Highly purified extract can be obtained by these sub critical extraction methods, therefore when the sub critical extraction thing of the core of Caulis et Folium Lini that contains germination, the good result that reduces sebum amount, pore refining, improves acne skin can be obtained.
The core of Caulis et Folium Lini extract that utilizes the sub critical extraction method that uses among the present invention is specifically with following method preparation.Utilize the sub critical extraction device at 50-200MPa core of Caulis et Folium Lini, preferably under the high pressure of 100MPa, decompose core of Caulis et Folium Lini, effective component extracting.Pressure is during less than 50MPa, abundant effective component extracting, and pressure is during greater than 200MPa, and relatively high pressure, the extracts active ingredients amount increases and is little, so extract under the pressure of above-mentioned scope.After the extraction, in filter, filter once, have in the filter of 0.45 μ m hole and filter once, in filter, filter once, remove foreign body and microorganism, obtain subcritical core of Caulis et Folium Lini extract with 0.2 μ m hole with 1.2 μ m holes.
Core of Caulis et Folium Lini extract of the present invention, the total amount of compositions can contain 0.01-97 weight % relatively, preferably contains the core of Caulis et Folium Lini extract of 60-90 weight %.Extract contain quantity not sufficient 0.01 weight % the time, can not obtain good result, and when surpassing 97 weight %, can have side effects and dosage form in solubility.
Compositions of the present invention is owing to contain germination core of Caulis et Folium Lini extract as effective ingredient, so have that skin aging prevents that effect, antioxidant effect, skin elasticity reinforced effects, wrinkle of skin from improving effect, the complexion improved by blood circulation is improved effect, skin irritation alleviation effects, dynamic equilibrium improve effect, elastic force reinforced effects, skin regeneration effect, dead bark removal effect, skin refuse cleaning effect, cutin are improved effect, skin-tightening effect, regulating effect, whitening effect.
Compositions of the present invention can contain the medium or the basic reagent that allow on cosmetic conduct and learning or the Dermatology carry out dosage formization.Can be to be applicable to partial all dosage forms, for example, can be provided as the folliculus dispersant that solution, gel, solid, anhydrous paste, oil phase are dispersed in emulsion, suspension, microemulsion, microcapsule, subparticle ball or the ion-type (liposome) and the nonionic of water
Form, perhaps frost, astringent, emulsion, powder, ointment, spraying and hide flaw clavate attitude.In addition, also can provide foam form or further contain the form of spraying (airosol) compositions of the propellant of compression.These compositionss can be according to the usual method preparation of this area.
In addition, compositions of the present invention can contain fatty material, organic solvent, lytic agent, concentrating agents, gel, softening agent, antioxidant, suspending agent, stabilizing agent, foaming agent (foaming agent), aromatic, surfactant, water, ion-type or nonionic emulsifier, filler, the metal ion disintegrating agent, chelating agen, preservative agent, vitamin, blocker, wetting agent, essential oil, dyestuff, pigment, hydrophilic or lipophile activating agent, normally used adjuvant in the cosmetic conduct and learning of any other compositions commonly used or the Dermatology field in lipid vesicle and the cosmetics.Above-mentioned adjuvant contains normally used amount in cosmetic conduct and learning or the Dermatology field.
In addition, compositions of the present invention is improved effect in order to increase skin, contains skin absorbs and promotes material.
Compositions of the present invention in the scope that does not influence the object of the invention, preferably can contain other compositions that can strengthen above-mentioned skin care effect except above-mentioned germination core of Caulis et Folium Lini extract.
The characteristic that contains the Dermatologic preparation composition of core of Caulis et Folium Lini extract by the core of Caulis et Folium Lini extract of the present invention, when being used for human body skin, pore refining reduces the sebum secretion amount, and improves acne skin.Particularly, when using the core of Caulis et Folium Lini extract of germination state, improve lignan content, when utilizing the sub critical extraction method to extract, obtain the high-purity extract, good pore shrinks, sebum reduces and acne skin improves so have.
The specific embodiment
Below by embodiment and test example, further specify composition of the present invention and effect.These embodiment and test example are just in order to help the understanding of the present invention, and category of the present invention and scope are not limited thereto.
The preparation of preparation example 1 germination core of Caulis et Folium Lini extract
After in 25 ℃ water, adding core of Caulis et Folium Lini, kept 7 hours, then core of Caulis et Folium Lini is immersed in the water, under 27 ℃ temperature conditions, implement illumination condition 18 hours repeatedly and germinateed the core of Caulis et Folium Lini that obtains germinateing after 6 days in 6 hours with dark condition.
The core of Caulis et Folium Lini of above-mentioned germination is put into 70 weight % Purified Waters and the alcoholic acid solvent of 30 weight %, placed 6 hours down, extract active component at 25 ℃.After the extraction, filter once in the filter with 1.2 μ m holes, filter once in the filter with 0.45 μ m hole, eliminate foreign body, utilize the filter with 0.2 μ m hole at last, eliminate microorganism, the core of Caulis et Folium Lini extract obtains germinateing.
The preparation of preparation example 2 subcritical germination core of Caulis et Folium Lini extracts
The germination core of Caulis et Folium Lini that will obtain with above-mentioned preparation example 1 same procedure utilizes the sub critical extraction device, effective component extracting under the high pressure of 100MPa.After the extraction, in filter, filter once, in filter, filter once, in filter, filter once, eliminate foreign body and microorganism, obtain subcritical germination core of Caulis et Folium Lini extract with 0.2 μ m hole with 0.45 μ m hole with 1.2 μ m holes.
The preparation of preparation example 3 subcritical core of Caulis et Folium Lini extracts
After the core of Caulis et Folium Lini pulverizing with the state that do not germinate, utilize the sub critical extraction device, effective component extracting under the high pressure of 100MPa.After the extraction, in filter, filter once, in filter, filter once, in filter, filter once, eliminate foreign body and microorganism, obtain subcritical core of Caulis et Folium Lini extract with 0.2 μ m hole with 0.45 μ m hole with 1.2 μ m holes.
Embodiment 1-3 and Comparative Examples 1-2
In order to estimate the pore contractive effect of the present composition, preparation has as the embodiment 1-3 of following table 1 composition and the astringent dosage form of Comparative Examples 1-2.Germination core of Caulis et Folium Lini extract, subcritical germination core of Caulis et Folium Lini extract and subcritical core of Caulis et Folium Lini extract use the prepared product of above-mentioned preparation example 1-2 and comparative preparation example 1, and the core of Caulis et Folium Lini extract is to use to be bought from Durae company.
Table 1
The pore of test example 1 germination core of Caulis et Folium Lini extract reduces effect and confirms
Selected because of 23 of the worried women more than 30 years old of pore, press the prescription of embodiment 1, apply the tangible position of pore every day, after applying for 2 weeks, utilize contact skin pore analysis programme to estimate the pore size, utilize the pore analysis programme, average pore size is divided into Three Estate, the number of each group of counting, it the results are shown in following table 2.
Table 2
Can find out that from the result of last table 2 cosmetic composition of the present invention can effectively reduce the pore size.
The sebum amount of test example 2 germination core of Caulis et Folium Lini extracts reduces effect and confirms
Selected because of 10 of the worried masculinity and femininities of hypersteatosis, press the prescription of embodiment 1, apply the position of face's hypersteatosis every day, after applying for 4 weeks, (Courage﹠Khazaka company Germany) measures the sebum amount, and it the results are shown in following table 3 to utilize sebumeter.
Table 3
| The experimenter | Sebum amount (μ g/cm before the test 2h) | 2 week of test back (μ g/cm 2h) | 4 week of test back (μ g/cm 2h) |
| 1 | 69 | 63 | 54 |
| 2 | 94 | 86 | 80 |
| 3 | 87 | 80 | 72 |
| 4 | 101 | 95 | 86 |
| 5 | 94 | 85 | 79 |
| 6 | 74 | 66 | 60 |
| 7 | 65 | 51 | 45 |
| 8 | 100 | 93 | 87 |
| 9 | 89 | 82 | 76 |
| 10 | 59 | 54 | 47 |
Can find out that from the result of last table 3 cosmetic composition of the present invention can effectively suppress sebum.
The sense evaluation of test example 3 pore contractive effects
At 20 of the big pore of worry among the women in 25-30 year, use the astringent of the foregoing description 1-3 and Comparative Examples 1-2 with using method with common cosmetic water, time around continuing to use,, skin is improved situation judge with following evaluation criterion according to the suggestion of user.It the results are shown in following table 4.
Evaluation criterion
+++: is very good improves effect;
++: significantly improve effect;
+: some improves effect;
±: do not improve effect, but do not worsen;
-: do not improve effect, and worsen.
Table 4
Shown in the result of above-mentioned table 4, compare Comparative Examples 1 that does not contain the core of Caulis et Folium Lini extract and the Comparative Examples 2 that contains common core of Caulis et Folium Lini extract, the embodiment 1-3 that contains germination core of Caulis et Folium Lini extract, subcritical germination core of Caulis et Folium Lini extract and subcritical core of Caulis et Folium Lini extract can confirm to have rapid and good pore contractive effect.
Test example 4 acnes are improved the sense evaluation of effect
At 20 of worry acne among the women in 19-26 year, use the astringent of the foregoing description 1-3 and Comparative Examples 1-2 with using method with common cosmetic water, time around continuing to use,, skin is improved situation judge with following evaluation criterion according to the suggestion of user.It the results are shown in following table 5.
Evaluation criterion
+++: is very good improves effect;
++: significantly improve effect;
+: some improves effect;
±: do not improve effect, but do not worsen;
-: do not improve effect, and worsen.
Table 5
Shown in the result of above-mentioned table 5, compare Comparative Examples 1 that does not contain the core of Caulis et Folium Lini extract and the Comparative Examples 2 that contains common core of Caulis et Folium Lini extract, the embodiment 1-3 that contains germination core of Caulis et Folium Lini extract, subcritical germination core of Caulis et Folium Lini extract and subcritical core of Caulis et Folium Lini extract can confirm to have rapid and good acne skin and improve effect.
Claims (7)
1. Dermatologic preparation composition is characterized in that, said composition contains germination core of Caulis et Folium Lini extract as effective ingredient.
2. Dermatologic preparation composition is characterized in that, said composition contains the sub critical extraction thing of core of Caulis et Folium Lini of the state of not germinateing as effective ingredient.
3. Dermatologic preparation composition according to claim 1, wherein, the core of Caulis et Folium Lini extract of described germination state utilizes the preparation of sub critical extraction method.
4. according to any described Dermatologic preparation composition in the claim 1 to 3, wherein, the total amount of compositions relatively, the content of described core of Caulis et Folium Lini extract is 0.01-97 weight %.
5. according to any described Dermatologic preparation composition in the claim 1 to 3, wherein, described compositions is a skin pore contraction Dermatologic preparation composition.
6. according to any described Dermatologic preparation composition in the claim 1 to 3, wherein, described compositions is a sebum minimizing Dermatologic preparation composition.
7. according to any described Dermatologic preparation composition in the claim 1 to 3, wherein, described compositions is an acne skin improvement Dermatologic preparation composition.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711308402.8A CN107854361A (en) | 2012-01-31 | 2012-04-23 | The application of the sub-critical extraction thing of the flaxseed for state of not germinateing |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| KR10-2012-0009326 | 2012-01-31 | ||
| KR1020120009326A KR101916824B1 (en) | 2012-01-31 | 2012-01-31 | Skin external composition comprising Linum usitatissimum L. seed extract |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
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| CN201711308402.8A Division CN107854361A (en) | 2012-01-31 | 2012-04-23 | The application of the sub-critical extraction thing of the flaxseed for state of not germinateing |
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| Publication Number | Publication Date |
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| CN103222937A true CN103222937A (en) | 2013-07-31 |
| CN103222937B CN103222937B (en) | 2018-08-21 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201711308402.8A Pending CN107854361A (en) | 2012-01-31 | 2012-04-23 | The application of the sub-critical extraction thing of the flaxseed for state of not germinateing |
| CN201210120600.2A Active CN103222937B (en) | 2012-01-31 | 2012-04-23 | Dermatologic preparation composition containing flaxseed extract |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201711308402.8A Pending CN107854361A (en) | 2012-01-31 | 2012-04-23 | The application of the sub-critical extraction thing of the flaxseed for state of not germinateing |
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| Country | Link |
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| KR (1) | KR101916824B1 (en) |
| CN (2) | CN107854361A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109846788A (en) * | 2019-03-29 | 2019-06-07 | 湖南御家化妆品制造有限公司 | A kind of moisturizing, moisturizing and/or antibacterial composition and its cosmetics of preparation |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20240050355A1 (en) * | 2022-08-11 | 2024-02-15 | Folashade Simpson | Topical skin treatment composition |
| CN115778859A (en) * | 2022-12-23 | 2023-03-14 | 李克明 | Skin conditioner |
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| FR2947727B1 (en) * | 2009-07-07 | 2011-08-05 | Sothys Paris | COSMETIC COMPOSITION FOR TOPICAL USE, KIT COMPRISING THE SAME, MODULATING COSMETIC PROCESS BASED ON THE AGING OF THE SKIN USING THE SAME |
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2012
- 2012-01-31 KR KR1020120009326A patent/KR101916824B1/en active IP Right Grant
- 2012-04-23 CN CN201711308402.8A patent/CN107854361A/en active Pending
- 2012-04-23 CN CN201210120600.2A patent/CN103222937B/en active Active
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| CN101129311A (en) * | 2007-09-18 | 2008-02-27 | 陈苏莉 | Creamier formulation containing turmeric and extractive of flax seed and method of producing the same |
| US20100113352A1 (en) * | 2008-11-06 | 2010-05-06 | Elliott Millstein | Retinol formulations and methods for their use |
| CN102058512A (en) * | 2009-03-30 | 2011-05-18 | 玫琳凯有限公司 | Topical skin care formulations |
| WO2011099964A1 (en) * | 2010-02-10 | 2011-08-18 | Biopelle, Inc. | Retinol formulations and methods for their use |
| CN102000009A (en) * | 2010-11-12 | 2011-04-06 | 中国农业科学院油料作物研究所 | Flaxseed oil-containing cleansing cream and preparation method thereof |
| CN102276665A (en) * | 2011-06-21 | 2011-12-14 | 晨光生物科技集团天津有限公司 | Method of extracting flax lignin from flax seed cake |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109846788A (en) * | 2019-03-29 | 2019-06-07 | 湖南御家化妆品制造有限公司 | A kind of moisturizing, moisturizing and/or antibacterial composition and its cosmetics of preparation |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103222937B (en) | 2018-08-21 |
| KR20130088226A (en) | 2013-08-08 |
| CN107854361A (en) | 2018-03-30 |
| KR101916824B1 (en) | 2018-11-08 |
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